CN105482957B - Rhizoma Polygonati extract and its sealwort wine, method for preparing sealwort spirit - Google Patents
Rhizoma Polygonati extract and its sealwort wine, method for preparing sealwort spirit Download PDFInfo
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- CN105482957B CN105482957B CN201510763088.7A CN201510763088A CN105482957B CN 105482957 B CN105482957 B CN 105482957B CN 201510763088 A CN201510763088 A CN 201510763088A CN 105482957 B CN105482957 B CN 105482957B
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Abstract
The invention discloses a kind of Rhizoma Polygonati extracts, extract and obtain by the following method：A. sealwort is crushed；B. gained sealwort powder is placed in extractor, the acid solution of the concentration 0.3 0.8% of 48 times of sealwort powder weight is added, impregnated 1 hour, be then heated to 60 80 DEG C, heated 13 hours, extracting solution is collected in filtering；C., the water that filtered granulated slag is added to 26 times of weight is heated to 55 DEG C, and it is 5.0 to adjust ph values, adds the complex enzyme of granulated slag water weight 0.5 1.5%, digests 2 hours, and enzymolysis liquid is collected in filtering；D. above-mentioned gained extracting solution is merged with enzymolysis liquid, it is neutrality to adjust ph values, is heated to 70 DEG C, adds 0.2 0.6% fining agent clarification 1 hour, and then refined filtration obtains refined filtration liquid；E. gained refined filtration liquid is concentrated under reduced pressure；F. gained concentrate is spray-dried to get Rhizoma Polygonati extract.
Description
Technical field
The present invention relates to a kind of Rhizoma Polygonati extract, a kind of sealwort wine and preparation method thereof is further related to.
Background technology
Sealwort also known as chicken head ginseng, tiger ginseng, are liliaceous plant P. kingianum, sealwort or the dry rhizome of David's-harp, Huang
Essence has the effects that lowering blood pressure and blood fat, hypoglycemic, atherosclerosis, anti-aging and antibacterial, and Siberian solomonseal rhizome polysaccharide also has
There is Immunestimulatory effect, can be used for the lung-dryness syndrome due to yin deficiency, dry cough lacks the chronic cough of phlegm and lung-kidney deficiency, weakness of the spleen and the stomach, not only tonifying spleen-yin, but also benefit
Temper, it may also be used for deficiency of kidney essence obtains dizzy, soreness and weakness of waist and knees, poliosis and quenches one's thirst, and is of great value Chinese medicine simply.
Existing method is mostly to be steep in wine, made tea with sealwort, and nutritive value does not make full use of.If science side can be used
Method extracts high-purity Rhizoma Polygonati extract from sealwort, and then recycling is such as configured to sealwort wine, that will make full use of its nutriture value
Value.
Invention content
The technical problem to be solved in the present invention is to provide a kind of to be carried with high-purity sealwort that scientific method is extracted from sealwort
Take object.A kind of sealwort wine and preparation method thereof prepared with Rhizoma Polygonati extract is also provided.
In order to solve the above-mentioned technical problem, Rhizoma Polygonati extract of the invention is extracted and is obtained by the following method：
A. sealwort is crushed；
B. gained sealwort powder is placed in extractor, the acid solution of the concentration 0.3-0.8% of 4-8 times of sealwort powder weight is added,
It impregnates 1 hour, is then heated to 60-80 DEG C, heat 1-3 hours, extracting solution is collected in filtering；
C., the water that filtered granulated slag is added to 2-6 times of weight is heated to 55 DEG C, and it is 5.0 to adjust ph values, adds granulated slag
The complex enzyme of water weight 0.5-1.5% digests 2 hours, and enzymolysis liquid is collected in filtering；
D. above-mentioned gained extracting solution is merged with enzymolysis liquid, it is neutrality to adjust ph values, is heated to 70 DEG C, adds 0.2-0.6%
Fining agent clarify 1 hour, then refined filtration obtain refined filtration liquid；
E. gained refined filtration liquid is concentrated under reduced pressure；
F. gained concentrate is spray-dried to get Rhizoma Polygonati extract.
B step, the acid are citric acid.
