CN105482995B - A kind of fragrance is produced and enriching apparatus - Google Patents
A kind of fragrance is produced and enriching apparatus Download PDFInfo
- Publication number
- CN105482995B CN105482995B CN201510976876.4A CN201510976876A CN105482995B CN 105482995 B CN105482995 B CN 105482995B CN 201510976876 A CN201510976876 A CN 201510976876A CN 105482995 B CN105482995 B CN 105482995B
- Authority
- CN
- China
- Prior art keywords
- fragrance
- pipe
- reaction
- reaction kettle
- kettle body
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M21/00—Bioreactors or fermenters specially adapted for specific uses
- C12M21/04—Bioreactors or fermenters specially adapted for specific uses for producing gas, e.g. biogas
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M23/00—Constructional details, e.g. recesses, hinges
- C12M23/36—Means for collection or storage of gas; Gas holders
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M23/00—Constructional details, e.g. recesses, hinges
- C12M23/38—Caps; Covers; Plugs; Pouring means
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M23/00—Constructional details, e.g. recesses, hinges
- C12M23/56—Floating elements
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M27/00—Means for mixing, agitating or circulating fluids in the vessel
- C12M27/02—Stirrer or mobile mixing elements
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M29/00—Means for introduction, extraction or recirculation of materials, e.g. pumps
- C12M29/04—Filters; Permeable or porous membranes or plates, e.g. dialysis
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M41/00—Means for regulation, monitoring, measurement or control, e.g. flow regulation
- C12M41/12—Means for regulation, monitoring, measurement or control, e.g. flow regulation of temperature
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M41/00—Means for regulation, monitoring, measurement or control, e.g. flow regulation
- C12M41/12—Means for regulation, monitoring, measurement or control, e.g. flow regulation of temperature
- C12M41/18—Heat exchange systems, e.g. heat jackets or outer envelopes
- C12M41/22—Heat exchange systems, e.g. heat jackets or outer envelopes in contact with the bioreactor walls
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M41/00—Means for regulation, monitoring, measurement or control, e.g. flow regulation
- C12M41/26—Means for regulation, monitoring, measurement or control, e.g. flow regulation of pH
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M41/00—Means for regulation, monitoring, measurement or control, e.g. flow regulation
- C12M41/30—Means for regulation, monitoring, measurement or control, e.g. flow regulation of concentration
- C12M41/34—Means for regulation, monitoring, measurement or control, e.g. flow regulation of concentration of gas
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Zoology (AREA)
- Genetics & Genomics (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- Sustainable Development (AREA)
- Analytical Chemistry (AREA)
- Clinical Laboratory Science (AREA)
- Molecular Biology (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Fats And Perfumes (AREA)
Abstract
Produced the present invention relates to a kind of fragrance and enriching apparatus, it includes reaction structure, reaction condition adjustment structure and fragrance enrichment structure；Reaction structure includes being provided with stirrer in reaction kettle body, the kettle cover for sealing reaction kettle body upper end open of upper end open, reaction kettle body；Reaction condition adjustment structure includes gas regulation structure, pH value adjustment structure and reaction temperature adjustment structure；Gas regulation structure is used to adjust the oxygen concentration in reaction kettle body；PH value adjustment structure is used to adjust the pH value in reaction kettle body, and reaction temperature adjustment structure is used to adjust the reaction temperature in reaction kettle body, and fragrance enrichment structure is enriched with for producing fragrance to reaction, while allowing the gas not being enriched with to return in reaction kettle body.The apparatus structure is simple, and cost is low, and operation is flexible, easy to use and reliable, it is easy to promote.
Description
Technical field
The present invention relates to a kind of device, produced more particularly to a kind of fragrance and enriching apparatus, more specifically to one
Plant biofermentation or Biocatalytic Conversion natural animal-plant raw material produces biological fragrance and is enriched with the device of fragrance, the device is used for
Trace analysis biofermentation or the fragrant process of Biocatalytic Conversion production and fragrance constituent.
Background technology
Essence and flavoring agent is widely used in food, beverage, feed, cosmetics, detergent, chemistry and field of medicaments.Mesh
Many flavor compounds of preceding in the market are from three aspects：
One is the natural perfume material that extraction is produced and come from plant and animal.Up to the present, certain plants and animal
It is still an important sources of spices, but the amount that these bioactive substances are present is often less, and they can only be precious at some
Very found in (plant) kind so that separation is very difficult.
Two be the synthetic perfume come from organic synthesis.With the development and the progress of analytical technology of synthetic organic chemistry,
People can separate and prepare on an industrial scale a considerable amount of spices.But, chemical synthesis often uses not friendly to environment
Good production technology, consumers are to chemical products or the class native compound of synthesis, production especially related to food and family expenses
Product, generate a kind of attitude of " chemistry is frightened ".The notice of consumer is just rapid to prepare and uses (micro-) biological source to biology
Flavor compounds --- spices direction changes, and tends to the product of " natural " or " organic ", has thus developed a source
In the spices market of biotechnology.
