CN105581923B - A kind of color make-up powder base is fixed composition and preparation method thereof - Google Patents
A kind of color make-up powder base is fixed composition and preparation method thereof Download PDFInfo
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- CN105581923B CN105581923B CN201610102457.2A CN201610102457A CN105581923B CN 105581923 B CN105581923 B CN 105581923B CN 201610102457 A CN201610102457 A CN 201610102457A CN 105581923 B CN105581923 B CN 105581923B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/896—Polysiloxanes containing atoms other than silicon, carbon, oxygen and hydrogen, e.g. dimethicone copolyol phosphate
- A61K8/897—Polysiloxanes containing atoms other than silicon, carbon, oxygen and hydrogen, e.g. dimethicone copolyol phosphate containing halogen, e.g. fluorosilicones
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
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Abstract
It fixes composition and preparation method thereof the present invention relates to a kind of color make-up powder base.A kind of color make-up powder base composition of fixing includes fluorination powder and silicone oil；The fluorination powder is that powder handles to obtain through C6 silicon fluoride coupling agent progress fluorinated surface.The present invention compounds specially treated fluorination powder material with traditional color make-up powder base product in color make-up powder base product；And according to the characteristic of fluorination powder wetting point and pour point, silicone oil raw material is selected first to be combined dispersion with it, to reach and the compatible stable system of traditional product system.The present invention such as drops low-surface-energy, hydrophobic, oleophobic to be fluorinated the physical and chemical performance of powder material new material, it is converted to the effect of fixation, to solve conventional formulation long-term existence because perspiration, bleed lead to fall the puzzlement of adornment, flower adornment, reach the advantages of fixing, solves born deficiency existing for such product and such as fall adornment, flower adornment.After powder base class product of the invention is put on face deeply, it is not easy to soak bisque because of oily sweat, to achieve the effect that fix.
Description
Technical field
The present invention relates to household chemicals technical fields, especially fix composition and its preparation side in a kind of color make-up powder base
Method.
Background technique
Color make-up powder base class product is a classification in cosmetics, refers mainly to the manufactured product based on powder class raw material, it
It include: muffin, blush, eye shadow, loose powder, foundation cream etc..Traditional color make-up powder base class product is always existed for a long time because perspiring, emitting
Oil (especially the people in summer and Oily is easier to perspire) makes the wetting of facial foundation layer, sweat stream, causes to spend adornment, fade, secretly
Color, the unabiding phenomenon of makeup, keep consumer very puzzled.In recent years, although occurring some products of fixing in the market, mostly
It is the oily cerul product in color make-up.Oily cerul product is to add some sizing film-forming resins in the product, makes it after makeup,
Skin surface film forming, to play the effect fixed, but also bring some unhappy feelings, such as allow people can feel skin it is tight,
It is airtight, makeup removing it is more difficult the problems such as.
Summary of the invention
It fixes composition and preparation method thereof the purpose of the present invention is to provide a kind of color make-up powder base, solves existing color make-up powder
Base class product is because perspiring, bleed leads to problems such as to spend adornment, makeup not lasting.
In order to achieve the above purpose, it adopts the following technical scheme that:
A kind of color make-up powder base is fixed composition, including fluorination powder and silicone oil；The fluorination powder is powder through C6 fluorine silicon
Alkane coupling agent carries out fluorinated surface and handles to obtain.Be fluorinated double thin powder of powder i.e. fluorinated surface processing, i.e., not only anti-sweat but also
Oil resistant.Fluorine is a kind of most effective essence for reducing surface free energy, and the titanium dioxide of perfluorinated surface treatment is added to powder base product
In also reduce the surface free energy of product simultaneously, slow down the aggregation between powder.Powder is fluorinated in addition to low-surface-energy drops in tool, is also had
There is hydrophobic, oleophobic characteristic.Its special materialization is obtained after being surface-treated with C6 silicon fluoride coupling agent to basic powder
The fluorination powder of energy, reapplies in color make-up product, and embody new functionality.The present invention is to utilize the unique of fluorination powder
Physical and chemical performance is applied in color make-up powder base product, so that it is changed product and is not easy to be moistened by oily sweat after skin surface in use
It is wet, to achieve the purpose that fix.And according to the characteristic of fluorination powder wetting point and pour point, silicone oil raw material is selected first to tie with it
Dispersion is closed, to reach and the compatible stable system of traditional product system.