B step, heating temperature are 60 DEG C, and heating time is 2 hours.
Step c, amount of water are 5 times, and enzyme addition is 1%.
The sealwort wine of the present invention is made of the raw material of following parts by weight：Sealwort extracting solution 3-8, glutinous rice wine juice 40-80, white wine
10-20, bamboo-leaves flavones 3-5.
It is preferred that being made of the raw material of following parts by weight：Sealwort extracting solution 6, glutinous rice wine juice 74, white wine 20, bamboo-leaves flavones 3.
The proportion of the sealwort extracting solution is 1.2-1.3.
The alcoholic strength of the white wine is 40%vol.
The method that the present invention prepares sealwort wine includes the following steps：
（1）Prepare glutinous rice wine juice
A. quality glutinous rice is cleaned up, the water of 3-5 times of weight is added, impregnated 8-10 hours, then drain；
B. the glutinous rice after draining the water carries out boiling, cooks postcooling；
C. the dry ferment of the distiller's yeast and 0.02-0.06% of the glutinous rice weight 1-3% after cooking is added, stirs evenly；
D. primary fermentation, the fermenting raw materials that will be stirred evenly, temperature control are 20-30 DEG C, and the time is 30-50 hours；
E. it ferments afterwards, fermentation material is added 1-3 times measures pure water and continue to ferment, temperature control is 18-25 DEG C, and the time is
80-120 hours；
F. the fermentation material to ferment after is squeezed with squeezer, is then filtered up to glutinous rice wine juice with filter；
（2）Prepare Rhizoma Polygonati extract
A. sealwort is crushed；
B. gained sealwort powder is placed in extractor, the acid solution of the concentration 0.3-0.8% of 4-8 times of sealwort powder weight is added,
It impregnates 1 hour, is then heated to 60-80 DEG C, heat 1-3 hours, extracting solution is collected in filtering；
C., the water that filtered granulated slag is added to 2-6 times of weight is heated to 55 DEG C, and it is 5.0 to adjust ph values, adds granulated slag
The complex enzyme of water weight 0.5-1.5% digests 2 hours, and enzymolysis liquid is collected in filtering；
D. above-mentioned gained extracting solution is merged with enzymolysis liquid, it is neutrality to adjust ph values, is heated to 70 DEG C, adds 0.2-0.6%
Fining agent clarify 1 hour, then refined filtration obtain refined filtration liquid；
E. gained refined filtration liquid is concentrated under reduced pressure up to sealwort extracting solution；
（3）Prepare sealwort wine
A. sealwort extracting solution, glutinous rice wine juice, white wine, bamboo-leaves flavones are placed in stirring Agitation Tank, are slowly heated to 35-50
DEG C, 10-30min is stirred, room temperature is then rapidly cooled to；
B. health liquor filter is used to filter to get sealwort wine again.
The health liquor filter-specific membrane aperture is 0.18um.
The method that the present invention extracts Rhizoma Polygonati extract, which uses acid and carries desmoenzyme, carries two kinds of novel process, original not destroying
While active ingredient, the distinctive fragrance of sealwort is remained, and improve the yield of effective ingredient.
The sealwort wine that the present invention produces not only has the nutritional ingredient of traditional rice wine, but also has been sufficiently reserved sealwort
Nutriment, it is the sealwort wine mellow in taste prepared, full of nutrition, and with work(such as boosting qi and nourishing yin, invigorating the spleen, moistening lung, kidney-nourishings
Effect.
The preparation method two-step fermentation of glutinous rice wine juice of the present invention can improve the nutritional ingredient and fragrance of wine juice, additionally it is possible to
Improve distillation yield.
The method of the present invention is easy to operate, it is easy to accomplish.
Specific implementation mode
The following detailed description of the embodiment of the method for the present invention, but it is not limited only to following embodiment.