Three be the spices come from microbial fermentation conversion or biological enzyme.A long time ago, people are unconscious
In the case of microorganism is make use of to produce spices, especially when preparing fermented food and beverage.In most cases, one
Typically, the microorganism species mixed determine the formation of fragrance that we want certain and complicated, such as cheese, acid
Taste in milk, soy sauce, beer, pickles etc..And the fragrant process of this bio, it usually needs it is raised to a few decaliter laboratory hairs several
Completed in the experiment of fermentation tank scale, and the enrichment of fragrance is to utilize to ventilate during the fermentation, will very volatile fragrance
Fermentation medium is taken away, so as to be tightly held by activated carbon at the exhaust apparatus of fermentation tank, the process such as reclaims through solvent extraction after
Complete.In existing spices preparation process, the problem of existing：
1st, whether solid-state fermentation tank or liquid fermentation tank, equipment price costliness, and installation for fermenting fermentation tank is general
Property is poor, it is difficult to meet scientific research institutions, laboratory research demand.
2nd, the required biomass material for being used to ferment is more, and production perfume quantity is big, could take fragrance out of by ventilation and by
Enrichment, for a small amount of vegetalitas or animal raw materials, it is impossible to the effective exploitation that conducts a research, prepares and detects in fermentation process
Fragrance component.
3rd, the inhomogeneity caught up with is blown to fermentation tank fragrance due to ventilating, fragrance hardly possible is reclaimed through adsorbing from the gas outlet of fermentation tank
To quantify, the fragrance of enrichment can not completely react the type and quantity of aroma substance in fermentation process.
The content of the invention
In view of the above-mentioned problems existing in the prior art, it is an object of the invention to provide one kind it is simple in construction, cost is low, operation
Flexible fragrance is produced and enriching apparatus.
To achieve the above object, the present invention is adopted the following technical scheme that：A kind of fragrance is produced and enriching apparatus, including reaction
Structure, reaction condition adjustment structure and fragrance enrichment structure；
The reaction kettle body of the reaction structure including upper end open, feed supplement structure and for sealing reaction kettle body upper end open
Kettle cover；
Piston is provided with the reaction kettle body, the inner wall sealing of the piston and reaction kettle body is slidably matched, and will reaction
Kettle is divided into independent two cavitys up and down, and the wherein top part of lower chamber is used to assemble gas, and part on the lower is used to put
Put reaction mass；The part of the lower chamber on the lower is provided with stirrer；The piston is provided with piston unidirectional stop valve,
The feed supplement structure includes feed container, feed supplement branch pipe and the control of additive raw material valve being arranged on feed supplement branch pipe, described
One end of feed supplement branch pipe is stretched into reaction kettle body through kettle wall, and the other end is connected with feed container；
The reaction condition adjustment structure includes gas regulation structure, pH value adjustment structure and reaction temperature adjustment structure；
The gas regulation structure includes dissolved oxygen meter, air bag, bladder manifolds, the gas control valve being arranged in bladder manifolds
Door and the dissolved oxygen instrument probe pipe being arranged on the kettle wall of lower chamber lower portion；The probe of the dissolved oxygen meter passes through dissolved oxygen instrument probe
Pipe is fixed on kettle wall, for the oxygen concentration in detection reaction kettle, and one end of bladder manifolds is connected with air bag, and the other end is worn
Cross kettle wall to stretch into reaction kettle body, gas control valve carries out switch control according to the probe value of dissolved oxygen meter；
The pH value adjustment structure includes pH and determines probe, soda acid tank, acid-base value regulation branch pipe, is arranged on acid-base value regulation
Acid-base value control valve on branch pipe determines probe pipe with the pH being arranged on the kettle wall of lower chamber lower portion；The pH is determined
Probe determines probe pipe by pH and is fixed on kettle wall, for the pH value in detection reaction kettle, the one of acid-base value regulation branch pipe
End is connected with soda acid tank, and the other end is stretched into reaction kettle body through kettle wall, and acid-base value control valve determines the spy of probe according to pH
Measured value carries out switch control；
The reaction temperature adjustment structure includes temperature testing equipment, for making reaction kettle body keep the structure of constant temperature and set
Put the temperature testing equipment probe installing pipe on the kettle wall of lower chamber lower portion；The probe of temperature testing equipment passes through temperature
Detection device probe installing pipe is fixed on kettle wall, and for the reaction temperature in detection reaction kettle, reaction kettle body keeps constant temperature
Structure according to the probe value of temperature testing equipment adjust reaction kettle body in reaction temperature；
The fragrance enrichment structure includes air inlet pipe, fragrance capturing structure and escape pipe；The inlet end of the air inlet pipe is worn
Kettle wall is crossed to stretch into reaction kettle body, and inlet end is located at the top part of lower chamber, the inlet end of air inlet pipe is unidirectional provided with air inlet
Air intake control valve door is additionally provided with stop valve, air inlet pipe；The outlet side of escape pipe is stretched into reaction kettle body through kettle cover, and outlet
End is located in upper cavity, and the outlet side of escape pipe, which is provided with outlet unidirectional stop valve, escape pipe, is additionally provided with leaving air control valve door；Enter
The outlet side of tracheae is connected with the inlet end of fragrance capturing structure, and the inlet end of escape pipe connects with the outlet side of fragrance capturing structure
It is logical.
