CN105484026B - human hair substitute and preparation method thereof - Google Patents
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- CN105484026B CN105484026B CN201610014753.7A CN201610014753A CN105484026B CN 105484026 B CN105484026 B CN 105484026B CN 201610014753 A CN201610014753 A CN 201610014753A CN 105484026 B CN105484026 B CN 105484026B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/35—Heterocyclic compounds
- D06M13/355—Heterocyclic compounds having six-membered heterocyclic rings
- D06M13/358—Triazines
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/12—Stretch-spinning methods
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/262—Sulfated compounds thiosulfates
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Abstract
The present invention relates to hair products technical field, and in particular to a kind of human hair substitute and preparation method thereof.The human hair substitute is made through stripping scale, stretching, setting, post processing successively using horse hair；It is described to be stretched as horse hair being fixed on after desquamating on stretcher in input stretching liquid, carry out being stretched to elongation under the conditions of 10 80 DEG C as 20 40%；By weight in terms of 100 parts of horse hairs, required stretching liquid is made up of following raw material in parts by weight：Mass concentration is 20 50% 36 200 parts of hydrogen peroxide, 17 50 parts of sodium pyrophosphate, 23 parts of AEO, 36 parts of lauryl sodium sulfate, 800 3000 parts of soft water, and is 7.5 9 with the pH value of the regulation stretching liquid of pH adjusting agent 1.Human hair substitute provided by the invention, performance is more nearly in-vitro human hair, soft, comfortable, good permeability, and is easy to arrange.The preparation method of the present invention, preparation technology is simple, easy to operate, suitable for industrialized production.
Description
Technical field
The present invention relates to hair products technical field, and in particular to a kind of human hair substitute and preparation method thereof.
Background technology
With the continuous improvement of people's living standards, also more and more higher, hair style species are also more next for pursuit of the people to fashion
It is more, it is such as volume, straight, long, short, in point, divide partially, etc., but during perming, hair top layer can be caused
Scale destroyed, hair internal structure is in unprotect state, make inside moisture and nutrient loss, be harmful to
Hair, scalp and hair follicle, it can be denatured more or less the keratoprotein of hair, hair is easily turned to be yellow, embrittlement, it is easily de-
Fall, lackluster, no elasticity, damage hair quality.And the various wig of style can then solve this problem well, different
Occasion, different needs of work, different moods, and before fashion, wig all provides irreplaceable effect, and false
Hair is worn convenient.Therefore, the demand of hair products is also increasingly increased severely, but produces main raw material(s) --- the in vitro people of hair products
Hair resource is but petered out.
In traditional hair product industry, it with in-vitro human hair is raw material production hair products to be all, its history is of long standing and well established, but
It is the continuous change with thought of people culture life, the people to wear one's hair long is fewer and fewer, prepares the long span people used in hair products
Hair is petered out, so the substitute for finding in-vitro human hair has turned into the most important thing of nowadays hair product industry.People adopt earliest
Human hair substitute is：The chemical synthetic fiber silks such as acrylics filament, dacron thread, polyvinyl chloride silk.But due to using these changes
Learn synthetic fibres substitute human hair production hair products when consumer wears in the presence of the compatibility with contact human skin, breathe freely
Having a good sweat property, active sense, elegant property are poor, are not easy the shortcomings of combing and appreciation effect be not true to nature, do not get consumer reception.
Find the great attention that human hair substitute has caused hair products enterprise.Have Some Enterprises up to now using chemistry
Synthetic fibres or the chemical fiber wire replacement in-vitro human hair production hair products for being mixed with partially protein, can be due to that these products are present
The defects of compatibility, active property with human contact, having a good sweat property difference, rush to wearer uncomfortable, especially summer wears
Wear sultry, and such wig is not easy to arrange, fidelity is inadequate, not enough truly, naturally, wearing effect is poor, can not meet consumer
Demand.People's Republic of China's Patent Office Publication is：One kind is disclosed in CN1699646A patent specification《Animal protein
Matter artificial hair and its production method》Although containing animal protein in " artificial hair " described in it, its content is often
Less than the half of its gross weight, acrylonitrile and acrylic nitrile derivates still containing 40-60%, the application properties of this " artificial hair "
Although being better than pure chemistry synthetic fibres, but still exist and contact human skin's compatibility, having a good sweat property, active sense, drift
Shifting property etc. is still not so good as natural animal protein fibre silk, can not meet consumer demand well.
