CN105477285A - Preparation method of mouthwash for treating yin deficiency type toothache - Google Patents
Preparation method of mouthwash for treating yin deficiency type toothache Download PDFInfo
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- CN105477285A CN105477285A CN201510918201.4A CN201510918201A CN105477285A CN 105477285 A CN105477285 A CN 105477285A CN 201510918201 A CN201510918201 A CN 201510918201A CN 105477285 A CN105477285 A CN 105477285A
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
- A61K36/815—Lycium (desert-thorn)
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/288—Taraxacum (dandelion)
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/756—Phellodendron, e.g. corktree
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/758—Zanthoxylum, e.g. pricklyash
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/80—Scrophulariaceae (Figwort family)
- A61K36/804—Rehmannia
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/80—Scrophulariaceae (Figwort family)
- A61K36/808—Scrophularia (figwort)
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/86—Violaceae (Violet family)
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8964—Anemarrhena
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- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0053—Mouth and digestive tract, i.e. intraoral and peroral administration
- A61K9/0063—Periodont
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- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
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Abstract
The invention discloses a preparation method of a mouthwash for treating yin deficiency type toothache, comprising following steps: step 1, extracting, drying and pulverizing a traditional Chinese medicine composition to obtain a material powder, wherein the traditional Chinese medicine composition comprises materials of following parts by weight: 12-18 parts of Cortex Lycii, 8-12 part of Cortex Moutan, 4-6 part of salt-fried Cortex Phellodendri, 5-8 parts of Rhizoma Anemarrhenae, 8-12 parts of Radix Rehmanniae, 8-12 parts of Radix Scrophulariae, 10-15 parts of Herba Taraxaci, 8-12 parts of Herba Violae, 8-12 parts of Herba Ecliptae, 8-12 parts of Radix Arnebiae seu lithospermi, 8-15 parts of Herba Menthae, 8-12 parts of Radix Zanthoxyli and 8-12 parts of Flos Eriocauli; step 2, subjecting the material powder and 60-70 % ethanol solution 10-30 times of the power by volume to mixing and extracting, and heating after extracting to evaporate ethanol to obtain an extract; step 3, adding distilled water to dilute the extract by 10-15 times to obtain this mouthwash.
Description
Technical field
The present invention relates to tcm field, particularly relate to a kind of preparation method for the treatment of the collutory of cloudy alveolar neuralgia.
Background technology
Doctor trained in Western medicine is thought toothache causes dental pulp by gingivitis and periodontitis, dental caries, decayed tooth or Fractured teeth mostly, namely caused by dental nerve infection.Be owing to not noting oral hygiene, tooth is subject to the long-time stimulus caused by tartar of soft tartar that the things such as around teeth food debris, antibacterial form and hard, and incorrect tooth-brushing habit, and the reasons such as vitamin deficiency caused.Use antibiotics anti-inflammation drugs to toothache is general, side effect is large, and often can not effect a radical cure.
Traditional Chinese Medicine thinks that toothache mainly comprises following a few class: 1, excess-fire toothache, and the cause of disease mostly is in wind heat invasion and attack or stomach-fire steams, and injure tooth body or gingiva, evil gathering does not fall apart, and QI and blood is detained, and general pain is fiercer, and dare not eat hot thing, red swelling of gingiva is more violent.2, toothache caused by fire of deficiency type, generally not too obvious, always have a dull ache, and the time continued is long, red swelling of gingiva is not too obvious, and arteries and veins is carefully fast than usual.3, toothache due to pathogenic wind-heat, dental pain, in paroxysmal, meet wind outbreak, affected part obtains cold then alleviation of pain, and then pain of being heated increases, red swelling of gingiva, whole body or have heating, aversion to cold, thirsty, red tongue, tongue white spirit, floating and rapid pulse.4, toothache due to stomach-fire, dental pain is violent, and more very, or the oozing of blood that comes to a head, swollenly connects the cheek to red swelling of gingiva, and headache, thirst and drinking, implication is smelly dirty, constipation, and yellow fur is thick.
But, lack the Chinese medicine composition to cloudy alveolar neuralgia at present, also there is no the pure Chinese medicine ingredients collutory effectively can treating cloudy alveolar neuralgia.
