CN107494862B - Cosmetic coffee containing periplaneta americana active ingredient - Google Patents
Cosmetic coffee containing periplaneta americana active ingredient Download PDFInfo
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/24—Extraction of coffee; Coffee extracts; Making instant coffee
- A23F5/36—Further treatment of dried coffee extract; Preparations produced thereby, e.g. instant coffee
- A23F5/40—Further treatment of dried coffee extract; Preparations produced thereby, e.g. instant coffee using organic additives, e.g. milk, sugar
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/63—Arthropods
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/32—Burseraceae (Frankincense family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8969—Polygonatum (Solomon's seal)
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- Biotechnology (AREA)
- Alternative & Traditional Medicine (AREA)
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Abstract
The invention relates to a beauty coffee containing periplaneta americana active ingredients, belonging to the technical field of health-care food. The beauty coffee comprises the following components in percentage by mass: 25-40% of coffee containing periplaneta americana extract, 1-6% of Chinese olive extract, 1-5% of rhizoma polygonati powder, 25-35% of brown sugar and 30-40% of trans-fatty acid-free non-dairy creamer; the invention adds the Chinese olive extract and the sealwort powder in the formula, supplements the beauty and health care efficacy of coffee, has the advantages of saving time and reducing cost, and the freeze-dried coffee containing the periplaneta americana extract has uniform components and uniform color, avoids the damage to the quality of the coffee in the high-temperature drying process in the production of spray-dried coffee or condensed aroma-enhanced coffee, well retains the flavor and taste of the roasted and ground coffee, greatly improves the quality of the instant coffee, and is widely drunk by consumers as a healthy drink.
Description
Technical Field
The invention belongs to the technical field of health-care food, and particularly relates to a beauty coffee containing an active component of periplaneta americana.
Background
Periplaneta americana (Periplaneta americana L.) belongs to the family Blatta, the class Insecta, the order Blattaria, the family Blattaria, is the largest volume in the family Blattaceae, and is one of the most successful groups of insects that are the most vital, oldest and to date, in the world. In recent years, pharmacological actions of the periplaneta americana are more and more researched, and the periplaneta americana is found to have the effects of resisting tumors, inflammation and viruses, regulating immune functions, reducing swelling, repairing, destroying nodules, detoxifying, resisting mutation, eliminating free radicals and the like.
The Chinese olive is a plant of the family of olivaceae, also called green olive, jian fruit and Chinese olive, the Chinese olive is the first plant of medicine and food dual-purpose resource published by Ministry of health, the consumption of folk in various provinces in south China is large, and the Chinese olive is not only an edible fresh fruit, but also a common resource of medicated diet, beverage and traditional Chinese medicine. Has effects of clearing away heat and toxic materials, relieving sore throat, and promoting fluid production, and can be used for treating sore throat, cough, sticky phlegm, dysphoria, thirst, fish and crab poisoning.
Rhizoma Polygonati has effects of invigorating qi, nourishing yin, invigorating spleen, moistening lung, and invigorating kidney. Meanwhile, the health-care tea also has the effects of resisting anoxia, fatigue and aging, reducing blood sugar, strengthening heart, enhancing immunity and metabolism.
Coffee belongs to one of three major beverages in the world, is gradually coming into the lives of people, is an indispensable beverage deeply favored and has the functions of warming the stomach and improving the spirit in a short time after being drunk.
At present, no coffee product containing the active ingredients of the periplaneta americana is found.
