CN105462730A - 一种茶花香型洗衣液 - Google Patents

一种茶花香型洗衣液 Download PDF

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CN105462730A
CN105462730A CN201510997995.8A CN201510997995A CN105462730A CN 105462730 A CN105462730 A CN 105462730A CN 201510997995 A CN201510997995 A CN 201510997995A CN 105462730 A CN105462730 A CN 105462730A
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camellia
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李志华
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Qingdao Chaoyang Huatai Management Consulting Services Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00Compositions of detergents, not provided for by one single preceding group
    • C11D10/04Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00Compositions of detergents, not provided for by one single preceding group
    • C11D10/04Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • C11D10/045Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00Compositions of detergents, not provided for by one single preceding group
    • C11D10/04Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • C11D10/047Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on cationic surface-active compounds and soap
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions
    • C11D11/0005Special cleaning and washing methods
    • C11D11/0011Special cleaning and washing methods characterised by the objects to be cleaned
    • C11D11/0017"Soft" surfaces, e.g. textiles
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials characterised by their shape or physical properties
    • C11D17/06Powder; Flakes; Free-flowing mixtures; Sheets
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38Cationic compounds
    • C11D1/62Quaternary ammonium compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/662Carbohydrates or derivatives

Abstract

本发明涉及一种茶花香型洗衣液。其组分重量配比为:18~35%的表面活性剂、0.005~0.03%的竹叶黄酮、1~2%的茶花提取物浓缩液、2~3%的酯基季铵盐、0.3~1.5%的皂粉、0.5~1%的柠檬酸钠、0.01~0.05%的无水氯化钙、0.6~4%的抗皱剂、2~5%的烷基糖苷、0.6~1.5%的茶皂素、0.5~2%的丙二醇、0.6~1.2%的酶制剂0.2~0.4%的防腐剂、1~2%的增稠剂和0.4~0.8%的薰衣草精油,余量为去离子水。它可对天然纤维织物的衣物进行柔化减少其起皱,对人体无刺激同时具有杀菌的功效,具有茶花的香味。