Summary of the invention
An object of the present invention is to solve at least the problems referred to above and/or defect, and the advantage will illustrated at least is below provided.
Another object of the present invention is to provide a kind of preparation method for the treatment of the collutory of cloudy alveolar neuralgia, can be effectively treated cloudy alveolar neuralgia collutory.
Other objects with some for achieving the above object, the present invention adopts following technical scheme
Treat a preparation method for the collutory of cloudy alveolar neuralgia, comprise the following steps:
Step 1, lixiviate, by Chinese medicine composition drying and crushing, obtain raw material powder, described Chinese medicine composition comprises the raw material of following weight portion: Cortex Lycii 12-18, Cortex Moutan 8-12, Cortex Phellodendri Amurensis (parched with salt) 4-6, Rhizoma Anemarrhenae 5-8, Radix Rehmanniae 8-12, Radix Scrophulariae 8-12, Herba Taraxaci 10-15, Herba Violae 8-12, Herba Ecliptae 8-12, Radix Arnebiae (Radix Lithospermi) 8-12, Herba Menthae 8-15, Radix Zanthoxyli 8-12 and Flos Eriocauli 8-12;
Step 2, by the 60-70% alcoholic solution mixing lixiviate of raw material powder with 10-30 times of volume, lixiviate terminates post-heating makes ethanol evaporation, obtains extract;
Step 3, by extract adding distil water dilution 10-15 doubly, obtain the cloudy alveolar neuralgia of described treatment collutory.
Preferably, in the preparation method of the collutory of the cloudy alveolar neuralgia of described treatment, in step 3 to the cloudy alveolar neuralgia for the treatment of collutory in add 0.05% sodium fluoride.
Preferably, in the preparation method of the collutory of the cloudy alveolar neuralgia of described treatment, in step 2, leach extraction method is substep extraction, and concrete grammar is:
Step 2.1, first time lixiviate, extraction temperature is 30-50 DEG C, extraction time 30-40 minute, filters and obtains the first lixiviating solution;
Step 2.2, second time lixiviate, mixed with ethanol by the trapped substance of first time lixiviate filtration and carry out second time lixiviate, extraction temperature is 60-80 DEG C, extraction time 20-30 minute, filters and obtains the second lixiviating solution;
Step 2.3, the first lixiviating solution to be mixed with the second lixiviating solution, be heated to 80-85 DEG C and make ethanol evaporation, obtain described extract.
The present invention at least comprises following beneficial effect: first, and the present invention utilizes the traditional Chinese medical science five elements and dialectical theory, and think that the cause of disease of cloudy alveolar neuralgia is: kidney governing bones, tooth being the surplus of the bone, deficiency of the kidney yin, hyperactivity of deficient fire, ties in gums, have a dull ache, and especially afternoon pain is heavier.Controlling should nourishing YIN to lower pathogenic fire, reducing swelling and alleviating pain.Cortex Lycii, Gan Hanping mends, and vital essence is filled and pathogenic fire moves back certainly, the heat of dispelling in gas; Cortex Moutan, heat, antiinflammatory, detumescence, pain relieving in blood of dispelling; Cortex Phellodendri Amurensis (parched with salt), nourishing YIN to lower pathogenic fire, removing toxic substances; The Rhizoma Anemarrhenae, nourishing YIN to lower pathogenic fire; The Radix Rehmanniae, tonification kidney water kidney-YIN being deficient; Radix Scrophulariae, removing heat from blood YIN nourishing, eliminating fire and detoxication; Herba Taraxaci, Herba Violae, heat-clearing and toxic substances removing, detumescence, pain relieving, antiinflammatory; Herba Ecliptae, liver and kidney tonifying; Radix Arnebiae (Radix Lithospermi), clearing away heat and cooling blood, removing toxic substances and promoting subsidence of swelling; Fructus Lycii, enriching yin and nourishing kidney; Flos Eriocauli, dispelling wind and heat pathogens, pain relieving.
Secondly, by can effectively treat cloudy alveolar neuralgia Chinese medicine composition carry out substep alcohol steep, make the collutory not only taking convenience of the cloudy alveolar neuralgia of prepared treatment, and be conducive to the absorption of effective ingredient, effectively treat cloudy alveolar neuralgia.
