CN105565383B - 纳米尺寸二维材料的溶剂热合成 - Google Patents

纳米尺寸二维材料的溶剂热合成 Download PDF

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Publication number
CN105565383B
CN105565383B CN201510660846.2A CN201510660846A CN105565383B CN 105565383 B CN105565383 B CN 105565383B CN 201510660846 A CN201510660846 A CN 201510660846A CN 105565383 B CN105565383 B CN 105565383B
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China
Prior art keywords
blocky
dimensional material
lithiumation
dimensional
thermal reaction
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CN201510660846.2A
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English (en)
Chinese (zh)
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CN105565383A (zh
Inventor
张瑞刚
凌晨
贾鸿飞
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Toyota Motor Corp
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Toyota Engineering and Manufacturing North America Inc
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G39/00—Compounds of molybdenum
    • C01G39/06—Sulfides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/02—Production of hydrogen; Production of gaseous mixtures containing hydrogen
    • C01B3/06—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of inorganic compounds containing electro-positively bound hydrogen with inorganic reducing agents
    • C01B3/08—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of inorganic compounds containing electro-positively bound hydrogen with inorganic reducing agents by reaction of inorganic compounds with metals
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/02—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/08—Intercalated structures, i.e. with atoms or molecules intercalated in their structure
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/20—Two-dimensional structures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/82—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by IR- or Raman-data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/20—Particle morphology extending in two dimensions, e.g. plate-like
    • C01P2004/24—Nanoplates, i.e. plate-like particles with a thickness from 1-100 nanometer
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Manufacture And Refinement Of Metals (AREA)
CN201510660846.2A 2014-10-29 2015-10-14 纳米尺寸二维材料的溶剂热合成 Expired - Fee Related CN105565383B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US14/526,929 US9409792B2 (en) 2014-10-29 2014-10-29 Solventhermal synthesis of nanosized two dimensional materials
US14/526,929 2014-10-29

Publications (2)

Publication Number Publication Date
CN105565383A CN105565383A (zh) 2016-05-11
CN105565383B true CN105565383B (zh) 2018-10-12

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Country Link
US (1) US9409792B2 (https=)
JP (1) JP6392195B2 (https=)
CN (1) CN105565383B (https=)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20180072947A1 (en) * 2016-09-12 2018-03-15 Nanoco Technologies Ltd. Solution-Phase Synthesis of Layered Transition Metal Dichalcogenide Nanoparticles
KR102526649B1 (ko) 2016-11-30 2023-04-27 삼성전자주식회사 이차원 물질을 포함하는 반도체소자 및 그 제조방법
CN108190960B (zh) * 2018-01-23 2020-05-08 福州大学 一种基于电解液溶剂热插锂剥离制备单层二硫化钼的方法
CN110776006B (zh) * 2018-07-27 2023-07-21 香港科技大学 用作锂/钠离子电池负极材料的超薄硫化锑纳米片的制备方法
EP4582386A4 (en) * 2022-08-31 2026-04-29 Univ Tohoku Layered material nanosheet production method, layered mos2 nanosheet, and layered graphite nanosheet

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012101457A1 (en) * 2011-01-28 2012-08-02 Isis Innovation Limited Exfoliation of layered materials
CN103275355A (zh) * 2013-05-20 2013-09-04 中国科学技术大学 一种有机改性二硫化钼纳米片层及其制备方法
CN103803651A (zh) * 2014-03-11 2014-05-21 新疆大学 一种制备二硫化钼纳米片的方法
CN103833081A (zh) * 2014-02-21 2014-06-04 桂林理工大学 一种表面含有反应性基团的二硫化钼纳米片的制备方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3933688A (en) 1974-07-12 1976-01-20 Exxon Research And Engineering Company Method for lithiating metal chalcogenides and intercalated products thereof
US4822590A (en) * 1986-04-23 1989-04-18 Simon Fraser University Forms of transition metal dichalcogenides
US7892514B2 (en) * 2007-02-22 2011-02-22 Nanotek Instruments, Inc. Method of producing nano-scaled graphene and inorganic platelets and their nanocomposites
CN103937329A (zh) 2014-05-09 2014-07-23 浙江大学 一种具有高稳定性的二硫化钼纳米片层分散液的制备方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012101457A1 (en) * 2011-01-28 2012-08-02 Isis Innovation Limited Exfoliation of layered materials
CN103275355A (zh) * 2013-05-20 2013-09-04 中国科学技术大学 一种有机改性二硫化钼纳米片层及其制备方法
CN103833081A (zh) * 2014-02-21 2014-06-04 桂林理工大学 一种表面含有反应性基团的二硫化钼纳米片的制备方法
CN103803651A (zh) * 2014-03-11 2014-05-21 新疆大学 一种制备二硫化钼纳米片的方法

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CN105565383A (zh) 2016-05-11
US20160122198A1 (en) 2016-05-05
US9409792B2 (en) 2016-08-09
JP6392195B2 (ja) 2018-09-19
JP2016088840A (ja) 2016-05-23

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Effective date of registration: 20190529

Address after: Aichi Prefecture, Japan

Patentee after: Toyota Motor Corp.

Address before: American Kentucky

Patentee before: TOYOTA MOTOR ENGINEERING & MANUFACTURING NORTH AMERICA, Inc.

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20181012