CN105482957A - Rhizoma polygonati extract, rhizoma polygonati wine thereof and rhizoma polygonati wine preparation method - Google Patents
Rhizoma polygonati extract, rhizoma polygonati wine thereof and rhizoma polygonati wine preparation method Download PDFInfo
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Abstract
The invention discloses a rhizoma polygonati extract. The rhizoma polygonati extract is obtained according to the steps of a, pulverizing rhizoma polygonati; b, placing obtained rhizoma polygonati powder in an extraction tank, adding 0.3-0.8% acid solution 4-8 times as heavy as the rhizoma polygonati powder, soaking for one hour, heating to 60-80 DEG C for 1-3 hours, filtering and collecting extracting solution; c, adding water 2-6 times as heavy as filtered powder dregs, heating to 55 DEG C, regulating a ph (potential of hydrogen) value to be 5.0, adding compound enzyme as much as 0.5-1.5% of the weight of powder dreg water, performing enzymolysis for 2 hours, filtering and collecting enzymatic hydrolysate; d, blending the extracting solution with the enzymatic hydrolysate, regulating a ph value to be neutral, heating to 70 DEG C, adding 0.2-0.6% clarifying agent to clarify for one hour, and performing refined filtration to obtain refined filtrate; e, subjecting the refined filtrate to vacuum concentration; f, subjecting concentrated solution to spray drying so as to obtain the rhizoma polygonati extract.
Description
Technical field
The present invention relates to a kind of Rhizoma Polygonati extract, also relate to a kind of sealwort wine and preparation method thereof.
Background technology
yellowessence has another name called chicken head ginseng, tiger ginseng, for the dry rhizome of liliaceous plant P. kingianum, sealwort or David's-harp, sealwort has hypotensive, reducing blood-fat, hypoglycemic, atherosclerosis, delay senility and effect such as antibacterial grade, polygonatum polysaccharide also has Immunestimulatory effect, can be used for the chronic cough of lung-dryness syndrome due to deficiency of YIN, the few phlegm of dry cough and YIN-deficiency of the lung and kidney, weakness of the spleen and the stomach, both tonifying spleen-yin, beneficial temper again, also can be used for deficiency of kidney essence and obtains dizzy, soreness of the waist and knees, early whitening of beard and hair and quenching one's thirst is of great value Chinese medicine simply.
Mostly existing method is to steep in wine with sealwort, make tea, and its nutritive value does not make full use of.If can extract high-purity Rhizoma Polygonati extract by scientific approach from sealwort and then utilize as being mixed with sealwort wine, that can make full use of its nutritive value.
Summary of the invention
The technical problem to be solved in the present invention is just to provide high-purity Rhizoma Polygonati extract that a kind of scientific approach extracts from sealwort.Sealwort wine also providing a kind of Rhizoma Polygonati extract to prepare and preparation method thereof.
In order to solve the problems of the technologies described above, Rhizoma Polygonati extract of the present invention extracts by the following method and obtains:
A. sealwort is pulverized;
B. gained sealwort powder is placed in extractor, adds the acid solution of sealwort grain weight amount 4-8 concentration 0.3-0.8% doubly, soak 1 hour, be then heated to 60-80 DEG C, heating 1-3 hour, filters, and collects extracting solution;
C. the granulated slag after filtration is added the water of 2-6 times of weight again, be heated to 55 DEG C, adjust ph value to be 5.0, then add the prozyme of granulated slag water weight 0.5-1.5%, enzymolysis 2 hours, filter, collect enzymolysis solution;
D. above-mentioned gained extracting solution and enzymolysis solution are merged, adjust ph value to be neutrality, be heated to 70 DEG C, then add 0.2-0.6% finings and clarify 1 hour, then essence filters to obtain smart filtrate;
E. by gained essence filtrate reduced in volume;
F. by gained concentrated solution spraying dry, Rhizoma Polygonati extract is obtained.
B step, described acid is citric acid.
B step, Heating temperature is 60 DEG C, and heat-up time is 2 hours.
Step c, amount of water is 5 times, and enzyme add-on is 1%.
Sealwort wine of the present invention is made up of the raw material of following weight part: sealwort extracting solution 3-8, sticky rice wine juice 40-80, white wine 10-20, Folium Bambosae flavone 3-5.