Disclosure of Invention
The invention aims to solve the defects of the prior art and provides the cosmetic coffee containing the periplaneta americana active component and the preparation method thereof.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
the cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 25-40% of coffee containing periplaneta americana extract, 1-6% of Chinese olive extract, 1-5% of rhizoma polygonati powder, 25-35% of brown sugar and 30-40% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises one of the following steps:
mixing an extracted concentrated solution of the periplaneta americana with the mass concentration of 5-10% and an extracted concentrated solution of the coffee with the mass concentration of 50-60% in an equal volume manner, concentrating the mixture until the mass concentration is 40-65%, and then carrying out vacuum freeze drying to obtain the coffee containing the periplaneta americana extract, wherein the mass concentration is calculated by solid matters;
secondly, extracting the periplaneta americana with alcohol, filtering, drying filter residues, then carrying out water extraction on the filter residues, drying the obtained water extraction liquid, and mixing the obtained powder with coffee powder according to the mass ratio of 2-5: mixing the materials in a ratio of 25-35 to obtain coffee containing the periplaneta americana extract;
thirdly, carrying out alcohol extraction on the periplaneta americana, filtering, drying filter residues, carrying out water extraction on the filter residues, concentrating an obtained water extraction solution to an extract shape, and mixing the obtained extract and coffee powder according to a mass ratio of 1-3: and (3) mixing the components in a ratio of 25-35 to obtain the coffee containing the periplaneta americana extract.
Further, preferably, the preparation method of the Chinese olive extract comprises the following steps: pulverizing fructus Canarii albi, soaking in 95% ethanol water solution, ultrasonic extracting, and concentrating the extractive solution under reduced pressure until there is no alcohol smell to obtain fructus Canarii albi extract. The preparation method of the olive extract is not limited thereto.
Further, preferably, the preparation method of the rhizoma polygonati powder comprises the following steps: cleaning silt on the surface of rhizoma Polygonati, removing the epidermis and root of rhizoma Polygonati, grinding, adding clear water, filtering, removing residue, and drying the filtrate to obtain rhizoma Polygonati powder. The method for preparing the rhizoma polygonati powder is not limited to the above method.
Further, preferably, the extraction concentrated solution of the periplaneta americana is an aqueous extraction concentrated solution of the periplaneta americana or an alcohol extraction concentrated solution of the periplaneta americana.
Further, preferably, the preparation method of the periplaneta americana extract concentrated solution comprises the steps of firstly extracting the periplaneta americana with alcohol, filtering, then taking filter residues, drying, then carrying out water extraction on the filter residues, and concentrating the water extraction solution to obtain the periplaneta americana extract concentrated solution.
Further, preferably, the preparation method of the coffee extract concentrate in (i) comprises: cleaning and removing impurities from raw coffee beans, baking the raw coffee beans conventionally, grinding the raw coffee beans until the granularity is 90-250 um, extracting the raw coffee beans at 90 ℃ and 6-9 bar by using water as an extraction solvent, and concentrating the extract in vacuum at-50 ℃ to obtain the coffee extraction concentrated solution. The method of preparing the coffee extract concentrate is not limited thereto.
The roasting of the invention can lead the substances contained in the coffee beans to generate complex physical and chemical reactions in the process to form special coffee aroma substances. In order to improve the extraction efficiency, roasted coffee beans are ground into particles with a certain particle size, and vacuum concentration is mainly adopted after extraction so as to facilitate subsequent drying operation.
Further, the drying method in (c) is preferably spray drying or freeze drying.
Further, preferably, the cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 28% of coffee containing periplaneta americana extract, 3% of Chinese olive extract, 1% of fine yellow powder, 33% of brown sugar and 35% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: the preparation method comprises the following steps of mixing 6% of periplaneta americana water extract concentrated solution and 50% of coffee extract concentrated solution in terms of solid matter in equal volume, concentrating until the mass concentration is 40% -65%, and then carrying out vacuum freeze drying to obtain the coffee containing the periplaneta americana extract. The technical scheme is that the optimal proportion is obtained through a plurality of tests, and the color, the taste and the fragrance of the coffee are mainly used as the basis in the experimental process.
In the process of preparing the olive extract, the crushing degree of the olive is not particularly limited.
The preparation method of the cosmetic coffee containing the periplaneta americana active ingredient is to uniformly mix the coffee containing the periplaneta americana extract, the Chinese olive extract, the fine yellow powder, the brown sugar and the non-trans fatty acid non-dairy creamer to obtain the instant cosmetic coffee containing the periplaneta americana active ingredient.
