CN105519734A - A honeysuckle bud and flower-dry ilex hainanensis leaf tea substitute and a preparing method thereof - Google Patents
A honeysuckle bud and flower-dry ilex hainanensis leaf tea substitute and a preparing method thereof Download PDFInfo
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- CN105519734A CN105519734A CN201511021878.4A CN201511021878A CN105519734A CN 105519734 A CN105519734 A CN 105519734A CN 201511021878 A CN201511021878 A CN 201511021878A CN 105519734 A CN105519734 A CN 105519734A
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- honeysuckle
- holly leaf
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/34—Tea substitutes, e.g. matè; Extracts or infusions thereof
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Abstract
The invention discloses a honeysuckle bud and flower-dry ilex hainanensis leaf tea substitute and a preparing method thereof. The method includes 1) a step of raw material treatment, namely a step of mixing honeysuckle bud and flower and dry ilex hainanensis leaves according to a ratio, steaming with steam and dipping in ice water, 2) a step of performing high-speed dispersion and emulsification treatment, namely a step of smashing the raw materials treated in the step 1), adding purified water the weight of which is same as the weight of the treated raw materials, adding the mixture into a high-speed dispersion and emulsification machine, and treating to obtain a high-speed dispersed emulsified substance, 3) a step of pressurization and extraction, namely a step of putting the emulsified substance treated in the step 2) into a high-pressure autoclave, adding the purified water the weight of which is same as the weight of the emulsified substance, increasing the pressure to 4 kg/cm<2>, making the pressure uniform, maintaining for 10-15 min, restoring to the atmospheric pressure in 1-3 s, and filtering to obtain an extract liquid, and 4) a step of collecting the extract liquid obtained in the step 3), drying to obtain powder and preparing into the tea substitute.
Description
Technical field
The present invention relates to tealeaves and preparing technical field thereof, particularly relate to a kind of honeysuckle hainan holly leaf alternative tea and preparation method thereof.
Background technology
Honeysuckle is the general designation of Chinese medicine and plant, is the flower that the dry flower of caprifoliaceae plant honeysuckle or band are just opened.Honeysuckle is China's conventional Chinese medicine, and applicating history is long.Within 2010, the version Pharmacopoeia of the People's Republic of China one records the dry flower of caprifoliaceae plant honeysuckle LonicerajaponicaThunb. or is with the flower just opened to be honeysuckle certified products medicinal material, and the flower that the dry flower of congener largeflower-like honeysuckle flower L.ranthoidesHand.-Mazz, lonicera hypoglauca miq L.hypoglaucaMiq. Lonicera confusa L.confusaDC. and fulvoushair honeysuckle flower, L.fulvotomentosaHsuetS.C.Cheng or band are just opened is then Honeysuckle flower.This widely used Chinese traditional herbs of honeysuckle, containing polysaccharide, organic acid, chlorogenic acid, Polyphenols and volatilization wet goods active ingredient, has antitumor, anti-oxidant, anti-inflammation, liver protecting and the effect such as clearing heat and detoxicating, is called as the rarity of Chinese medicine.Be usually used in carbuncle to swell furunculosis, larynx numbness, erysipelas, warm blood fulminant dysentery, anemopyretic cold, the diseases such as warm disease heating.Prescription containing honeysuckle is used for by tcm clinical practice the treatment of gout.
Hainan holly leaf, derives from the dry leaf of holly plant hainan holly leaf (IlexhainanensisMerr.).Hainan holly leaf is distributed in Guangxi, Guangdong, Hainan, Guizhou and southeastern Yunnan, and in the hillside thick forest being born in height above sea level 500-1000m or sparse woods, the whole year can adopt, aboundresources.Hainan holly leaf has long Medicinal history, has recorded in " Guangxi Chinese medicine standard ", and its preparation mountain green tea decompression sheet is recorded in Chinese medicine ministry standard (mark numbering: WS3-B-2838-98).Hainan holly leaf is made tea drink more, there is clearing heat and detoxicating, swelling and pain relieving, blood circulation and channel invigorating effect, be mainly used in hypotensive, reducing blood lipid, norcholesterol, also for the hemiplegia caused by coronary heart disease, cerebrovas-cularaccident, and the treatment of the illness such as anemopyretic cold, cough with lung heat, edema of throat, tonsillitis, dysentery.Develop at present and become several formulations (as mountain green tea decompression sheet, compound Shanlucha Capsule, two stretch of flatland in a hilly area agent etc.).Main chemical compositions in hainan holly leaf is triterpene and saponins, flavones ingredient, simultaneously also containing other chemical composition such as coffee mesitoyl quinine acid, hemiterpene glycosides (ester) class.Up to now, from hainan holly leaf, separation obtains more than 80 compound.
