CN106630756A - Stone curing agent and preparation method thereof - Google Patents
Stone curing agent and preparation method thereof Download PDFInfo
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- CN106630756A CN106630756A CN201611173451.0A CN201611173451A CN106630756A CN 106630756 A CN106630756 A CN 106630756A CN 201611173451 A CN201611173451 A CN 201611173451A CN 106630756 A CN106630756 A CN 106630756A
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- curing agent
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- stone material
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/10—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C04B26/18—Polyesters; Polycarbonates
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a stone curing agent and a preparation method thereof. The stone curing agent is prepared from the following formula components in parts by mass: 1 to 3 parts of a light-stabilization multifunctional adjuvant, 2 to 4 parts of a mixed crosslinking agent, 5 to 15 parts of polyester hot melt adhesive, 10 to 12 parts of paraffin, 6 to 8 parts of conductive carbon black, 4 to 6 parts of polyvinyl butyral, 5 to 7 parts of triethylene tetramine, 2 to 4 parts of solvent oil, 5 to 7 parts of basalt fiber, 10 to 20 parts of bisphenol-A epoxy resin, 4 to 6 parts of tetraethoxysilane and 1 to 2 parts of a waterproofing agent. The stone curing agent is prepared by mixing two different crosslinking agents, so that the curing efficiency of the stone curing agent is improved. The curing efficiency of the stone curing agent disclosed by the invention is 3 to 5 times that of the conventional curing agent.
Description
Technical field
The present invention relates to curing agent field, in particular to a kind of stone material curing agent and preparation method thereof.
Background technology
In stone material production field, because the rate of decay of mine each several part is different, it is particle knot to exploit the woollen for obtaining
Structure, this woollen is difficult to cut into bulk, it is difficult to transport, and it is big that post-production makes stone material finished product difficulty.Traditional method is profit
This loose woollen is set to be bonded into stone with curing agent, but curing agent curing efficiency of the prior art is low, one cube
Stone material needs just complete within more than 5 hours solidification, greatly reduces production and transport efficiency.
The content of the invention
The invention provides a kind of stone material curing agent and preparation method thereof, the present invention is using two kinds of different crosslinking agent mixing
Prepare, improve the curing efficiency of stone material curing agent, the curing efficiency of the stone material curing agent of the present invention is the 3 of traditional curing agent
～5 times.
For achieving the above object, the present invention provides following technical scheme：
A kind of stone material curing agent and preparation method thereof, is made up of following mass fraction formula components：The stable multifunctional assistant of light
Agent 1-3 parts, mixed cross-linker 2-4 parts, polyester hot-melt adhesive 5-15 parts, paraffin 10-12 parts, conductive black 6-8 parts, polyvinyl alcohol contracting
Butyraldehyde 4-6 parts, triethylene tetramine 5-7 parts, solvent naphtha 2-4 parts, basalt fibre 5-7 parts, bisphenol A type epoxy resin 10-20 parts,
Tetraethyl orthosilicate 4-6 parts, waterproofing agent 1-2 parts.
Further：It is made up of following mass fraction formula components：Stable 1 part of the multifunctional assistant of light, 2 parts of mixed cross-linker,
5 parts of polyester hot-melt adhesive, 10 parts of paraffin, 6 parts of conductive black, 4 parts of polyvinyl butyral resin, 5 parts of triethylene tetramine, 2 parts of solvent naphtha,
5 parts of basalt fibre, 10 parts of bisphenol A type epoxy resin, 4 parts of tetraethyl orthosilicate, 1 part of waterproofing agent.
Further：It is made up of following mass fraction formula components：Stable 2 parts of the multifunctional assistant of light, 3 parts of mixed cross-linker,
10 parts of polyester hot-melt adhesive, 11 parts of paraffin, 7 parts of conductive black, 5 parts of polyvinyl butyral resin, 6 parts of triethylene tetramine, solvent naphtha 3
Part, 6 parts of basalt fibre, 15 parts of bisphenol A type epoxy resin, 5 parts of tetraethyl orthosilicate, 1.5 parts of waterproofing agent.
Further：It is made up of following mass fraction formula components：Stable 3 parts of the multifunctional assistant of light, 4 parts of mixed cross-linker,
15 parts of polyester hot-melt adhesive, 12 parts of paraffin, 8 parts of conductive black, 6 parts of polyvinyl butyral resin, 7 parts of triethylene tetramine, solvent naphtha 4
Part, 7 parts of basalt fibre, 20 parts of bisphenol A type epoxy resin, 6 parts of tetraethyl orthosilicate, 2 parts of waterproofing agent.