Further, when preparation first by the silicone oil and the fluorination powder after mixing, then carry out mixing for full formula
It closes.Be conducive to reach system uniform and stable.
Further, the C6 silicon fluoride coupling agent is tridecafluoro-n-octyltriethoxysilane.
The surface treating agent of selection is complete (13) the fluorine octyltri-ethoxysilane screened through test of many times, molecule
Formula is as follows:
The siloxy of tridecafluoro-n-octyltriethoxysilane, facile hydrolysis become active silanol, with substrate surface-
OH-COOH and oxygen-containing group are because chemically reacting；There are 5-CF on oxoalkyl group chain2, and by-a CF3Sealing end, surface are free
Can be ultralow, enabling processed powder also has extremely low surface, is not easy wetted.F-C chain is 6 C atoms, will not generate poison
Property and environmental problem.
Further, the fluorination powder is in fluorination titanium dioxide, fluorination talcum powder, fluorination toner or fluoronated mica powder
It is one or more.Fluorination powder fluorination titanium dioxide, fluorination talcum powder, fluorination toner, fluoronated mica powder etc. all have reduction table
Face energy, hydrophobic, the big physical and chemical performance of oleophobic three.By in the corresponding color make-up powder base class product of its application, stringent corresponding preparation process is complete
At production, the function of products innovation will be given --- it fixes, will not sweat because of skin of face, bleed causes dressing to destroy,
Lasting dressing effect is especially made in summer, and adornment was not taken off up to 10 hours.Also there is good skin sense (not tight, saturating simultaneously
Gas is good), makeup removing is easy and (is free of film forming agent).
Further, the color make-up powder base fixes composition as muffin, and the muffin includes following components and percentage composition:
Talcum powder 47.7%, mica powder 22%, magnesium stearate 8%, fluorination titanium dioxide 8%, silicon powder 5%, dimethicone 4%, mixing
Oily 5%, appropriate toner, preservative 0.3%.
Further, color make-up powder base composition of fixing is to fix eye shadow, the eye shadow of fixing include following components and
Percentage composition: talcum powder 44.7%, mica powder 20%, magnesium stearate 6%, fluorination titanium dioxide 6%, kaolin 4%, dimethyl-silicon
Oily 3%, miscella 6%, toner 7%, preservative 0.3%, pearl powder 3%.
Further, the color make-up powder base fix composition be BB foundation emulsion, the BB foundation emulsion include following components and
Percentage composition: PEG-10 Polydimethylsiloxane 3%, sorbitan sesquioleate 0.5%, montmorillonite 2 .5%, the poly- diformazan of ring five
Radical siloxane/cyclohexasiloxane (PMX-0345Fluid) 12%, isononyl isononanoate 5%, Parleam 4%, trihydroxy
Stearin 0.4%, Dimethicone Crosspolymer/ring five dimethyl silicone polymer (silicone Elastomer
Blend) 0.4%, ring five dimethyl silicone polymer/trimethylsiloxysilicates (KF-7312J) 2%, fluorination powder 8%；It goes
Ionized water 51.2%, glycerol 5%, propylene glycol 5%, epsom salt 1%, liquid preservative 0.3%.Liquid preservative includes
DMDM H, IPBC and water.
