CN105601122A - 玻璃板调节 - Google Patents

玻璃板调节 Download PDF

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CN105601122A
CN105601122A CN201610008983.2A CN201610008983A CN105601122A CN 105601122 A CN105601122 A CN 105601122A CN 201610008983 A CN201610008983 A CN 201610008983A CN 105601122 A CN105601122 A CN 105601122A
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conditioning agent
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acetone
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保罗·赛夫科
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Bo Long International Co., Ltd.
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Abstract

本发明涉及玻璃板调节。调节剂(典型地用于修复玻璃板中的瑕疵)包含在密封容器中，密封容器自身设置在柔性外部有壁容器内部。施加到外部柔性有壁容器的压力能够导致调节剂从内部调节剂容器中释放。调节剂制剂可包括与一种或多种底涂添加剂组合的吸湿溶剂(例如丙酮)，以给用于修复的玻璃板的表面打底。

Description

玻璃板调节
本申请是申请日为2010年11月9日，申请号为201080050900.7，发明名称为“玻璃板调节”的申请的分案申请。
本发明涉及玻璃板(glazingpanel)的调节，具体地涉及用于修复的玻璃板的调节。
玻璃板中的破裂、开裂或碎片(通常称为瑕疵(flaw))能够使用修复装置例如类似于WO-A-0134373中公开的真空修复装置来修复。树脂被引入瑕疵中(即碎片、开裂或破裂)，并且真空设备给树脂和瑕疵除气。为了提高修复质量，已知在填充树脂和使用真空之前，通过丙酮处理瑕疵以从瑕疵驱出尽可能多的湿气。丙酮与瑕疵中的任何湿气混合并增强蒸发。修复期间，瑕疵中的水分对于修复过程的质量是有害的。如果丙酮(其是吸湿的)在使用前已经被湿气污染，则可能出现问题。
已经设计一种改进的技术和装置，用于在进行修复过程之前输送、存储和使用用于调节玻璃板中瑕疵或破裂的试剂。
(1)根据第一方面，本发明提供用于调节用于修复的玻璃板的装置，该装置包括包含在密封的内部调节剂容器中的调节剂；该调节剂容器设置在柔性外部有壁容器内部；其中施加到外部柔性有壁容器的压力能够导致调节剂从内部调节剂容器中释放。
典型地，内部容器的完整性受到损失(为了导致调节剂从内部调节剂容器中释放)，而没有损失柔性外部有壁容器的结构完整性。
(2)根据(1)的装置，优选地，密封的内部调节剂容器是有效地不能渗透的(实质上不能透水的)，以防止湿气进入容器中与调节剂混合。
(3)根据(1)或(2)的装置，典型地，被施加用于弯曲外部容器的壁的手动挤捏压力(在食指和拇指之间)能够引起密封的内部调节剂容器的裂开或破碎，导致调节剂从内部调节剂容器中释放。
(4)根据(1)至(3)中任一项的装置，内部调节剂容器优选地包括具有易碎/易破碎壁的容器，优选地为玻璃指管。
(5)根据(1)至(4)中任一项的装置，外部柔性有壁容器包括塑料材料。
(6)根据(1)至(5)中任一项的装置，优选地，内部密封的调节剂容器以滑动配合关系的方式设置在柔性外部有壁容器内部，其中外部容器的壁与内部密封的调节剂容器相邻。这防止调节剂容器关于外部容器的移动，而这种移动可能以其他方式导致对调节剂容器的损伤。
有益地，外部容器和内部密封的调节剂容器是细长容器，优选地同轴布置。
优选地，内部密封的调节剂容器沿着外部容器的大部分长度延伸。
(7)根据(1)至(6)中任一项的装置，优选地，外部柔性有壁容器设有出口(优选地为喷嘴)，该出口允许调节剂分配到装置的外部。
(8)根据(1)至(7)中任一项的装置，其中所述出口包括喷嘴。
(9)根据(7)或(8)的装置，优选地，在内部调节剂容器开始破裂的情形下，调节剂可流过外部容器中的开口，但是内部调节剂容器的破裂碎片保留在外部容器内。
