CN105476879A - 一种指甲油及其制备方法 - Google Patents

一种指甲油及其制备方法 Download PDF

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CN105476879A
CN105476879A CN201610006253.9A CN201610006253A CN105476879A CN 105476879 A CN105476879 A CN 105476879A CN 201610006253 A CN201610006253 A CN 201610006253A CN 105476879 A CN105476879 A CN 105476879A
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董川
梁中远
宋胜梅
王慧萍
双少敏
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Abstract

本发明提供了一种指甲油及其制备方法，指甲油组分包括荧烷型隐色体染料、乙醇、显色剂、填料、珠光粉和成膜剂。制备方法是先将成膜剂PVB加入乙醇中，搅拌，完全溶解后，加入荧烷型隐色体染料，再加入显色剂，搅拌使之完全溶解。之后加入填料，搅拌10分钟，再加入珠光粉，搅拌30-40分钟，最后加入成膜剂PVP，搅拌20分钟可即可制得产品。本发明制作方法简单，产品使用安全，不含对人体有害的增塑剂，不使用有毒、低毒以及刺激性溶剂，可明显减少对指甲的伤害，并且在温水中浸泡5分钟或者冷水中浸泡10分钟后即可完整揭除，易于清洗变换，随时可以保持指甲的干净美观，并具有一定的抵御紫外线的功能。