A kind of preparation method of muffin, mainly comprises the steps that
(1) each component is proportionally weighed；
(2) fluorination titanium dioxide and dimethicone are separately added into ingredients pot, with 700 revs/min of 1-3 points of revolving speed stirring
Clock；
(3) talcum powder, mica powder, silicon powder, toner and magnesium stearate are sequentially added, is stirred with 3000 revs/min of revolving speed
It mixes 3-5 minutes；
(4) miscella is heated to 90 DEG C, preservative is added, poured into after being completely melt in oil tank with 700 revs/min of turn
Speed stirring, miscella is sprayed into ingredients pot；
(5) stirring is adjusted to 3000 revs/min, and stirring is shut down after 3-9 minutes, and temperature of charge should be less than 65 DEG C；
(6) after being sieved, by the mold requirement press-powder of different products shapes.
A kind of preparation method for eye shadow of fixing, mainly comprises the steps that
(1) each component is proportionally weighed；
(2) fluorination titanium dioxide and dimethicone are mixed in ingredients pot, with 700 revs/min of 1-3 points of revolving speed stirring
Clock stirs evenly；
(3) talcum powder, mica powder, magnesium stearate, kaolin, toner are sequentially added again, with 3000 revs/min turn
Speed stirring 3-6 minutes；
(4) miscella is heated to 90 DEG C, preservative is added, pours into oil tank after being completely melt；
(5) pearl powder is added to stir evenly in ingredients pot with 700 revs/min of revolving speed, then mixing obtained by step (4)
Oil sprays into ingredients pot；
(6) stirring 3-9 minutes is accelerated with 3000 revs/min of revolving speed, shut down, it is canned.
A kind of preparation method of BB foundation emulsion, mainly comprises the steps that
(1) each component is proportionally weighed；
(2) first ring five dimethyl silicone polymer/cyclohexasiloxane (PMX-0345 Fluid), dimethyl silicone polymer are handed over
Linked polymer/ring five dimethyl silicone polymer (silicone Elastomer Blend) and ring five dimethyl silicone polymer/tri-
Methyl siloxy esters of silicon acis (KF-7312J) is mixed in a container, and fluorination powder is added under stiring, is uniformly mixed spare；
(3) PEG-10 Polydimethylsiloxane, sorbitan sesquioleate, montmorillonite, isononyl isononanoate, hydrogenation is poly-
Isobutene, trihydroxy stearin sequentially add in oily phase pot, and it is uniform to be heated to 85~90 DEG C of stirring fusings；
(4) deionized water, glycerol, propylene glycol, epsom salt are sequentially added into water phase pot, is heated to 80~85 DEG C of stirrings
To dissolving completely；
(5) mixture obtained by above-mentioned steps (2) is poured under stiring in oily phase pot obtained by step (3), is stirred
It is even；
(6) first the material in oily phase pot obtained by step (5) is pumped into emulsion pot, and with 50~60 revs/min of revolving speed
Stirring, then the material in water phase pot obtained by step (4) is slowly pumped into emulsion pot, it opens homogenizer 3~5 minutes, stops equal
After matter, continue to stir, be cooled to 50 DEG C of addition liquid preservatives, uniformly shuts down.
Compared with prior art, the present invention is color by specially treated fluorination powder material and tradition in color make-up powder base product
Adornment powder base product compounding；And according to the characteristic of fluorination powder wetting point and pour point, silicone oil raw material is selected first to be combined with it point
It dissipates, to reach and the compatible stable system of traditional product system.The present invention is to be fluorinated the materialization of powder material new material
Low-surface-energy, hydrophobic, oleophobic can be such as dropped, the effect of fixation is converted to, to solve conventional formulation long-term existence because perspiring, emitting
Oil leads to fall the puzzlement of adornment, flower adornment, reaches the advantages of fixing, and solves born deficiency existing for such product and such as falls adornment, flower adornment；System
Selection silicone oil raw material first carries out the mixing of full formula again after mixing therewith when standby, and it is uniform and stable to reach system.The present invention
Powder base class product be put on face deeply after, be not easy to soak bisque because of oily sweat, to achieve the effect that fix.
