CN105640830A - 一种海洋天然抗菌组合物及其用途 - Google Patents

一种海洋天然抗菌组合物及其用途 Download PDF

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CN105640830A
CN105640830A CN201610027594.4A CN201610027594A CN105640830A CN 105640830 A CN105640830 A CN 105640830A CN 201610027594 A CN201610027594 A CN 201610027594A CN 105640830 A CN105640830 A CN 105640830A
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marine natural
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李国超
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Sino clean (Dalian) Environmental Protection Technology Co., Ltd.
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Abstract

本发明提供一种海洋天然抗菌组合物，其以重量百分比计包含如下组分：二酸化珪素22-28％、水素水64-70％、阿魏酸0.5-1.5％、儿茶素0.5-1.5％、香叶醇0.5-1.5％、稻壳萃取物1-3％、绿茶萃取物1-3％、玫瑰萃取物0.5-1.5％。本发明涉及的混合物可显著抑制细菌生长，作为消臭喷雾用于客厅地毯除菌，消除室内异味、室内的宠物体味、狗屋臭气、厕所臭、垃圾臭、车内臭、鞋臭等，作为天然的海洋抗菌药物抗菌消臭适用范围广、效果显著。

Description

一种海洋天然抗菌组合物及其用途
技术领域
本发明涉及一种海洋天然抗菌组合物及其用途，属于医药卫生领域。
背景技术
随着人民生活水平的提高，人们对生活质量的要求也越来越高，臭味的存在更加受到重视。在日常生活中，室内、室外垃圾、宠物体味、厕所臭、垃圾臭、车内臭、鞋臭等。臭气的种类很多，主要是由于气体中含有以下五类化合物：(1)含硫化合物，如H2S、SO2、硫醇、硫醚；(2)含氮的化合物，如胺类、酰胺、吲哚；(3)卤素及其衍生物，如氯气、卤代烃；(4)烃类，包括烷烃、烯烃、炔烃、芳香烃；(5)含氧有机物，包括醇、醛、酚、酮、酯、有机酸等。
这些大量存在的恶臭严重影响了人们的生活，使生活质量和环境质量均有所下降，臭味的去除势在必行。臭味的去除方法主要有化学法、物化法和生物法。由于引起恶臭的臭源物质种类不同，应当采取的除臭方法也不同。对于臭源物质为H2S、NH3等无机小分子的臭气，其去除采用氧化法较为适应，而对于臭源物质是烃、醇、酚、酯等有机物的臭气，其去除采用催化氧化或生物法较为合适。另外，可以将吸附法与化学法或生物法结合起来，首先将臭源物质吸附于吸附剂表面，再利用催化氧化使其分解或利于微生物作用使其转化为无害物质。在化学法除臭方面，除臭氧和高铁酸盐之外的廉价氧化剂应继续开发和利用，除纳米TiO2、Pt等之外的催化剂活性成分的研究有待进一步深入，尤其是光催化方法中的廉价光催化剂有待开发。在物化除臭法中，吸附剂改性有利于除臭效率的提高，由于吸附剂再生要消耗能量，则原料来源广、廉价且高吸附量的吸附剂将在除臭市场有较强的竞争力。在生物除臭法中，可以借鉴吸附、过滤、吸收等物化方法设计工艺，但采用生物法时首先应该考虑臭源物质的生物去除可能性和去除效率，其次要做好微生物驯化工作，以提高除臭效率。
然而，以上大部分方法除臭过程中操作繁琐，成本高，使用不方便，还有可能造成二次污染，且大部分除臭制剂中均添加防腐剂、香精等材料以稳定除臭抗菌产品保质期、增加味觉适应性，而防腐剂、香精均属于人工材料添加剂，对环境或人体难免会造成二次污染。
