CN105496860A - Compound herbal toothpaste for middle-age and old-age persons - Google Patents
Compound herbal toothpaste for middle-age and old-age persons Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/42—Cucurbitaceae (Cucumber family)
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/65—Paeoniaceae (Peony family), e.g. Chinese peony
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/80—Scrophulariaceae (Figwort family)
- A61K36/804—Rehmannia
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- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/591—Mixtures of compounds not provided for by any of the codes A61K2800/592 - A61K2800/596
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Abstract
The invention relates to compound herbal toothpaste for middle-age and old-age persons, in particular to toothpaste containing extracts of fructus momordicae, rhizomes of rehmannia and red peony roots, a preparation method thereof and application to improving gingival atrophy. The toothpaste is prepared from, by mass, 25-30 parts of Chinese herbal medicine, 1-1.2 parts of Chinese herbal medicine additives, 15-20 parts of calcium phosphate, 1-3 parts of hydroxyethyl cellulose, 10-20 parts of glycerin, 0.01 part of saccharin, 0.5 part of grapefruit oil and 90-100 parts of water. In the Chinese herbal medicine, the weight proportion of fructus momordicae, rhizomes of rehmannia and red peony roots is 10:0.5:1, in the Chinese herbal medicine additives, the weight proportion of indigo naturalis, root bark of peony trees, lithospermum purpurocaeruleum and indigowoad leaves is 1:1:2:1.5, the Chinese herbal medicine additives can effectively inhibit loss of vitamin C in the Chinese herbal medicine extracts and the toothpaste, and the medicine effect is kept for a long time. The toothpaste can effectively improve the gingival senile symptoms of middle-age and old-age persons and is simple in manufacturing technology and low in cost.
Description
Technical field
The present invention relates to a kind of person in middle and old age's compound recipe herbaceous toothpaste, the toothpaste particularly containing Fructus Momordicae, the Radix Rehmanniae, Radix Paeoniae Rubra extract, and preparation method thereof.
Background technology
With advancing age, the physical function of people declines gradually, and skin, tooth also start " aging " gradually, and for aging, most people feels the disease that can not be cured.Therefore, after old people's gingiva senile symptom starts performance, generally can not take any mode to treat.Although we cannot stop aging, can slow down aging.The main manifestations of gingiva aging is gingival atrophy.
Current research shows, the principal element of gingival atrophy is gingiva malnutrition, with advancing age, the nutrition that gingiva is absorbed by digestive system is fewer and feweri, especially ascorbic absorption obviously reduces, and causes gingiva to produce malnutrition, under gingiva is in malnutrition for a long time, gingiva will constantly atrophy, finally shows as aging.Gingival atrophy often shows as that root of the tooth is exposed, red swelling of gingiva, gingival hemorrhage, teeth space become large, odontoseisis etc.
At present, the toothpaste for the aging of person in middle and old age's gingiva is rare, and mica filled polypropylene can effectively treat gingiva aging, but due to cost high, price is high, and make in mid-aged population, utilization rate is low.
Summary of the invention
Containing abundant vitamin C and fructose, glucose, protein to the description of Fructus Momordicae in " traditional Chinese medical science pharmacopeia ", and containing the necessary trace element of 16 kinds of human bodies and extensive element, containing higher potassium, calcium, magnesium, selenium, wherein contained elemental selenium has coronary heart disease control, defying age, the pharmacological action such as anticancer, to arrange in pairs or groups again the disinfecting, antimicrobial effect of the Radix Rehmanniae and Radix Paeoniae Rubra, can effectively improve person in middle and old age's gingival atrophy.
Abundant vitamin C is rich in Fructus Momordicae, but because light and heat can make vitamin C loss more in leaching process, and the toothpaste finished product made, vitamin loss speed is fast, the duration of efficacy of toothpaste is short, by grinding extraction and in Fructus Momordicae, the Radix Rehmanniae, Radix Paeoniae Rubra extracting solution, add Indigo Naturalis that weight ratio is 1:1:2:1.5, loss that Cortex Moutan, Radix Arnebiae (Radix Lithospermi), Folium Isatidis extracting solution effectively can suppress vitamin, keep permanent drug effect.
