CN105484030A - Post-treatment technology for all-cotton fabric - Google Patents

Post-treatment technology for all-cotton fabric Download PDF

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Publication number
CN105484030A
CN105484030A CN201511004954.0A CN201511004954A CN105484030A CN 105484030 A CN105484030 A CN 105484030A CN 201511004954 A CN201511004954 A CN 201511004954A CN 105484030 A CN105484030 A CN 105484030A
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China
Prior art keywords
parts
fabric
dip
cotton fabric
cotton
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CN201511004954.0A
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Chinese (zh)
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CN105484030B (en
Inventor
徐锦
宣加杰
单宝
印美娟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ningbo weiketekuo Home Textile Co.,Ltd.
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Shaoxing High Sun Apparel & Textiles Co Ltd
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Priority to CN201511004954.0A priority Critical patent/CN105484030B/en
Publication of CN105484030A publication Critical patent/CN105484030A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/325—Amines
    • D06M13/328—Amines the amino group being bound to an acyclic or cycloaliphatic carbon atom
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/402—Amides imides, sulfamic acids
    • D06M13/419—Amides having nitrogen atoms of amide groups substituted by hydroxyalkyl or by etherified or esterified hydroxyalkyl groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/04—Vegetal fibres
    • D06M2101/06—Vegetal fibres cellulosic

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses a post-treatment technology for an all-cotton fabric. The post-treatment technology comprises the following steps: (1) adding the fabric to a dipping liquid for dipping; (2) drying the completely dipped fabric; (3) baking the dried fabric; (4) pre-shrinking the baked fabric to obtain a finished product, wherein the dipping liquid in the step (1) is prepared from the following components in parts by weight: 20-80 parts of a dust-proofing agent, 150-220 parts of a no silicone softener, 5-15 parts of a color fixing agent, 2-15 parts of a neutralizer and 200-300 parts of a solvent. Aiming at the all-cotton fabric, the post-treatment technology disclosed by the invention achieves the dustproof effect on the all-cotton fabric.