Embodiment one
Rhizoma Polygonati extract is extracted and is obtained by the following method：
A. sealwort dry plate 10kg is crushed；
B. gained sealwort powder is placed in extractor, the citric acid solution of addition 50L concentration 0.3%, immersion 1 hour, then
60 DEG C are heated to, is heated 2 hours, extracting solution is collected in filtering；
C. filtered granulated slag is added into 50L water, is heated to 55 DEG C, it is 5.0 to adjust ph values, adds granulated slag water weight 1%
Complex enzyme, digest 2 hours, filtering, collect enzymolysis liquid, complex enzyme is cellulase and amylase its weight ratio 2:1；
D. above-mentioned gained extracting solution is merged with enzymolysis liquid, it is neutrality to adjust ph values, is heated to 70 DEG C, adds 0.3% clarification
Agent clarify 1 hour, then refined filtration obtain refined filtration liquid；
E. gained refined filtration liquid is concentrated under reduced pressure into 10L；
F. gained concentrate is spray-dried to get Rhizoma Polygonati extract.
The sealwort wine of the present invention is made of the raw material of following parts by weight：Sealwort extracting solution 6, glutinous rice wine juice 74, high quality liquor
20, bamboo-leaves flavones 3.
The proportion of sealwort extracting solution is 1.2.
The alcoholic strength of white wine is 40%vol.
The method that the present invention prepares sealwort wine includes the following steps：
（1）Prepare glutinous rice wine juice
A. quality glutinous rice is cleaned up, the water of 3 times of weight is added, impregnated 9 hours, then drain；
B. the glutinous rice after draining the water carries out boiling, cooks postcooling；
C. the distiller's yeast of the glutinous rice weight 1% after cooking and 0.03% dry ferment is added, stirs evenly；
D. primary fermentation, the fermenting raw materials that will be stirred evenly, temperature control are 20 DEG C, and the time is 30 hours；
E. it ferments afterwards, fermentation material, which is added 1 times of amount pure water, to be continued to ferment, and temperature control is 18 DEG C, and the time is 120 small
When；
F. the fermentation material to ferment after is squeezed with squeezer, is then filtered up to glutinous rice wine juice with filter；
（2）Prepare sealwort extracting solution
A. sealwort is crushed；
B. gained sealwort powder is placed in extractor, the acid solution of the concentration 0.3% of 4 times of sealwort powder weight is added, impregnate 1
Hour, 60 DEG C are then heated to, is heated 3 hours, extracting solution is collected in filtering；
C., the water that filtered granulated slag is added to 2 times of weight is heated to 55 DEG C, and it is 5.0 to adjust ph values, adds granulated slag water
The complex enzyme of weight 0.5% digests 2 hours, and enzymolysis liquid is collected in filtering；
D. above-mentioned gained extracting solution is merged with enzymolysis liquid, it is neutrality to adjust ph values, is heated to 70 DEG C, adds 0.3% clarification
Agent clarify 1 hour, then refined filtration obtain refined filtration liquid；
E. gained refined filtration liquid is concentrated under reduced pressure；
F. gained concentrate is spray-dried to get Rhizoma Polygonati extract；
（3）Prepare sealwort wine
A. sealwort extracting solution, glutinous rice wine juice, white wine, bamboo-leaves flavones are placed in stirring Agitation Tank, are slowly heated to 35 DEG C,
30min is stirred, room temperature is then rapidly cooled to；
B. health liquor filter is used to filter to get sealwort wine again.
Health liquor filter-specific membrane aperture is 0.18um.
Embodiment two
Rhizoma Polygonati extract is extracted and is obtained by the following method：
A. sealwort dry plate 100kg is crushed；
B. gained sealwort powder is placed in extractor, the citric acid solution of addition 600L concentration 0.8%, immersion 1 hour, so
After be heated to 80 DEG C, heat 2 hours, extracting solution is collected in filtering；
C. filtered granulated slag is added into 600L water, is heated to 55 DEG C, it is 5.0 to adjust ph values, adds granulated slag water weight
1% complex enzyme digests 2 hours, and enzymolysis liquid is collected in filtering；
D. above-mentioned gained extracting solution is merged with enzymolysis liquid, it is neutrality to adjust ph values, is heated to 70 DEG C, adds 0.4% clarification
Agent clarify 1 hour, then refined filtration obtain refined filtration liquid；
E. gained refined filtration liquid is concentrated under reduced pressure into 100L；
F. gained concentrate is spray-dried to get Rhizoma Polygonati extract.
The sealwort wine of the present invention is made of the raw material of following parts by weight：Sealwort extracting solution 3, glutinous rice wine juice 40, white wine 15, bamboo
Leaf flavones 3.
