CN105596236A - Low-foam solubilizer composition - Google Patents
Low-foam solubilizer composition Download PDFInfo
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- CN105596236A CN105596236A CN201610030743.2A CN201610030743A CN105596236A CN 105596236 A CN105596236 A CN 105596236A CN 201610030743 A CN201610030743 A CN 201610030743A CN 105596236 A CN105596236 A CN 105596236A
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- ppg
- solubilizer
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- butylol polyether
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4993—Derivatives containing from 2 to 10 oxyalkylene groups
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/49—Solubiliser, Solubilising system
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a low-foam solubilizer composition. The low-foam solubilizer composition comprises, by mass percent concentration, 20.0%-90.0% of hydrogenated castor oil polyoxyethylene ether, 0.1%-25.0% of PPG-butanol polyether and/or polyethoxysorbate and 9.0%-55.0% of ethyoxydiglycol. The low-foam solubilizer composition is capable of effectively assisting oil-soluble substances in dissolving in water; the low-foam solubilizer composition can be applied to products requiring late addition of oil-soluble components without increasing formulation stability burden; the low-foam solubilizer composition is suitable for most aqueous solution systems without influences on system stability. The low-foam solubilizer composition does not increase foam burden of products, is free of skin irritation and can be used at low temperature without heating and dissolving.
Description
Technical field
The invention belongs to household chemicals field, relate to the solubilizer in a kind of cosmetics, is a kind of specificallyLow bubble solubilizer composition.
Background technology
In the last few years, in cosmetics, toner, Essence, the aqueous products such as facial mask become more and more popular. ByIn the needs in market, and cosmetic formulations teacher is in order to give product better experience, all can be chosen in bodyIn system, add the oil soluble materials such as some greases, active matter, essence, anticorrisive agent. But, under general case,These lipophilic components are difficult to be dissolved in formula system, can not form homogeneous phase. Therefore, solubilizer is just in this classIn adornment product, played vital effect, reason is that solubilizer can be used as bridge, can help oily melt intoDivide and be dissolved in water, and form the homogeneous system of transparent and homogeneous.
Solubilising is that the oiliness composition of some slightly soluble or indissolubles in water is under the effect of surfactant, in solventIncrease solubility and form the process of solution. Solubilizer is the surfactant with solubilising power, by changingThe interface energy of profit material, by soluble in water molten oil material. On market, solubilizer composition is mainly with non-ionic surfaceActivating agent and anion surfactant are main.
Solubilizer is of a great variety in the market, and solubilizing effect is also different, has advantage separately, but allThere are some problems. For example: solubilizing effect is not good; Large to skin irritation; Increase system foam burden; IncreaseAdd the sticky sense of product; Composite class solubilizer low-temperature stratification, separate out; Some solubilizer winter is solid-state, needsAfter heating for dissolving, use, so just caused certain energy waste and used trouble etc.
Summary of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of low bubble solubilizer composition, instituteIt is not good that this low bubble solubilizer composition of stating has solved solubilizer solubilizing effect of the prior art, and skin is hadThe technical problem of damage.
The invention provides a kind of low bubble solubilizer composition, comprise rilanit special APEO, PPG-Butylol polyether and/or polyethoxy sorbitol ester, ethoxydiglycol, described rilanit special polyoxyethyleneThe mass percent concentration of ether in composition is 20.0%-90.0%; Described PPG-butylol polyether and/or poly-The mass percent concentration of ethyoxyl sorbitol ester in composition is 0.1%-25.0%, described ethyoxyl twoThe mass percent concentration of glycol in composition is 9.0%-55.0%.
Further, described rilanit special APEO is rilanit special APEO-40, hydrogenChange the combination of a kind of in castor oil polyoxyethylene ether-60 or two kinds.
Further, described PPG-butylol polyether be PPG-5-butylol polyether-5, PPG-7-butylol polyether-4,PPG-7-butylol polyether-10, PPG-10-butylol polyether-9, PPG-12-butylol polyether-12, PPG-12-butanols gatherEther-16, PPG-15-butylol polyether-20, PPG-17-butylol polyether-17, PPG-26-butylol polyether-26, PPG-28-Butylol polyether-35, PPG-33-butylol polyether-45, PPG-36-butylol polyether-36 or PPG-38-butanols are poly-One or more kinds of combinations in ether-37.
Further, described polyethoxy sorbitol ester is polyethoxy sorbitan monolaurate, poly-ethoxyBase sorbitol monostearate, polyethoxy sorbierite tristearate or polyethoxy sorbierite list oleic acidOne or more kinds of combinations in ester.
Further, described ethoxydiglycol is diethylene glycol ether.