As optimization, in addition to the hoop connector for kettle cover and reaction kettle body upper end to be tightly secured together.
As optimization, sealing ring is provided between the reaction kettle body and kettle cover.
As optimization, in addition to piston rod, the lower end of the piston rod is fixedly connected with the piston, and upper end is stretched out from kettle cover,
Upper cover of piston rod is provided with Simmer ring, and the upper surface of the Simmer ring and kettle cover offsets.
As optimization, the structure for making reaction kettle body keep constant temperature includes the kettle wall of reaction kettle body, and the kettle wall is by internal layer
Constituted with outer layer, there is the cavity for holding liquid medium between the internal layer and outer layer, and the cavity has liquid outlet and liquid
Body import；Isothermal liquid medium is contained with the cavity.
As optimization, the fragrance capturing structure includes multiple fragrance being serially connected and catches pipe.
As optimization, the fragrance catches the sorbing material or organic solvent or water being provided with pipe for adsorbed gas.
As optimization, the multiple fragrance catch part fragrance in pipe catch set in pipe sorbing material or organic solvent or
Water, it is blank pipe that another part fragrance, which catches pipe, and is placed in freezing progress enriched gas in liquid nitrogen.
As optimization, the bladder manifolds are positioned at the part between kettle wall and gas control valve, acid-base value regulation branch pipe
Part, air inlet pipe between kettle wall and acid-base value control valve are located at air inlet unidirectional stop valve and fragrance capturing structure air inlet
Part, escape pipe between end are located at part and feed supplement branch between outlet unidirectional stop valve and fragrance capturing structure outlet side
Pipe is located at partly is respectively equipped with microporous barrier between kettle wall and control of additive raw material valve.
Relative to prior art, the invention has the advantages that：
1st, fragrance disclosed by the invention is produced and enriching apparatus, and simple in construction, cost is low, and operation is flexible, it is easy to use can
Lean on, highly versatile, can be widely applied to scientific research institutions, Corporation R ＆ D mechanism meets laboratory research demand, it is easy to promote.
2nd, fragrance disclosed by the invention is produced and enriching apparatus, compact, and dismounting, cleaning, filling material are flexible,
The required of animal or plant nature biomass material for being used to ferment is few, for a small amount of vegetalitas or animal raw materials, can be effective
The exploitation that conducts a research prepares biological fragrance.
3rd, fragrance disclosed by the invention is produced and enriching apparatus, sets effective biological fragrance enriching apparatus, difficulty of processing
It is low, it is easy to assemble, it is easy to install, save cost；By manual lifting or pushing piston handle, piston reciprocating fortune is promoted
Turn, fragrance enters fragrance enrichment pipe and is captured in driving chamber B, saves energy consumption；Gas can be discharged comprehensively in chamber B simultaneously,
Participate in exchanging enrichment, the aroma substance in elution fragrance enrichment pipe is dissolved by solvent, eluent can be used for quantitative analysis fragrance
Type and quantity.
4th, fragrance disclosed by the invention is produced and enriching apparatus, effective biological fragrance enriching apparatus is set, by efficient
Fragrance enrichment pipe, uniformly effectively captures the biological fragrance that biofermentation conversion is produced, is biofermentation and Biocatalytic Conversion
The multicomponent quantitative analysis research and timely trace analysis spices for producing spices produce process analysis procedure analysis there is provided strong instrument.
Brief description of the drawings
Fig. 1 is the structure diagram of fragrance of the present invention generation and enriching apparatus.
Embodiment
The present invention is described in further detail below.
In the description of the invention, it is to be understood that term " on ", " under ", " top ", " bottom " " interior ", " outer " etc. are indicated
Orientation or position relationship be based on orientation shown in the drawings or position relationship, be for only for ease of description the present invention and simplification retouch
State, rather than indicate or imply that the device or element of meaning there must be specific orientation, with specific azimuth configuration and operation,
Therefore it is not considered as limiting the invention.