The object of this invention is to provide a kind of person in middle and old age's compound recipe herbaceous toothpaste, can effectively treat person in middle and old age's gingival atrophy, and technique is simple, cost is low.
Another object of the present invention is to provide a kind of preparation method of person in middle and old age's compound recipe herbaceous toothpaste.
Another object of the present invention is to provide the application of a kind of person in middle and old age's compound recipe herbaceous toothpaste old gingival atrophy aspect in the treatment.
Technical scheme of the present invention is:
A kind of person in middle and old age's compound recipe herbaceous toothpaste, comprises Chinese herbal medicine 25-30 part, Chinese herbal medicine additive 1-1.2 part, calcium phosphate 15-20 part, hydroxyethyl-cellulose 1-3 part, glycerol 10-20 part, 0.01 part, glucide, grape-fruit seed oil 0.5 part, water 90-100 part in mass ratio in its composition.
A kind of person in middle and old age's compound recipe herbaceous toothpaste, wherein Chinese herbal medicine is Fructus Momordicae, the Radix Rehmanniae, the Radix Paeoniae Rubra of weight ratio 10:0.5:1.
A kind of person in middle and old age's compound recipe herbaceous toothpaste, wherein Chinese herbal medicine additive is the Indigo Naturalis of weight ratio 1:1:2:1.5, Cortex Moutan, Radix Arnebiae (Radix Lithospermi), Folium Isatidis.
A kind of preparation method of person in middle and old age's compound recipe herbaceous toothpaste:
(1) Fructus Momordicae, the Radix Rehmanniae, Radix Paeoniae Rubra 25-30 part is taken by weight 10:0.5:1, mix and use soak with ethanol 15 minutes, grind in alcoholic solution, continue to soak 1h, by 100 orders (150 microns) screen filtration, collect the liquid that sieves, unsifted residual medicine is continued add ethanol grinding, continue collection to sieve liquid, without obvious left drug to sieve;
(2) take Indigo Naturalis, Cortex Moutan, Radix Arnebiae (Radix Lithospermi), Folium Isatidis 1-1.2 part by weight 1:1:2:1.5, add water after mixing, 100 DEG C decoct after 20 minutes, and 70 DEG C decoct 1h, and cooling is filtered, and collects filtrate;
(3) filtrate in step (2) being joined step (1) sieves in liquid, and after mix homogeneously, after lucifuge leaves standstill 3h, being concentrated into relative density is 1.1-1.15, and spraying dry obtains Chinese herbal medicine extract dry powder;
(4) by hydroxyethyl-cellulose 1-3 part, glycerol 10-20 part, grape-fruit seed oil 0.5 part, water 90-100 part, put into glue pot, stir, then add 0.01 part, glucide, be stirred to translucent, then leave standstill 1-2h, then add the calcium phosphate of the obtained Chinese herbal medicine extract dry powder of step (3) and 15-20 part; Stir 1-2h, obtain mastic; After again mastic being ground by grinder, obtained toothpaste.
Advantage of the present invention is:
1. technique is simple, and cost is low;
2. Chinese herbal medicine additive effectively can suppress ascorbic loss in extracts of Chinese herbal medicine and toothpaste, keeps permanent drug effect;
3. can effectively treat person in middle and old age's gingival atrophy.