Further：Preparation method of the present invention has following steps：
Step one, by above-mentioned mixed cross-linker and polyester hot-melt adhesive according to ratio 1:2.3 mixing and stirrings, are mixed
Crosslinking agent；
Step 2, by paraffin, conductive black, polyvinyl butyral resin, triethylene tetramine, solvent naphtha, basalt fibre, double
Phenol A type epoxy resin, tetraethyl orthosilicate are mixed, while stirring while pouring step one gained mixed cross-linker into；
Step 3, step 2 gained plus the stable multifunctional assistant of light and waterproofing agent will be entered, and continue to stir and obtain stone in 30 minutes
Material curing agent.
The invention has the beneficial effects as follows：The present invention is mixed with using two kinds of different crosslinking agents, improves stone material solidification
The curing efficiency of agent, the curing efficiency of the stone material curing agent of the present invention is 3～5 times of traditional curing agent.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the invention, rather than the embodiment of whole.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all
Belong to the scope of protection of the invention.
Embodiment one：
A kind of stone material curing agent is made up of following mass fraction formula components：The stable multifunctional assistant 1-3 parts of light, mixing are handed over
Connection agent 2-4 parts, polyester hot-melt adhesive 5-15 parts, paraffin 10-12 parts, conductive black 6-8 parts, polyvinyl butyral resin 4-6 parts, three second
Alkene tetramine 5-7 parts, solvent naphtha 2-4 parts, basalt fibre 5-7 parts, bisphenol A type epoxy resin 10-20 parts, tetraethyl orthosilicate 4-6
Part, waterproofing agent 1-2 parts.
Embodiment two：
A kind of stone material curing agent is made up of following mass fraction formula components：Stable 1 part of the multifunctional assistant of light, mixing crosslinking
2 parts of agent, 5 parts of polyester hot-melt adhesive, 10 parts of paraffin, 6 parts of conductive black, 4 parts of polyvinyl butyral resin, 5 parts of triethylene tetramine, solvent
2 parts of oil, 5 parts of basalt fibre, 10 parts of bisphenol A type epoxy resin, 4 parts of tetraethyl orthosilicate, 1 part of waterproofing agent.
Embodiment three：
A kind of stone material curing agent is made up of following mass fraction formula components：Stable 2 parts of the multifunctional assistant of light, mixing crosslinking
It is 3 parts of agent, 10 parts of polyester hot-melt adhesive, 11 parts of paraffin, 7 parts of conductive black, 5 parts of polyvinyl butyral resin, 6 parts of triethylene tetramine, molten
3 parts of agent oil, 6 parts of basalt fibre, 15 parts of bisphenol A type epoxy resin, 5 parts of tetraethyl orthosilicate, 1.5 parts of waterproofing agent.
Example IV：
A kind of stone material curing agent is made up of following mass fraction formula components：Stable 3 parts of the multifunctional assistant of light, mixing crosslinking
It is 4 parts of agent, 15 parts of polyester hot-melt adhesive, 12 parts of paraffin, 8 parts of conductive black, 6 parts of polyvinyl butyral resin, 7 parts of triethylene tetramine, molten
4 parts of agent oil, 7 parts of basalt fibre, 20 parts of bisphenol A type epoxy resin, 6 parts of tetraethyl orthosilicate, 2 parts of waterproofing agent.
Embodiment five：
A kind of preparation method preparation method of stone material curing agent comprises the steps：
Step one, by above-mentioned mixed cross-linker and polyester hot-melt adhesive according to ratio 1:2.3 mixing and stirrings, are mixed
Crosslinking agent；
Step 2, by paraffin, conductive black, polyvinyl butyral resin, triethylene tetramine, solvent naphtha, basalt fibre, double
Phenol A type epoxy resin, tetraethyl orthosilicate are mixed, while stirring while pouring step one gained mixed cross-linker into；
Step 3, step 2 gained plus the stable multifunctional assistant of light and waterproofing agent will be entered, and continue to stir and obtain stone in 30 minutes
Material curing agent.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that for clarity those skilled in the art should
Using specification as an entirety, the technical scheme in each embodiment can also Jing it is appropriately combined, form those skilled in the art
Understandable other embodiment.
Claims (5)
1. a kind of stone material curing agent, it is characterised in that：It is made up of following mass fraction formula components：
The stable multifunctional assistant 1-3 parts of light, mixed cross-linker 2-4 parts, polyester hot-melt adhesive 5-15 parts, paraffin 10-12 parts, conductive charcoal
Black 6-8 parts, polyvinyl butyral resin 4-6 parts, triethylene tetramine 5-7 parts, solvent naphtha 2-4 parts, basalt fibre 5-7 parts, bisphenol-A
Type epoxy resin 10-20 parts, tetraethyl orthosilicate 4-6 parts, waterproofing agent 1-2 parts.