Honeysuckle, hainan holly leaf, in field wide market such as pharmaceutical sector and beverage/food industry.At present, the functional component both at home and abroad for honeysuckle, hainan holly leaf is separated, Isolation and purification, and the exploitation of the beverage such as compound, cold tea type, achieves huge progress.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, honeysuckle hainan holly leaf alternative tea provide a kind of mouthfeel to be suitable for, being convenient for carrying and preparation method thereof.
The present invention is achieved by the following technical solution:
A preparation method for honeysuckle hainan holly leaf alternative tea, comprises the steps:
1) Feedstock treating: honeysuckle and hainan holly leaf are proportionally mixed, first uses steamed, and then soak in frozen water;
2) high speed dispersion emulsification treatment: step 1) raw material after process is smashed, add the pure water of identical weight, put into the process of high speed dispersion mulser, obtain high speed dispersion emulsion;
3) pressurised extraction: by step 2) process after emulsion, put into pressure pan, add the pure water of identical weight, be forced into 4kg/cm
2, make its pressure uniform, and keep 10-15min, then in 1-3s, recover normal pressure, filter, obtain extract;
4) step 3 is collected) extract that obtains, dry, obtain powder, prepare alternative tea.
Step 1 of the present invention) described in honeysuckle and hainan holly leaf proportionally mix, preferably mix according to 1-3:2-3 part by weight;
Described steamed, preferred 2-3min, soaks preferred 3-5min in frozen water.
Step 2) described in high speed dispersion emulsification treatment, preferred rotating speed 2000-3000r/min, time 10-20min.
Step 4) described in drying, preferably spray drying, described prepares alternative tea, can with reference to prior art, after adding auxiliary material, prepare the product of the forms such as tea in bag, beverage, electuary.
The present invention also comprises the honeysuckle hainan holly leaf alternative tea adopting above preparation method to obtain.It is good that the honeysuckle hainan holly leaf alternative tea that the present invention obtains drinks mouthfeel, without bitter taste, has obvious inhibitory action, have fragrant to hepatitis, similar in profile, smell, color to common tea product, can drink as tea product.
Compared with prior art, tool of the present invention has the following advantages:
1, the present invention first adopts steam to fumigate plant material, destroy volatile oil in plant, remove taste bad in vegetable oil, and then frozen water is adopted to soak, the activity of destruction and inhibitory enzyme, prevent enzyme in plant from, on the impact of product color, ensure that the color and luster of honeysuckle hainan holly leaf alternative tea and the balance of mouthfeel.
2, the rotor of high speed dispersion mulser is when High Rotation Speed, produce material ejection from the elongated cuts (slit) rotated that very large centrifugal force makes to be processed, and under the acting in conjunction of stator, make the material be processed be subject to the active force of two aspects: force it by the positive force of slit and the resistance that stops it to pass through.Meanwhile, when processed material sprays from slit, be also subject to the shear action of slit, and the rotational shear produced by turning stator relative motion makes under the effect of multi-acting force material obtain homogeneous, emulsification.It is narrow that the plant material processed has particle distribution range, good evenness, and without dead angle, material 100% is by the feature of dispersion and emulsion.
3, current.The high pressure of food or ultra high pressure treatment, in the high pressure or ultrahigh pressure vessel of sealing, the pressure that food applies hundreds of MPa is processed as medium with liquid (mainly water), under high pressure, protein in food, the macromolecular structure materials such as starch change, consequently protein denaturation, starch gelatinization, enzyme deactivation, microbial death, compared with heating treatment process, the maximum superiority of HIGH PRESSURE TREATMENT is, it is to the flavor substance of food, vitamin, pigments etc. are impact not, nutrition loss seldom, but the pressure of HIGH PRESSURE TREATMENT is larger just can be effective.The present invention is by " being forced into 4kg/cm
2, make its pressure uniform, and keep 10-15min, then in 1-3s, recover normal pressure "; the pressure of employing is far smaller than existing high pressure technique pressure used, and by instantaneously pressure being reduced to 0, the active material in plant is isolated; compared to existing technology, effective, the time is short.
Detailed description of the invention
With embodiment, the invention will be further described below, but the present invention is not limited to these embodiments.