Preferably be made up of the raw material of following weight part: sealwort extracting solution 6, sticky rice wine juice 74, white wine 20, Folium Bambosae flavone 3.
The proportion of described sealwort extracting solution is 1.2-1.3.
The alcoholic strength of described white wine is 40%vol.
The method that the present invention prepares sealwort wine comprises the steps:
(1) sticky rice wine juice is prepared
A. quality glutinous rice is cleaned up, add the water of 3-5 times of weight, soak 8-10 hour, then drain;
B. the glutinous rice after draining the water is carried out boiling, cook rear cooling;
C. add the distiller's yeast of glutinous rice weight 1-3% after cooking and the dry yeast of 0.02-0.06%, stir;
D. primary fermentation, by the fermenting raw materials stirred, temperature controls as 20-30 DEG C, and the time is 30-50 hour;
E. secondary fermentation, adds 1-3 times amount pure water again and continues fermentation by fermentation material, temperature controls as 18-25 DEG C, and the time is 80-120 hour;
F. the fermentation material squeezing machine through secondary fermentation is squeezed, then filter with filter and obtain sticky rice wine juice;
(2) Rhizoma Polygonati extract is prepared
A. sealwort is pulverized;
B. gained sealwort powder is placed in extractor, adds the acid solution of sealwort grain weight amount 4-8 concentration 0.3-0.8% doubly, soak 1 hour, be then heated to 60-80 DEG C, heating 1-3 hour, filters, and collects extracting solution;
C. the granulated slag after filtration is added the water of 2-6 times of weight again, be heated to 55 DEG C, adjust ph value to be 5.0, then add the prozyme of granulated slag water weight 0.5-1.5%, enzymolysis 2 hours, filter, collect enzymolysis solution;
D. above-mentioned gained extracting solution and enzymolysis solution are merged, adjust ph value to be neutrality, be heated to 70 DEG C, then add 0.2-0.6% finings and clarify 1 hour, then essence filters to obtain smart filtrate;
E. namely gained essence filtrate reduced in volume is obtained sealwort extracting solution;
(3) sealwort wine is prepared
A. sealwort extracting solution, sticky rice wine juice, white wine, Folium Bambosae flavone are placed in and stir Agitation Tank, be slowly heated to 35-50 DEG C, stir 10-30min, be then cooled to normal temperature rapidly;
B. use health promoting wine metre filter again, obtain sealwort wine.
Described health promoting wine filter-specific membrane pore size is 0.18um.
The method that the present invention extracts Rhizoma Polygonati extract have employed acid and carries desmoenzyme and carry two kinds of novel process, while not destroying original active ingredient, remains the distinctive fragrance of sealwort, and improves the yield of effective ingredient.
The sealwort wine that the present invention produces, not only has the nutritive ingredient of traditional rice wine, and fully remains the nutritive substance of sealwort, the sealwort wine mellow in taste prepared, nutritious, and has the effects such as boosting qi and nourishing yin, invigorating the spleen, moistening lung, kidney-nourishing.
Preparation method's two stage fermentation of sticky rice wine juice of the present invention, can improve nutritive ingredient and the fragrance of wine juice, can also improve the yield of liquor.
Method of the present invention is simple to operate, is easy to realize.
Embodiment
The following detailed description of the embodiment of the inventive method, but be not limited only to following examples.
Embodiment one
Rhizoma Polygonati extract extracts by the following method and obtains:
A. sealwort dry plate 10kg is pulverized;
B. gained sealwort powder is placed in extractor, adds the citric acid solution of 50L concentration 0.3%, soak 1 hour, be then heated to 60 DEG C, heat 2 hours, filter, collect extracting solution;
C. the granulated slag after filtration is added 50L water again, be heated to 55 DEG C, adjust ph value to be 5.0, then add the prozyme of granulated slag water weight 1%, enzymolysis 2 hours, filter, collect enzymolysis solution, prozyme is cellulase and its weight ratio 2:1 of amylase;
D. above-mentioned gained extracting solution and enzymolysis solution are merged, adjust ph value to be neutrality, be heated to 70 DEG C, then add 0.3% finings and clarify 1 hour, then essence filters to obtain smart filtrate;
E. by gained essence filtrate reduced in volume to 10L;
F. by gained concentrated solution spraying dry, Rhizoma Polygonati extract is obtained.
Sealwort wine of the present invention is made up of the raw material of following weight part: sealwort extracting solution 6, sticky rice wine juice 74, high quality liquor 20, Folium Bambosae flavone 3.