Detailed description of the invention
Fig. 1 is the powder mixed powder containing fluorination and is directed to the wetting point comparison diagram of various greases without fluorination powder mixed powder；
Fig. 2 is the powder mixed powder containing fluorination and is directed to the pour point comparison diagram of various greases without fluorination powder mixed powder.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, the present invention is made into one below in conjunction with attached drawing
Step ground detailed description.
Embodiment 1
Fluorination powder includes that fluorination titanium dioxide, fluorination talcum powder, fluorination toner or fluoronated mica powder, fluorinated surface are handled
One or more of double thin powder.Fluorination powder is that powder surface treated agent tridecafluoro-n-octyltriethoxysilane carries out
Fluorinated surface handles to obtain.
Fig. 1 and Fig. 2 is respectively the powder mixed powder containing fluorination and is directed to the wetting of various greases without fluorination powder mixed powder
The comparison diagram of point, pour point.The wetting point of the powder mixed powder containing fluorination is free from fluorination powder in alkane as can be seen from Figure 1
More than twice of mixed powder wetting point；The wetting point of the powder mixed powder containing fluorination is free from fluorination powder mixed powder in advanced property ester
Nearly twice of wetting point；The wetting point of the powder mixed powder containing fluorination is with without fluorination powder mixed powder wetting point ratio in silicone oil
It is closer to.As can be seen from Figure 2 the pour point ratio of the powder mixed powder containing fluorination is higher by without fluorination powder mixed powder pour point
Very much.The pour point of the powder mixed powder containing fluorination is flowed with without fluorination powder mixed powder in alkane, advanced property ester and silicone oil
Point gap gradually decreases.It can be concluded that, silicone oil raw material is selected first to be combined dispersion, Ke Yida with fluorination powder from Fig. 1 and Fig. 2
To with the compatible stable system of traditional product system.
Embodiment 2
A kind of BB foundation emulsion, including following components and percentage composition: smooth times of PEG-10 Polydimethylsiloxane 3%, sorb
Half oleate 0.5%, montmorillonite 2 .5%, ring five dimethyl silicone polymer/cyclohexasiloxane mixture (PMX-
0345Fluid) 12%, isononyl isononanoate 5%, Parleam 4%, trihydroxy stearin 0.4%, polydimethylsiloxanes
Mixture (silicone Elastomer Blend) 0.4%, ring five of alkane cross-linked polymer and ring five dimethyl silicone polymer
The double thin powder 8% of the mixture (KF-7312J) 2% of dimethyl silicone polymer and trimethylsiloxysilicates, fluorination treatment；
Deionized water 51.2%, glycerol 5%, propylene glycol 5%, epsom salt 1%, liquid preservative 0.3%.
The preparation method of BB foundation emulsion, mainly comprises the steps that
(1) each component is proportionally weighed；
(2) first by mixture (PMX-0345Fluid), the poly dimethyl of ring five dimethyl silicone polymer and cyclohexasiloxane
Mixture (silicone Elastomer Blend) He Huanwu of Dimethicone Crosspolymer and ring five dimethyl silicone polymer
The mixture (KF-7312J) of dimethyl silicone polymer and trimethylsiloxysilicates is mixed in a container, is added under stiring
B phase is uniformly mixed spare；
(3) PEG-10 Polydimethylsiloxane, sorbitan sesquioleate, montmorillonite, isononyl isononanoate, hydrogenation is poly-
Isobutene, trihydroxy stearin sequentially add in oily phase pot, and it is uniform to be heated to 85~90 DEG C of stirring fusings；
(4) deionized water, glycerol, propylene glycol, epsom salt are sequentially added into water phase pot, is heated to 80~85 DEG C of stirrings
To dissolving completely；
(5) mixture obtained by above-mentioned steps (2) is poured under stiring in oily phase pot obtained by step (3), is stirred
It is even；
(6) first the material in oily phase pot obtained by step (5) is pumped into emulsion pot, and with 50~60 revs/min of revolving speed
Stirring, then the material in water phase pot obtained by step (4) is slowly pumped into emulsion pot, it opens homogenizer 3~5 minutes, stops equal
After matter, continue to stir, be cooled to 50 DEG C of addition liquid preservatives, uniformly shuts down.