The content of the invention
It is an object of the invention to provide a kind of human hair substitute, its performance is more nearly in-vitro human hair, more soft, easypro
Suitable, good permeability, and be easy to arrange.
The present invention also aims to provide a kind of preparation method of human hair substitute, the preparation method is simple, convenient, easy
In control, suitable for industrialization promotion.
In order to realize the above object the present invention adopts the following technical scheme that：
A kind of preparation method of human hair substitute, including horse hair is made through stripping scale, stretching, setting, post processing successively；
The stripping scale, which is handled, is：Horse hair is first put into the sulphur for 85-97% through formic acid or mass concentration at room temperature
Horse hair agitated reaction 30-50 minutes, is then taken out, rushed into pH=1-2 sodium dichloro cyanurate solution by acid regulation
Wash, the horse hair after flushing is then put into pH adjusted dose 1 regulation into pH=8-10 alkaline water again, in 40-50 DEG C of condition
Lower immersion treatment 20-50min, then take out and be washed with water only；By weight in terms of 100 parts of horse hairs, required dichlord isocyanurice acid
Sodium solution is made up of following raw material in parts by weight：Sodium dichloro cyanurate 5-10 parts, water 1000-3000 parts, required alkaline water
500-3000 parts；
It is described to be stretched as：Horse hair after stripping scale processing is fixed on stretcher in input stretching liquid, at 10-80 DEG C
Under the conditions of carry out being stretched to elongation and reach 20-40%；By weight in terms of 100 parts of horse hairs, required stretching liquid is in parts by weight
It is made up of following raw material：Hydrogen peroxide 36-200 part, sodium pyrophosphate 17-50 parts, fatty alcohol polyoxy second that mass concentration is 20-50%
Alkene ether 2-3 parts, lauryl sodium sulfate 3-6 parts, soft water 800-3000 parts, and be with the pH value of the regulation stretching liquid of pH adjusting agent 1
7.5-9。
The ammoniacal liquor that the pH adjusting agent 1 is soda ash or mass concentration is 20-50%.
It is described to be shaped to the horse hair after stretching being put into shaping liquid the immersion 1-3 hours under the conditions of 40-80 DEG C, determined
Shape；By weight in terms of 100 parts of horse hairs, required shaping liquid is made up of following raw material in parts by weight：Glyoxal 10-40 parts, water
800-3000 parts, and adjusted with pH adjusting agent 2 to style keeping liquid pH=1-3,.
The pH adjusting agent 2 is formic acid or acetic acid.
The post processing is to put into the horse hair after setting in aftertreatment fluid to be incubated 10-50min under the conditions of 30-60 DEG C；
By weight in terms of 100 parts of horse hairs, required aftertreatment fluid is made up of following raw material in parts by weight：Cetyl trimethyl bromination
Ammonium 2-6 parts, solid content be 28-38% aminosiloxane emulsion 3-6 parts, isomerous tridecanol polyoxyethylene ether 1-2 parts, water
1000-2000 parts.
Also include drying the horse hair after the post processing under the conditions of 60-90 DEG C, produce.
A kind of human hair substitute, is made by above-mentioned preparation method.
Use horse hair to prepare a kind of and natural human hair for raw material it is an object of the invention to provide one kind to tie in chemistry
The all very close human hair substitute of structure practical performance etc..Natural horse hair is in chemical constitution, physical and chemical performance etc. and day
Right human hair is quite similar, and their main chemical compositions are animal protein, but horse hair is compared with human hair, its wool top compared with
Slightly, quality is stiff, and feel is coarse, and it is infeasible directly to bring and substitute human hair production hair products.Therefore, the present invention is first by horse
The scale on tail surface is partly or entirely peeled off, its surface is become smooth exquisiteness, and then it is soaked and stretched in liquid is stretched,
It is attenuated, it is elongated after, then shaped and post-processed, produce the human hair substitute of the present invention.
The preparation method of the present invention has further the advantage that：
1st, the present invention is in acid condition partly or entirely shelled the scale on horse hair surface using two isocyanuric acid sodium solutions
Fall without damaging horse hair cortical layer and internal fiber, its surface is become smooth exquisiteness, closer to human hair texture；
2nd, present invention stretching liquid used, makes horse hair not broken in drawing process, drawing effect is more preferable；
3rd, the horse hair after aftertreatment fluid processing used in the present invention, more soft, smooth, texture is more preferable, presses close to human hair texture.