Embodiment 1:
A preparation method for honeysuckle hainan holly leaf alternative tea, comprises the steps:
1) Feedstock treating: by honeysuckle and hainan holly leaf according to 1:3 part by weight, first use steamed 2min, and then soak 5min in frozen water;
2) high speed dispersion emulsification treatment: step 1) raw material after process is smashed, add the pure water of identical weight, put into the process of high speed dispersion mulser, rotating speed 2000r/min, time 20min, obtain high speed dispersion emulsion;
3) pressurised extraction: by step 2) process after emulsion, put into pressure pan, add the pure water of identical weight, be forced into 4kg/cm
2, make its pressure uniform, and keep 15min, then in 1-3s, recover normal pressure, filter, obtain extract;
4) step 3 is collected) extract that obtains, spraying dry, obtains powder, prepares tea in bag.
Embodiment 2:
A preparation method for honeysuckle hainan holly leaf alternative tea, comprises the steps:
1) Feedstock treating: by honeysuckle and hainan holly leaf according to 2:3 part by weight, first use steamed 3min, and then soak 4min in frozen water;
2) high speed dispersion emulsification treatment: step 1) raw material after process is smashed, add the pure water of identical weight, put into the process of high speed dispersion mulser, rotating speed 3000r/min, time 15min, obtain high speed dispersion emulsion;
3) pressurised extraction: by step 2) process after emulsion, put into pressure pan, add the pure water of identical weight, be forced into 4kg/cm
2, make its pressure uniform, and keep 12min, then in 1-3s, recover normal pressure, filter, obtain extract;
4) step 3 is collected) extract that obtains, dry, obtain powder, add auxiliary material, make beverage.
Embodiment 3:
A preparation method for honeysuckle hainan holly leaf alternative tea, comprises the steps:
1) Feedstock treating: by honeysuckle and hainan holly leaf according to 3:2 part by weight, first use steamed 2min, and then soak 3min in frozen water;
2) high speed dispersion emulsification treatment: step 1) raw material after process is smashed, add the pure water of identical weight, put into the process of high speed dispersion mulser, rotating speed 2500r/min, time 10min, obtain high speed dispersion emulsion;
3) pressurised extraction: by step 2) process after emulsion, put into pressure pan, add the pure water of identical weight, be forced into 4kg/cm
2, make its pressure uniform, and keep 10min, then in 1-3s, recover normal pressure, filter, obtain extract;
4) step 3 is collected) extract that obtains, dry, obtain powder, add auxiliary material, make electuary.
Comparative example 1:
Honeysuckle and hainan holly leaf according to the mixing of 1:3 part by weight, the Aqueous extracts obtained after direct water extraction, after concentrated, dry powder.
Comparative example 2:
Accurately take the hainan holly leaf powder 5g of drying and sieving, after petroleum ether degreasing depigmentation, add 70% ethanol by solid-to-liquid ratio 1:20,2h is extracted in 80 DEG C of water-baths, and filter, filter residue adds equivalent solvent extraction 1 time again, merging filtrate, Vacuum Concentration, to paste, obtains powder in 40 DEG C of vacuum drying.
Experimental example: pharmaceutical composition of the present invention is to the clinical efficacy of hepatitis
Experiment material: the powder that the embodiment of the present invention 1 prepares.
Experiment place: affiliated hospital of Medical Colleges Of Guilin.
1, case and method
2013-2014, connect and control Patients with Viral Hepatitis 122 example, the male sex 72 example, women 50 example, age is in 17-62 year, higher than normal 2-10 doubly, higher than normal 2-10 doubly, Bil is higher than 2-6 times of normal value for AST for ALT, but nonjoinder cirrhosis, without other severe complications, lactation and non-pregnancy get rid of the hepatic disorder patient that medicine and other reasons cause, and before entering group, March had not taken and protected the liver and antiviral drugs.122 examples are viral is divided into treatment group and control group at random, treatment group 60 example, wherein the male sex 30 example, women 30 example, 35 years old mean age, hepatitis A, the third liver 20 example, hepatitis B 40 example, oxyhepatitis 25 example, chronic hepatitis 35 example; Control group 62 example, the wherein male sex 32 example, women 30 example, 31 years old mean age, hepatitis A, the third liver 20 example, hepatitis B 42 example, oxyhepatitis 30 example, chronic hepatitis 32 example.Two groups of cases have comparativity.Primary Care is vitamin and Inosine tablets.
Observation index treatment before, treatment after two weeks, January, February patient's liver function, renal function, routine blood test, coagulation function, treat terminate the above-mentioned indices of rear whole check.
Usage and dosage: treatment group uses embodiment 1 to obtain powder, 5g/ time, oral, one day three times; Control group uses comparative example 1 (30 example), comparative example 2 (32 example) obtains powder, 5g/ time, oral, one day three times; 30d is 1 course for the treatment of, continues 1 course for the treatment of.