(10)根据(1)至(9)中任一项的装置，有益地，外部容器包括结合到接收器部分的封闭部分，以将内部调节剂容器固定在外部容器的内部。有益地，封闭部分延伸以通过内部调节剂容器的端部封闭。
(11)根据(10)的装置，在一些实施方式中，优选地，封闭部分包括喷嘴。
(12)根据(1)至(11)中任一项的装置，优选地，调节剂包括溶剂。
(13)根据(12)的装置，其中调节剂包括吸湿溶剂。
(14)根据(1)至(13)中任一项的装置，在一些实现形式中，调节剂包括丙酮。
(15)根据(1)至(14)中任一项的装置，另外，在一些实施方式中，调节剂包括溶剂和一种或多种底涂添加剂(primeradditive)以给用于修复的玻璃板的表面打底。
(16)根据(15)的装置，在一些实施方式中，底涂添加剂可包括用于涂覆玻璃板的表面以加速修复树脂流动的材料。
(17)根据(15)或(16)的装置，在一些实施方式中，底涂添加剂可包括用于涂覆玻璃板表面以加速聚合物交联的材料，以提高修复树脂的结合强度。
(18)根据(1)至(17)中任一项的装置，在一些实施方式中，外部容器的内部永久地与装置的外部周围大气连通。
(19)根据第二方面，本发明提供制造根据任一项之前权利要求所述装置的方法，其中调节剂密封在调节剂容器中，且调节剂容器设置在柔性部外有壁容器的内部。
(20)根据(19)的方法，其中所述外部容器包括结合到接收器部分的封闭部分，以将所述内部调节剂容器固定在所述外部容器的内部。
(21)根据(20)的方法，其中所述封闭部分包括喷嘴。
本发明此方面的优选特征根据那些在前的描述。
(22)根据另一方面，本发明提供修复玻璃板中的瑕疵的方法，该方法包括：
使用根据任一项之前权利要求所述的装置来将调节剂分配到瑕疵中；
将修复材料分配到瑕疵中以实现修复。
(23)根据又一方面，本发明提供用于调节用于修复的玻璃板的调节剂制剂，调节剂制剂包括与一种或多种底涂添加剂组合以给用于修复的玻璃板的表面打底的吸湿溶剂(例如丙酮)。
(24)根据(23)的调节剂，其中所述底涂添加剂包括用于涂覆所述玻璃板的表面以加速修复树脂流动的化学物质。
(25)根据(23)或(24)的调节剂，其中所述底涂添加剂包括用于涂覆所述玻璃板的表面以加速交联的化学物质，以提高修复树脂的结合强度。
(26)根据(23)至(25)中的任一项所述的调节剂，其中所述溶剂包括丙酮。
(27)根据(23)至(26)中的任一项所述的调节剂，其中所述添加剂材料包括丙烯酸和/或有机硅烷材料。
(28)根据(23)至(27)中的任一项所述的调节剂，其中所述调节剂包括具有百分之一或更少体积比的底涂添加剂的丙酮。
(29)根据(27)或(28)的调节剂，其中所述添加剂包括0.4％或更少体积比的丙烯酸。
(30)根据另一方面，本发明提供一种调节玻璃板中的瑕疵以准备修复的方法，所述方法包括施用制剂，所述制剂包括与一种或多种底涂添加剂组合以给用于修复的所述玻璃板的表面打底的吸湿溶剂(例如丙酮)。
现将仅参照图1通过示例的方式进一步描述本发明，其中图1为根据本发明的装置的示意图。
参照附图，其中图1显示以安瓿1的形式的调节剂输送系统/分配器，包括具有细长塑料柔性壁的管2，管2具有封闭端3和喷嘴端4。细长易碎玻璃指管5定位在具有柔性壁的塑料管2内部，指管5在塑料外管内同轴地布置。如以下将更详细描述的，易碎玻璃指管5是有效密封的内部容器且包含调节剂6，调节剂6典型地以液体形式。
内部密封的调节剂容器指管5以滑动配合关系的方式设置在柔性外部有壁管2内部，其中外部管2的壁沿着装置的大部分长度与内部密封的调节剂指管5相邻。这防止了调节剂指管5关于外管2移动，而这种移动可能以其他方式导致调节剂指管5的意外破碎。
具有柔性壁的塑料管2以两部分的形式制造。接收器管部分2a在管的与封闭端3相对的端部处具有打开端3。喷嘴构件8布置为坐落于接收器管部分2a的打开端3内。制造期间，包含调节剂6的易碎玻璃指管5通过管的打开端7而放到具有柔性壁的塑料管2内部中。喷嘴构件8然后坐落到管2的打开端7中并被超声焊接或热焊接。典型地，喷嘴构件8由比接收器管部分2a更刚性的塑料材料制成。
该布置使得当挤捏指压作用到具有柔性壁的塑料管2的纵向侧壁时，导致易碎玻璃指管5破碎且液体形式的调节剂能够根据需要穿出分配器安瓿1的喷嘴构件8以输送到玻璃板瑕疵。易碎玻璃指管5因而是具有薄壁的玻璃并可以例如为钠玻璃。可提供过滤器以防止玻璃碎片经由喷嘴构件通过，然而选择合适的玻璃能够使得此过滤器的需求是多余的。