The proportion of sealwort extracting solution is 1.2.
The alcoholic strength of white wine is 40%vol.
The method that the present invention prepares sealwort wine comprises the steps:
(1) sticky rice wine juice is prepared
A. quality glutinous rice is cleaned up, add the water of 3 times of weight, soak 9 hours, then drain;
B. the glutinous rice after draining the water is carried out boiling, cook rear cooling;
C. add the distiller's yeast of glutinous rice weight 1% after cooking and the dry yeast of 0.03%, stir;
D. primary fermentation, by the fermenting raw materials stirred, it is 20 DEG C that temperature controls, and the time is 30 hours;
E. secondary fermentation, fermentation material is added 1 times amount pure water again and continue fermentation, it is 18 DEG C that temperature controls, and the time is 120 hours;
F. the fermentation material squeezing machine through secondary fermentation is squeezed, then filter with filter and obtain sticky rice wine juice;
(2) sealwort extracting solution is prepared
A. sealwort is pulverized;
B. gained sealwort powder is placed in extractor, adds the acid solution of the concentration 0.3% of sealwort grain weight amount 4 times, soak 1 hour, be then heated to 60 DEG C, heat 3 hours, filter, collect extracting solution;
C. the granulated slag after filtration is added the water of 2 times of weight again, be heated to 55 DEG C, adjust ph value to be 5.0, then add the prozyme of granulated slag water weight 0.5%, enzymolysis 2 hours, filter, collect enzymolysis solution;
D. above-mentioned gained extracting solution and enzymolysis solution are merged, adjust ph value to be neutrality, be heated to 70 DEG C, then add 0.3% finings and clarify 1 hour, then essence filters to obtain smart filtrate;
E. by gained essence filtrate reduced in volume;
F. by gained concentrated solution spraying dry, Rhizoma Polygonati extract is obtained;
(3) sealwort wine is prepared
A. sealwort extracting solution, sticky rice wine juice, white wine, Folium Bambosae flavone are placed in and stir Agitation Tank, be slowly heated to 35 DEG C, stir 30min, be then cooled to normal temperature rapidly;
B. use health promoting wine metre filter again, obtain sealwort wine.
Health promoting wine filter-specific membrane pore size is 0.18um.
Embodiment two
Rhizoma Polygonati extract extracts by the following method and obtains:
A. sealwort dry plate 100kg is pulverized;
B. gained sealwort powder is placed in extractor, adds the citric acid solution of 600L concentration 0.8%, soak 1 hour, be then heated to 80 DEG C, heat 2 hours, filter, collect extracting solution;
C. the granulated slag after filtration is added 600L water again, be heated to 55 DEG C, adjust ph value to be 5.0, then add the prozyme of granulated slag water weight 1%, enzymolysis 2 hours, filter, collect enzymolysis solution;
D. above-mentioned gained extracting solution and enzymolysis solution are merged, adjust ph value to be neutrality, be heated to 70 DEG C, then add 0.4% finings and clarify 1 hour, then essence filters to obtain smart filtrate;
E. by gained essence filtrate reduced in volume to 100L;
F. by gained concentrated solution spraying dry, Rhizoma Polygonati extract is obtained.
Sealwort wine of the present invention is made up of the raw material of following weight part: sealwort extracting solution 3, sticky rice wine juice 40, white wine 15, Folium Bambosae flavone 3.
The proportion of sealwort extracting solution is 1.3.
The alcoholic strength of white wine is 40%vol.