Human hair substitute obtained by preparation method of the present invention, its chemical component are mainly the animal that natural animal albumen is formed
Azelon silk, its performance are more nearly in-vitro human hair, and texture is soft, smooth, comfortable, good permeability, and is easy to arrange, and presses close to
Human hair texture.
Embodiment
Embodiment 1
A kind of human hair substitute, is prepared by following methods：
(1) scale is shelled：At room temperature, take 6g sodium dichloro cyanurate to be dissolved into 2kg soft water and obtain dichloro isocyanuric urine
Acid sodium solution, then 100g horse hair is put into the solution, stirred, then add the industry that mass fraction is 95%
Sulfuric acid stirs regulation solution to pH=2, then occasional agitation, after 30 minutes, taking-up horse hair is put into again after being rinsed with soft water
2kg is adjusted into Ph=8 soft water with the ammoniacal liquor that mass concentration is 35%, is heated to 45 DEG C, occasional agitation, after reacting 34 minutes
The aqueous solution is bled off, is cleaned with soft water；
(2) stretch：First, configuration stretching liquid：Soft water 3kg is weighed, adds the hydrogen peroxide that mass concentration is 30% wherein
180ml, industrial sodium pyrophosphate 20g, AEO 3g, lauryl sodium sulfate 6g, used after the dissolving of above solute
The ammoniacal liquor that mass concentration is 35% adjusts pH value of solution=8；
Horse hair after step (1) processing is fixed on stretcher, put into the stretching liquid, is keeping solution temperature
Stretched under the conditions of 35 DEG C, take out when horse hair is stretched to growth by 25%, rinsed with soft water；
(3) shape：Style keeping liquid is configured first, weighs soft water 2kg, adds the industrial glyoxal 80g that mass fraction is 30%,
Adjusted to pH=2, then put into the horse hair after step (2) stretching in the style keeping liquid, and style keeping liquid is heated up with acetic acid
To 70 DEG C, heat-insulation soaking takes out after 2 hours, is cleaned with soft water；
(4) post-process：First, aftertreatment fluid is configured, weighs soft water 2kg, adds cetyl trimethylammonium bromide 6g, Gu
Content is 33% aminosiloxane emulsion 5g, isomerous tridecanol polyoxyethylene ether 1.5g, is then heated to 50 DEG C, stirring is equal
It is even, then the horse hair after step (3) setting processing put into the aftertreatment fluid and immersion treatment 30 under the conditions of being kept for 50 DEG C
Minute；
(5) dry：Put the horse hair after step (4) post processing into baking room, dry, obtain under the conditions of 80 DEG C
Product.
Embodiment 2
A kind of human hair substitute, is prepared by following methods：
(1) scale is shelled：At room temperature, take 5g sodium dichloro cyanurate to be dissolved into 1kg soft water and obtain dichloro isocyanuric urine
Acid sodium solution, then 100g horse hair is put into the solution, stirred, then add the industry that mass fraction is 97%
Sulfuric acid regulation solution pH to pH=1, after stirring, then occasional agitation took out after horse hair is rinsed with soft water and thrown again after 40 minutes
Enter into 0.5kg soft water, the soft water is adjusted to pH=9 with the ammoniacal liquor that mass concentration is 20%, then added the alkaline soft water
For heat to 40 DEG C, occasional agitation, reaction bleeds off the aqueous solution after 50 minutes, then is cleaned with soft water；
(2) stretch：First, configuration stretching liquid：Soft water 2.8kg is weighed, adds the dioxygen that mass concentration is 20% wherein
Water 35ml, industrial sodium pyrophosphate 18g, AEO 2g, lauryl sodium sulfate 5g, are used after the dissolving of above solute
The ammoniacal liquor that mass concentration is 20% adjusts solution PH=9；
Horse hair after step (1) processing is fixed on stretcher, put into the stretching liquid, is keeping solution temperature
Stretched under the conditions of 50 DEG C, take out when horse hair is stretched to growth by 30%, rinsed with soft water；
(3) shape：Style keeping liquid is configured first, weighs soft water 2.5kg, adds the industrial glyoxal that mass fraction is 30%
60g, adjusted to pH=2.5 with acetic acid, then put into the horse hair after step (2) stretching in the style keeping liquid, and will sizing
Liquid is warming up to 80 DEG C, and heat-insulation soaking takes out after 2.5 hours, is cleaned with soft water；
(4) post-process：First, aftertreatment fluid is configured, weighs soft water 1.6kg, adds cetyl trimethylammonium bromide 5g,
Solid content is 28% aminosiloxane emulsion 4.5g, isomerous tridecanol polyoxyethylene ether 2g, is then heated to 45 DEG C, stirring is equal
It is even, then the horse hair after step (3) setting processing put into the aftertreatment fluid and immersion treatment 25 under the conditions of being kept for 45 DEG C
Minute；
(5) dry：Put the horse hair after step (4) post processing into baking room, dry, obtain under the conditions of 60 DEG C
Product.