Embodiment 3
A kind of muffin, including following components and percentage composition: talcum powder 47.7%, mica powder 22%, magnesium stearate 8%,
It is fluorinated titanium dioxide 8%, silicon powder 5%, dimethicone 4%, miscella 5%, appropriate toner, preservative 0.3%.
The preparation method of muffin, mainly comprises the steps that
(1) each component is proportionally weighed；
(2) fluorination titanium dioxide and dimethicone are separately added into ingredients pot, with 700 revs/min of 1-3 points of revolving speed stirring
Clock；
(3) talcum powder, mica powder, silicon powder, toner and magnesium stearate are sequentially added, is stirred with 3000 revs/min of revolving speed
It mixes 3-5 minutes；
(4) miscella is heated to 90 DEG C, preservative is added, poured into after being completely melt in oil tank with 700 revs/min of turn
Speed stirring, miscella is sprayed into ingredients pot；
(5) stirring is adjusted to 3000 revs/min, and stirring is shut down after 3-9 minutes, and temperature of charge should be less than 65 DEG C；
(6) after being sieved, by the mold requirement press-powder of different products shapes.
Embodiment 4
One kind is fixed eye shadow, including following components and percentage composition: talcum powder 44.7%, mica powder 20%, magnesium stearate
6%, titanium dioxide 6%, kaolin 4%, dimethicone 3%, miscella 6%, toner 7%, preservative 0.3%, pearly-lustre are fluorinated
Powder 3%.
It fixes the preparation method of eye shadow, mainly comprises the steps that
(1) each component is proportionally weighed；
(2) fluorination titanium dioxide and dimethicone are mixed in ingredients pot, with 700 revs/min of 1-3 points of revolving speed stirring
Clock stirs evenly；
(3) talcum powder, mica powder, magnesium stearate, kaolin, toner are sequentially added again, with 3000 revs/min turn
Speed stirring 3-6 minutes；
(4) miscella is heated to 90 DEG C, preservative is added, pours into oil tank after being completely melt；
(5) pearl powder is added to stir evenly in ingredients pot with 700 revs/min of revolving speed, then mixing obtained by step (4)
Oil sprays into ingredients pot；
(6) stirring 3-9 minutes is accelerated with 3000 revs/min of revolving speed, shut down, it is canned.
The BB foundation emulsion being prepared respectively according to embodiment 2-4, muffin and eye shadow of fixing are tested as follows: being taken
It BB foundation emulsion that the traditional BB foundation emulsion or muffin of amount or fix eye shadow and embodiment 2-4 are prepared respectively, muffin and fixes
Eye shadow compares, and finds BB foundation emulsion of the invention, muffin and fixes that eye shadow will not sweat because of skin of face, bleed leads to adornment
Hold flower adornment, fade or dark-coloured.Even if lasting dressing effect can also be made in summer, adornment was not taken off up to 10 hours.It will not
Generation allows people that can feel that skin is tight, the unhappy feeling such as airtight.They are being smeared to the same area on the inside of elbow deeply respectively
Region, removed ornaments and formal dress with the makeup remover of the different brands of equivalent, this experiment using the brands such as all madders of Maybelline, DHC makeup remover
Experimental comparison, a few money makeup removers can complete removals.It can be seen that the present invention improves, strengthens the effect of fixing of traditional product,
But the difficult puzzlement of makeup removing is not resulted in.
Above disclosed is only presently preferred embodiments of the present invention, cannot limit the right of the present invention with this certainly
Range, therefore equivalent changes made in accordance with the claims of the present invention, are still within the scope of the present invention.