鉴于此，寻求一种既能够达到抑菌除臭功效，又不使用防腐剂、香精等人工添加剂的抗菌除臭品，将除臭抗菌效果最大化的体现出来，是本发明亟待解决的问题。
发明内容
因此，本发明提供一种既可以协同抑菌除臭，又可以适用于日常生活，且除臭抑菌作用范围广泛、无毒无害、天然的抗菌组合物。
为此，本发明提供一种海洋天然抗菌组合物，其以重量百分比计包含如下组分：二酸化珪素22-28％、水素水64-70％、阿魏酸0.5-1.5％、儿茶素0.5-1.5％、香叶醇0.5-1.5％、稻壳萃取物1-3％、绿茶萃取物1-3％、玫瑰萃取物0.5-1.5％。
所述的海洋天然抗菌组合物，其以重量百分比计，优选包含如下组分:二酸化珪素5％、水素水67％、阿魏酸1％、儿茶素1％、香叶醇1％、稻壳萃取物2％、绿茶萃取物2％、玫瑰萃取物1％。
所述的海洋天然抗菌组合物，形态为液体或喷雾。
其中，二酸化珪素，是从海洋化石中提取出来的粉状物，不能完全溶于水，具有防菌、除臭、除臭、驱虫的作用。稻壳萃取物、绿茶萃取物、玫瑰萃取物均为市售可购买的原材料。
发明还提供一种海洋天然抗菌水，在常温下，将所述的海洋天然抗菌组合物中的材料放入搅拌机中搅拌25-30分钟，过滤后包装即得抗菌水。
本发明还提供一种所述的海洋天然抗菌组合物或抗菌水在化妆品或护理产品中的用途。
所述化妆品或护理产品为除臭剂、抑菌剂或空气清新剂，优选适用于客厅地毯除菌，消除室内异味、室内的宠物体味、狗屋臭气、厕所臭、垃圾臭、车内臭、鞋臭等。
经上述工艺生产的抗菌水或除臭喷雾，气味芬芳宜人，无香精、无刺激成分，经长期货架贮存试验(常温下3年)及反复耐热(40±1℃，24小时恢复室温后，液体正常，不浑浊、无沉淀)、耐寒(-15±1℃，24小时恢复室温后，体系正常，无浑浊、沉淀现象)，且破坏性试验，产品各项感观指标、理化指标、卫生指标均符合相应的国家标准。
本发明的上述技术方案相比现有技术具有以下优点：
本发明所述的海洋天然抗菌组合物，达到了各种原料混合使用时相互协同增效的效果，且抗菌、除臭效果强，解决了现有技术中抗菌除臭产品中常添加防腐剂、香精等添加剂时带来的二次污染，且使用过程中操作复杂、成本高、使用受到限制的技术问题。和现有技术中除臭产品使用时相比，具有协同增效效果，既可以适用于日常生活，同时除臭抑菌作用范围广泛、无毒无害，属于一种天然的抗菌组合物，从而最大程度发挥抗菌除臭的功效。
具体实施方式
为了使本发明的目的、技术方案及优点更加清楚明白，以下结合实施例，对本发明进行进一步详细说明。
实施例1抗菌水的制备
海洋天然抗菌水，含有以下组分:二酸化珪素25g、水素水67g、阿魏酸1g、儿茶素1g、香叶醇1g、稻壳萃取物2g、绿茶萃取物2g、玫瑰萃取物1g，在常温下上述原材料放入搅拌机中搅拌30分钟，过滤后包装即得抗菌水。
实施例2抗菌水的制备
海洋天然抗菌水，含有以下组分:二酸化珪素22g、水素水70g、阿魏酸0.5g、儿茶素0.5g、香叶醇1.5g、稻壳萃取物1g、绿茶萃取物3g、玫瑰萃取物1.5g，在常温下上述原材料放入搅拌机中搅拌25分钟，过滤后包装即得抗菌水。
实施例3抗菌水的制备
海洋天然抗菌水，含有以下组分:二酸化珪素28g、水素水65g、阿魏酸1g、儿茶素0.5g、香叶醇0.5g、稻壳萃取物3g、绿茶萃取物1g、玫瑰萃取物1g，在常温下上述原材料放入搅拌机中搅拌28分钟，过滤后包装即得抗菌水。
对比例1抗菌水的制备
海洋天然抗菌水，含有以下组分:二酸化珪素20g、水素水70g、阿魏酸1g、儿茶素1g、香叶醇1g、稻壳萃取物3g、绿茶萃取物3g、玫瑰萃取物1g，在常温下上述原材料放入搅拌机中搅拌30分钟，过滤后包装即得抗菌水。
对比例2抗菌水的制备
海洋天然抗菌水，含有以下组分:二酸化珪素25g、水素水60g、阿魏酸2g、儿茶素2g、香叶醇2g、稻壳萃取物2g、绿茶萃取物4g、玫瑰萃取物3g，在常温下上述原材料放入搅拌机中搅拌30分钟，过滤后包装即得抗菌水。
对比例3抗菌水的制备
海洋天然抗菌水，含有以下组分:二酸化珪素30g、水素水62g、阿魏酸1g、儿茶素1g、香叶醇1g、稻壳萃取物2g、绿茶萃取物2g、玫瑰萃取物1g，在常温下上述原材料放入搅拌机中搅拌30分钟，过滤后包装即得抗菌水。