A large number of experiments show that the periplaneta americana extract concentrated solution with the mass concentration of 5-10% and the coffee extract concentrated solution with the mass concentration of 50% are mixed in equal volume and then concentrated to the mass concentration of 40-65%, and then the mixture is subjected to vacuum freeze drying to obtain the periplaneta americana extract-containing coffee, wherein the particle components are uniform and uniform in color, and micropores left when water vapor escapes are fully distributed in the particles and are similar to sponge.
In practical tests, when the concentration of the extracted concentrated solution of the periplaneta americana is more than 15%, the extracted concentrated solution of the periplaneta americana has certain efficacy, but the taste of the extract of the periplaneta americana is extremely strong, the mouthfeel is not good, the cost is high, the interests of drinkers can be influenced to different degrees, after freeze drying and deodorization, although the mouthfeel can be greatly improved, the addition amount of the extracted concentrated solution of the periplaneta americana is too high or too low, so that the beauty coffee containing the active ingredients of the periplaneta americana is not fragrant and mellow, has poor mouthfeel grade indexes, and is not easy to accept by consumers. Meanwhile, researches show that if the addition amounts of the Chinese olive extract and the sealwort powder are too high or too low, the beauty coffee containing the periplaneta americana active component is not fragrant and mellow, has poor taste grade index and is not easy to accept by consumers.
In the research of the invention, the concentrated American cockroach extract solution and the concentrated coffee extract solution are mixed in equal volume, the obtained mixed solution is concentrated, the dissolution time and hardness of coffee particles are influenced due to different water contents after concentration, the coffee particles containing the American cockroach extract prepared from the dilute solution have low density and influence the taste in different degrees although the dissolution time is short, the color of the coffee particles is light, the mixed solution needs to be concentrated in vacuum to the mass concentration of 40-65%, and then the taste and the color of the obtained product are better after vacuum freeze drying.
Compared with the prior art, the invention has the beneficial effects that:
the American cockroach extract, the Chinese olive extract, the fine yellow powder, the coffee and the like are combined to prepare the coffee beverage with the beauty effect, and the coffee beverage has the effects of eliminating free radicals, resisting wrinkles, resisting aging and whitening; meanwhile, the periplaneta americana extraction is complex in process, so that the problem that the periplaneta americana is difficult to prepare and eat in ordinary families is solved.
The invention adds the Chinese olive extract and the sealwort powder in the formula, supplements the beauty and health care efficacy of coffee, has the advantages of saving time and reducing cost, and the freeze-dried coffee containing the periplaneta americana extract has uniform components and uniform color, avoids the damage to the quality of the coffee in the high-temperature drying process in the production of spray-dried coffee or condensed aroma-enhanced coffee, well retains the flavor and taste of the roasted and ground coffee, greatly improves the quality of the instant coffee, and is widely drunk by consumers as a healthy drink.
The invention concentrates the mixed solution of the extracted concentrated solution of the periplaneta americana and the extracted concentrated solution of the coffee to the mass concentration of 40-65 percent, so as to improve the drying efficiency and reduce the equipment investment and the energy consumption; secondly, controlling the specific gravity of finished product particles; can ensure the product to have enough hardness and quick dissolution effect.
The coffee provided by the invention not only has the nutrition and the effect of the coffee, but also has the effects of a certain amount of periplaneta americana and other extracts, such as the effects of promoting tissue repair, eliminating free radicals, whitening, locking water and moisturizing. It is infused with boiling water, and is immediately dissolved, has good texture state, no residue insoluble substance, and strong coffee aroma.
Drawings
FIG. 1 is a graph showing a change in moisture content of the stratum corneum;
FIG. 2 is a graph of the change in trans-epidermal water loss.
Detailed Description
The present invention will be described in further detail with reference to examples.