The method that the present invention prepares sealwort wine comprises the steps:
(1) sticky rice wine juice is prepared
A. quality glutinous rice is cleaned up, add the water of 5 times of weight, soak 10 hours, then drain;
B. the glutinous rice after draining the water is carried out boiling, cook rear cooling;
C. add the distiller's yeast of glutinous rice weight 3% after cooking and the dry yeast of 0.06%, stir;
D. primary fermentation, by the fermenting raw materials stirred, it is 30 DEG C that temperature controls, and the time is 30 hours;
E. secondary fermentation, fermentation material is added 3 times amount pure water again and continue fermentation, it is 25 DEG C that temperature controls, and the time is 80 hours;
F. the fermentation material squeezing machine through secondary fermentation is squeezed, then filter with filter and obtain sticky rice wine juice;
(2) Rhizoma Polygonati extract is prepared
A. sealwort is pulverized;
B. gained sealwort powder is placed in extractor, adds the acid solution of the concentration 0.8% of sealwort grain weight amount 8 times, soak 1 hour, be then heated to 80 DEG C, heat 1 hour, filter, collect extracting solution;
C. the granulated slag after filtration is added the water of 6 times of weight again, be heated to 55 DEG C, adjust ph value to be 5.0, then add the prozyme of granulated slag water weight 1.5%, enzymolysis 2 hours, filter, collect enzymolysis solution;
D. above-mentioned gained extracting solution and enzymolysis solution are merged, adjust ph value to be neutrality, be heated to 70 DEG C, then add 0.6% finings and clarify 1 hour, then essence filters to obtain smart filtrate;
E. namely gained essence filtrate reduced in volume is obtained sealwort extracting solution;
(3) sealwort wine is prepared
A. sealwort extracting solution, sticky rice wine juice, white wine, Folium Bambosae flavone are placed in and stir Agitation Tank, be slowly heated to 50 DEG C, stir 10min, be then cooled to normal temperature rapidly;
B. use health promoting wine metre filter again, obtain sealwort wine.
Health promoting wine filter-specific membrane pore size is 0.18um.
White wine adopts the common distilling liquor brewageed with high quality sorghum, wheat, glutinous rice, rice and millet.Also the distilling liquor of market public offering can be adopted.
Claims (10)
1. a Rhizoma Polygonati extract, is characterized in that extracting by the following method and obtaining:
A. sealwort is pulverized;
B. gained sealwort powder is placed in extractor, adds the acid solution of sealwort grain weight amount 4-8 concentration 0.3-0.8% doubly, soak 1 hour, be then heated to 60-80 DEG C, heating 1-3 hour, filters, and collects extracting solution;
C. the granulated slag after filtration is added the water of 2-6 times of weight again, be heated to 55 DEG C, adjust ph value to be 5.0, then add the prozyme of granulated slag water weight 0.5-1.5%, enzymolysis 2 hours, filter, collect enzymolysis solution;
D. above-mentioned gained extracting solution and enzymolysis solution are merged, adjust ph value to be neutrality, be heated to 70 DEG C, then add 0.2-0.6% finings and clarify 1 hour, then essence filters to obtain smart filtrate;
E. by gained essence filtrate reduced in volume;
F. by gained concentrated solution spraying dry, Rhizoma Polygonati extract is obtained.
2. Rhizoma Polygonati extract according to claim 1, it is characterized in that: b step, described acid is citric acid.
3. Rhizoma Polygonati extract according to claim 1, it is characterized in that: b step, Heating temperature is 60 DEG C, and heat-up time is 2 hours.
4. Rhizoma Polygonati extract according to claim 1, it is characterized in that: step c, amount of water is 5 times, and enzyme add-on is 1%.
5. a sealwort wine, is characterized in that being made up of the raw material of following weight part: sealwort extracting solution 3-8, sticky rice wine juice 40-80, white wine 10-20, Folium Bambosae flavone 3-5.
6. sealwort wine according to claim 5, is characterized in that being made up of the raw material of following weight part: sealwort extracting solution 6, sticky rice wine juice 74, white wine 20, Folium Bambosae flavone 3.
7. sealwort wine according to claim 5, is characterized in that: the proportion of described sealwort extracting solution is 1.2-1.3.
8. sealwort wine according to claim 5, is characterized in that: the alcoholic strength of described white wine is 40%vol.