实验例1本发明实施例及对比例的去除脚臭的效果研究比较
上述实施例1-3和对比例1-3制得的抗菌水，分别经50名30～50岁脚气情况严重的受试者连续试用2周，对比分析评价上述各实施例或对比例中所制得的化妆品的足部抑菌除臭效果以及汗腺出汗情况。其中，所述的足部抑菌除臭效果为脚臭、脚痒、脚趾红斑、脚部脱皮等的改善情况，下表中分别列出轻微改善和明显得到改善的百分比，结果见表1。使用时每日早中晚三次喷于患有脚气的部位及具有臭气的整只脚周围。
表1.抗菌组合物对除脚臭、抑菌效果表的影响
同时，由表1可见，本发明实施例1-3对于脚臭的去除、以及细菌导致的脚部红痒、蜕皮均有较好的效果，且通过优化发明的组分及用量，其效果均优于对比例中的抗菌水。提示本发明抗菌水组合物具有提高较好的抑菌除臭的功效，在试用过程中均未发现刺激性及过敏现象。
实验例2抑菌灭菌实验研究比较
参照美国化妆品、盥洗用品和香精协会(CTFA)推荐的防腐体系效能评价方法，以
CTFA推荐的经典的为期28天的灭菌单次挑战实验。
1.测试微生物：皮肤癣菌(包括真菌、念珠菌、霉菌、细菌)
2.接种的方式和数量
(1)接种的方式：采用混合接种
(2)接种的数量：将各菌种接种于合适的培养基中，于28℃(真菌)、36℃(念珠菌)、28℃(霉菌)、37℃(细菌)培养箱中培养。真菌、念珠菌、霉菌培养72小时，细菌培养48小时后，挑选典型的菌落于灭菌的液体培养基中制成一定浓度的真菌、念珠菌、霉菌、细菌混合悬液，置于冰箱冷藏备用。真菌、念珠菌、霉菌每克悬液含菌量均为1×105CFU/g或CFU/ml；细菌每克悬液含菌量为1×106CFU/g或CFU/ml。
3.微生物挑战实验
称取实施例1-3及对比例1-3中抗菌水样品，加入灭菌的容器内，加入混合真菌、念珠菌、霉菌、细菌悬液，充分混匀，使每克样品含真菌、念珠菌、霉菌量均为1×105CFU/g或CFU/ml；细菌量为1×106CFU/g或CFU/ml，然后置于28℃下。在接菌的0、7、14、21、28天取样分析：准确称取10克样品，加到含有玻璃小球和90ml灭菌生理盐水的锥形瓶内，充分震荡混匀，此悬液为1：10稀释液，然后再用生理盐水按1：10依次稀释。真菌28℃下培养72小时、念珠菌36℃下培养72小时、霉菌28℃下培养72小时，细菌37℃下培养48小时，按平板倾注法计数样品中含菌量。
4.评价方法
在28天样品中含真菌、念珠菌、霉菌或细菌在10CFU/g～100CFU/g(CFU/ml)，表明该样品对皮肤癣菌有较强的抑杀效果，通过挑战试验，在第7天下降到1000CFU/g(CFU/m1)以下视为通过，其它视为不通过。
5.实验结果
在接种的0、14和28天取样检测，样品抑菌灭菌测验结果见表2。
表2抗菌组合物对真菌、念珠菌、霉菌或细菌的影响
由表2可见，本发明实施例1-3对于真菌、念珠菌、霉菌或细菌均有较好的抑制效果，且通过优化发明的组分及用量，其抑菌效果均优于对比例中的抗菌水。提示本发明抗菌水组合物具有提高较好的抑菌的功效。
实验例3去除硫化氢、氨气的实验研究比较
采用硫化氢、氨气作为臭气的代表，浓度均用气体检测管检测，评价方法：t检测评价实验在100×70×50cm的有机玻璃操作箱中进行，以此模仿室内或室外垃圾堆等恶臭。箱体有一可打开或密闭的操作口。臭气发生后密闭，待扩散稳定取样测定臭气浓度。通过操作口将抗菌水均匀向箱内喷雾，然后封闭，测定消除后臭气浓度。通过计算消除前后臭气浓度的百分比计算消除率。
表3.抗菌组合物对硫化氢、氨气的影响
由表3可见，本发明实施例1-3对于硫化氢、氨水等臭气均有较好的抑制效果，且通过优化发明的组分及用量，其抑菌效果均优于对比例中的抗菌水。提示本发明抗菌水组合物具有提高较好的除臭的功效。
显然，上述实施例中采用的效果实验仅仅是为清楚地说明所作的举例，而并非对实施方式及使用范围的限定。对于所属领域的普通技术人员来说，在上述说明的基础上还可以做出其它不同形式的变化或变动。这里无需也无法对所有的实施方式及使用效果予以穷举。而由此所引伸出的显而易见的变化或变动仍处于本发明创造的保护范围之中。