Description

一种茶花香型洗衣液
技术领域
[0001]本发明涉及一种茶花香型洗衣液。
背景技术
[0002]天然纤维织物,特别是棉织物具有手感自然、吸湿透气、抗静电、穿着舒适、经济实惠等优点,所以深受人们的喜爱,在织物纤维中,以棉纤维的产量最大、应用最广,不过纯棉织物有弹性差、易起皱、洗后需熨烫,而且易受微生物的侵袭导致纤维霉变和脆损的缺点。
发明内容
[0003]本发明旨在解决上述技术问题,提供了一种茶花香型洗衣液,它可对天然纤维织物的衣物进行柔化减少其起皱,对人体无刺激同时具有杀菌的功效,具有茶花的香味,其采用的技术方案如下:
[0004] 一种茶花香型洗衣液,其特征在于,其组分重量配比为:18〜35%的表面活性剂、0.005〜0.03 %的竹叶黄酮、1〜2 %的茶花提取物浓缩液、2〜3 %的酯基季铵盐、0.3〜1.5%的皂粉、0.5〜1 %的柠檬酸钠、0.01〜0.05%的无水氯化钙、0.6〜4%的抗皱剂、2〜5%的烷基糖苷、0.6〜1.5%的茶皂素、0.5〜2%的丙二醇、0.6〜1.2%的酶制剂0.2〜0.4 %的防腐剂、1〜2 %的增稠剂和0.4〜0.8 %的薰衣草精油,余量为去离子水。
[0005]在上述技术方案基础上,所述茶花提取物浓缩液由下述过程制备:
[0006] (1)取成熟茶花,洗净剥皮、切片,用pH为4.0-4.5的酸溶液浸泡,再用95°C_100°C热水热烫,冷却,加入一定量的水打浆,浆液备用;
[0007] (2)浆液温度保持在42-45°C,用酸调pH至2.0-2.5,加入胃蛋白酶或果胶酶,搅匀后,维持pH至2.0-2.5,温度为42-45°C的条件下水解;
[0008] (3)用碱将水解后的浆液调pH至8.5-9.0,加入胰酶,搅匀后,维持pH至8.5-9.0,42-45°C的条件水解,酶解结束后加热升温进行酶灭活,降温至室温;
[0009 ] (4)用酸调pH至6.0-7.0,进行固液分离,除去茶花肉残渣,收集滤过液,备用;
[0010] (5)将滤过液用DEAE层析柱进行吸附,用酸性磷酸盐缓冲液洗脱;
[0011 ] (6)洗脱液用滤膜进行超滤,收集滤出液,即得茶花提取物浓缩液。
[0012]在上述技术方案基础上,所述酯基季铵盐为1-甲基-1-油酰胺乙基-2-油酸基咪唑林硫酸甲酯铵。
[0013]本发明具有如下优点:可对天然纤维织物的衣物进行柔化减少其起皱,对人体无刺激同时具有杀菌的功效,具有茶花的香味。
具体实施方式
[0014] 实施例1
[0015] 一种茶花香型洗衣液,其特征在于,其组分重量配比为:35%的表面活性剂、0.03%的竹叶黄酮、2%的茶花提取物浓缩液、3%的酯基季铵盐、1.5%的皂粉、1 %的柠檬酸钠、0.05 %的无水氯化钙、4%的抗皱剂、5 %的烷基糖苷、1.5 %的茶皂素、2 %的丙二醇、
0.6%的酶制剂0.2%的防腐剂、2%的增稠剂和0.4%的薰衣草精油,余量为去离子水。
[0016]优选的,所述茶花提取物浓缩液由下述过程制备:
[0017] (1)取成熟茶花,洗净剥皮、切片,用pH为4.0-4.5的酸溶液浸泡,再用95°C_100°C热水热烫,冷却,加入一定量的水打浆,浆液备用;
[0018] (2)浆液温度保持在42-45°C,用酸调pH至2.0-2.5,加入胃蛋白酶或果胶酶,搅匀后,维持pH至2.0-2.5,温度为42-45°C的条件下水解;
[0019] (3)用碱将水解后的浆液调pH至8.5-9.0,加入胰酶,搅匀后,维持pH至8.5-9.0,42-45°C的条件水解,酶解结束后加热升温进行酶灭活,降温至室温;
[0020] (4)用酸调pH至6.0-7.0,进行固液分离,除去茶花肉残渣,收集滤过液,备用;
[0021 ] (5)将滤过液用DEAE层析柱进行吸附,用酸性磷酸盐缓冲液洗脱;
[0022] (6)洗脱液用滤膜进行超滤,收集滤出液,即得茶花提取物浓缩液。
[0023]优选的,所述酯基季铵盐为1-甲基-1-油酰胺乙基-2-油酸基咪唑林硫酸甲酯铵。
[0024] 实施例2
[0025] 一种茶花香型洗衣液,其特征在于,其组分重量配比为:18%的表面活性剂、0.005 %的竹叶黄酮、1 %的茶花提取物浓缩液、2 %的酯基季铵盐、1.5 %的皂粉、1 %的柠檬酸钠、0.05 %的无水氯化钙、0.6 %的抗皱剂、2 %的烷基糖苷、0.6%的茶皂素、0.5%的丙二醇、0.6%的酶制剂0.4%的防腐剂、2%的增稠剂和0.4%的薰衣草精油,余量为去离子水。
[0026]优选的,所述茶花提取物浓缩液由下述过程制备:
[0027] (1)取成熟茶花,洗净剥皮、切片,用pH为4.0-4.5的酸溶液浸泡,再用95°C_100°C热水热烫,冷却,加入一定量的水打浆,浆液备用;
[0028] (2)浆液温度保持在42-45°C,用酸调pH至2.0-2.5,加入胃蛋白酶或果胶酶,搅匀后,维持pH至2.0-2.5,温度为42-45°C的条件下水解;
[0029] (3)用碱将水解后的浆液调pH至8.5-9.0,加入胰酶,搅匀后,维持pH至8.5-9.0,42-45°C的条件水解,酶解结束后加热升温进行酶灭活,降温至室温;
[0030] (4)用酸调pH至6.0-7.0,进行固液分离,除去茶花肉残渣,收集滤过液,备用;
[0031 ] (5)将滤过液用DEAE层析柱进行吸附,用酸性磷酸盐缓冲液洗脱;
[0032] (6)洗脱液用滤膜进行超滤,收集滤出液,即得茶花提取物浓缩液。
[0033]优选的,所述酯基季铵盐为1-甲基-1-油酰胺乙基-2-油酸基咪唑林硫酸甲酯铵。
[0034]对所公开的实施例的上述说明,使本领域技术人员能够实现或使用本发明。对这些实施例的多种修改对本领域技术人员来说将是显而易见的,本文中所定义的一般原理可以在不脱离本发明的原理或范围的情况下,在其它实施例中实现。因此,本发明将不会被限制于本文所示的这些实施例,而是要符合与本文所公开的原理和新颖特点相一致的最宽的范围。