It will be appreciated by those skilled in the art that the following examples are illustrative of the invention only and should not be taken as limiting the scope of the invention. The examples do not specify particular techniques or conditions, and are performed according to the techniques or conditions described in the literature in the art or according to the product specifications. The materials or equipment used are not indicated by manufacturers, and all are conventional products available by purchase.
Example 1
The cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 25% of coffee containing periplaneta americana extract, 1% of Chinese olive extract, 1% of fine yellow powder, 33% of brown sugar and 40% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: and (3) mixing the water extraction concentrated solution of the periplaneta americana with the mass concentration of 5% and the coffee extraction concentrated solution with the mass concentration of 50% in an equal volume by solid matter, concentrating to the mass concentration of 40%, and then carrying out vacuum freeze drying to obtain the coffee containing the periplaneta americana extract.
Example 2
The cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 30% of coffee containing periplaneta americana extract, 6% of Chinese olive extract, 3% of rhizoma polygonati powder, 30% of brown sugar and 31% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: and (3) mixing the alcohol extract concentrated solution of the periplaneta americana with the mass concentration of 8% and the coffee extract concentrated solution with the mass concentration of 60% in an equal volume, concentrating until the mass concentration is 50%, and then carrying out vacuum freeze drying to obtain the coffee containing the periplaneta americana extract.
Example 3
The cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 40% of coffee containing periplaneta americana extract, 3% of Chinese olive extract, 2% of fine yellow powder, 25% of brown sugar and 30% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: and (3) mixing the extracted concentrated solution of the periplaneta americana with the mass concentration of 10% and the extracted concentrated solution of the coffee with the mass concentration of 55% in an equal volume, concentrating until the mass concentration is 65%, and then carrying out vacuum freeze drying to obtain the coffee containing the periplaneta americana extract.
The preparation method of the extraction concentrated solution of the periplaneta americana comprises the steps of extracting the periplaneta americana with alcohol, filtering, drying filter residues, extracting the filter residues with water, and concentrating the water extraction solution to obtain the extraction concentrated solution.
The preparation method of the coffee extract concentrated solution comprises the following steps: cleaning and removing impurities from raw coffee beans, baking the raw coffee beans conventionally, grinding the raw coffee beans until the granularity is 90-250 um, extracting the raw coffee beans at 90 ℃ and 6-9 bar by using water as an extraction solvent, and concentrating the extract in vacuum at-50 ℃ to obtain the coffee extraction concentrated solution.
The preparation method of the Chinese olive extract comprises the following steps: pulverizing fructus Canarii albi, soaking in 95% ethanol water solution, ultrasonic extracting, and concentrating the extractive solution under reduced pressure until there is no alcohol smell to obtain fructus Canarii albi extract.
The preparation method of the rhizoma polygonati powder comprises the following steps: cleaning silt on the surface of rhizoma Polygonati, removing the epidermis and root of rhizoma Polygonati, grinding, adding clear water, filtering, removing residue, and drying the filtrate to obtain rhizoma Polygonati powder.
Example 4
The cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 26% of coffee containing periplaneta americana extract, 4% of Chinese olive extract, 5% of fine yellow powder, 35% of brown sugar and 30% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: and (3) mixing the extracted concentrated solution of the periplaneta americana with the mass concentration of 7% and the extracted concentrated solution of the coffee with the mass concentration of 50% in an equal volume manner according to the solid content, concentrating the mixture until the mass concentration is 55%, and then carrying out vacuum freeze drying to obtain the coffee containing the periplaneta americana extract.
The preparation method of the extraction concentrated solution of the periplaneta americana comprises the steps of extracting the periplaneta americana with alcohol, filtering, drying filter residues, extracting the filter residues with water, and concentrating the water extraction solution to obtain the extraction concentrated solution.
Example 5
The cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 28% of coffee containing periplaneta americana extract, 3% of Chinese olive extract, 1% of fine yellow powder, 33% of brown sugar and 35% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: and (3) mixing the water extraction concentrated solution of the periplaneta americana with the mass concentration of 6% and the coffee extraction concentrated solution with the mass concentration of 50% in an equal volume according to the solid content, concentrating until the mass concentration is 50%, and then carrying out vacuum freeze drying to obtain the coffee containing the periplaneta americana extract.