Produced and enriching apparatus referring to a kind of fragrance of Fig. 1, including reaction structure, reaction condition adjustment structure and fragrance are rich
Structure set；
The reaction kettle body 1 of the reaction structure including upper end open, feed supplement structure and opened for sealing the upper end of reaction kettle body 1
The kettle cover 24 of mouth；Also include the hoop connector 39 for being used to kettle cover 24 and the upper end of reaction kettle body 1 being tightly secured together.Answer kettle
Sealing ring 25 is provided between body 1 and kettle cover 24.The sealing between reaction kettle body 1 and kettle cover 24 is improved, is conducive to the life of fragrance
Production and enrichment.Sealing ring is provided between reaction kettle body and kettle cover, and is fixed using hoop connector, makes kettle cover 24 and reaction kettle body
1 forms an organic whole, it is easy to flexibly dismounting, cleaning and filling material, and can sterilize offline.
Piston 37 is provided with the reaction kettle body 1, the inner wall sealing of the piston 37 and reaction kettle body 1 is slidably matched, and
Reaction kettle body 1 is divided into independent two cavitys up and down, the wherein top part of lower chamber is used to assemble gas, part on the lower
For placing response material；The part of the lower chamber on the lower is provided with stirrer 3；The piston 37 is provided with piston unidirectional cutoff
Valve 36, piston unidirectional stop valve 36 is used to make the gas in upper cavity enter lower chamber, while preventing the gas in lower chamber from entering
Enter upper cavity；Upper cavity is designated as chamber A, and the top part of lower chamber can be designated as chamber B, and the part of lower chamber on the lower can be designated as chamber
Room C, referring to Fig. 1.Cavity C is used for placing response material, and reaction mass undergoes microbial fermentation or bioconversion catalysis produces gas
Body, the air accumulation is full of chamber B in chamber B.Kettle 1 is not limited to the shape of diagram, can be cylindricality, square, ellipse
The practicality shape such as shape, triangle, trapezoidal.The setting of stirrer 3 contributes to the mixing of reaction mass in reaction kettle body 1.Stirrer 3
Can be magnetic stir bar or bead or molecular sieve, magnetic stir bar can be rotated under magnetic stirring apparatus effect；Bead or
Molecular sieve can shake in shaking table.
Also include piston rod 21, the lower end of the piston rod 21 is fixedly connected with piston 37, and upper end is stretched out from kettle cover 24, it is living
Simmer ring 15 is arranged with stopper rod 21, and the upper surface of the Simmer ring 15 and kettle cover 24 offsets.The setting of Simmer ring 15
Primarily to more preferably, more easily keeping the sealing of kettle, and reaction system is prevented to be contaminated；The setting of piston rod 21
Primarily to convenient artificial operation piston is moved up and down, when it is implemented, handle can also be set on the top of piston rod 21
20。
The feed supplement structure includes feed container 19, feed supplement branch pipe 28 and the control of additive raw material valve being arranged on feed supplement branch pipe 28
22, one end of the feed supplement branch pipe 28 is stretched into reaction kettle body 1 through kettle wall, and the other end is connected with feed container 19；Feed supplement knot
Structure is used to supplement the nutriment for reacting and needing to reaction kettle body 1.
The reaction condition adjustment structure includes gas regulation structure, pH value adjustment structure and reaction temperature adjustment structure；
The gas regulation structure includes dissolved oxygen meter, air bag 9, bladder manifolds 6, the gas control being arranged in bladder manifolds 6
Valve 8 processed and the dissolved oxygen instrument probe pipe 29 being arranged on the kettle wall of lower chamber lower portion；The probe of the dissolved oxygen meter passes through molten
Oxygen instrument probe pipe 29 is fixed on kettle wall, for the oxygen concentration in detection reaction kettle 1, one end and the air bag 9 of bladder manifolds 6
Connection, the other end is stretched into reaction kettle body 1 through kettle wall, and gas control valve 8 carries out switch control according to the probe value of dissolved oxygen meter
System；When it is implemented, the oxygen concentration in the reaction kettle body 1 that staff detects according to dissolved oxygen meter is filled with accordingly in air bag 9
Gas, further according to dissolved oxygen meter detect reaction kettle body 1 in oxygen concentration size control gas control valve 8 switch, control
Gas in air bag 9 processed enters in reaction kettle body 1, so as to control the oxygen concentration in reaction kettle body 1.
, can be for oxygen, air or containing different oxygen concentrations in air bag for oxygen consumption or amphimicrobian fermentation or catalyzed conversion
Air；Can be the inert gases such as nitrogen or carbon dioxide in air bag for anaerobic fermentation or catalyzed conversion.