Claims (3)

1.一种茶花香型洗衣液,其特征在于,其组分重量配比为:18〜35%的表面活性剂、0.005〜0.03 %的竹叶黄酮、1〜2 %的茶花提取物浓缩液、2〜3 %的酯基季铵盐、0.3〜1.5%的皂粉、0.5〜1 %的柠檬酸钠、0.01〜0.05%的无水氯化钙、0.6〜4%的抗皱剂、2〜5%的烷基糖苷、0.6〜1.5%的茶皂素、0.5〜2%的丙二醇、0.6〜1.2%的酶制剂0.2〜0.4 %的防腐剂、1〜2 %的增稠剂和0.4〜0.8 %的薰衣草精油,余量为去离子水。
2.根据权利要求1所述的一种茶花香型洗衣液,其特征在于:所述茶花提取物浓缩液由下述过程制备: (1)取成熟茶花,洗净剥皮、切片,用pH为4.0-4.5的酸溶液浸泡,再用95°C_100°C热水热烫,冷却,加入一定量的水打浆,浆液备用; (2)浆液温度保持在42-45°C,用酸调pH至2.0_2.5,加入胃蛋白酶或果胶酶,搅匀后,维持pH至2.0-2.5,温度为42-45°C的条件下水解; (3)用碱将水解后的浆液调pH至8.5-9.0,加入胰酶,搅匀后,维持pH至8.5-9.0,42-45°C的条件水解,酶解结束后加热升温进行酶灭活,降温至室温; (4)用酸调pH至6.0-7.0,进行固液分离,除去茶花肉残渣,收集滤过液,备用; (5)将滤过液用DEAE层析柱进行吸附,用酸性磷酸盐缓冲液洗脱; (6)洗脱液用滤膜进行超滤,收集滤出液,即得茶花提取物浓缩液。
3.根据权利要求1或2所述的一种茶花香型洗衣液,其特征在于:所述酯基季铵盐为1-甲基-1-油酰胺乙基-2-油酸基咪唑林硫酸甲酯铵。
CN201510997995.8A 2015-12-25 2015-12-25 一种茶花香型洗衣液 Pending CN105462730A (zh)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106987466A (zh) * 2017-04-07 2017-07-28 淮北市相山区靖函洗涤用品店 一种衣物湿洗液
CN110591844A (zh) * 2019-09-29 2019-12-20 广州香枝化妆品有限公司 一种植物除螨抑螨洗衣液及其制备方法

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CN104403857A (zh) * 2014-11-24 2015-03-11 青岛市市南区隆德中医药研究所 一种可柔化衣物的洗衣液
CN104450214A (zh) * 2014-11-28 2015-03-25 青岛市市南区隆德中医药研究所 一种高效抑菌杀菌洗衣液
CN104473845A (zh) * 2014-11-27 2015-04-01 青岛市市南区隆德中医药研究所 一种具有茶花香味的洗发水

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Publication number Priority date Publication date Assignee Title
CN104403856A (zh) * 2014-11-24 2015-03-11 青岛市市南区隆德中医药研究所 一种可柔化衣物的洗衣液
CN104403857A (zh) * 2014-11-24 2015-03-11 青岛市市南区隆德中医药研究所 一种可柔化衣物的洗衣液
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106987466A (zh) * 2017-04-07 2017-07-28 淮北市相山区靖函洗涤用品店 一种衣物湿洗液
CN110591844A (zh) * 2019-09-29 2019-12-20 广州香枝化妆品有限公司 一种植物除螨抑螨洗衣液及其制备方法

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