Description

一种指甲油及其制备方法
技术领域：
本发明涉及化妆用品，具体地说属于一种指甲油及其制备方法。
背景技术：
目前市场上常见的指甲油多使用硝化纤维为成膜剂，酞酸酯为增塑剂，丙酮和乙酸乙酯为溶剂，其主要缺陷在于：作为指甲油成膜剂的硝化纤维是易燃易爆危险品，生产和使用工程具有很大的危险性；酞酸酯等增塑剂会影响人的生育能力，严重危害人体健康；丙酮和乙酸乙酯做溶剂，具有一定的毒性和刺激性(丙酮为易制毒品的管制试剂)；指甲油涂好后，必须要用含有多种有机溶剂的洗甲水擦除，使用不方便，经常洗甲会危害指甲健康。
指甲油的发展趋势是：成膜剂稳定化，不使用硝化纤维等易燃易爆成膜剂；溶剂无毒化，不使用丙酮、乙酸乙酯等低毒刺激性溶剂；不添加增塑剂；涂抹后不使用有机溶剂即可卸除。
专利CN1260167A硝化纤维为成膜剂，虽然可以得到成膜性好、耐磨的指甲油，但硝化纤维易燃易爆，储存与使用过程危险性大，不利于可持续发展。专利CN102397198A以乙酸乙酯、丙酮等为溶剂，该类配方调配得当可以得到高光泽、强附着力和强耐水性的指甲油，但存在如下缺点：1、具有刺激性气味，强烈刺鼻的气味吸入后会引起身体不适；2、使用后对人体的指甲和皮肤刺激性较大，长期使用有较大的伤害；3、接触化纤类衣物和一般塑料都会造成溶解性腐蚀。专利CN100346770C以水、水性成膜剂、颜料和香精等添加剂搅拌混合而成。该类配方调配得当可以得到低气味、低刺激性、高光泽、对化纤衣物和塑料不会溶解性腐蚀的指甲油，但存在如下缺点：1、耐水性差，遇水容易脱落；2、附着力不好，与有机溶剂型指甲油比有很大差距。
发明内容：
本发明的目的在于提供一种指甲油及其制备方法。该指甲油不使用硝化纤维作为成膜剂，使生产储运更安全；不含丙酮和乙酸乙酯等刺激性溶剂，使其无刺激性气味和毒性；指甲油涂在指甲上后具有一定的防水性，在日常洗手等情况下不会被擦除、溶解；同时，在温水或者冷水中浸泡一定时间后即可完整揭除，易于清洗变换。
本发明提供的一种指甲油，其组分按重量份数计包括：荧烷型隐色体染料0.1-0.5，乙醇75-90，显色剂0.3-1，填料0.1-0.5，珠光粉0.1-0.5，成膜剂PVB6-20，成膜剂PVP0.3-3。
所述的指甲油，其组分按重量份数计还可以包括0.01-0.03的香精，如间甲氧基肉桂酸等。
所述的填料为纳米级白炭黑；
所述的显色剂是草酸；
所述的荧烷型隐色体染料为荧烷红((3,3-双(N-辛基-2-甲基吲哚)邻苯二甲内酯))，荧烷黄(N,N-二甲基-4-(2-(2-(辛基氧基)苯基)-6-苯基吡啶-4-基)苯胺)，结晶紫内酯(6-二甲氨基-3,3-双(4-二甲基氨基苯基)苯酞)，荧烷绿(2'-(二苄基氨基)-6'-(二乙氨基)荧烷)。
本发明提供的一种指甲油的制备方法，包括如下步骤：按上述组分重量份数配比，将成膜剂PVB加入乙醇中，搅拌，完全溶解后，加入荧烷型隐色体染料，再加入显色剂，搅拌使之完全溶解。之后加入填料，搅拌10分钟，再加入珠光粉，搅拌30-40分钟，最后加入成膜剂PVP，搅拌20分钟(之后如选择加入香料，在加入香料后，继续搅拌5分钟)即可制得产品。
与现有技术相比，本发明不使用丙酮、乙酸乙酯等有毒、刺激性溶剂，不产生有毒VOC；不添加加硝化纤维，生产、储运安全；不添加酞酸酯等塑化剂，不危害人体健康；本发明采用荧烷型隐色体染料，指甲油易于擦除，在温水中浸泡5分钟或者冷水中浸泡10分钟后即可完整揭除，不慎滴到衣服上，可以使用乙醇擦洗，环保方便。该指甲油无毒、无刺激性气味。对指甲无害，不产生任何污染，配制方便，易于生产，还具有防紫外线的作用。
具体实施方式：
实施例1：
将4.5g成膜剂PVB加入30ml乙醇中，搅拌，完全溶解后，加入0.1g荧烷型隐色体染料荧烷红，再加入0.2g显色剂草酸，搅拌使之完全溶解。之后加入0.5g填料纳米级白炭黑，搅拌10分钟，再加入0.1g珠光粉，搅拌30-40分钟，最后加入0.5g成膜剂PVP，搅拌20分钟，所得为红色指甲油。
实施例2：
将4.5g成膜剂PVB加入30ml乙醇中，搅拌，完全溶解后，加入0.1g荧烷型隐色体染料荧烷红，再加入0.2g显色剂草酸，搅拌使之完全溶解。之后加入0.5g填料纳米级白炭黑，搅拌10分钟，再加入0.1g珠光粉，搅拌30-40分钟，最后加入0.5g成膜剂PVP，搅拌20分钟。再加入0.1g间甲氧基肉桂酸，搅拌5分钟。所得为带有香味的红色指甲油。
实施例3：
将4.5g成膜剂PVB加入30ml乙醇中，搅拌，完全溶解后，加入0.1g荧烷型隐色体染料荧烷黄，再加入0.2g显色剂草酸，搅拌使之完全溶解。之后加入0.5g填料纳米级白炭黑，搅拌10分钟，再加入0.1g珠光粉，搅拌30-40分钟，最后加入0.5g成膜剂PVP，搅拌20分钟，所得为黄色指甲油。
实施例4：
将4.5g成膜剂PVB加入30ml乙醇中，搅拌，完全溶解后，加入0.1g荧烷型隐色体染料荧烷黄，再加入0.2g显色剂草酸，搅拌使之完全溶解。之后加入0.5g填料纳米级白炭黑，搅拌10分钟，再加入0.1g珠光粉，搅拌30-40分钟，最后加入0.5g成膜剂PVP，搅拌20分钟，再加入0.1g间甲氧基肉桂酸，搅拌5分钟。所得为带有香味的黄色指甲油。
实施例5：
将4.5g成膜剂PVB加入30ml乙醇中，搅拌，完全溶解后，加入0.1g荧烷型隐色体染料结晶紫内酯，再加入0.2g显色剂草酸，搅拌使之完全溶解。之后加入0.5g填料纳米级白炭黑，搅拌10分钟，再加入0.1g珠光粉，搅拌30-40分钟，最后加入0.5g成膜剂PVP，搅拌20分钟。所得为紫色指甲油。
实施例6：
将4.5g成膜剂PVB加入30ml乙醇中，搅拌，完全溶解后，加入0.1g荧烷型隐色体染料结晶紫内酯，再加入0.2g显色剂草酸，搅拌使之完全溶解。之后加入0.5g填料纳米级白炭黑，搅拌10分钟，再加入0.1g珠光粉，搅拌30-40分钟，最后加入0.5g成膜剂PVP，搅拌20分钟，再加入0.1g间甲氧基肉桂酸，搅拌5分钟。所得为带有香味的紫色指甲油。
实施例7：
将4.5g成膜剂PVB加入30ml乙醇中，搅拌，完全溶解后，加入0.1g荧烷型隐色体染料荧烷绿，再加入0.2g显色剂草酸，搅拌使之完全溶解。之后加入0.5g填料纳米级白炭黑，搅拌10分钟，再加入0.1g珠光粉，搅拌30-40分钟，最后加入0.5g成膜剂PVP，搅拌20分钟。所得为绿色指甲油。
实施例8：
将4.5g成膜剂PVB加入30ml乙醇中，搅拌，完全溶解后，加入0.1g荧烷型隐色体染料荧烷绿，再加入0.2g显色剂草酸，搅拌使之完全溶解。之后加入0.5g填料纳米级白炭黑，搅拌10分钟，再加入0.1g珠光粉，搅拌30-40分钟，最后加入0.5g成膜剂PVP，搅拌20分钟，再加入0.1g间甲氧基肉桂酸，搅拌5分钟。所得为带有香味的绿色指甲油。