The preparation method of the coffee extraction concentrated solution comprises the following steps: cleaning and removing impurities from raw coffee beans, baking the raw coffee beans conventionally, grinding the raw coffee beans until the granularity is 90-250 um, extracting the raw coffee beans at 90 ℃ and 6-9 bar by using water as an extraction solvent, and concentrating the extract in vacuum at-50 ℃ to obtain the coffee extraction concentrated solution.
The preparation method of the Chinese olive extract comprises the following steps: pulverizing fructus Canarii albi, soaking in 95% ethanol water solution, ultrasonic extracting, and concentrating the extractive solution under reduced pressure until there is no alcohol smell to obtain fructus Canarii albi extract.
The preparation method of the rhizoma polygonati powder comprises the following steps: cleaning silt on the surface of rhizoma Polygonati, removing the epidermis and root of rhizoma Polygonati, grinding, adding clear water, filtering, removing residue, and drying the filtrate to obtain rhizoma Polygonati powder.
Example 6
The cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 25% of coffee containing periplaneta americana extract, 6% of Chinese olive extract, 5% of rhizoma polygonati powder, 30% of brown sugar and 34% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: extracting the periplaneta americana with alcohol, filtering, drying filter residue, then carrying out water extraction on the filter residue, carrying out spray drying on the obtained water extraction solution, and mixing the obtained powder and coffee powder according to the mass ratio of 2: 25 to obtain the coffee containing the periplaneta americana extract;
example 7
The cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 33% of coffee containing periplaneta americana extract, 1% of Chinese olive extract, 1% of fine yellow powder, 30% of brown sugar and 35% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: extracting the periplaneta americana with alcohol, filtering, drying filter residue, then carrying out water extraction on the filter residue, and mixing the obtained powder and coffee powder according to the mass ratio of 3: 30 to obtain the coffee containing the periplaneta americana extract;
example 8
The cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 35% of coffee containing periplaneta americana extract, 5% of Chinese olive extract, 5% of rhizoma polygonati powder, 25% of brown sugar and 30% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: extracting the periplaneta americana with alcohol, filtering, drying filter residue, then carrying out water extraction on the filter residue, carrying out freeze drying on the water extract of the obtained water extract, and mixing the obtained powder and coffee powder according to the mass ratio of 5: 35 to obtain the coffee containing the periplaneta americana extract;
the preparation method of the coffee extraction concentrated solution comprises the following steps: cleaning and removing impurities from raw coffee beans, baking the raw coffee beans conventionally, grinding the raw coffee beans until the granularity is 90-250 um, extracting the raw coffee beans at 90 ℃ and 6-9 bar by using water as an extraction solvent, and concentrating the extract in vacuum at-50 ℃ to obtain the coffee extraction concentrated solution.
The preparation method of the Chinese olive extract comprises the following steps: pulverizing fructus Canarii albi, soaking in 95% ethanol water solution, ultrasonic extracting, and concentrating the extractive solution under reduced pressure until there is no alcohol smell to obtain fructus Canarii albi extract.
The preparation method of the rhizoma polygonati powder comprises the following steps: cleaning silt on the surface of rhizoma Polygonati, removing the epidermis and root of rhizoma Polygonati, grinding, adding clear water, filtering, removing residue, and drying the filtrate to obtain rhizoma Polygonati powder.
Example 9
The cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 27% of coffee containing periplaneta americana extract, 1% of Chinese olive extract, 5% of rhizoma polygonati powder, 32% of brown sugar and 35% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: extracting periplaneta americana with alcohol, filtering, drying filter residue, then extracting the filter residue with water, concentrating the obtained water extract to extract, wherein the mass ratio of the obtained extract to coffee powder is 2: 25 to obtain the coffee containing the periplaneta americana extract.