The pH value adjustment structure includes pH and determines probe, soda acid tank 16, acid-base value regulation branch pipe 27, is arranged on acid-base value
The acid-base value control valve 17 and pH being arranged on the kettle wall of lower chamber lower portion on regulation branch pipe 27 determines probe pipe 30；
The pH determines probe and is fixed on by pH measure probe pipes 30 on kettle wall, for the pH value in detection reaction kettle 1, acid-base value
One end of regulation branch pipe 27 is connected with soda acid tank 16, and the other end is stretched into reaction kettle body 1 through kettle wall, acid-base value control valve 17
Switch control is carried out according to the pH probe values for determining probe；When it is implemented, staff determines the detection of probe according to pH
Feed supplement enters in reaction kettle body 1 in the switch of pH value control acid-base value control valve 17 in reaction kettle body 1, control soda acid tank 16
Amount, so as to control the pH value in reaction kettle body 1.
The reaction temperature adjustment structure includes temperature testing equipment, for making reaction kettle body keep the structure of constant temperature and set
Put the temperature testing equipment probe installing pipe 5 on the kettle wall of lower chamber lower portion；The probe of temperature testing equipment passes through temperature
Degree detection device probe installing pipe 5 is fixed on kettle wall, and for the reaction temperature in detection reaction kettle 1, reaction kettle body is kept
The structure of constant temperature adjusts the reaction temperature in reaction kettle body according to the probe value of temperature testing equipment；The temperature testing equipment can be with
It is thermometer or other existing equipments.
The structure for making reaction kettle body keep constant temperature includes the kettle wall of reaction kettle body 1, and the kettle wall is by internal layer and outer layer structure
Into, there is the cavity 2 for holding liquid medium between the internal layer and outer layer, and the cavity has liquid outlet 26 and liquid-inlet
4；Isothermal liquid medium is contained with the cavity 2.When specifically implementing, liquid outlet 26, liquid-inlet 4 and temperature controller
Connection forms closed-loop path, so as to realize the control to liquid medium temperature in cavity 2, and then realization pair by temperature controller
The thermostatic control of the interior reaction temperature of reaction kettle body 1.Reaction kettle body is set to keep the structure of constant temperature can be with water bath with thermostatic control, directly will be anti-
Answer kettle 1 to be placed in water bath with thermostatic control and realize constant temperature.
When it is implemented, the reaction temperature in the reaction kettle body 1 that staff detects according to temperature testing equipment adjusts permanent
The temperature of tepidarium, or regulation are arranged on the temperature of the liquid medium between kettle wall internal layer and outer layer, so as to realize that regulation is anti-
Answer the purpose of kettle interior reaction temperature.
The fragrance enrichment structure includes air inlet pipe 33, fragrance capturing structure and escape pipe 14；The air inlet pipe 33 is entered
Gas end 31 is stretched into reaction kettle body 1 through kettle wall, and inlet end 31 is located at the top part of lower chamber, the inlet end of air inlet pipe 33
31 are provided with air inlet unidirectional stop valve 32, and air intake control valve door 34 is additionally provided with air inlet pipe 33；The outlet side 38 of escape pipe 14 is passed through
Kettle cover 24 is stretched into reaction kettle body 1, and outlet side 38 is located in upper cavity, and the outlet side 38 of escape pipe 14 is unidirectionally cut provided with outlet
Leaving air control valve door 13 is additionally provided with only valve 40, escape pipe 14；The outlet side of air inlet pipe 33 and the inlet end of fragrance capturing structure
Connection, the inlet end of escape pipe 14 is connected with the outlet side of fragrance capturing structure.
Fragrance capturing structure includes multiple fragrance being serially connected and catches pipe, and fragrance, which catches to be provided with pipe, to be used to adsorb
The sorbing material or organic solvent or water of gas.Sorbing material can be nano-fiber material, activated carbon or resin, and fragrance is caught
In pipe when being provided for the sorbing material or organic solvent or water of adsorbed gas, can be placed in 50 degree above freezing to subzero 150 degree it is cold
Freeze and absorb.The mode of this enriched gas is simple and easy to apply.
It can also be that blank pipe is placed in freezing progress enriched gas in liquid nitrogen that fragrance, which catches pipe,.As optimization, fragrance catches knot
Structure can also be the combination of diversified forms, such as multiple fragrance catch part fragrance in pipe and catch the interior setting sorbing material of pipe or have
Machine solvent or water, it is blank pipe that another part fragrance, which catches pipe, and is placed in freezing progress enriched gas in liquid nitrogen.Referring to Fig. 1, fragrance
Capturing structure catches pipe 10 by the fragrance connected and fragrance catches pipe 11 and constituted, when it is implemented, pipe 10 can be caught in fragrance
Interior setting sorbing material or organic solvent or water, and it is that blank pipe is placed in freezing progress enriched gas in liquid nitrogen that fragrance, which catches pipe 11,.