2. a kind of stone material curing agent according to claim 1, it is characterised in that：By following mass fraction formula components group
Into：
Light stable 1 part of multifunctional assistant, 2 parts of mixed cross-linker, 5 parts of polyester hot-melt adhesive, 10 parts of paraffin, 6 parts of conductive black, poly- second
4 parts of enol butyral, 5 parts of triethylene tetramine, 2 parts of solvent naphtha, 5 parts of basalt fibre, 10 parts of bisphenol A type epoxy resin, positive silicon
4 parts of acetoacetic ester, 1 part of waterproofing agent.
3. a kind of stone material curing agent according to claim 1, it is characterised in that：By following mass fraction formula components group
Into：
It is stable 2 parts of the multifunctional assistant of light, 3 parts of mixed cross-linker, 10 parts of polyester hot-melt adhesive, 11 parts of paraffin, 7 parts of conductive black, poly-
5 parts of vinyl butyral, 6 parts of triethylene tetramine, 3 parts of solvent naphtha, 6 parts of basalt fibre, 15 parts of bisphenol A type epoxy resin, just
5 parts of silester, 1.5 parts of waterproofing agent.
4. a kind of stone material curing agent according to claim 1, it is characterised in that：By following mass fraction formula components group
Into：
It is stable 3 parts of the multifunctional assistant of light, 4 parts of mixed cross-linker, 15 parts of polyester hot-melt adhesive, 12 parts of paraffin, 8 parts of conductive black, poly-
6 parts of vinyl butyral, 7 parts of triethylene tetramine, 4 parts of solvent naphtha, 7 parts of basalt fibre, 20 parts of bisphenol A type epoxy resin, just
6 parts of silester, 2 parts of waterproofing agent.
5. a kind of a kind of preparation method of stone material curing agent according to claim 1, it is characterised in that：Including following step
Suddenly：
Step one, by above-mentioned mixed cross-linker and polyester hot-melt adhesive according to ratio 1:2.3 mixing and stirrings, obtain mixing crosslinking
Agent；
Step 2, by paraffin, conductive black, polyvinyl butyral resin, triethylene tetramine, solvent naphtha, basalt fibre, bisphenol-A
Type epoxy resin, tetraethyl orthosilicate are mixed, while stirring while pouring step one gained mixed cross-linker into；
Step 3, step 2 gained plus the stable multifunctional assistant of light and waterproofing agent will be entered, and continue to stir and obtain within 30 minutes stone material and consolidate
Agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611173451.0A CN106630756A (en) | 2016-12-19 | 2016-12-19 | Stone curing agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611173451.0A CN106630756A (en) | 2016-12-19 | 2016-12-19 | Stone curing agent and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN106630756A true CN106630756A (en) | 2017-05-10 |
Family
ID=58823176
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611173451.0A Pending CN106630756A (en) | 2016-12-19 | 2016-12-19 | Stone curing agent and preparation method thereof |
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| CN (1) | CN106630756A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107721290A (en) * | 2017-11-27 | 2018-02-23 | 倪修俊 | Compound thermal insulation mortar of the wheat stalk granular polystyrene of a kind of waterproof fireproofing and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104479108A (en) * | 2014-11-27 | 2015-04-01 | 东莞暨南大学研究院 | Epoxy resin curing agent applied to marble stones and preparation method thereof |
| CN104557134A (en) * | 2015-01-08 | 2015-04-29 | 黄文辉 | Reinforced curing agent for natural stones |
| CN104557135A (en) * | 2015-01-08 | 2015-04-29 | 黄文辉 | Rough stone block hardening agent and hardening method thereof |
| CN105482755A (en) * | 2015-12-31 | 2016-04-13 | 林初煌 | Antistatic modified hot melt adhesive and preparation method thereof |
| CN105481295A (en) * | 2016-01-07 | 2016-04-13 | 黄利文 | Stone curing agent and preparation method thereof |
-
2016
- 2016-12-19 CN CN201611173451.0A patent/CN106630756A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104479108A (en) * | 2014-11-27 | 2015-04-01 | 东莞暨南大学研究院 | Epoxy resin curing agent applied to marble stones and preparation method thereof |
| CN104557134A (en) * | 2015-01-08 | 2015-04-29 | 黄文辉 | Reinforced curing agent for natural stones |
| CN104557135A (en) * | 2015-01-08 | 2015-04-29 | 黄文辉 | Rough stone block hardening agent and hardening method thereof |
| CN105482755A (en) * | 2015-12-31 | 2016-04-13 | 林初煌 | Antistatic modified hot melt adhesive and preparation method thereof |
| CN105481295A (en) * | 2016-01-07 | 2016-04-13 | 黄利文 | Stone curing agent and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 竹涛等: "《物理性污染控制》", 30 April 2014 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107721290A (en) * | 2017-11-27 | 2018-02-23 | 倪修俊 | Compound thermal insulation mortar of the wheat stalk granular polystyrene of a kind of waterproof fireproofing and preparation method thereof |
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