CN105481295A - Stone curing agent and preparation method thereof - Google Patents
Stone curing agent and preparation method thereof Download PDFInfo
- Publication number
- CN105481295A CN105481295A CN201610003699.6A CN201610003699A CN105481295A CN 105481295 A CN105481295 A CN 105481295A CN 201610003699 A CN201610003699 A CN 201610003699A CN 105481295 A CN105481295 A CN 105481295A
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- CN
- China
- Prior art keywords
- parts
- solidifying agent
- stone material
- linker
- solvent
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/10—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C04B26/14—Polyepoxides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J163/00—Adhesives based on epoxy resins; Adhesives based on derivatives of epoxy resins
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Epoxy Resins (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a stone curing agent and a preparation method thereof. The stone curing agent is prepared from, by weight, 5-8 parts of triethylene tetramine, 10-22 parts of bisphenol-A-type epoxy resin, 10-15 parts of diethylenetriamine, 3-5 parts of a NO.3 waterproof agent, 5-8 parts of a mixed crosslinking agent and 25-40 parts of solvent, wherein the mixed crosslinking agent is prepared by mixing a 7672 type crosslinking agent with a 7028 type crosslinking agent according to the ratio of 1:2.3. According to the stone curing agent and the preparation method thereof, the stone curing agent is prepared by mixing the two different crosslinking agents, and therefore the curing efficiency of the stone curing agent is improved and is 3-5 times of that of a traditional curing agent.
Description
Technical field
The present invention relates to a kind of solidifying agent and preparation method thereof, in particular a kind of stone material solidifying agent and preparation method thereof.
Background technology
In stone material production field, because the rate of decay of mine each several part is different, exploiting the woollen obtained is grain pattern, and this woollen is difficult to cut into bulk, is difficult to transport, and it is large that post-production makes stone material finished product difficulty.Traditional method utilizes solidifying agent to make this loose woollen be bonded into stone, but solidifying agent curing efficiency of the prior art is low, and the stone material of a cube needs just can complete solidification in more than 5 hours, greatly reduces production and transport efficiency.
Summary of the invention
The object of the present invention is to provide a kind of stone material solidifying agent and preparation method thereof, be intended to solve the too low technical problem of traditional solidifying agent curing efficiency.
Technical scheme of the present invention is as follows: a kind of stone material solidifying agent, and wherein, its composition of raw materials is made up of each component of following parts by weight:
Triethylene tetramine 5 ~ 8 parts;
Bisphenol A type epoxy resin 10 ~ 22 parts;
Diethylenetriamine 10 ~ 15 parts;
Water-resisting agent No. 33 ~ 5 parts;
Mixed cross-linker 5 ~ 8 parts;
Solvent 25 ~ 40 parts;
Described mixed cross-linker is that 7672 type linking agents and 7028 type linking agents mix according to ratio 1:2.3.
Preferably, described solvent is No. 120 solvent oils.
Preferably, stone material solidifying agent composition of raw materials is made up of each component of following parts by weight:
Triethylene tetramine 5 parts;
Bisphenol A type epoxy resin 18 parts;
Diethylenetriamine 12 parts;
Water-resisting agent No. 33 parts;
Mixed cross-linker 6 parts;
Solvent 28 parts.
Preferably, stone material solidifying agent composition of raw materials is made up of each component of following parts by weight:
Triethylene tetramine 8 parts;
Bisphenol A type epoxy resin 22 parts;
Diethylenetriamine 15 parts;
Water-resisting agent No. 35 parts;
Mixed cross-linker 8 parts;
Solvent 40 parts.
The invention also discloses the preparation method of stone material solidifying agent, it is characterized in that, comprise the following steps:
A1, by 7672 type linking agents and 7028 type linking agents according to ratio 1:2.3 mixing and stirring, obtain mixed cross-linker;
A2, by triethylene tetramine, bisphenol A type epoxy resin, diethylenetriamine and the solvent parts by weight mix and blend according to setting, stir simultaneously and pour mixed cross-linker into;
A3, add No. 3, water-resisting agent, continue stirring and obtain stone material solidifying agent in 30 minutes.
Beneficial effect of the present invention: the invention discloses a kind of stone material solidifying agent and preparation method thereof, two kinds of different linking agents are utilized to be mixed with, improve the curing efficiency of stone material solidifying agent, the curing efficiency of stone material solidifying agent of the present invention is 3 ~ 5 times of traditional solidifying agent.
Embodiment
For making object of the present invention, technical scheme and advantage clearly, clearly, the present invention is described in more detail below to enumerate embodiment.
Embodiment 1
The stone material solidifying agent composition of raw materials of the present embodiment is made up of each component of following parts by weight:
Triethylene tetramine 5 parts;
Bisphenol A type epoxy resin 18 parts;
Diethylenetriamine 12 parts;
Water-resisting agent No. 33 parts;
Mixed cross-linker 6 parts;
Solvent 28 parts.
Wherein, mixed cross-linker is mixed according to ratio 1:2.3 by 7672 type linking agents and 7028 type linking agents.Concrete, 7672 type linking agents and 7028 type linking agents all adopt 7672 type linking agents and the 7028 type linking agents of DOW CORNING plate.By adopting two kinds of linking agents to be mixed with solidifying agent, facilitate the reaction of each composition (especially resin) in solidifying agent greatly, thus improve curing efficiency.The curing efficiency of the solidifying agent of the present embodiment is 3 times of common solidifying agent, and solidifying one cube of stone material only needed less than 2 hours.