Embodiment 3
A kind of human hair substitute, is prepared by following methods：
(1) scale is shelled：At room temperature, take 10g sodium dichloro cyanurate to be dissolved into 3kg soft water and obtain dichloro isocyanuric urine
Acid sodium solution, then 100g horse hair is put into the solution, stirred, then add the industry that mass fraction is 85%
Sulfuric acid regulation solution pH to pH=2, after stirring, then occasional agitation took out after horse hair is rinsed with soft water and thrown again after 50 minutes
Enter into 3kg soft water, and adjusted the soft water to pH=10 with the ammoniacal liquor that mass concentration is 50%, then add the alkaline soft water
For heat to 50 DEG C, occasional agitation, reaction bleeds off the aqueous solution after 20 minutes, then is cleaned with soft water；
(2) stretch：First, configuration stretching liquid：Soft water 2.3kg is weighed, adds the dioxygen that mass concentration is 50% wherein
Water 100ml, industrial sodium pyrophosphate 17g, AEO 2.6g, lauryl sodium sulfate 5.5g, treats that above solute is molten
After solution pH value of solution=9 are adjusted with the ammoniacal liquor that mass concentration is 50%；
Horse hair after step (1) processing is fixed on stretcher, put into the stretching liquid, is keeping solution temperature
Stretched under the conditions of 10 DEG C, take out when horse hair is stretched to growth by 20%, rinsed with soft water；
(3) shape：Style keeping liquid is configured first, weighs soft water 3.0kg, adds the industrial glyoxal that mass fraction is 30%
70g, adjusted to pH=1.5 with acetic acid, then put into the horse hair after step (2) stretching in the style keeping liquid, and will sizing
Liquid is warming up to 66 DEG C, and heat-insulation soaking takes out after 3 hours, is cleaned with soft water；
(4) post-process：First, aftertreatment fluid is configured, weighs soft water 1.8kg, adds cetyl trimethylammonium bromide
4.5g, solid content are 38% aminosiloxane emulsion 6g, isomerous tridecanol polyoxyethylene ether 1.8g, are then heated to 30 DEG C,
Stir, then the horse hair after step (3) setting processing is put into the aftertreatment fluid and soaked under the conditions of being kept for 30 DEG C
Processing 50 minutes；
(5) dry：Put the horse hair after step (4) post processing into baking room, dry, obtain under the conditions of 90 DEG C
Product.
Embodiment 4
A kind of human hair substitute, is prepared by following methods：
(1) scale is shelled：At room temperature, take 8g sodium dichloro cyanurate to be dissolved into 2.5kg soft water and obtain dichloro isocyanide
Uric acid sodium solution, then 100g horse hair is put into the solution, stirred, then added formic acid and adjust pH value of solution to pH
=2, after stirring, then occasional agitation took out after horse hair is rinsed with soft water and put into again in 2.5kg soft water after 38 minutes, and
The soft water is adjusted to pH=8.5 with the ammoniacal liquor that mass concentration is 38%, the alkaline soft water is then heated to 43 DEG C, interruption is stirred
Mix, reaction bleeds off the aqueous solution after 32 minutes, then is cleaned with soft water；
(2) stretch：First, configuration stretching liquid：Soft water 0.8kg is weighed, adds the dioxygen that mass concentration is 35% wherein
Water 150ml, industrial sodium pyrophosphate 50g, AEO 2.4g, lauryl sodium sulfate 3g, treat that above solute dissolves
Afterwards pH value of solution=7.5 are adjusted with the ammoniacal liquor that mass concentration is 38%；
Horse hair after step (1) processing is fixed on stretcher, put into the stretching liquid, is keeping solution temperature
Stretched under the conditions of 80 DEG C, take out when horse hair is stretched to growth by 40%, rinsed with soft water；
(3) shape：Style keeping liquid is configured first, weighs soft water 0.8kg, adds the industrial glyoxal that mass fraction is 30%
133g, adjusted to pH=3 with formic acid, then put into the horse hair after step (2) stretching in the style keeping liquid, and by style keeping liquid
40 DEG C are warming up to, heat-insulation soaking takes out after 1 hour, is cleaned with soft water；
(4) post-process：First, aftertreatment fluid is configured, weighs soft water 1kg, adds cetyl trimethylammonium bromide 2g, Gu
Content is 35% aminosiloxane emulsion 3g, isomerous tridecanol polyoxyethylene ether 1g, is then heated to 60 DEG C, stirs,
Then the horse hair after step (3) setting processing is put into the aftertreatment fluid and immersion treatment 10 is divided under the conditions of 60 DEG C of holding
Clock；
(5) dry：Put the horse hair after step (4) post processing into baking room, dry, obtain under the conditions of 70 DEG C
Product.