Part is embodied by explanation below by other advantage of the present invention, target and feature, part also will by research and practice of the present invention by those skilled in the art is understood.
Detailed description of the invention
Below the present invention is elaborated, can implement according to this after consulting this description to make those of ordinary skill in the art.
Treat a preparation method for the collutory of cloudy alveolar neuralgia, comprise the following steps:
Step 1, lixiviate, by Chinese medicine composition drying and crushing, obtain raw material powder, described Chinese medicine composition comprises the raw material of following weight portion: Cortex Lycii 12-18, Cortex Moutan 8-12, Cortex Phellodendri Amurensis (parched with salt) 4-6, Rhizoma Anemarrhenae 5-8, Radix Rehmanniae 8-12, Radix Scrophulariae 8-12, Herba Taraxaci 10-15, Herba Violae 8-12, Herba Ecliptae 8-12, Radix Arnebiae (Radix Lithospermi) 8-12, Herba Menthae 8-15, Radix Zanthoxyli 8-12 and Flos Eriocauli 8-12;
Step 2, by the 60-70% alcoholic solution mixing lixiviate of raw material powder with 10-30 times of volume, lixiviate terminates post-heating makes ethanol evaporation, obtains extract;
Step 3, by extract adding distil water dilution 10-15 doubly, obtain the cloudy alveolar neuralgia of described treatment collutory.
The present invention utilizes the traditional Chinese medical science five elements and dialectical theory, and think that the cause of disease of cloudy alveolar neuralgia is: kidney governing bones, tooth being the surplus of the bone, deficiency of the kidney yin, hyperactivity of deficient fire, ties in gums, have a dull ache, and especially afternoon pain is heavier.Controlling should nourishing YIN to lower pathogenic fire, reducing swelling and alleviating pain.Cortex Lycii, Gan Hanping mends, and vital essence is filled and pathogenic fire moves back certainly, the heat of dispelling in gas; Cortex Moutan, heat, antiinflammatory, detumescence, pain relieving in blood of dispelling; Cortex Phellodendri Amurensis (parched with salt), nourishing YIN to lower pathogenic fire, removing toxic substances; The Rhizoma Anemarrhenae, nourishing YIN to lower pathogenic fire; The Radix Rehmanniae, tonification kidney water kidney-YIN being deficient; Radix Scrophulariae, removing heat from blood YIN nourishing, eliminating fire and detoxication; Herba Taraxaci, Herba Violae, heat-clearing and toxic substances removing, detumescence, pain relieving, antiinflammatory; Herba Ecliptae, liver and kidney tonifying; Radix Arnebiae (Radix Lithospermi), clearing away heat and cooling blood, removing toxic substances and promoting subsidence of swelling; Fructus Lycii, enriching yin and nourishing kidney; Flos Eriocauli, dispelling wind and heat pathogens, pain relieving.
The present invention by can effectively treat cloudy alveolar neuralgia Chinese medicine composition carry out substep alcohol steep, make the collutory not only taking convenience of the cloudy alveolar neuralgia of prepared treatment, and be conducive to the absorption of effective ingredient, effectively treat cloudy alveolar neuralgia.
In the preparation method of the collutory of the cloudy alveolar neuralgia of described treatment, in step 3 to the cloudy alveolar neuralgia for the treatment of collutory in add 0.05% sodium fluoride.
In the preparation method of the collutory of the cloudy alveolar neuralgia of described treatment, in step 2, leach extraction method is substep extraction, and concrete grammar is:
Step 2.1, first time lixiviate, extraction temperature is 30-50 DEG C, extraction time 30-40 minute, filters and obtains the first lixiviating solution;
Step 2.2, second time lixiviate, mixed with ethanol by the trapped substance of first time lixiviate filtration and carry out second time lixiviate, extraction temperature is 60-80 DEG C, extraction time 20-30 minute, filters and obtains the second lixiviating solution;
Step 2.3, the first lixiviating solution to be mixed with the second lixiviating solution, be heated to 80-85 DEG C and make ethanol evaporation, obtain described extract.