Detailed description of the invention
Embodiment 1
A kind of preparation method of person in middle and old age's compound recipe herbaceous toothpaste:
(1) Fructus Momordicae, the Radix Rehmanniae, Radix Paeoniae Rubra 25 parts is taken by weight 10:0.5:1, mix and use soak with ethanol 15 minutes, grind in alcoholic solution, continue to soak 1h, by 100 orders (150 microns) screen filtration, collect the liquid that sieves, unsifted residual medicine is continued add ethanol grinding, continue collection to sieve liquid, without obvious left drug to sieve;
(2) take Indigo Naturalis, Cortex Moutan, Radix Arnebiae (Radix Lithospermi), Folium Isatidis 1 part by weight 1:1:2:1.5, add water after mixing, 100 DEG C decoct after 20 minutes, and 70 DEG C decoct 1h, and cooling is filtered, and collects filtrate;
(3) filtrate in step (2) being joined step (1) sieves in liquid, and after mix homogeneously, after lucifuge leaves standstill 3h, being concentrated into relative density is 1.1, and spraying dry obtains Chinese herbal medicine extract dry powder;
(4) by hydroxyethyl-cellulose 1.5 parts, glycerol 15 parts, grape-fruit seed oil 0.5 part, 100 parts, water, put into glue pot, stir, then add 0.01 part, glucide, be stirred to translucent, then leave standstill 2h, then add the calcium phosphate of the obtained Chinese herbal medicine extract dry powder of step (3) and 18 parts; Stir 2h, obtain mastic; After again mastic being ground by grinder, obtained toothpaste.
Embodiment 2
A kind of preparation method of person in middle and old age's compound recipe herbaceous toothpaste:
(1) Fructus Momordicae, the Radix Rehmanniae, Radix Paeoniae Rubra 30 parts is taken by weight 10:0.5:1, mix and use soak with ethanol 15 minutes, grind in alcoholic solution, continue to soak 1h, by 100 orders (150 microns) screen filtration, collect the liquid that sieves, unsifted residual medicine is continued add ethanol grinding, continue collection to sieve liquid, without obvious left drug to sieve;
(2) take Indigo Naturalis, Cortex Moutan, Radix Arnebiae (Radix Lithospermi), Folium Isatidis 1.2 parts by weight 1:1:2:1.5, add water after mixing, 100 DEG C decoct after 20 minutes, and 70 DEG C decoct 1h, and cooling is filtered, and collects filtrate;
(3) filtrate in step (2) being joined step (1) sieves in liquid, and after mix homogeneously, after lucifuge leaves standstill 3h, being concentrated into relative density is 1.15, and spraying dry obtains Chinese herbal medicine extract dry powder;
(4) by hydroxyethyl-cellulose 3 parts, glycerol 10 parts, grape-fruit seed oil 0.5 part, 95 parts, water, put into glue pot, stir, then add 0.01 part, glucide, be stirred to translucent, then leave standstill 1.5h, then add the calcium phosphate of the obtained Chinese herbal medicine extract dry powder of step (3) and 15 parts; Stir 1h, obtain mastic; After again mastic being ground by grinder, obtained toothpaste.
Embodiment 3
A kind of preparation method of person in middle and old age's compound recipe herbaceous toothpaste:
(1) Fructus Momordicae, the Radix Rehmanniae, Radix Paeoniae Rubra 28 parts is taken by weight 10:0.5:1, mix and use soak with ethanol 15 minutes, grind in alcoholic solution, continue to soak 1h, by 100 orders (150 microns) screen filtration, collect the liquid that sieves, unsifted residual medicine is continued add ethanol grinding, continue collection to sieve liquid, without obvious left drug to sieve;
(2) take Indigo Naturalis, Cortex Moutan, Radix Arnebiae (Radix Lithospermi), Folium Isatidis 1.1 parts by weight 1:1:2:1.5, add water after mixing, 100 DEG C decoct after 20 minutes, and 70 DEG C decoct 1h, and cooling is filtered, and collects filtrate;
(3) filtrate in step (2) being joined step (1) sieves in liquid, and after mix homogeneously, after lucifuge leaves standstill 3h, being concentrated into relative density is 1.12, and spraying dry obtains Chinese herbal medicine extract dry powder;
(4) by hydroxyethyl-cellulose 1 part, glycerol 20 parts, grape-fruit seed oil 0.5 part, 90 parts, water, put into glue pot, stir, then add 0.01 part, glucide, be stirred to translucent, then leave standstill 1h, then add the calcium phosphate of the obtained Chinese herbal medicine extract dry powder of step (3) and 20 parts; Stir 1.5h, obtain mastic; After again mastic being ground by grinder, obtained toothpaste.