典型地，调节剂6将包括丙酮混合物或溶液。丙酮已知在增强蒸发并因而将湿气驱出玻璃板瑕疵是有用的，并且本发明的分配器装置中的输送有助于确保试剂已经准备使用且在存储的任何阶段期间(可能漫长)不可能被进入安瓿1内的试剂中的湿气所污染。易碎玻璃指管5提供湿气屏障，且具有柔性壁的塑料管2形式的分配器内的密封使得玻璃被破碎且试剂的分配以安全且充分的方式实现成为可能，而玻璃碎片不会从装置中分配。该装置是一次使用的，并且调节剂是工厂剂量且环境密封的。该装置提供存储和运输容器并且还提供分配器/涂敷器装置。
在一些实施方式中，优选地，典型地为溶剂(示例为丙酮)的干燥剂与底涂剂组合使用，其中的底涂剂旨在并能够执行与玻璃板瑕疵之间的底涂相互作用。底涂相互作用可包括给瑕疵的表面涂覆一种材料，该材料能提高内部填充树脂的固化，增强树脂的流动或者与树脂相互作用以提高粘结强度。
在示例性实施方式中，溶液包括99.2％的溶剂(丙酮)和大约小于1％的底涂剂(例如0.4％的丙烯酸和0.4％的甲基丙烯酰氧基硅烷)。在应用于瑕疵之后，瑕疵中的丙酮被蒸发，留下底涂化学物质。底涂化学物质涂覆瑕疵的内表面。除了增强树脂的流动以完全渗透瑕疵之外，底涂化学物质与树脂重复作用并与其交联，以提高整体的粘结强度(试验中将此增加15-18％)。
其他的溶剂种类被尝试但是未被发现能提供最佳解决方案，例如，乙醇和甲醇是用于脱水的好溶剂。然而，两种溶剂均溶解典型地出现在层压交通工具挡风玻璃中的PVB夹层，并因而是较不优选的。
还尝试了其他的化学添加剂。1％、0.5％和0.25％的挡风玻璃修复树脂被尝试作为丙酮中的添加剂。所有的三种混合物均显示关于粘合和变湿的最小益处。建议的问题是溶液中的树脂包含光引发剂且因而易受保存期限考虑的影响，因为安瓿允许UV通过。有机硅烷和丙烯酸添加剂也被尝试过。
硅烷为结合剂且被化学地结合到玻璃表面，并交联到树脂聚合物中，增加树脂的粘附力。丙烯酸还结合到玻璃并在硅烷结合过程中用作加速剂。在丙酮中尝试了2％、1％和0.5％的有机硅烷/丙烯酸。
最好的结果是在1％的水平。0.8％被选择为最佳以保持丙烯酸的水平<0.5％，这被发现具有有益的结果。
将调节剂用于瑕疵并且经过足够的时间以允许瑕疵中的湿气蒸发/被驱出之后，能够通过使树脂填充并固化在瑕疵中来进行修复。为此目的,可使用例如WO01/343373中所示的真空修复装置。
测试被进行以比较各种结构和其他参数的效果。
1.保存期限
测试被进行以确定包含在干透溶液样品(丙酮)中的水分或湿气的量。
*丙酮为吸湿材料，即其适于从其环境中吸收水分。
样品#1对照-直接来自瓶的新丙酮-0.3％的水分
样品#2存储在塑料瓶中的丙酮。样品已经存储在仓库中4个月-6.8％的水分。
样品#3玻璃安瓿中的丙酮。样品已经存储在仓库中4个月-0.33％的水分。
2.粘附力
已经进行测试以确定干透溶液中底涂剂的效果。
*向干透溶液中添加粘附力促进剂。
溶液被用于玻璃并被允许蒸发。玻璃样品与HPX-II树脂粘结。测量搭接的剪切强度。
样品#1对照-3350psi
样品#2来自硬件存储的不受控丙酮(污染物)-2178psi
样品#3玻璃安瓿中的底涂剂-3982psi
3.变湿和流动特征
测试被进行以确定底涂剂溶液是否影响树脂与玻璃表面相互作用的方式。
测量树脂在玻璃上的接触角以确定变湿/流动。
表面 初始角 50秒时的角
未底涂的玻璃 22 13
底涂的玻璃 16 9
结果显示，底涂的样品具有比对照(未处理的)低很多的接触角。这意味着底涂剂有助于变湿和改进树脂的流动性能。
结果清晰地显示，在安瓿中使用变干存在技术优势。底涂剂的添加还增加了树脂的性能。

Claims (7)

1.一种调节剂制剂，用于调节用于修复的玻璃板，所述调节剂制剂包括与一种或多种底涂添加剂组合以给用于修复的所述玻璃板的表面打底的吸湿溶剂(例如丙酮)。
2.根据权利要求1所述的调节剂，其中所述底涂添加剂包括用于涂覆所述玻璃板的表面以加速修复树脂流动的化学物质。
3.根据权利要求1或权利要求2所述的调节剂，其中所述底涂添加剂包括用于涂覆所述玻璃板的表面以加速交联的化学物质，以提高修复树脂的结合强度。
4.根据权利要求1到3中的任一项所述的调节剂，其中所述溶剂包括丙酮。
5.根据权利要求1到4中的任一项所述的调节剂，其中所述添加剂材料包括丙烯酸和/或有机硅烷材料。
6.根据权利要求1到5中的任一项所述的调节剂，其中所述调节剂包括具有百分之一或更少体积比的底涂添加剂的丙酮。
7.根据权利要求5或权利要求6所述的调节剂，其中所述添加剂包括0.4％或更少体积比的丙烯酸。
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