Claims (7)

1.一种海洋天然抗菌组合物，其以重量百分比计包含如下组分：二酸化珪素22-28％、水素水64-70％、阿魏酸0.5-1.5％、儿茶素0.5-1.5％、香叶醇0.5-1.5％、稻壳萃取物1-3％、绿茶萃取物1-3％、玫瑰萃取物0.5-1.5％。
2.根据权利要求1所述的海洋天然抗菌组合物，其特征在于，其以重量百分比计包含如下组分:二酸化珪素5％、水素水67％、阿魏酸1％、儿茶素1％、香叶醇1％、稻壳萃取物2％、绿茶萃取物2％、玫瑰萃取物1％。
3.根据权利要求1-2任一项所述的海洋天然抗菌组合物，其特征在于，所述组合物的形态为液体或喷雾。
4.一种海洋天然抗菌水，其特征在于，在常温下，将权利要求1-3任一项所述的海洋天然抗菌组合物中的材料放入搅拌机中搅拌25-30分钟，过滤后包装即得抗菌水。
5.一种含有权利要求1-4之一所述的海洋天然抗菌组合物在化妆品或护理产品中的用途。
6.根据权利要求5所述的用途，其特征在于，所述化妆品或护理产品为除臭剂、抑菌剂或空气清新剂。
7.根据权利要求5-6任一项所述的用途，其特征在于，所述用途适用于客厅地毯除菌，消除室内异味、室内的宠物体味、狗屋臭气、厕所臭、垃圾臭、车内臭、鞋臭等。
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