Embodiment 4
A kind of preparation method of person in middle and old age's compound recipe herbaceous toothpaste:
(1) Fructus Momordicae, the Radix Rehmanniae, Radix Paeoniae Rubra 27 parts is taken by weight 10:0.5:1, mix and use soak with ethanol 15 minutes, grind in alcoholic solution, continue to soak 1h, by 100 orders (150 microns) screen filtration, collection is sieved liquid, continue unsifted residual medicine to add ethanol grinding, continue collection and to sieve liquid, without obvious left drug to sieve, it is 1.11 that the liquid that will sieve is concentrated into relative density, and spraying dry obtains Chinese herbal medicine extract dry powder;
(2) by hydroxyethyl-cellulose 1.5 parts, glycerol 15 parts, grape-fruit seed oil 0.5 part, 95 parts, water, put into glue pot, stir, then add 0.01 part, glucide, be stirred to translucent, then leave standstill 1.5h, then add the calcium phosphate of the obtained Chinese herbal medicine extract dry powder of step (1) and 15 parts; Stir 2h, obtain mastic; After again mastic being ground by grinder, obtained toothpaste.
Embodiment 5
A kind of preparation method of person in middle and old age's compound recipe herbaceous toothpaste:
(1) Fructus Momordicae, the Radix Rehmanniae, Radix Paeoniae Rubra 27 parts is taken by weight 10:0.5:1, mix and use soak with ethanol 15 minutes, grind in alcoholic solution, continue to soak 1h, by 100 orders (150 microns) screen filtration, collect the liquid that sieves, unsifted residual medicine is continued add ethanol grinding, continue collection to sieve liquid, without obvious left drug to sieve;
(2) take Indigo Naturalis, Cortex Moutan, Radix Arnebiae (Radix Lithospermi), Folium Isatidis 0.9 part by weight 1:1:2:1.5, add water after mixing, 100 DEG C decoct after 20 minutes, and 70 DEG C decoct 1h, and cooling is filtered, and collects filtrate;
(3) filtrate in step (2) being joined step (1) sieves in liquid, and after mix homogeneously, after lucifuge leaves standstill 3h, be concentrated into 1.13, spraying dry obtains Chinese herbal medicine extract dry powder;
(4) by hydroxyethyl-cellulose 2 parts, glycerol 17 parts, grape-fruit seed oil 0.5 part, 95 parts, water, put into glue pot, stir, then add 0.01 part, glucide, be stirred to translucent, then leave standstill 2h, then add the calcium phosphate of the obtained Chinese herbal medicine extract dry powder of step (3) and 17 parts; Stir 1h, obtain mastic; After again mastic being ground by grinder, obtained toothpaste.
Embodiment 6
A kind of preparation method of person in middle and old age's compound recipe herbaceous toothpaste:
(1) Fructus Momordicae, the Radix Rehmanniae, Radix Paeoniae Rubra 30 parts is taken by weight 10:0.5:1, mix and use soak with ethanol 15 minutes, grind in alcoholic solution, continue to soak 1h, by 100 orders (150 microns) screen filtration, collect the liquid that sieves, unsifted residual medicine is continued add ethanol grinding, continue collection to sieve liquid, without obvious left drug to sieve;
(2) take Indigo Naturalis, Cortex Moutan, Radix Arnebiae (Radix Lithospermi), Folium Isatidis 1.3 parts by weight 1:1:2:1.5, add water after mixing, 100 DEG C decoct after 20 minutes, and 70 DEG C decoct 1h, and cooling is filtered, and collects filtrate;
(3) filtrate in step (2) being joined step (1) sieves in liquid, and after mix homogeneously, after lucifuge leaves standstill 3h, be concentrated into 1.12, spraying dry obtains Chinese herbal medicine extract dry powder;
(4) by hydroxyethyl-cellulose 2.5 parts, glycerol 12 parts, grape-fruit seed oil 0.5 part, 95 parts, water, put into glue pot, stir, then add 0.01 part, glucide, be stirred to translucent, then leave standstill 2h, then add the calcium phosphate of the obtained Chinese herbal medicine extract dry powder of step (3) and 19 parts; Stir 1.5h, obtain mastic; After again mastic being ground by grinder, obtained toothpaste.
