CN105561626A - Built-in ultrasonic stirring crystallizer - Google Patents

Built-in ultrasonic stirring crystallizer Download PDF

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Publication number
CN105561626A
CN105561626A CN201610129030.1A CN201610129030A CN105561626A CN 105561626 A CN105561626 A CN 105561626A CN 201610129030 A CN201610129030 A CN 201610129030A CN 105561626 A CN105561626 A CN 105561626A
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CN
China
Prior art keywords
ultrasonic
hollow shaft
built
oscillator
group
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610129030.1A
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Chinese (zh)
Inventor
徐翔
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Individual
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Individual
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Publication date
Application filed by Individual filed Critical Individual
Priority to CN201610129030.1A priority Critical patent/CN105561626A/en
Publication of CN105561626A publication Critical patent/CN105561626A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0081Use of vibrations, e.g. ultrasound
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D2009/0086Processes or apparatus therefor

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  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention relates to a crystallizer, in particular relates to a built-in ultrasonic stirring crystallizer. The built-in ultrasonic stirring crystallizer comprises a barrel body, wherein a hollow shaft is arranged in the position of a central axis of the barrel body; two ends of the hollow shaft penetrate through the barrel body; two sides of the hollow shaft are provided with multiple vibrator groups; multiple ultrasonic vibrators are arranged in the vibrator groups; one end of the hollow shaft is provided with an electric brush group; one end of the electric brush group is connected with the ultrasonic vibrators through wires, and the other end of the electric brush group is connected with an ultrasonic generator through a wire. According to the built-in ultrasonic stirring crystallizer disclosed by the invention, the built-in ultrasonic stirring crystallizer can be prevented from scaling to a certain degree, the unsaturation degree of a solution can be rapidly released by ultrasonic waves, uniform growth of crystals is promoted, materials are prevented from concentrating and crystallizing on a heat exchange interface, and dirt on the scaled heat exchange interface can be removed by the ultrasonic waves; the ultrasonic vibrators are enough close to the heat exchange interface, a using effect of removing the dirt is ensured, and the energy consumption is lower.