Further, also comprise surfactant and solvent, the weight of described surfactant accounts for described solubilisingThe 10.0%-80.0% of agent composition total weight; The weight of described solvent accounts for described solubilizer composition total weight0.1％-60.0％。
The present invention also provides the application in cosmetics of above-mentioned solubilizer composition.
Further, the 0.1%-8.0% that the addition of described solubilizer is cosmetics quality.
Outward appearance of the present invention is yellow to weak yellow liquid, and normal temperature is liquid form, is applied to toner, essenceChina's liquid, the low alcohol such as facial mask, without in alcohol aqua cosmetics, effectively helps oily molten material soluble in water; Be applied to and needWill after add in lipophilic component product, do not increase formulation stability burden; Be applicable to most of aqua system, andSystem stability is not had to impact. Low bubble solubilizer composition of the present invention does not increase product foam burden; RightSkin does not have excitant; Low temperature does not need heating for dissolving to use.
The present invention compares with prior art, and its technological progress is significant. The present invention can be used for low bubble, needs to increaseThe cosmetics such as molten oily matter, makeup removing, have solved the deficiency of prior art and product.
Detailed description of the invention
To the technical scheme of various embodiments of the present invention be carried out to clear, complete description below, obviously, institute is describedEmbodiment be only a part of embodiment of the present invention, instead of whole embodiment. Based in the present inventionEmbodiment, those of ordinary skill in the art obtain under the prerequisite of not making creative work all otherEmbodiment, belongs to the scope that the present invention protects.
The low bubble solubilizer of one provided by the invention composition, its composition comprises: rilanit special APEO,Poly-and/or the polyethoxy sorbitol ester of PPG-butylol polyether, ethoxydiglycol.
The weight of described rilanit special APEO accounts for described solubilizer composition total weight20.0％-90.0％；
It is total that described PPG-butylol polyether and/or the weight of polyethoxy sorbitol ester account for described solubilizer compositionThe 0.1%-25.0% of weight;
Concrete, described PPG-butylol polyether and/or polyethoxy sorbitol ester refer to described PPG-fourthAlcohol polyethers and/combination of any one or two kinds of arbitrary proportions in polyethoxy sorbitol ester.
The weight of described ethoxydiglycol accounts for the 9.0%-55.0% of described solubilizer composition total weight.
It should be noted that, according to common practise, concrete hundred of the composition that solubilizer composition of the present invention containsDividing content sum is absolutely.
In following more preferably scope, by three specific embodiments, select three kinds of commercially available solubilizer, steepThe performance comparison test of foam and solubilizing effect.
Wherein,
The addition of described rilanit special APEO-40 is: its weight accounts for solubilizer composition gross weight20.0%, 25.0%, 30.0%, 35.0%, 40.0%, 45.0%, 50.0% the 20.0%-70.0% of amount, such as:,55.0%, 60.0%, 65.0%, 70.0%, 75.0%, 80.0% or the scope between any two numerical value wherein,Be preferably 45.0%-60.0%.
The addition of described rilanit special APEO-40 is preferably: its weight accounts for solubilizer composition35.0%, 37.0%, 39.0%, 41.0%, 43.0%, 45.0% the 45.0%-70.0% of gross weight, such as:,47.0%, 49.0%, 51.0%, 53.0%, 55.0%, 57.0%, 59.0%, 60.0% or wherein any twoScope between numerical value, more preferably 55.0%-70.0%.
The addition of described PPG-28-butylol polyether-35 is: its weight accounts for solubilizer gross weight0.1%, 1.0%, 2.0%, 3.0%, 4.0%, 5.0%, 6.0%, 7.0%, 8.0% 0.1%-15.0%, such as:,9.0%, 10.0%, 11.0%, 12.0%, 13.0%, 14.0%, 15.0% wherein between any two numerical valueScope, is preferably 0.1%-10.0%.
The addition of described PPG-28-butylol polyether-35 is preferably: its weight accounts for solubilizer gross weight0.1%-10.0%, such as: 0.1%, 0.5%, 1.0.%, 1.5%, 2.5%, 3.0%, 3.5%, 4.0%, 4.5%,5.0%, 6.0%, 6.5%, 7.0%, 7.5%, 8.0%, 8.5%, 9.0%, 10.0% or wherein any twoScope between numerical value, more preferably 0.5%-6.0%.
The addition of described polyethoxy sorbitol monooleate is: its weight accounts for solubilizer gross weight0.1%, 1.0%, 2.0%, 3.0%, 4.0%, 5.0%, 6.0%, 7.0%, 8.0% 5.0%-25.0%, such as:,9.0％、10.0％、11.0％、12.0％、13.0％、14.0％、15.0％、16.0％、17.0％、18.0％、19.0%, 20.0%, 21.0%, 22.0%, 23.0%, 24.0%, 25.0% or wherein between any two numerical valueScope, be preferably 5.0%-10.0%.