Horse hair used in embodiment 1-4, it also can be replaced the mixture or horse-hair of horse-hair and horse hair.
Claims (7)
- A kind of 1. preparation method of human hair substitute, it is characterised in that including by horse hair successively through stripping scale, stretching, setting, after Processing is made；The stripping scale, which is handled, is：First horse hair is put at room temperature and adjusted through formic acid or mass concentration for 85-97% sulfuric acid Horse hair agitated reaction 30-50 minutes, is then taken out, rinsed, so into pH=1-2 sodium dichloro cyanurate solution by section The horse hair after flushing is put into pH adjusted dose 1 regulation into pH=8-10 alkaline water again afterwards, soaked under the conditions of 40-50 DEG C 20-50min is handled, then takes out and is washed with water only；By weight in terms of 100 parts of horse hairs, required sodium dichloro cyanurate solution It is made up of in parts by weight following raw material：Sodium dichloro cyanurate 5-10 parts, water 1000-3000 parts, required alkaline water 500- 3000 parts；It is described to be stretched as：Horse hair after stripping scale processing is fixed on stretcher in input stretching liquid, in 10-80 DEG C of condition Under carry out being stretched to elongation and reach 20-40%；By weight in terms of 100 parts of horse hairs, required stretching liquid is made up of following raw material in parts by weight：Mass concentration is 20- 60% hydrogen peroxide 36-200 parts, sodium pyrophosphate 17-50 parts, AEO 2-3 parts, lauryl sodium sulfate 3-6 Part, soft water 800-3000 parts, and be 7.5-9 with the pH value of the regulation stretching liquid of pH adjusting agent 1.
- 2. the preparation method of human hair substitute according to claim 1, it is characterised in that the pH adjusting agent 1 is soda ash Or the ammoniacal liquor that mass concentration is 20-50%.
- 3. the preparation method of human hair substitute according to claim 1, it is characterised in that described to be shaped to after stretching Horse hair is put into shaping liquid the immersion 1-3 hours under the conditions of 40-80 DEG C, is shaped；By weight in terms of 100 parts of horse hairs, required shaping liquid is made up of following raw material in parts by weight：Glyoxal 10-40 parts, water 800-3000 parts, and adjusted with pH adjusting agent 2 to style keeping liquid pH=1-3.
- 4. the preparation method of human hair substitute according to claim 3, it is characterised in that the pH adjusting agent 2 is formic acid Or acetic acid.
- 5. the preparation method of human hair substitute according to claim 1, it is characterised in that the post processing is after shaping Horse hair input aftertreatment fluid in 10-50min is incubated under the conditions of 30-60 DEG C；By weight in terms of 100 parts of horse hairs, required aftertreatment fluid is made up of following raw material in parts by weight：Cetyl trimethyl Ammonium bromide 2-6 parts, solid content be 28-38% aminosiloxane emulsion 3-6 parts, isomerous tridecanol polyoxyethylene ether 1-2 parts, water 1000-2000 parts.
- 6. the preparation method of human hair substitute according to claim 1, it is characterised in that also include after the post processing Horse hair dried under the conditions of 60-90 DEG C, produce.
- 7. a kind of human hair substitute, it is characterised in that be made as the preparation method described in claim 1-6.
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