Example 10
The cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 39% of coffee containing periplaneta americana extract, 5% of Chinese olive extract, 1% of rhizoma polygonati powder, 25% of brown sugar and 30% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: extracting periplaneta americana with alcohol, filtering, drying filter residue, then extracting the filter residue with water, concentrating the obtained water extract to extract, wherein the mass ratio of the obtained extract to coffee powder is 1: 35 to obtain the coffee containing the periplaneta americana extract.
Example 11
The cosmetic coffee containing the periplaneta americana active ingredient comprises the following components in percentage by mass: 25-40% of coffee containing periplaneta americana extract, 1-6% of Chinese olive extract, 1-5% of rhizoma polygonati powder, 25-35% of brown sugar and 30-40% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: extracting periplaneta americana with alcohol, filtering, drying filter residue, then extracting the filter residue with water, concentrating the obtained water extract to extract, wherein the mass ratio of the obtained extract to coffee powder is 3: 28 to obtain the coffee containing the periplaneta americana extract.
The preparation method of the coffee extraction concentrated solution comprises the following steps: cleaning and removing impurities from raw coffee beans, baking the raw coffee beans conventionally, grinding the raw coffee beans until the granularity is 90-250 um, extracting the raw coffee beans at 90 ℃ and 6-9 bar by using water as an extraction solvent, and concentrating the extract in vacuum at-50 ℃ to obtain the coffee extraction concentrated solution.
The preparation method of the Chinese olive extract comprises the following steps: pulverizing fructus Canarii albi, soaking in 95% ethanol water solution, ultrasonic extracting, and concentrating the extractive solution under reduced pressure until there is no alcohol smell to obtain fructus Canarii albi extract.
The preparation method of the rhizoma polygonati powder comprises the following steps: cleaning silt on the surface of rhizoma Polygonati, removing the epidermis and root of rhizoma Polygonati, grinding, adding clear water, filtering, removing residue, and drying the filtrate to obtain rhizoma Polygonati powder.
Test example 1 effects of coffee of the present invention on anti-wrinkle and anti-photoaging effects on skin
The control group was given regular coffee, the test group was coffee of example 5 of the present invention, and 10 adult hairless mice were each gavaged with coffee at a dose of 700mg/kg daily and a gavage volume of 0.1ml/10g for 2 weeks. The TEWL (water loss rate through the epidermis) was measured on the days, 3 days and 4 days after the irradiation of the ultraviolet rays (wavelength 200-275 nm, power 1.5W), and a significant decrease of the TEWL was found, which indicates that the coffee of the present invention exerts a protective effect on the epidermal penetration barrier and increases the ultraviolet dose, and the wrinkle formation of each mouse was measured according to the wrinkle grade scoring table by administering the coffee of the present invention example 5, and the result showed that the ultraviolet-induced wrinkle formation rate was decreased by 32% (P < 0.001) after the administration of the coffee of the present invention example 5.
Test example 2
1. Influence of periplaneta americana coffee on skin health after sun exposure
The control group was given regular coffee, and the test group was coffee of example 3 according to the present invention, and 10 men were given afternoon drinking for 4 weeks at a drinking amount of 320 ml/day and then continuously used at 0.054J/cm in their back area2To 0.135J/cm2Dose of ultraviolet (UVA + UVB 0.45Mw/cm2) And (4) irradiating. The lowest red spot dose (MED) was measured before and after drinking the coffee of example 5 of the present invention, respectively, and the results showed that drinking periplaneta americana coffee increased MED by 23.17% on average (P < 0.01), indicating that periplaneta americana coffee helped to promote the health of the skin after sun exposure.