The addition of described polyethoxy sorbitol monooleate is preferably: its weight accounts for solubilizer gross weight0.1%-10.0%, such as: 0.1%, 0.5%, 1.0.%, 1.5%, 2.5%, 3.0%, 3.5%, 4.0%, 4.5%,5.0%, 6.0%, 6.5%, 7.0%, 7.5%, 8.0%, 8.5%, 9.0%, 10.0% or wherein any twoScope between numerical value, more preferably 0.1%-5.0%.
The addition of described ethoxydiglycol is: its weight accounts for the 9.9%-55.0% of solubilizer gross weight, than9.0%, 13.0%, 16.0%, 19.0%, 22.0%, 25.0%, 28.0%, 31.0%, 34.0%, 37.0% as:,40.0%, 43.0%, 46.0%, 49.0%, 55% or the scope between any two numerical value wherein, be preferably9.0％-40.0％。
The addition of described ethoxydiglycol is preferably: its weight accounts for solubilizer gross weight10.0%, 12.0%, 14.0%, 16.0%, 18.0%, 20.0%, 22.0%, 24.0% 9.0%-40.0%, such as:,26.0%, 28.0%, 30.0%, 32.0%, 34.0%, 36.0%, 38.0%, 40.0% or wherein any twoScope between numerical value, more preferably 15.0%-30.0%.
The present embodiment is in above-mentioned more preferably scope, and more preferably proportioning is as follows for the addition of each composition:
Embodiment 1
Embodiment 2
Embodiment 3
Foam, the report of solubilizing effect contrast test
1 explanation:
The concrete percentage composition sum of solubilizer composition ingredient of the present invention is absolutely;
Solubilizer composition (embodiment 1, embodiment 2, embodiment 3) used in following test is thisBright described low bubble solubilizer composition;
Selected commercially available solubilizer contrast test sample is its up-to-date batch of sample;
The selected commercially available solubilizer of contrast test is not limited only to this three commercially available class solubilizer.
2 test materials:
1. embodiment 1, embodiment 2, embodiment 3 are low bubble solubilizer composition of the present invention;
2. solubilizer 1 is rilanit special APEO, purchased from BASF AG;
3. solubilizer 2 is ethoxylation C12-14Alcohol, ethoxylated hydrogenated castor oil and 1,2-C12-16-ethyoxyl,The composition of propoxyl group ethylene glycol, purchased from BASF AG;
4. solubilizer 3 is the composition of ethoxylated hydrogenated castor oil, PPG-26-butylol polyether-26 and water,Purchased from SENSIENT company;
5.VE acetate, purchased from DSM N. V.;
6. the fragrance of a flower, fruital, costustoot essence, purchased from IFF company;
Compound lard be by purchased from WILMAR company pungent/capric acid glyceryl ester with purchased from SASOL public affairsThe mixture of the isomery 16 alcohol compositions of department, selected mixed proportion is 1:1;
8. solid grease is hydrogenated coconut oil glyceride, purchased from Cremer company.
3 experimental enviroments:
25 DEG C ± 1 DEG C of laboratory temperature.
4 concrete contrast tests:
4.1 foam volume contrast tests
4.1.1 test procedure
1. taking respectively test sample 1g adds in 99g water;
2. the 100g sample weighing up is respectively charged in identical closed container to machinery concussion 60 times;
3. after shaking, the foam height while measuring and record 0min, 5min with ruler immediately.
4.1.2 result of the test
Concrete comparing result is in table 1.
Table 1 embodiment 1 and commercially available solubilizer foam height comparing result
4.2 solubilizing effect contrast tests
4.2.1 test procedure
1. added beaker to mix 1% by hydrotrope and solubilizer, mixing time is 1min;
2. deionized water is added by hydrotrope and solubilizer mixture, add to 100%;
3. mixed solution is stirred;
4. observe mixed solution transparency, if system is transparent, record is now by hydrotrope and solubilizer ratio;
If system is opaque, increase solubilizer consumption, repeating step 1-3, until system is transparent,Record is by hydrotrope and solubilizer ratio.
4.2.2 result of the test
Concrete comparing result is in table 2.
Table 2 embodiment 1 and commercially available solubilizer solubilizing effect comparing result
5 conclusions
Comprehensive above comparative test result, solubilizer composition of the present invention, specifically can reach following effect:
Rilanit special APEO-40, PPG-28-butylol polyether-35 and/or poly-ethoxy that the present invention adoptsBase sorbitol ester and the composite use of ethoxydiglycol three, solubilizing effect is better, can effective solubilization VE vinegarAcid esters, various flavor essence, grease, and be not limited to this three classes material, concrete solubilising ratio with by hydrotrope,Be decided according to the actual requirements; Solubilizer composition foam provided by the invention is low, can not bring foam negative to productLoad.