Description

A kind of aftertreatment technology of all-cotton fabric
Technical field
The present invention relates to textile industry, more particularly, it relates to a kind of aftertreatment technology of all-cotton fabric.
Background technology
Cotton, annual herb plant, fruit is as peach, and the fiber of interior adularescent and the seed of pitchy, fiber is for weaving and wadding clothing.The fabric be made into cotton yarn or cotton and cotton chemical mixed yarn line is just referred to the various cotton fabrics that cotton makes.
As a kind of natural fiber, cotton products start these people very early and applied.Because it has warming, comfortableness preferably, it is the favor that the fabric being only second to animal fur is subject to people.Belong to pure natural substance because of it especially, planting patterns is simple, and have cotton planting base throughout the country, widespread adoption in every respect.People are also more inclined to and select all cotton products.
All cotton products compared with the fiber of Prof. Du Yucang, because itself just belongs to cellulose, can not as artificial fiber, electrostatic is easily gathered in surface, therefore can't add antistatic additive in the production technology of all cotton products.
But, no matter put into tumble dryer inner heating drying after all-cotton fabric is cleaning in the suitable use procedure of production process, dehydration, its cloth cover is easy to be stained with fine hair, when normal use, it is more difficultly stained with fine hair, but be but easy to produce electrostatic under drying condition, particularly when rotating cage is dried, the silicone oil finishing agent simultaneously added in Final finishing process, this auxiliary agent at high temperature also can have adsorptivity to fine hair.
Summary of the invention
For the deficiency that prior art exists, the object of this reality invention is to provide a kind of aftertreatment technology preventing the all-cotton fabric of fine hair.
For achieving the above object, the invention provides following technical scheme:
An aftertreatment technology for all-cotton fabric, comprising:
Step one: fabric is added to dip in liquid dip;
Step 2: fabric completely will be dipped and dry;
Step 3: the fabric of having dried is baked;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition
Nonionic dust-proofing agent: 20 ~ 80 parts;
Without silicone oil softener 150 ~ 220 parts;
5 ~ 15 parts, color-fixing agent;
Neutralizer 2 ~ 15 parts;
Solvent 200 ~ 300 parts.
As preferred further: described dust-proofing agent is double hydroxyethyl laurylamide.
As preferred further: described neutralizer is TRIS buffer.
As preferred further: described is dioctadecyl dimethyl ammonium chloride without silicone oil softener.
As preferred further: the bake out temperature in described step 2 is 50 ~ 120 DEG C, and described drying time is 30 ~ 120 minutes.
As preferred further: the baking temperature in described step 3 is 150 ~ 180 DEG C, and the time of baking is 2 ~ 10 minutes.
As preferred further: described TRIS buffer pH is 8 ~ 9.
As further preferably: described in dip liquid and also comprise 5 ~ 15 parts of gluconic acid sodium salts.
Wherein, key of the present invention is to dip choosing of liquid.The solvent that the solvent dipped in liquid can select water, ethanol etc. common.The selection of softener is selected the softener of not silicate-containing oil, avoid silicone oil in oven dry situation, can adhesiveness be had, the problem of fine hair can be adhered to.Selecting dioctadecyl dimethyl ammonium chloride without in the selection of silicone oil softener, dioctadecyl dimethyl ammonium chloride is a kind of surfactant, can the use of substituted for silicon oils softener, reaches the close even better effect with silicone oil simultaneously.
And in the selection of dust-proofing agent; preferred double hydroxyethyl laurylamide; because cotton goods are string; therefore; first because selecting the surfactant that can not produce corrosion to fabric fibre in the selection of dust-proofing agent; and double hydroxyethyl laurylamide is as a kind of non-ionic antistatic agent, for the integrality of protective plant fiber, there is good effect.Meanwhile, have good compatibility with without silicone oil softener dioctadecyl dimethyl ammonium chloride, both can dissolve mutually, can not produce the excessive concentration of local, and the problem that local concentration is too low, itself just has compatibility.Dioctadecyl dimethyl ammonium chloride also has certain antistatic property simultaneously, its action principle is different from nonionic surface active agent double hydroxyethyl laurylamide, be equivalent to use composite with it, can make the antistatic effect of all-cotton fabric when the condition under daily different situation, both can play better effect at composite use.
And dip in the system of liquid whole, need to add neutralizer, overall pH value is controlled by neutralizer, this is the mainly cellulose due to all cotton products, cellulose has the feature of alkaline-resisting not resistance to calculation, therefore, needs control ph, ensure that the all-cotton fabric that whole system is produced has good intensity, intensity can not be produced because hydrolysis occurs for it and decline.Therefore the preferred TRIS buffer of antistatic additive is as a kind of pH buffer, pH value of solution can be made to remain on the weak base state of 8 ~ 9, this state is conducive to all cotton fibers most and preserves, TRIS buffer also ensure that the activity of double hydroxyethyl laurylamide and dioctadecyl dimethyl ammonium chloride simultaneously, double hydroxyethyl laurylamide and dioctadecyl dimethyl ammonium chloride can be made better to be combined with cotton fiber, improve dust-proof effect, place fine hair and adhere to.
Preferred interpolation gluconic acid sodium salt, strengthens the stability of double hydroxyethyl laurylamide and dioctadecyl dimethyl ammonium chloride on the one hand, in long-time use procedure, also can play good dust-proof effect.
Detailed description of the invention
Embodiment 1:
Step one: fabric is added to dip in liquid dip;
Step 2: will dip fabric completely and dry, bake out temperature is 50 DEG C, and described drying time is 110 minutes;
Step 3: the fabric of having dried is baked, baking temperature is 150 DEG C, and the time of baking is 3 minutes;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition:
Clariant SAS-93(nonionic dust-proofing agent) 20 parts;
Assistant officer peak CT(is without silicone oil softener) 200 parts;
Good grand scientific and technological Goon701(color-fixing agent) 5 parts;
TRIS buffer (neutralizer) 15 parts;
250 parts, water.
Embodiment 2:
Step one: fabric is added to dip in liquid dip;
Step 2: will dip fabric completely and dry, bake out temperature is 80 DEG C, and described drying time is 60 minutes;
Step 3: the fabric of having dried is baked, baking temperature is 170 DEG C, and the time of baking is 5 minutes;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition:
LG-DOW AEO-9(nonionic dust-proofing agent) 50 parts;
LG-DOW JFC(is without silicone oil softener) 220 parts;
Bayer Bitterfeld GmbH TJ-100(color-fixing agent) 10 parts;
Ammonia-ammonium chloride buffer (neutralizer) 10 parts;
250 parts, water.
Embodiment 3:
Step one: fabric is added to dip in liquid dip;
Step 2: will dip fabric completely and dry, bake out temperature is 110 DEG C, and described drying time is 40 minutes;
Step 3: the fabric of having dried is baked, baking temperature is 180 DEG C, and the time of baking is 5 minutes;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition:
Coral 6501(double hydroxyethyl laurylamide) 80 parts;
The sub-D1821(dioctadecyl dimethyl ammonium chloride in sieve ground) 150 parts;
Bayer Bitterfeld GmbH TJ-100(color-fixing agent) 15 parts;
TRIS buffer (neutralizer) 5 parts;
250 parts, water.
Embodiment 4:
Step one: fabric is added to dip in liquid dip;
Step 2: will dip fabric completely and dry, bake out temperature is 110 DEG C, and described drying time is 40 minutes;
Step 3: the fabric of having dried is baked, baking temperature is 180 DEG C, and the time of baking is 5 minutes;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition:
Coral 6501(double hydroxyethyl laurylamide) 20 parts;
The sub-D1821(dioctadecyl dimethyl ammonium chloride in sieve ground) 200 parts;
Bayer Bitterfeld GmbH TJ-100(color-fixing agent) 5 parts;
TRIS buffer (neutralizer) 15 parts;
250 parts, water;
Gluconic acid sodium salt: 10 parts.
Embodiment 5:
Step one: fabric is added to dip in liquid dip;
Step 2: will dip fabric completely and dry, bake out temperature is 110 DEG C, and described drying time is 40 minutes;
Step 3: the fabric of having dried is baked, baking temperature is 150 DEG C, and the time of baking is 2 minutes;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition:
Coral 6501(double hydroxyethyl laurylamide) 50 parts;
The sub-D1821(dioctadecyl dimethyl ammonium chloride in sieve ground) 220 parts;
Bayer Bitterfeld GmbH TJ-100(color-fixing agent) 10 parts;
TRIS buffer (neutralizer) 10 parts;
250 parts, water;
Gluconic acid sodium salt: 10 parts.
Embodiment 6:
Step one: fabric is added to dip in liquid dip;
Step 2: will dip fabric completely and dry, bake out temperature is 110 DEG C, and described drying time is 40 minutes;
Step 3: the fabric of having dried is baked, baking temperature is 150 DEG C, and the time of baking is 2 minutes;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition:
Coral 6501(double hydroxyethyl laurylamide) 50 parts;
The sub-D1821(dioctadecyl dimethyl ammonium chloride in sieve ground) 220 parts;
Bayer Bitterfeld GmbH TJ-100(color-fixing agent) 10 parts;
Ammonia-ammonium chloride buffer (neutralizer) 10 parts;
250 parts, water;
Gluconic acid sodium salt: 10 parts.
Comparative example 1:
Step one: fabric is added to dip in liquid dip;
Step 2: will dip fabric completely and dry, bake out temperature is 110 DEG C, and described drying time is 40 minutes;
Step 3: the fabric of having dried is baked, baking temperature is 150 DEG C, and the time of baking is 2 minutes;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition:
The sub-D1821(dioctadecyl dimethyl ammonium chloride in sieve ground) 220 parts;
Bayer Bitterfeld GmbH TJ-100(color-fixing agent) 10 parts;
TRIS buffer (neutralizer) 10 parts;
250 parts, water;
Gluconic acid sodium salt: 10 parts.
Comparative example 2:
Step one: fabric is added to dip in liquid dip;
Step 2: will dip fabric completely and dry, bake out temperature is 110 DEG C, and described drying time is 40 minutes;
Step 3: the fabric of having dried is baked, baking temperature is 150 DEG C, and the time of baking is 2 minutes;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition:
Coral 6501(double hydroxyethyl laurylamide) 50 parts;
Bayer Bitterfeld GmbH TJ-100(color-fixing agent) 10 parts;
TRIS buffer (neutralizer) 10 parts;
250 parts, water.
Comparative example 3:
Step one: fabric is added to dip in liquid dip;
Step 2: will dip fabric completely and dry, bake out temperature is 110 DEG C, and described drying time is 40 minutes;
Step 3: the fabric of having dried is baked, baking temperature is 150 DEG C, and the time of baking is 2 minutes;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition:
Coral 6501(double hydroxyethyl laurylamide) 50 parts;
The sub-D1821(dioctadecyl dimethyl ammonium chloride in sieve ground) 220 parts;
Bayer Bitterfeld GmbH TJ-100(color-fixing agent) 10 parts;
TRIS buffer (neutralizer) 10 parts;
250 parts, water.
Comparative example 4:
Step one: fabric is added to dip in liquid dip;
Step 2: will dip fabric completely and dry, bake out temperature is 110 DEG C, and described drying time is 40 minutes;
Step 3: the fabric of having dried is baked, baking temperature is 150 DEG C, and the time of baking is 2 minutes;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition:
Bayer Bitterfeld GmbH TJ-100(color-fixing agent) 10 parts;
250 parts, water.
Comparative example 5:
Step one: fabric is added to dip in liquid dip;
Step 2: will dip fabric completely and dry, bake out temperature is 110 DEG C, and described drying time is 40 minutes;
Step 3: the fabric of having dried is baked, baking temperature is 150 DEG C, and the time of baking is 2 minutes;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition:
Antistatic additive SN(cationic antistatic agent) 50 parts;
Silicone oil 220 parts;
Bayer Bitterfeld GmbH TJ-100(color-fixing agent) 10 parts;
Ammonia-ammonium chloride buffer (neutralizer) 10 parts;
250 parts, water.
Test method
Test 1: by the cotton cloth through embodiment and comparative example post processing, cut 1M 2area, with 1M 2wool product together clean, put into tumble dryer after cleaning and dry, measure cotton cloth fine hair adhered area.
Test 2: by the cotton cloth through embodiment and comparative example post processing, cut 1M 2area, with 1M 2wool product together 10 cleanings, put into tumble dryer after cleaning and dry, measure cotton cloth fine hair adhered area.
Test 3: by the cotton cloth through embodiment and comparative example post processing, cut 1M 2area, with 1M 2wool product together 30 cleanings, put into tumble dryer after cleaning and dry, measure cotton cloth fine hair adhered area.
Test 4: measure fabric intensity by HIV instrument.
Test 5: after 10 cleanings, measures fabric intensity by HIV instrument.
Test 6: after 30 cleanings, measures fabric intensity by HIV instrument.
By above-mentioned test data, can draw, by adding nonionic dust-proofing agent and without silicone oil softener, the dust tightness of all-cotton fabric can being strengthened, reduce the adhesion of fine hair, meanwhile, also ensure that the mechanical strength of all-cotton fabric.As can be seen from comparative example 4, although although add conventional antistatic additive and softener also can play certain dust-proof effect, can the serious mechanical strength reducing all-cotton fabric.Particularly after with the addition of gluconic acid sodium salt, further ensure after repeatedly use procedure, all-cotton fabric still has good anti-dust performance and mechanical strength.
The above is only the preferred embodiment of the present invention, protection scope of the present invention be not only confined to above-described embodiment, and all technical schemes belonged under thinking of the present invention all belong to protection scope of the present invention.It should be pointed out that for those skilled in the art, some improvements and modifications without departing from the principles of the present invention, these improvements and modifications also should be considered as protection scope of the present invention.