2. Periplaneta americana coffee water-locking and moisture-keeping and whitening efficacy test for skin
Because the skin has poor water locking effect or the skin lacks water due to little water supplement, the skin is characterized in that: dry, rough, loose, rough and deep wrinkles, prolonged water shortage, extrinsic photoaging and ultraviolet irradiation, resulting in increased pigmentation spots, telangiectasia and sallow complexion. The 48 healthy adult populations were randomly divided into periplaneta americana coffee group and a control group. 24 Periplaneta americana coffee groups (8 males, 16 females and 18-40 years old) and 24 control groups (9 males, 15 females and 18-40 years old).
Periplaneta americana coffee group: by adopting the coffee of the embodiment 8 of the invention, the brewing dosage is 280ml after lunch, and the drinking habit is according to personal preference, and the coffee is continuously drunk for 2 months.
Control group: the common coffee is brewed, the same amount of 280ml of the coffee is brewed after lunch every day, and the drinking habit is according to personal preference, and the coffee is continuously drunk for 2 months.
Skin elasticity and skin texture were observed by measuring the water content of the stratum Corneum (CAP), the transepidermal water loss rate (TEWL) of the skin at 5 and 8 weeks of drinking, respectively. The periplaneta americana coffee group improved the coarseness in texture analysis compared to the regular coffee group. Meanwhile, the water content in the horny layer also showed an increasing tendency, and the curve of the change value of the water content in the horny layer is shown in fig. 1. The trans-epidermal water loss rate (TEWL) decreased significantly, with the change profile shown in figure 2. The transepidermal water loss (TC) per unit area per unit time is reduced. The water-locking and moisture-keeping effects are good, the skin looseness of the exposed part of the periplaneta americana coffee group is obviously improved, the different degrees of pigment spots are reduced, and the skin moistening glossiness is improved. The change values of the water Content (CAP) and the transepidermal water loss rate (TEWL) of the stratum corneum are shown in table 1:
TABLE 1 CAP and TEWL test mean, variance results
Note: CAP represents the moisture content (%) of the stratum corneum of the skin, Δ CAP represents the difference between the moisture content of the stratum corneum of the skin and the base value (0) day, TEWL represents the transepidermal water loss rate (%), ΔTEWL represents the difference between the transepidermal water loss rate of the skin and the base value (0) day, TC represents the ratio of the transepidermal water loss rate of the skin to the moisture content of the stratum corneum of the skin, and TC drop indicates good water-locking and moisturizing effects.
The experimental result shows that compared with the common coffee, the moisture content of the skin horny layer of the coffee of the invention is improved obviously in 5 weeks and 8 weeks of drinking, the water loss rate through the epidermis is obviously reduced compared with the control group, and the moisturizing effect of the coffee group for treating the periplaneta americana is good.
Test example 3: observation of synergy test
The products of example 5 were drunk by 50 healthy people in three groups, the first group was different from example 5 in that the products of example 5 did not contain olive extract and polygonatum powder, and the third group was drunk with olive extract and polygonatum powder in the same amount as the products of example 5; 16 cases in the first group, 18 cases in the second group, and 16 cases in the third group; the drinking amount is 280ml, and the drinking time is up to 7 weeks;
the results show that people drinking the three groups of products have the advantages of improving the skin laxity of the exposed part, increasing the skin tissue vitality and having less wrinkles; the moisture content of the horny layer of the skin of people drinking the first group of products is obviously improved, and the water loss rate through the epidermis is obviously reduced; the skin glossiness is improved and the skin improvement effect is more obvious. The third group had a slight effect, but the effect was the worst of the three groups. The water content of the three groups of skin cuticles and the change value of the per-epidermal water loss rate are shown in table 2:
TABLE 2 CAP and TEWL test mean, variance results
Note: CAP represents the moisture content (%) of the stratum corneum of the skin, Δ CAP represents the difference between the moisture content of the stratum corneum of the skin and the base value (0) day, TEWL represents the transepidermal water loss rate (%), ΔTEWL represents the difference between the transepidermal water loss rate of the skin and the base value (0) day, TC represents the ratio of the transepidermal water loss rate of the skin to the moisture content of the stratum corneum of the skin, and TC drop indicates good water-locking and moisturizing effects.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (6)