Description

Built-in ultrasonic wave agitated crystallizer
Technical field
The present invention relates to a kind of crystallizer, be specifically related to a kind of built-in ultrasonic wave agitated crystallizer.
Background technology
Traditional crystallizer easily produces wall built-up at crystallization process, heat exchange interface place easily produces the problem such as fouling and blocking, and existing ultrasound wave descaling equipment can not go deep into solution inside, and energy consumption is higher, crystal can not be impelled to be formed uniformly, in the easy crystallization in heat exchange interface place.
Summary of the invention
In order to the deficiency in solving the problems of the technologies described above, the object of the invention is to: provide a kind of built-in ultrasonic wave agitated crystallizer, energy consumption is lower, material effectively can be prevented in the crystallization of heat exchange interface place, prevent fouling.
The technical scheme that the present invention adopts for its technical problem of solution is:
Described built-in ultrasonic wave agitated crystallizer, comprise cylindrical shell, the axis place of cylindrical shell is provided with hollow shaft, the two ends of hollow shaft are through cylindrical shell, the both sides of described hollow shaft are provided with multiple oscillator group, and the inside of oscillator group is provided with multiple ultrasonic oscillator, and one end of hollow shaft is provided with brush group, one end of described brush group is connected to ultrasonic oscillator by wire, and the other end is connected to supersonic generator by wire.
During use, the ultrasonic oscillator being crystallizer inside by brush group and wire is powered, the ultrasonic wave produced by ultrasonic oscillator is discharged rapidly and uniformly by the supersaturation liquid of inner barrel, in cylindrical shell, the degree of supersaturation of solution can be low-temperature receiver from inner barrel or thermal source, such as insert the electrical bar of inner barrel, also can be the low-temperature receiver from outside or thermal source, such as, on device housings, make chuck, in chuck, pass into raw steam or recirculated cooling water; Hollow shaft can clockwise or rotate counterclockwise, and then drives oscillator group to rotate in cylindrical shell, plays the effect of stirring, and can ensure the stable of convection transfer rate; Supersonic generator can control hyperacoustic frequency and intensity, and then controls the synthesis speed of crystal.
Further preferably, oscillator group is evenly distributed in the both sides of hollow shaft.
Further preferably, the wire between brush group and ultrasonic oscillator is positioned at the inside of hollow shaft, and hollow shaft can realize rotating and reverse.
Further preferably, the outside of oscillator group is wrapped in anticorrosive coat, mainly plays etch-proof effect.
Further preferably, the outside of oscillator group employs anti-corrosion material and processes, and mainly plays etch-proof effect.
Compared with prior art, the present invention has following beneficial effect:
1, equipment scaling can be prevented to a certain extent;
2, ultrasonic wave energy discharges the degree of unsaturation of solution fast, promotes that crystal grows uniformly, prevents material from concentrating on the crystallization of heat exchange interface place;
3, ultrasonic wave energy removes the dirt in the heat exchange interface of fouling, and ultrasonic oscillator from heat exchange interface position enough close to, the result of use taken out stains can be ensured;
4, equipment gos deep into the inside of solution, compares normal ultrasound waves scale removal, and its energy consumption is lower;
5, the shake subarray rotated can reduce the use amount of shake.
Accompanying drawing explanation
Fig. 1 structural representation of the present invention.
In figure: 1, oscillator group; 2, supersonic generator; 3, hollow shaft; 4, brush group; 5, cylindrical shell; 6, ultrasonic oscillator.
Detailed description of the invention
Below in conjunction with accompanying drawing, the embodiment of the present invention is described further:
Embodiment 1
As shown in Figure 1, built-in ultrasonic wave agitated crystallizer of the present invention, comprise cylindrical shell 5, the axis place of cylindrical shell 5 is provided with hollow shaft 3, and the two ends of hollow shaft 3 are through cylindrical shell 5, and the both sides of described hollow shaft 3 are provided with multiple oscillator group 1, the inside of oscillator group 1 is provided with multiple ultrasonic oscillator 6, one end of hollow shaft 3 is provided with brush group 4, and one end of described brush group 4 is connected to ultrasonic oscillator 6 by wire, and the other end is connected to supersonic generator 2 by wire.
Wherein, oscillator group 1 is evenly distributed in the both sides of hollow shaft 3; Wire between brush group 4 and ultrasonic oscillator 6 is positioned at the inside of hollow shaft 3, and hollow shaft 3 can realize rotating and reverse; The outside of oscillator group 1 is wrapped in anticorrosive coat, mainly plays etch-proof effect.
Embodiment 2
On the basis of embodiment 1, the outside of oscillator group 1 can also use anti-corrosion material to process, and mainly plays etch-proof effect.
Concrete use procedure of the present invention:
During use, the ultrasonic oscillator 6 being crystallizer inside by brush group 4 and wire is powered, the ultrasonic wave produced by ultrasonic oscillator 6 is discharged rapidly and uniformly by the supersaturation liquid of cylindrical shell 5 inside, in cylindrical shell 5, the degree of supersaturation of solution can be low-temperature receiver from cylindrical shell 5 inside or thermal source, such as insert the electrical bar of inner barrel, also can be the low-temperature receiver from outside or thermal source, such as, on device housings, make chuck, in chuck, pass into raw steam or recirculated cooling water; Hollow shaft 3 can clockwise or rotate counterclockwise, and then drives oscillator group 1 to rotate in cylindrical shell 5, plays the effect of stirring, and can ensure the stable of convection transfer rate; Supersonic generator 2 can control hyperacoustic frequency and intensity, and then controls the synthesis speed of crystal.