Claims (8)

1. an aftertreatment technology for all-cotton fabric, comprising:
Step one: fabric is added to dip in liquid dip;
Step 2: fabric completely will be dipped and dry;
Step 3: the fabric of having dried is baked;
Step 4: the fabric baked is carried out preshrunk and obtains finished product;
Dip liquid in described step one, comprise following weight portion composition
Dust-proofing agent 20 ~ 80 parts;
Without silicone oil softener 150 ~ 220 parts;
5 ~ 15 parts, color-fixing agent;
Neutralizer 2 ~ 15 parts;
Solvent 200 ~ 300 parts.
2. the aftertreatment technology of a kind of all-cotton fabric according to claim 1, is characterized in that: described dust-proofing agent is double hydroxyethyl laurylamide.
3. the aftertreatment technology of a kind of all-cotton fabric according to claim 1 and 2, is characterized in that: described neutralizer is TRIS buffer.
4. the aftertreatment technology of a kind of all-cotton fabric according to claim 3, is characterized in that: described is dioctadecyl dimethyl ammonium chloride without silicone oil softener.
5. the aftertreatment technology of a kind of all-cotton fabric according to claim 1, is characterized in that: the bake out temperature in described step 2 is 50 ~ 120 DEG C, and described drying time is 30 ~ 120 minutes.
6. the aftertreatment technology of a kind of all-cotton fabric according to claim 1, is characterized in that: the baking temperature in described step 3 is 150 ~ 180 DEG C, and the time of baking is 2 ~ 10 minutes.
7. the aftertreatment technology of a kind of all-cotton fabric according to claim 3, is characterized in that: described TRIS buffer pH is 8 ~ 9.
8. the aftertreatment technology of a kind of all-cotton fabric according to claim 1, is characterized in that: described in dip liquid and also comprise 5 ~ 15 parts of gluconic acid sodium salts.
CN201511004954.0A 2015-12-29 2015-12-29 A kind of aftertreatment technology of all-cotton fabric Active CN105484030B (en)

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Cited By (1)

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Publication number Priority date Publication date Assignee Title
CN110258115A (en) * 2019-06-18 2019-09-20 广州市盈科化工科技有限公司 A kind of nanometer of dedusting agent and preparation method thereof and application method

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