The proportion of sealwort extracting solution is 1.3.
The alcoholic strength of white wine is 40%vol.
The method that the present invention prepares sealwort wine includes the following steps：
（1）Prepare glutinous rice wine juice
A. quality glutinous rice is cleaned up, the water of 5 times of weight is added, impregnated 10 hours, then drain；
B. the glutinous rice after draining the water carries out boiling, cooks postcooling；
C. the distiller's yeast of the glutinous rice weight 3% after cooking and 0.06% dry ferment is added, stirs evenly；
D. primary fermentation, the fermenting raw materials that will be stirred evenly, temperature control are 30 DEG C, and the time is 30 hours；
E. it ferments afterwards, fermentation material, which is added 3 times of amount pure water, to be continued to ferment, and temperature control is 25 DEG C, and the time is 80 hours；
F. the fermentation material to ferment after is squeezed with squeezer, is then filtered up to glutinous rice wine juice with filter；
（2）Prepare Rhizoma Polygonati extract
A. sealwort is crushed；
B. gained sealwort powder is placed in extractor, the acid solution of the concentration 0.8% of 8 times of sealwort powder weight is added, impregnate 1
Hour, 80 DEG C are then heated to, is heated 1 hour, extracting solution is collected in filtering；
C., the water that filtered granulated slag is added to 6 times of weight is heated to 55 DEG C, and it is 5.0 to adjust ph values, adds granulated slag water
The complex enzyme of weight 1.5% digests 2 hours, and enzymolysis liquid is collected in filtering；
D. above-mentioned gained extracting solution is merged with enzymolysis liquid, it is neutrality to adjust ph values, is heated to 70 DEG C, adds 0.6% clarification
Agent clarify 1 hour, then refined filtration obtain refined filtration liquid；
E. gained refined filtration liquid is concentrated under reduced pressure up to sealwort extracting solution；
（3）Prepare sealwort wine
A. sealwort extracting solution, glutinous rice wine juice, white wine, bamboo-leaves flavones are placed in stirring Agitation Tank, are slowly heated to 50 DEG C,
10min is stirred, room temperature is then rapidly cooled to；
B. health liquor filter is used to filter to get sealwort wine again.
Health liquor filter-specific membrane aperture is 0.18um.
White wine is used with common distilled spirit made of the brewing of high quality sorghum, wheat, glutinous rice, rice and millet.Also may be used
With using the distilled spirit of market public offering.