As optimization, the bladder manifolds 6 are positioned at the part between kettle wall and gas control valve 8, acid-base value regulation branch
Pipe 27 is located at air inlet unidirectional stop valve 32 positioned at the part between kettle wall and acid-base value control valve 17, air inlet pipe 33 and fragrance is caught
The part between structure inlet end, escape pipe 14 is caught to be located between outlet unidirectional stop valve 40 and fragrance capturing structure outlet side
Part and feed supplement branch pipe 28, which are located at, is partly respectively equipped with microporous barrier 35 between kettle wall and control of additive raw material valve 22.The setting of microporous barrier
Microbial cells can be prevented to be disengaged with fragrance, or microorganism enters in reaction kettle body 1 in isolation pipeline, the biological fragrance production of influence
It is raw.
Fragrance that the present invention is provided is produced and enriching apparatus has simple in construction, simplifies difficulty of processing, production cost is low,
Experimental provision is easy to operate, and fragrance enrichment can be quantified, be conducive to the analysis to fragrance component.
The operation principle of the present invention is as follows：
Rotated or shaken by stirrer in cavity C 3 and gas in kettle inner cavity chamber C is driven, promoted to the perfume (or spice) in cavity C
Gas composition is discharged into chamber B；Staff, is pressed downward piston rod handle 20, promotes piston 37 to move downward, chamber B
Middle gas passes through unidirectional stop valve 32 by the inlet end 31 of air inlet pipe 33, is enriched with into gas enrichment pipe 10 and gas enrichment pipe 11
Afterwards, the gas not being enriched with continues on through outlet individual event stop valve 40 on escape pipe 14, the outlet side 38 of escape pipe 14 and entered
Chamber A.Then, staff, is lifted up piston rod handle 20, pulls piston 37 to rise, the gas in compressing chamber A, warp
Entered by piston unidirectional stop valve 36 in chamber B, so, fragrance is produced in cavity C and discharged into kettle inner cavity chamber B, in people
Work is manually under the effect of forces piston 37 downwards, and the fragrance in chamber B is pressed into fragrance and caught in pipe, the gas at large caught
Into in chamber A.
Staff, is lifted up piston rod handle 20, pulls piston 37 to rise, the gas in compressing chamber A, via work
Fill in unidirectional stop valve 36 to enter in chamber B, complete one cycle.And so on, carried by manual depression or above, kettle is promoted back and forth
Interior gas is effectively pressed into enrichment system, when gas passes through fragrance enrichment pipe, and fragrance is caught pipe seizure and be enriched with by fragrance.
Finally illustrate, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although with reference to compared with
The present invention is described in detail good embodiment, it will be understood by those within the art that, can be to skill of the invention
Art scheme is modified or equivalent substitution, and without departing from the objective and scope of technical solution of the present invention, it all should cover at this
Among the right of invention.
Claims (9)
1. a kind of fragrance is produced and enriching apparatus, it is characterised in that：It is rich including reaction structure, reaction condition adjustment structure and fragrance
Structure set；
The reaction kettle body (1) of the reaction structure including upper end open, feed supplement structure and opened for sealing reaction kettle body (1) upper end
The kettle cover (24) of mouth；
Piston (37) is provided with the reaction kettle body (1), the inner wall sealing slip of the piston (37) and reaction kettle body (1) is matched somebody with somebody
Close, and reaction kettle body (1) is divided into independent two cavitys up and down, the wherein top part of lower chamber is used to assemble gas, leaned on
Under part be used for placing response material；The part of the lower chamber on the lower is provided with stirrer (3)；The piston (37) is provided with
Piston unidirectional stop valve (36),
The feed supplement structure includes feed container (19), feed supplement branch pipe (28) and the control of additive raw material being arranged on feed supplement branch pipe (28)
Valve (22), one end of the feed supplement branch pipe (28) is stretched into reaction kettle body (1) through kettle wall, and the other end connects with feed container (19)
It is logical；
The reaction condition adjustment structure includes gas regulation structure, pH value adjustment structure and reaction temperature adjustment structure；
The gas regulation structure includes dissolved oxygen meter, air bag (9), bladder manifolds (6), the gas being arranged in bladder manifolds (6)
Control valve (8) and the dissolved oxygen instrument probe pipe (29) being arranged on the kettle wall of lower chamber lower portion；The probe of the dissolved oxygen meter