Embodiment 7
Random selecting gingival atrophy patient, totally 147 people, wherein male patient 91 people, female patient 56 people, age distribution: 35 years old-45 years old 46 people, 46 years old-60 years old 40 people, 61 years old-75 years old 26 people, more than 75 years old 35 people, patient condition shows as that root of the tooth is exposed, red swelling of gingiva, gingival hemorrhage, pain.The personnel of participating in the experiment are divided into 7 groups, and 1-6 group uses toothpaste prepared by embodiment 1-6, and 7 groups use conventional toothpaste, sooner or later each brush teeth, and brush teeth 2-3 minute at every turn, avoid pungent and diet before sleeping, 1 month experimental period;
Obvious improvement: red swelling of gingiva and bleeding disappear, and root of the tooth is over half to be wrapped up by gingiva, and pain disappears, and continue a week more than;
Effective improvement: red swelling of gingiva and bleeding disappear, and root of the tooth is exposed not obvious, and pain weakens or disappears;
Invalid: red swelling of gingiva, bleeding do not improve or increase the weight of, and root of the tooth is exposed;
| Group number | 1 | 2 | 3 | 4 | 5 | 6 | 7 |
| Number | 23 | 21 | 22 | 19 | 20 | 22 | 20 |
| Obvious improvement | 20 | 20 | 19 | 5 | 6 | 5 | 7 |
| Effective improvement | 1 | 1 | 2 | 6 | 9 | 8 | 9 |
| Invalid | 2 | 0 | 1 | 8 | 5 | 9 | 4 |
The toothpaste obtained by embodiment 1-3 that conclusion: group number 1-3 uses, component and content are all within the scope of the invention, the toothpaste obtained by embodiment 4-6 that group number 4-6 uses, component or content is not within the scope of the invention, contrast groups 7, visible embodiment 1-3 better effects if, embodiment 2 is optimal case, 4-6 group less effective.
Embodiment 8
The relation of Vitamin C content and Chinese herbal medicine additive addition in experimentation Chinese herbal medicine Fructus Momordicae, the Radix Rehmanniae, Radix Paeoniae Rubra extracting solution, in embodiment 1,2,3,5,6 step (3) leave standstill after extracting solution be experimental group, in embodiment 4, the liquid that sieves of step (1) gained is matched group, extracting solution and the liquid that sieves are divided into 6 groups, test one group every 1h, result is as follows:
Toothpaste obtained in embodiment 1-6 respectively gets 1, measures its vitamin content, and every test in 1 month once, result is as follows:
Conclusion: in embodiment 1-3, Chinese herbal medicine additive component and content are all within the scope of the invention, visible vitamin content is stablized, in embodiment 4-6, Chinese herbal medicine additive component or content is not within the scope of the invention, visible vitamin loss is obvious, and embodiment 4 does not add Chinese herbal medicine additive, and vitamin loss is the fastest.
Claims (5)
1. person in middle and old age's compound recipe herbaceous toothpaste, is characterized in that: comprise Chinese herbal medicine 25-30 part, Chinese herbal medicine additive 1-1.2 part, calcium phosphate 15-20 part, hydroxyethyl-cellulose 1-3 part, glycerol 10-20 part, 0.01 part, glucide, grape-fruit seed oil 0.5 part, water 90-100 part in its composition in mass ratio.
2. a kind of person in middle and old age's compound recipe herbaceous toothpaste according to claim 1, is characterized in that: Chinese herbal medicine is Fructus Momordicae, the Radix Rehmanniae, the Radix Paeoniae Rubra of weight ratio 10:0.5:1.