Embodiment provided by the invention combination mutually in any way as required, obtains by this combinationTechnical scheme, also within the scope of the invention.
Obviously, those skilled in the art can carry out various changes and modification and not depart from of the present invention the present inventionSpirit and scope. Like this, if to of the present invention these amendment and modification belong to the claims in the present invention and etc.Within scope with technology, the present invention also comprise these change and modification interior.
Claims (8)
1. one kind low bubble solubilizer composition, it is characterized in that: comprise rilanit special APEO, PPG-butylol polyether and/or polyethoxy sorbitol ester, ethoxydiglycol, the mass percent concentration of described rilanit special APEO in composition is 20.0%-90.0%; Described PPG-butylol polyether and/or the mass percent concentration of polyethoxy sorbitol ester in composition are 0.1%-25.0%, and the mass percent concentration of described ethoxydiglycol in composition is 9.0%-55.0%.
2. the low bubble solubilizer of one according to claim 1 composition, is characterized in that: described rilanit special APEO is the combination of a kind of in rilanit special APEO-40, rilanit special APEO-60 or two kinds.
3. the low bubble solubilizer of one according to claim 1 composition, it is characterized in that: described PPG-butylol polyether is PPG-5-butylol polyether-5, PPG-7-butylol polyether-4, PPG-7-butylol polyether-10, PPG-10-butylol polyether-9, PPG-12-butylol polyether-12, PPG-12-butylol polyether-16, PPG-15-butylol polyether-20, PPG-17-butylol polyether-17, PPG-26-butylol polyether-26, PPG-28-butylol polyether-35, PPG-33-butylol polyether-45, PPG-36-butylol polyether-36, or the one or more kinds of combinations in PPG-38-butylol polyether-37.
4. the low bubble solubilizer of one according to claim 1 composition, is characterized in that: described polyethoxy sorbitol ester is the one or more kinds of combinations in polyethoxy sorbitan monolaurate, polyethoxy sorbitol monostearate, polyethoxy sorbierite tristearate or polyethoxy sorbitol monooleate.
5. the low bubble solubilizer of one according to claim 1 composition, is characterized in that: described ethoxydiglycol is diethylene glycol ether.
6. the low bubble solubilizer of one according to claim 1 composition, is characterized in that: also comprise surfactant and solvent, the weight of described surfactant accounts for the 10.0%-80.0% of described solubilizer composition total weight; The weight of described solvent accounts for the 0.1%-60.0% of described solubilizer composition total weight.
7. the application of solubilizer composition claimed in claim 1 in cosmetics.
8. application according to claim 7, is characterized in that, the 0.1%-8.0% that the addition of described solubilizer is cosmetics quality.
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| CN201610030743.2A CN105596236A (en) | 2016-01-18 | 2016-01-18 | Low-foam solubilizer composition |
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| CN201610030743.2A CN105596236A (en) | 2016-01-18 | 2016-01-18 | Low-foam solubilizer composition |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106580736A (en) * | 2016-11-29 | 2017-04-26 | 广州市禾基生物科技有限公司 | Solubilizing grease composition, application thereof and cosmetic prepared from same |
| CN114426909A (en) * | 2022-02-22 | 2022-05-03 | 伊利诺斯工具制品有限公司 | Carbon deposit cleaning method |
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| DE102012010206A1 (en) * | 2012-05-15 | 2013-11-21 | Koray Kaynak | Non-alcoholic 'colognes' substitute product |
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2016
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| JP2002212052A (en) * | 2001-01-15 | 2002-07-31 | Hajime Ito | External preparation |
| CN101674801A (en) * | 2007-01-31 | 2010-03-17 | 西巴控股公司 | cationic dyes |
| DE102012010206A1 (en) * | 2012-05-15 | 2013-11-21 | Koray Kaynak | Non-alcoholic 'colognes' substitute product |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106580736A (en) * | 2016-11-29 | 2017-04-26 | 广州市禾基生物科技有限公司 | Solubilizing grease composition, application thereof and cosmetic prepared from same |
| CN106580736B (en) * | 2016-11-29 | 2018-04-17 | 广州市禾基生物科技有限公司 | A kind of composition and its application and cosmetics prepared therefrom of solubilising grease |
| CN114426909A (en) * | 2022-02-22 | 2022-05-03 | 伊利诺斯工具制品有限公司 | Carbon deposit cleaning method |
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Application publication date: 20160525 |