It is fixed on by dissolved oxygen instrument probe pipe (29) on kettle wall, for the oxygen concentration in detection reaction kettle (1), bladder manifolds (6)
One end connected with air bag (9), the other end is stretched into reaction kettle body (1) through kettle wall, and gas control valve (8) is according to dissolved oxygen meter
Probe value carry out switch control；
The pH value adjustment structure includes pH and determines probe, soda acid tank (16), acid-base value regulation branch pipe (27), is arranged on acid-base value
Adjust the acid-base value control valve (17) on branch pipe (27) and the pH being arranged on the kettle wall of lower chamber lower portion determines probe
Manage (30)；The pH determines probe and is fixed on by pH measure probe pipes (30) on kettle wall, in detection reaction kettle (1)
PH value, one end of acid-base value regulation branch pipe (27) is connected with soda acid tank (16), and the other end stretches into reaction kettle body (1) through kettle wall
Interior, acid-base value control valve (17) carries out switch control according to the pH probe values for determining probe；
The reaction temperature adjustment structure includes temperature testing equipment, for making reaction kettle body keep the structure of constant temperature and be arranged on
Temperature testing equipment probe installing pipe (5) on the kettle wall of lower chamber lower portion；The probe of temperature testing equipment passes through temperature
Detection device probe installing pipe (5) is fixed on kettle wall, and for the reaction temperature in detection reaction kettle (1), reaction kettle body is protected
The structure of constant temperature is held according to the reaction temperature in the probe value of temperature testing equipment regulation reaction kettle body；
The fragrance enrichment structure includes air inlet pipe (33), fragrance capturing structure and escape pipe (14)；The air inlet pipe (33)
Inlet end (31) is stretched into reaction kettle body (1) through kettle wall, and inlet end (31) is located at the top part of lower chamber, air inlet pipe
(33) inlet end (31), which is provided with air inlet unidirectional stop valve (32), air inlet pipe (33), is additionally provided with air intake control valve door (34)；Go out
The outlet side (38) of tracheae (14) is stretched into reaction kettle body (1) through kettle cover (24), and outlet side (38) are located in upper cavity, go out
The outlet side (38) of tracheae (14), which is provided with outlet unidirectional stop valve (40), escape pipe (14), is additionally provided with leaving air control valve door
(13)；The outlet side of air inlet pipe (33) is connected with the inlet end of fragrance capturing structure, and the inlet end of escape pipe (14) is caught with fragrance
Catch the outlet side connection of structure.
2. fragrance as claimed in claim 1 is produced and enriching apparatus, it is characterised in that：Also include for by kettle cover (24) and instead
The hoop connector (39) for answering kettle (1) upper end to be tightly secured together.
3. fragrance as claimed in claim 1 is produced and enriching apparatus, it is characterised in that：The reaction kettle body (1) and kettle cover
(24) sealing ring (25) is provided between.
4. fragrance as claimed in claim 1 is produced and enriching apparatus, it is characterised in that：Also include piston rod (21), the piston
The lower end of bar (21) is fixedly connected with piston (37), and upper end is stretched out from kettle cover (24), and piston rod is arranged with sealing on (21)
Enclose (15), and the upper surface of the Simmer ring (15) and kettle cover (24) offsets.
5. the fragrance as described in claim any one of 1-4 is produced and enriching apparatus, it is characterised in that：It is described to protect reaction kettle body
Holding the structure of constant temperature includes the kettle wall of reaction kettle body (1), and the kettle wall is made up of internal layer and outer layer, has between the internal layer and outer layer
There is the cavity (2) for holding liquid medium, and the cavity has liquid outlet (26) and liquid-inlet (4)；Contained in the cavity (2)
It is placed with isothermal liquid medium.
6. fragrance as claimed in claim 4 is produced and enriching apparatus, it is characterised in that：The fragrance capturing structure includes multiple
The fragrance being serially connected catches pipe.
7. fragrance as claimed in claim 6 is produced and enriching apparatus, it is characterised in that：The fragrance, which catches to be provided with pipe, to be used for
The sorbing material or organic solvent or water of adsorbed gas.
8. fragrance as claimed in claim 6 is produced and enriching apparatus, it is characterised in that：The multiple fragrance catches part in pipe
Fragrance catches and sorbing material or organic solvent or water is set in pipe, and it is blank pipe that another part fragrance, which catches pipe, and is placed in liquid nitrogen
Freezing carries out enriched gas.