Claims (5)

1. a built-in ultrasonic wave agitated crystallizer, comprise cylindrical shell (5), it is characterized in that, the axis place of cylindrical shell (5) is provided with hollow shaft (3), the two ends of hollow shaft (3) are through cylindrical shell (5), the both sides of described hollow shaft (3) are provided with multiple oscillator group (1), the inside of oscillator group (1) is provided with multiple ultrasonic oscillator (6), one end of hollow shaft (3) is provided with brush group (4), one end of described brush group (4) is connected to ultrasonic oscillator (6) by wire, the other end is connected to supersonic generator (2) by wire.
2. built-in ultrasonic wave agitated crystallizer according to claim 1, is characterized in that, oscillator group (1) is evenly distributed in the both sides of hollow shaft (3).
3. built-in ultrasonic wave agitated crystallizer according to claim 1, is characterized in that, the wire between brush group (4) and ultrasonic oscillator (6) is positioned at the inside of hollow shaft (3).
4. built-in ultrasonic wave agitated crystallizer according to claim 1 and 2, is characterized in that, the outside of oscillator group (1) is wrapped in anticorrosive coat.
5. built-in ultrasonic wave agitated crystallizer according to claim 1 and 2, is characterized in that, the outside of oscillator group (1) employs anti-corrosion material and processes.
CN201610129030.1A 2016-03-07 2016-03-07 Built-in ultrasonic stirring crystallizer Pending CN105561626A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610129030.1A CN105561626A (en) 2016-03-07 2016-03-07 Built-in ultrasonic stirring crystallizer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610129030.1A CN105561626A (en) 2016-03-07 2016-03-07 Built-in ultrasonic stirring crystallizer

Publications (1)

Publication Number Publication Date
CN105561626A true CN105561626A (en) 2016-05-11

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610129030.1A Pending CN105561626A (en) 2016-03-07 2016-03-07 Built-in ultrasonic stirring crystallizer

Country Status (1)

Country Link
CN (1) CN105561626A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105854780A (en) * 2016-06-06 2016-08-17 无锡市翱宇特新科技发展有限公司 Chemical reaction kettle with adjustable stirring temperature
CN107774173A (en) * 2017-12-01 2018-03-09 温州中壹技术服务有限公司 A kind of high efficiency nonstorage calorifier
CN110354777A (en) * 2019-07-31 2019-10-22 河北兰升生物科技有限公司 Reaction unit of a kind of ultrasonic wave added crystallization and application thereof and preparation method using the device

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201482478U (en) * 2009-07-21 2010-05-26 广东工业大学 Photocatalytic reaction apparatus using ultrasonic waves to prevent and remove scale
CN203030032U (en) * 2012-10-15 2013-07-03 中国工程物理研究院化工材料研究所 Ultrasonic crystallizer and ultrasonic vibrating spear
CN205391796U (en) * 2016-03-07 2016-07-27 徐翔 Built -in ultrasonic wave agitated crystallizer

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201482478U (en) * 2009-07-21 2010-05-26 广东工业大学 Photocatalytic reaction apparatus using ultrasonic waves to prevent and remove scale
CN203030032U (en) * 2012-10-15 2013-07-03 中国工程物理研究院化工材料研究所 Ultrasonic crystallizer and ultrasonic vibrating spear
CN205391796U (en) * 2016-03-07 2016-07-27 徐翔 Built -in ultrasonic wave agitated crystallizer

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105854780A (en) * 2016-06-06 2016-08-17 无锡市翱宇特新科技发展有限公司 Chemical reaction kettle with adjustable stirring temperature
CN107774173A (en) * 2017-12-01 2018-03-09 温州中壹技术服务有限公司 A kind of high efficiency nonstorage calorifier
CN110354777A (en) * 2019-07-31 2019-10-22 河北兰升生物科技有限公司 Reaction unit of a kind of ultrasonic wave added crystallization and application thereof and preparation method using the device
CN110354777B (en) * 2019-07-31 2024-03-12 兰升生物科技集团股份有限公司 Method for preparing cis-para-substituted cyclohexylamino nitrile maleate by using reaction device of ultrasonic-assisted crystallization

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Application publication date: 20160511

RJ01 Rejection of invention patent application after publication