3. a kind of person in middle and old age's compound recipe herbaceous toothpaste according to claim 1, is characterized in that: Chinese herbal medicine additive is weight ratio 1:1:2:1.5 Indigo Naturalis, Cortex Moutan, Radix Arnebiae (Radix Lithospermi), Folium Isatidis.
4. a kind of person in middle and old age's compound recipe herbaceous toothpaste according to claim 1, is characterized in that:
A kind of preparation method of person in middle and old age's compound recipe herbaceous toothpaste:
(1) Fructus Momordicae, the Radix Rehmanniae, Radix Paeoniae Rubra 25-30 part is taken by weight 10:0.5:1, mix and use soak with ethanol 15 minutes, grind in alcoholic solution, continue to soak 1h, by 100 orders (150 microns) screen filtration, collect the liquid that sieves, unsifted residual medicine is continued add ethanol grinding, continue collection to sieve liquid, without obvious left drug to sieve;
(2) take Indigo Naturalis, Cortex Moutan, Radix Arnebiae (Radix Lithospermi), Folium Isatidis 1-1.2 part by weight 1:1:2:1.5, add water after mixing, 100 DEG C decoct after 20 minutes, and 70 DEG C decoct 1h, and cooling is filtered, and collects filtrate;
(3) filtrate in step (2) being joined step (1) sieves in liquid, and after mix homogeneously, after lucifuge leaves standstill 3h, being concentrated into relative density is 1.1-1.15, and spraying dry obtains Chinese herbal medicine extract dry powder;
(4) by hydroxyethyl-cellulose 1-3 part, glycerol 10-20 part, grape-fruit seed oil 0.5 part, water 90-100 part, put into glue pot, stir, then add 0.01 part, glucide, be stirred to translucent, then leave standstill 1-2h, then add the calcium phosphate of the obtained Chinese herbal medicine extract dry powder of step (3) and 15-20 part; Stir 1-2h, obtain mastic; After again mastic being ground by grinder, obtained toothpaste.
5. a kind of person in middle and old age's compound recipe herbaceous toothpaste according to claim 4, is characterized in that:
A kind of preparation method of person in middle and old age's compound recipe herbaceous toothpaste:
(1) Fructus Momordicae, the Radix Rehmanniae, Radix Paeoniae Rubra 30 parts is taken by weight 10:0.5:1, mix and use soak with ethanol 15 minutes, grind in alcoholic solution, continue to soak 1h, by 100 orders (150 microns) screen filtration, collect the liquid that sieves, unsifted residual medicine is continued add ethanol grinding, continue collection to sieve liquid, without obvious left drug to sieve;
(2) take Indigo Naturalis, Cortex Moutan, Radix Arnebiae (Radix Lithospermi), Folium Isatidis 1.2 parts by weight 1:1:2:1.5, add water after mixing, 100 DEG C decoct after 20 minutes, and 70 DEG C decoct 1h, and cooling is filtered, and collects filtrate;
(3) filtrate in step (2) being joined step (1) sieves in liquid, and after mix homogeneously, after lucifuge leaves standstill 3h, being concentrated into relative density is 1.15, and spraying dry obtains Chinese herbal medicine extract dry powder;
(4) by hydroxyethyl-cellulose 3 parts, glycerol 10 parts, grape-fruit seed oil 0.5 part, 95 parts, water, put into glue pot, stir, then add 0.01 part, glucide, be stirred to translucent, then leave standstill 1.5h, then add the calcium phosphate of the obtained Chinese herbal medicine extract dry powder of step (3) and 15 parts; Stir 1h, obtain mastic; After again mastic being ground by grinder, obtained toothpaste.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114306193A (en) * | 2021-12-03 | 2022-04-12 | 梁红利 | Degradable whitening glue |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| KR930000059B1 (en) * | 1990-04-24 | 1993-01-08 | 태평양화학 주식회사 | Dental composition |
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Application publication date: 20160420 |