Claims (8)
1. a kind of sealwort wine, it is characterised in that be made of the raw material of following parts by weight：Sealwort extracting solution 3-8, glutinous rice wine juice 40-
80, white wine 10-20, bamboo-leaves flavones 3-5；
Preparation method includes the following steps：
（1）Prepare glutinous rice wine juice
1a. cleans up quality glutinous rice, and the water of 3-5 times of weight is added, and impregnates 8-10 hours, then drains；
Glutinous rice after 1b. will drain the water carries out boiling, cooks postcooling；
The dry ferment of the distiller's yeast and 0.02-0.06% of the glutinous rice weight 1-3% after cooking is added in 1c., stirs evenly；
1d. primary fermentations, the fermenting raw materials that will be stirred evenly, temperature control are 20-30 DEG C, and the time is 30-50 hours；
It ferments after 1e., fermentation material is added 1-3 times measures pure water and continue to ferment, temperature control is 18-25 DEG C, time 80-
120 hours；
1f. squeezes the fermentation material to ferment after with squeezer, is then filtered up to glutinous rice wine juice with filter；
（2）Prepare sealwort extracting solution
2a. crushes sealwort；
Gained sealwort powder is placed in extractor by 2b., and the acid solution of the concentration 0.3-0.8% of 4-8 times of sealwort powder weight, leaching is added
Bubble 1 hour is then heated to 60-80 DEG C, heats 1-3 hours, and extracting solution is collected in filtering；
Filtered granulated slag is added the water of 2-6 times of weight by 2c., is heated to 55 DEG C, and it is 5.0 to adjust ph values, adds granulated slag water
The complex enzyme of weight 0.5-1.5% digests 2 hours, and enzymolysis liquid is collected in filtering；
2d. merges above-mentioned gained extracting solution with enzymolysis liquid, and it is neutrality to adjust ph values, is heated to 70 DEG C, it is clear to add 0.2-0.6%
Clear agent clarifies 1 hour, and then refined filtration obtains refined filtration liquid；
Gained refined filtration liquid is concentrated under reduced pressure up to sealwort extracting solution 2e.；
（3）Prepare sealwort wine
Sealwort extracting solution, glutinous rice wine juice, white wine, bamboo-leaves flavones are placed in stirring Agitation Tank by 3a., are slowly heated to 35-50 DEG C,
10-30min is stirred, room temperature is then rapidly cooled to；
3b. uses health liquor filter to filter to get sealwort wine again.
2. sealwort wine according to claim 1, it is characterised in that：2b steps, the acid are citric acid.
3. sealwort wine according to claim 1, it is characterised in that：2b steps, heating temperature are 60 DEG C, and heating time is 2 small
When.
4. sealwort wine according to claim 1, it is characterised in that：2c steps, amount of water are 5 times, and enzyme addition is 1%.
5. sealwort wine according to claim 1, it is characterised in that be made of the raw material of following parts by weight：It is sealwort extracting solution 6, glutinous
Rice wine juice 74, white wine 20, bamboo-leaves flavones 3.
6. sealwort wine according to claim 1, it is characterised in that：The proportion of the sealwort extracting solution is 1.2-1.3.
7. sealwort wine according to claim 1, it is characterised in that：The alcoholic strength of the white wine is 40%vol.
8. sealwort wine according to claim 1, it is characterised in that：The health liquor filter-specific membrane aperture is 0.18um.
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| CN106367263A (en) * | 2016-08-31 | 2017-02-01 | 沈飞 | Rhizoma polygonati mixed wine and brewing method thereof |
| CN106754116A (en) * | 2016-11-23 | 2017-05-31 | 青海七彩花生物科技有限公司 | A kind of northern Chinese caterpillar Fungus health liquor |
| CN106754102A (en) * | 2017-03-31 | 2017-05-31 | 贵州古耕农牧业发展有限公司 | A kind of sealwort wine and preparation method thereof |
| CN107136508A (en) * | 2017-07-05 | 2017-09-08 | 广州市天河华南发展有限公司 | A kind of composition for improving human nutrition balance and its preparation method and application |
| CN107232544A (en) * | 2017-07-05 | 2017-10-10 | 广州市天河华南发展有限公司 | A kind of composition of nourishing-yin, lowering blood-sugar and its preparation method and application |
| CN108112985A (en) * | 2017-11-08 | 2018-06-05 | 湖南省中医药研究院 | A kind of method for medical and edible dual purpose plant calcium oxalate crystal growth in healthy needle of degrading |
| CN108065371A (en) * | 2018-01-05 | 2018-05-25 | 浙江新篁生物技术有限公司 | A kind of drinks electuary and its manufacturing method |
| CN108841536A (en) * | 2018-08-09 | 2018-11-20 | 重庆市银蜂四云创圆农业开发有限公司 | A kind of sealwort wine preparation process containing Rhizoma Polygonati extract |
| CN113136280A (en) * | 2021-04-26 | 2021-07-20 | 宜宾学院 | Natural bamboo rice wine beverage and preparation method thereof |
| CN114480059A (en) * | 2022-01-10 | 2022-05-13 | 湖南省大观溪生物科技有限公司 | Polygonatum sibiricum health wine and production device thereof |
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