Claims (4)
- The composition 1. a kind of color make-up powder base is fixed, which is characterized in that including fluorination powder and silicone oil；The fluorination powder is powder Through C6Silicon fluoride coupling agent carries out fluorinated surface and handles to obtain, and the silicone oil is first uniformly mixed by when preparation with the fluorination powder Afterwards, then the mixing of full formula is carried out, color make-up powder base composition of fixing is muffin or eye shadow of fixing；The muffin includes following components and percentage composition: talcum powder 47.7%, mica powder 22%, magnesium stearate 8%, titanium fluoride White powder 8%, silicon powder 5%, dimethicone 4%, miscella 5%, appropriate toner, preservative 0.3%；The eye shadow of fixing includes following components and percentage composition: talcum powder 44.7%, mica powder 20%, magnesium stearate 6%, fluorine Change titanium dioxide 6%, kaolin 4%, dimethicone 3%, miscella 6%, toner 7%, preservative 0.3%, pearl powder 3%.
- 2. color make-up powder base is fixed composition according to claim 1, which is characterized in that the C6Silicon fluoride coupling agent is 13 Fluorine octyltri-ethoxysilane.
- 3. color make-up powder base is fixed the preparation method of composition according to claim 1, which is characterized in that the color make-up powder base is fixed Composition for cosmetics is muffin, is mainly comprised the steps that(1) each component is proportionally weighed；(2) fluorination titanium dioxide and dimethicone are separately added into ingredients pot, are stirred 1-3 minutes with 700 revs/min of revolving speed；(3) talcum powder, mica powder, silicon powder, toner and magnesium stearate are sequentially added, 3-5 is stirred with 3000 revs/min of revolving speed Minute；(4) miscella is heated to 90 DEG C, preservative is added, pours into after being completely melt in oil tank and is stirred with 700 revs/min of revolving speed It mixes, miscella is sprayed into ingredients pot；(5) stirring is adjusted to 3000 revs/min, and stirring is shut down after 3-9 minutes, and temperature of charge should be less than 65 DEG C；(6) after being sieved, by the mold requirement press-powder of different products shapes.
- 4. color make-up powder base is fixed the preparation method of composition according to claim 1, which is characterized in that the color make-up powder base is fixed Composition for cosmetics is eye shadow of fixing, and is mainly comprised the steps that(1) each component is proportionally weighed；(2) fluorination titanium dioxide and dimethicone are mixed in ingredients pot, are stirred 1-3 minutes with 700 revs/min of revolving speed, It stirs evenly；(3) talcum powder, mica powder, magnesium stearate, kaolin, toner are sequentially added again, is stirred with 3000 revs/min of revolving speed It mixes 3-6 minutes；(4) miscella is heated to 90 DEG C, preservative is added, pours into oil tank after being completely melt；(5) pearl powder is added in ingredients pot, is stirred evenly with 700 revs/min of revolving speed, then the spray of miscella obtained by step (4) Enter in ingredients pot；(6) stirring 3-9 minutes is accelerated with 3000 revs/min of revolving speed, shut down, it is canned.
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| CN107242979B (en) * | 2017-07-04 | 2020-09-18 | 上海蔻沣生物科技有限公司 | Pre-emulsified slurry of hydrophobic and oleophobic powder, preparation method and application thereof |
| CN107753316A (en) * | 2017-12-08 | 2018-03-06 | 中山市美源化妆品有限公司 | A kind of face's flash of light emulsion formulations |
| CN108553317B (en) * | 2018-05-03 | 2019-08-30 | 浙江艳庄化妆品有限公司 | A kind of color make-up used suitable for sensitive skin crowd |
| WO2022030284A1 (en) * | 2020-08-07 | 2022-02-10 | 株式会社 資生堂 | Base coat agent for coating-type body corrective film and method for using same |
| CN114469764B (en) * | 2021-12-29 | 2024-04-05 | 上海蔻沣生物科技有限公司 | Fullerene and powder functional compound and preparation method and application thereof |
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Denomination of invention: A makeup powder based fixing composition and its preparation method Effective date of registration: 20221028 Granted publication date: 20190405 Pledgee: Shantou SME financing Company limited by guarantee Pledgor: SHANTOU QIWEI INDUSTRIAL CO.,LTD. Registration number: Y2022440000289 |