Substep lixiviate can make effective ingredient more fully discharge, and improves curative effect of medication.
Although embodiment of the present invention are open as above, but it is not restricted to listed in description and embodiment utilization, it can be applied to various applicable the field of the invention completely, for those skilled in the art, can easily realize other amendment, therefore do not deviating under the general concept that claim and equivalency range limit, the present invention is not limited to specific details.
Claims (3)
1. treat a preparation method for the collutory of cloudy alveolar neuralgia, it is characterized in that, comprise the following steps:
Step 1, lixiviate, by Chinese medicine composition drying and crushing, obtain raw material powder, described Chinese medicine composition comprises the raw material of following weight portion: Cortex Lycii 12-18, Cortex Moutan 8-12, Cortex Phellodendri Amurensis (parched with salt) 4-6, Rhizoma Anemarrhenae 5-8, Radix Rehmanniae 8-12, Radix Scrophulariae 8-12, Herba Taraxaci 10-15, Herba Violae 8-12, Herba Ecliptae 8-12, Radix Arnebiae (Radix Lithospermi) 8-12, Herba Menthae 8-15, Radix Zanthoxyli 8-12 and Flos Eriocauli 8-12;
Step 2, by the 60-70% alcoholic solution mixing lixiviate of raw material powder with 10-30 times of volume, lixiviate terminates post-heating makes ethanol evaporation, obtains extract;
Step 3, by extract adding distil water dilution 10-15 doubly, obtain the collutory of the cloudy alveolar neuralgia of described treatment.
2. the preparation method of the collutory of the cloudy alveolar neuralgia for the treatment of as claimed in claim 1, is characterized in that, in step 3 to the cloudy alveolar neuralgia for the treatment of collutory in add 0.05% sodium fluoride.
3. the preparation method of the collutory of the cloudy alveolar neuralgia for the treatment of as claimed in claim 1, is characterized in that, in step 2, leach extraction method is substep extraction, and concrete grammar is:
Step 2.1, first time lixiviate, extraction temperature is 30-50 DEG C, extraction time 30-40 minute, filters and obtains the first lixiviating solution;
Step 2.2, second time lixiviate, mixed with ethanol by the trapped substance of first time lixiviate filtration and carry out second time lixiviate, extraction temperature is 60-80 DEG C, extraction time 20-30 minute, filters and obtains the second lixiviating solution;
Step 2.3, the first lixiviating solution to be mixed with the second lixiviating solution, be heated to 80-85 DEG C and make ethanol evaporation, obtain described extract.
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Citations (4)
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CN1416870A (en) * | 2002-12-12 | 2003-05-14 | 胡莉 | Toothache treating Chinese medicine |
CN101380410A (en) * | 2007-09-05 | 2009-03-11 | 凌沛学 | Medicine for treating hyperactivity of fire due to yin deficiency and preparation method of the formulation thereof |
CN103007012A (en) * | 2013-01-06 | 2013-04-03 | 牛俊芝 | Traditional Chinese medicine composition for treating toothaches and preparation method thereof |
CN105106428A (en) * | 2015-08-18 | 2015-12-02 | 白善夫 | Traditional Chinese medicine composition for treating toothache and method for preparing traditional Chinese medicine composition |
-
2015
- 2015-12-10 CN CN201510918201.4A patent/CN105477285A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1416870A (en) * | 2002-12-12 | 2003-05-14 | 胡莉 | Toothache treating Chinese medicine |
CN101380410A (en) * | 2007-09-05 | 2009-03-11 | 凌沛学 | Medicine for treating hyperactivity of fire due to yin deficiency and preparation method of the formulation thereof |
CN103007012A (en) * | 2013-01-06 | 2013-04-03 | 牛俊芝 | Traditional Chinese medicine composition for treating toothaches and preparation method thereof |
CN105106428A (en) * | 2015-08-18 | 2015-12-02 | 白善夫 | Traditional Chinese medicine composition for treating toothache and method for preparing traditional Chinese medicine composition |
Non-Patent Citations (2)
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张璞玉: "分型辩治牙痛120例", 《四川中医》 * |
陈三斌等: "《新编240种实用化工产品配方与制造》", 31 March 2004, 金盾出版社 * |
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