9. fragrance as claimed in claim 1 is produced and enriching apparatus, it is characterised in that：The bladder manifolds (6) are located at kettle wall
Part between gas control valve (8), acid-base value regulation branch pipe (27) be located at kettle wall and acid-base value control valve (17) it
Between part, air inlet pipe (33) be located at part between air inlet unidirectional stop valve (32) and fragrance capturing structure inlet end, outlet
Manage part and feed supplement branch pipe (28) position that (14) are located between outlet unidirectional stop valve (40) and fragrance capturing structure outlet side
Microporous barrier (35) is partly respectively equipped between kettle wall and control of additive raw material valve (22).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510976876.4A CN105482995B (en) | 2015-12-22 | 2015-12-22 | A kind of fragrance is produced and enriching apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510976876.4A CN105482995B (en) | 2015-12-22 | 2015-12-22 | A kind of fragrance is produced and enriching apparatus |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105482995A CN105482995A (en) | 2016-04-13 |
| CN105482995B true CN105482995B (en) | 2017-09-29 |
Family
ID=55670276
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510976876.4A Active CN105482995B (en) | 2015-12-22 | 2015-12-22 | A kind of fragrance is produced and enriching apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105482995B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105907604B (en) * | 2016-05-19 | 2018-04-17 | 西安建筑科技大学 | A kind of single cylinder Stirver for methane tank |
| CN109456880B (en) * | 2018-12-20 | 2022-07-19 | 中国检验检疫科学研究院 | On-site rapid nucleic acid extraction tube and use method thereof |
| CN110257227B (en) * | 2019-06-20 | 2020-08-04 | 江南大学 | Bioreactor for animal cell culture |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7517665B1 (en) * | 2000-05-03 | 2009-04-14 | Elias Hakalehto | Method and apparatus for concentrating and searching of microbiological specimens |
| WO2009067513A1 (en) * | 2007-11-20 | 2009-05-28 | 3M Innovative Properties Company | Sample preparation container and method |
| CN101393087B (en) * | 2008-10-23 | 2010-11-03 | 公安部上海消防研究所 | On site volatile residue evidence extracting device for public security fire protection |
| CN102749236A (en) * | 2012-06-19 | 2012-10-24 | 宁波大学 | Gas internal circulation separation absorption device for enriching volatile substance and application method thereof |
| CN205420408U (en) * | 2015-12-22 | 2016-08-03 | 波顿（上海）生物技术有限公司 | Fragrance produces and enrichment device |
-
2015
- 2015-12-22 CN CN201510976876.4A patent/CN105482995B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN105482995A (en) | 2016-04-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Dinuccio et al. | Gaseous emissions from the storage of untreated slurries and the fractions obtained after mechanical separation | |
| CN105482995B (en) | A kind of fragrance is produced and enriching apparatus | |
| CN105016802B (en) | A kind of bioreactor and the method using bioreactor conversion solid organic castoff | |
| US20120077243A1 (en) | Closed Bioreactor | |
| CN102864073B (en) | Device for dry and wet co-production of hydrogen and methane by using kitchen garbage and using method thereof | |
| CN105084966B (en) | A kind of film liner container-type installation for fermenting and utilize the device carry out compost, deodorization method | |
| CN103509724B (en) | Low yield fusel oil yeast and application thereof to lowing of content of fusel oil in Xiaoqu raw wine | |
| CN207958386U (en) | A kind of microbial fermentation equipment | |
| CN207891279U (en) | A kind of aerobic composting device | |
| CN106520552B (en) | A kind of biological reactor for cell culture | |
| CN103320273A (en) | Household fruit wine fermentation equipment | |
| CN102167627A (en) | Method for additionally applying carbon dioxide air fertilizer to warm-house booth through agricultural organic waste fermentation | |
| JP2009273399A (en) | Culture apparatus and culture method | |
| CN105754851B (en) | A kind of biology fragrance generates and fragrance enriching apparatus | |
| CN205420408U (en) | Fragrance produces and enrichment device | |
| CN205420419U (en) | Biological fragrance produces and fragrance enrichment device | |
| KR20110104852A (en) | The automatic effective - microorganisms fermentation unit | |
| CN108458944B (en) | Device and method for measuring technological parameters of composting of cellulose substances | |
| US9340806B2 (en) | Method of initiating acetic fermentation under industrial conditions | |
| CN108771115A (en) | A kind of GABA enrichments powder, preparation method thereof | |
| CN207313453U (en) | A kind of sludge composting one disposal plant | |
| CN211770325U (en) | Portable device of carbon dioxide generator | |
| CN109942326A (en) | A kind of organic fertilizer compost fermentation device and method | |
| CN206970593U (en) | A kind of culture device for anaerobic bacteria | |
| CN104509520A (en) | Controlled-atmosphere heating plate system for quickly estimating lethal characteristics of pests |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| EE01 | Entry into force of recordation of patent licensing contract | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20160413 Assignee: Shenzhen xinshengrui Biotechnology Co.,Ltd. Assignor: BOTON (SHANGHAI) BIOTECHNOLOGY Co.,Ltd. Contract record no.: X2022980009383 Denomination of invention: An aroma generation and enrichment device Granted publication date: 20170929 License type: Common License Record date: 20220705 |