Claims (7)

1.一种指甲油，其特征在于，组分按重量份数计包括：荧烷型隐色体染料0.1-0.5，乙醇75-90，显色剂0.3-1，填料0.1-0.5，珠光粉0.1-0.5，成膜剂PVB6-20，成膜剂PVP0.3-3。
2.如权利要求1所述的一种指甲油，其特征在于，组分按重量份数计还包括0.01-0.03的香精。
3.如权利要求1或2所述的一种指甲油，其特征在于，所述的填料为纳米级白炭黑。
4.如权利要求1或2所述的一种指甲油，其特征在于，所述的显色剂是草酸。
5.如权利要求1或2所述的一种指甲油，其特征在于，所述的荧烷型隐色体染料为荧烷红、荧烷黄、结晶紫内酯或荧烷绿。
6.如权利要求2所述的一种指甲油，其特征在于，所述的香精为间甲氧基肉桂酸。
7.一种指甲油的制备方法，其特征在于，包括如下步骤：按权利要求1所述的组分重量份数配比，将成膜剂PVB加入乙醇中，搅拌，完全溶解后，加入荧烷型隐色体染料，再加入显色剂，搅拌使之完全溶解；之后加入填料，搅拌10分钟，再加入珠光粉，搅拌30-40分钟，最后加入成膜剂PVP，搅拌20分钟即制得产品。
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105963155A (zh) * 2016-06-14 2016-09-28 山西大学 一种能指示剥离时机的易于清除的指甲油
CN105997555A (zh) * 2016-05-13 2016-10-12 山西大学 一种可用温水水洗褪色的染色发蜡及其制备方法

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