1. The beauty coffee containing the periplaneta americana active component is characterized by comprising the following components in percentage by mass: 25-40% of coffee containing periplaneta americana extract, 1-6% of Chinese olive extract, 1-5% of rhizoma polygonati powder, 25-35% of brown sugar and 30-40% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises one of the following steps:
mixing 5-10% of periplaneta americana extract concentrated solution and 50-60% of coffee extract concentrated solution in terms of solid matter in equal volume, concentrating the mixture until the mass concentration is 40-65%, and then performing vacuum freeze drying to obtain coffee containing the periplaneta americana extract;
secondly, extracting the periplaneta americana with alcohol, filtering, drying filter residues, then carrying out water extraction on the filter residues, drying the obtained water extraction liquid, and mixing the obtained powder with coffee powder according to the mass ratio of 2-5: mixing the materials in a ratio of 25-35 to obtain coffee containing the periplaneta americana extract;
thirdly, carrying out alcohol extraction on the periplaneta americana, filtering, drying filter residues, carrying out water extraction on the filter residues, concentrating an obtained water extraction solution to an extract shape, and mixing the obtained extract and coffee powder according to a mass ratio of 1-3: mixing the materials in a ratio of 25-35 to obtain coffee containing the periplaneta americana extract;
the preparation method of the Chinese olive extract comprises the following steps: crushing Chinese olive, soaking in 95 vol% ethanol water solution, ultrasonic extracting, and concentrating the extractive solution under reduced pressure until no alcohol smell is produced to obtain Chinese olive extract;
the preparation method of the rhizoma polygonati powder comprises the following steps: cleaning silt on the surface of rhizoma Polygonati, removing the epidermis and root of rhizoma Polygonati, grinding, adding clear water, filtering, removing residue, and drying the filtrate to obtain rhizoma Polygonati powder.
2. The beauty coffee containing the periplaneta americana active ingredient as claimed in claim 1, wherein the extraction concentrate of (i) the periplaneta americana is an aqueous extraction concentrate of the periplaneta americana or an alcohol extraction concentrate of the periplaneta americana.
3. The beauty coffee containing the periplaneta americana active ingredient according to claim 1, wherein the periplaneta americana extract concentrate is prepared by extracting the periplaneta americana with alcohol, filtering, drying the filter residue, extracting the filter residue with water, and concentrating the water extract to obtain the periplaneta americana extract concentrate.
4. The beauty coffee containing the periplaneta americana active ingredient according to claim 1, wherein the preparation method of the coffee extract concentrate in (i) comprises the following steps: cleaning and removing impurities from raw coffee beans, baking the raw coffee beans conventionally, grinding the raw coffee beans until the granularity is 90-250 um, extracting the raw coffee beans at the temperature of 90 ℃ and under the pressure of 6-9 bar by using water as an extraction solvent, and concentrating the extract in vacuum at the temperature of-50 ℃ to obtain the coffee extraction concentrated solution.
5. The cosmetic coffee containing the periplaneta americana active ingredient according to claim 1, wherein the drying method in (ii) is spray drying or freeze drying.
6. The American cockroach active ingredient-containing cosmetic coffee according to claim 1, which comprises the following components in percentage by mass: 28% of coffee containing periplaneta americana extract, 3% of Chinese olive extract, 1% of fine yellow powder, 33% of brown sugar and 35% of trans-fatty acid-free non-dairy creamer;
the preparation method of the coffee containing the periplaneta americana extract comprises the following steps: the preparation method comprises the following steps of mixing 6% of periplaneta americana water extract concentrated solution and 50% of coffee extract concentrated solution in terms of solid matter in equal volume, concentrating until the mass concentration is 40% -65%, and then carrying out vacuum freeze drying to obtain the coffee containing the periplaneta americana extract.
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| CN101558874A (en) * | 2009-05-22 | 2009-10-21 | 杨卫祖 | American cockroach-honey refined flavor cream and preparation method thereof |
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