9. prepare a method for sealwort wine described in claim 5, it is characterized in that comprising the steps:
(1) sticky rice wine juice is prepared
A. quality glutinous rice is cleaned up, add the water of 3-5 times of weight, soak 8-10 hour, then drain;
B. the glutinous rice after draining the water is carried out boiling, cook rear cooling;
C. add the distiller's yeast of glutinous rice weight 1-3% after cooking and the dry yeast of 0.02-0.06%, stir;
D. primary fermentation, by the fermenting raw materials stirred, temperature controls as 20-30 DEG C, and the time is 30-50 hour;
E. secondary fermentation, adds 1-3 times amount pure water again and continues fermentation by fermentation material, temperature controls as 18-25 DEG C, and the time is 80-120 hour;
F. the fermentation material squeezing machine through secondary fermentation is squeezed, then filter with filter and obtain sticky rice wine juice;
(2) sealwort extracting solution is prepared
A. sealwort is pulverized;
B. gained sealwort powder is placed in extractor, adds the acid solution of sealwort grain weight amount 4-8 concentration 0.3-0.8% doubly, soak 1 hour, be then heated to 60-80 DEG C, heating 1-3 hour, filters, and collects extracting solution;
C. the granulated slag after filtration is added the water of 2-6 times of weight again, be heated to 55 DEG C, adjust ph value to be 5.0, then add the prozyme of granulated slag water weight 0.5-1.5%, enzymolysis 2 hours, filter, collect enzymolysis solution;
D. above-mentioned gained extracting solution and enzymolysis solution are merged, adjust ph value to be neutrality, be heated to 70 DEG C, then add 0.2-0.6% finings and clarify 1 hour, then essence filters to obtain smart filtrate;
E. namely gained essence filtrate reduced in volume is obtained sealwort extracting solution;
(2) sealwort wine is prepared
A. sealwort extracting solution, sticky rice wine juice, white wine, Folium Bambosae flavone are placed in and stir Agitation Tank, be slowly heated to 35-50 DEG C, stir 10-30min, be then cooled to normal temperature rapidly;
B. use health promoting wine metre filter again, obtain sealwort wine.
10. method according to claim 9, is characterized in that: described health promoting wine filter-specific membrane pore size is 0.18um.
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| CN106754116A (en) * | 2016-11-23 | 2017-05-31 | 青海七彩花生物科技有限公司 | A kind of northern Chinese caterpillar Fungus health liquor |
| CN106754102A (en) * | 2017-03-31 | 2017-05-31 | 贵州古耕农牧业发展有限公司 | A kind of sealwort wine and preparation method thereof |
| CN107136508A (en) * | 2017-07-05 | 2017-09-08 | 广州市天河华南发展有限公司 | A kind of composition for improving human nutrition balance and its preparation method and application |
| CN107232544A (en) * | 2017-07-05 | 2017-10-10 | 广州市天河华南发展有限公司 | A kind of composition of nourishing-yin, lowering blood-sugar and its preparation method and application |
| CN108065371A (en) * | 2018-01-05 | 2018-05-25 | 浙江新篁生物技术有限公司 | A kind of drinks electuary and its manufacturing method |
| CN108112985A (en) * | 2017-11-08 | 2018-06-05 | 湖南省中医药研究院 | A kind of method for medical and edible dual purpose plant calcium oxalate crystal growth in healthy needle of degrading |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106367263A (en) * | 2016-08-31 | 2017-02-01 | 沈飞 | Rhizoma polygonati mixed wine and brewing method thereof |
| CN106754116A (en) * | 2016-11-23 | 2017-05-31 | 青海七彩花生物科技有限公司 | A kind of northern Chinese caterpillar Fungus health liquor |
| CN106754102A (en) * | 2017-03-31 | 2017-05-31 | 贵州古耕农牧业发展有限公司 | A kind of sealwort wine and preparation method thereof |
| CN107136508A (en) * | 2017-07-05 | 2017-09-08 | 广州市天河华南发展有限公司 | A kind of composition for improving human nutrition balance and its preparation method and application |
| CN107232544A (en) * | 2017-07-05 | 2017-10-10 | 广州市天河华南发展有限公司 | A kind of composition of nourishing-yin, lowering blood-sugar and its preparation method and application |
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| CN108065371A (en) * | 2018-01-05 | 2018-05-25 | 浙江新篁生物技术有限公司 | A kind of drinks electuary and its manufacturing method |
| CN108841536A (en) * | 2018-08-09 | 2018-11-20 | 重庆市银蜂四云创圆农业开发有限公司 | A kind of sealwort wine preparation process containing Rhizoma Polygonati extract |
| CN113136280A (en) * | 2021-04-26 | 2021-07-20 | 宜宾学院 | Natural bamboo rice wine beverage and preparation method thereof |
| CN114480059A (en) * | 2022-01-10 | 2022-05-13 | 湖南省大观溪生物科技有限公司 | Polygonatum sibiricum health wine and production device thereof |
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