The preparation process of the solidifying agent of the present embodiment is as follows:
A1, by 7672 type linking agents and 7028 type linking agents according to ratio 1:2.3 mixing and stirring, obtain mixed cross-linker;
A2, by triethylene tetramine, bisphenol A type epoxy resin, diethylenetriamine and the solvent parts by weight mix and blend according to setting, stir simultaneously and pour mixed cross-linker into;
A3, add No. 3, water-resisting agent, continue stirring and obtain stone material solidifying agent in 30 minutes.
Embodiment 2
The present embodiment is basic identical with embodiment 1, unlike, the stone material solidifying agent composition of raw materials of the present embodiment is made up of each component of following parts by weight:
Triethylene tetramine 8 parts;
Bisphenol A type epoxy resin 22 parts;
Diethylenetriamine 15 parts;
Water-resisting agent No. 35 parts;
Mixed cross-linker 8 parts;
Solvent 40 parts.
Wherein, mixed cross-linker is mixed according to ratio 1:2.3 by 7672 type linking agents and 7028 type linking agents.
Wherein, solvent is No. 120 solvent oils.
The curing efficiency of the solidifying agent of the present embodiment is 5 times of Common curing agents, and solidifying one cube of stone material only needs 1 hour.
Should be understood that, application of the present invention is not limited to above-mentioned citing, for those of ordinary skills, can be improved according to the above description or convert, and all these improve and convert the protection domain that all should belong to claims of the present invention.
Claims (5)
1. a stone material solidifying agent, is characterized in that, its composition of raw materials is made up of each component of following parts by weight:
Triethylene tetramine 5 ~ 8 parts;
Bisphenol A type epoxy resin 10 ~ 22 parts;
Diethylenetriamine 10 ~ 15 parts;
Water-resisting agent No. 33 ~ 5 parts;
Mixed cross-linker 5 ~ 8 parts;
Solvent 25 ~ 40 parts;
Described mixed cross-linker is that 7672 type linking agents and 7028 type linking agents mix according to ratio 1:2.3.
2. stone material solidifying agent according to claim 1, is characterized in that, described solvent is No. 120 solvent oils.
3. stone material solidifying agent according to claim 1 and 2, is characterized in that, its composition of raw materials is made up of each component of following parts by weight:
Triethylene tetramine 5 parts;
Bisphenol A type epoxy resin 18 parts;
Diethylenetriamine 12 parts;
Water-resisting agent No. 33 parts;
Mixed cross-linker 6 parts;
Solvent 28 parts.
4. stone material solidifying agent according to claim 1 and 2, is characterized in that, its composition of raw materials is made up of each component of following parts by weight:
Triethylene tetramine 8 parts;
Bisphenol A type epoxy resin 22 parts;
Diethylenetriamine 15 parts;
Water-resisting agent No. 35 parts;
Mixed cross-linker 8 parts;
Solvent 40 parts.
5. a preparation method for the stone material solidifying agent as described in claim 1 ~ 4 any one, is characterized in that, comprise the following steps:
A1, by 7672 type linking agents and 7028 type linking agents according to ratio 1:2.3 mixing and stirring, obtain mixed cross-linker;
A2, by triethylene tetramine, bisphenol A type epoxy resin, diethylenetriamine and the solvent parts by weight mix and blend according to setting, stir simultaneously and pour mixed cross-linker into;
A3, add No. 3, water-resisting agent, continue stirring and obtain stone material solidifying agent in 30 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610003699.6A CN105481295A (en) | 2016-01-07 | 2016-01-07 | Stone curing agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610003699.6A CN105481295A (en) | 2016-01-07 | 2016-01-07 | Stone curing agent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105481295A true CN105481295A (en) | 2016-04-13 |
Family
ID=55668624
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610003699.6A Pending CN105481295A (en) | 2016-01-07 | 2016-01-07 | Stone curing agent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105481295A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106630756A (en) * | 2016-12-19 | 2017-05-10 | 钦州市科学技术开发中心 | Stone curing agent and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09316303A (en) * | 1996-05-29 | 1997-12-09 | Mitsubishi Rayon Co Ltd | Epoxy resin composition and its preparation |
| CN102690080A (en) * | 2012-06-06 | 2012-09-26 | 湖南柯盛新材料有限公司 | Rough stone block reinforcement adhesive and using method thereof |
| CN102898070A (en) * | 2011-11-03 | 2013-01-30 | 苏州拓博琳新材料科技有限公司 | Bio-based artificial quartz stone and production process thereof |
| CN104557135A (en) * | 2015-01-08 | 2015-04-29 | 黄文辉 | Rough stone block hardening agent and hardening method thereof |
| CN104557134A (en) * | 2015-01-08 | 2015-04-29 | 黄文辉 | Reinforced curing agent for natural stones |
-
2016
- 2016-01-07 CN CN201610003699.6A patent/CN105481295A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09316303A (en) * | 1996-05-29 | 1997-12-09 | Mitsubishi Rayon Co Ltd | Epoxy resin composition and its preparation |
| CN102898070A (en) * | 2011-11-03 | 2013-01-30 | 苏州拓博琳新材料科技有限公司 | Bio-based artificial quartz stone and production process thereof |
| CN102690080A (en) * | 2012-06-06 | 2012-09-26 | 湖南柯盛新材料有限公司 | Rough stone block reinforcement adhesive and using method thereof |
| CN104557135A (en) * | 2015-01-08 | 2015-04-29 | 黄文辉 | Rough stone block hardening agent and hardening method thereof |
| CN104557134A (en) * | 2015-01-08 | 2015-04-29 | 黄文辉 | Reinforced curing agent for natural stones |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106630756A (en) * | 2016-12-19 | 2017-05-10 | 钦州市科学技术开发中心 | Stone curing agent and preparation method thereof |
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20160413 |
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| WD01 | Invention patent application deemed withdrawn after publication |