2, efficacy determination
Be as the criterion according to clinical symptom disappearance, be divided into recovery from illness, effective, invalid.
Recovery from illness: Clinical symptom and sign disappears, recover normal, Serum ALT, AST, Bil all recover normal.
Effective: the basic or major part of Clinical symptom and sign disappears, and Serum ALT, AST, Bi1 have one to recover normal.
Invalid: Clinical symptom and sign is without improvement, and Index for examination has no improvement.
3, curative effect is summed up
Table 1: the improvement of symptom and sign before and after two groups of treatments
Table 2: the improvement of ALT, AST, Bil before and after two groups of treatments
The all cases for the treatment of results are taken medicine no headache dizziness, heating, fash, alopecia, and joint pain is hemorrhage, degradation bad reaction under appetite.
Claims (5)
1. a preparation method for honeysuckle hainan holly leaf alternative tea, is characterized in that, comprises the steps:
1) Feedstock treating: honeysuckle and hainan holly leaf are proportionally mixed, first uses steamed, and then soak in frozen water;
2) high speed dispersion emulsification treatment: step 1) raw material after process is smashed, add the pure water of identical weight, put into the process of high speed dispersion mulser, obtain high speed dispersion emulsion;
3) pressurised extraction: by step 2) process after emulsion, put into pressure pan, add the pure water of identical weight, be forced into 4kg/cm
2, make its pressure uniform, and keep 10-15min, then in 1-3s, recover normal pressure, filter, obtain extract;
4) step 3 is collected) extract that obtains, dry, obtain powder, prepare alternative tea.
2. the preparation method of a kind of honeysuckle hainan holly leaf alternative tea according to claim 1, is characterized in that: step 1) described in honeysuckle and hainan holly leaf proportionally mix, mix according to 1-3:2-3 part by weight.
3. the preparation method of a kind of honeysuckle hainan holly leaf alternative tea according to claim 1, is characterized in that: step 1) described in steamed 2-3min, soak 3-5min in frozen water.
4. the preparation method of a kind of honeysuckle hainan holly leaf alternative tea according to claim 1, is characterized in that: step 2) described in high speed dispersion emulsification treatment, rotating speed 2000-3000r/min, time 10-20min.
5. the honeysuckle hainan holly leaf alternative tea that the preparation method according to any one of claim 1-4 obtains.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511021878.4A CN105519734A (en) | 2015-12-30 | 2015-12-30 | A honeysuckle bud and flower-dry ilex hainanensis leaf tea substitute and a preparing method thereof |
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| CN201511021878.4A CN105519734A (en) | 2015-12-30 | 2015-12-30 | A honeysuckle bud and flower-dry ilex hainanensis leaf tea substitute and a preparing method thereof |
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| CN105519734A true CN105519734A (en) | 2016-04-27 |
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| CN201511021878.4A Pending CN105519734A (en) | 2015-12-30 | 2015-12-30 | A honeysuckle bud and flower-dry ilex hainanensis leaf tea substitute and a preparing method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106490246A (en) * | 2017-01-05 | 2017-03-15 | 冯德进 | A kind of three snake gallbladder teas and preparation method thereof |
| CN106490247A (en) * | 2017-01-05 | 2017-03-15 | 冯德进 | A kind of snake gallbladder tea and preparation method thereof |
| CN107927280A (en) * | 2018-01-15 | 2018-04-20 | 浦北县利民农产品产销专业合作社 | It is a kind of persistently to keep brewing golden flower fruit teas of color and luster and preparation method thereof |
| CN108094633A (en) * | 2018-01-15 | 2018-06-01 | 浦北县利民农产品产销专业合作社 | It is a kind of persistently to keep brewing yearning between lovers fruit tea of color and luster and preparation method thereof |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103652155A (en) * | 2013-10-18 | 2014-03-26 | 梅州广通制药有限公司 | Instant molecular health-care tea |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106490246A (en) * | 2017-01-05 | 2017-03-15 | 冯德进 | A kind of three snake gallbladder teas and preparation method thereof |
| CN106490247A (en) * | 2017-01-05 | 2017-03-15 | 冯德进 | A kind of snake gallbladder tea and preparation method thereof |
| CN107927280A (en) * | 2018-01-15 | 2018-04-20 | 浦北县利民农产品产销专业合作社 | It is a kind of persistently to keep brewing golden flower fruit teas of color and luster and preparation method thereof |
| CN108094633A (en) * | 2018-01-15 | 2018-06-01 | 浦北县利民农产品产销专业合作社 | It is a kind of persistently to keep brewing yearning between lovers fruit tea of color and luster and preparation method thereof |
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Application publication date: 20160427 |