CN105456456A - Dental ulcer oral solution and preparation method thereof - Google Patents

Dental ulcer oral solution and preparation method thereof Download PDF

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Publication number
CN105456456A
CN105456456A CN201510980887.XA CN201510980887A CN105456456A CN 105456456 A CN105456456 A CN 105456456A CN 201510980887 A CN201510980887 A CN 201510980887A CN 105456456 A CN105456456 A CN 105456456A
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extracting
preparation
sterilizing
liquid
subsequent use
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张丽楠
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Chongqing Lehu Technology Co Ltd
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Chongqing Lehu Technology Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
    • A61K35/56—Materials from animals other than mammals
    • A61K35/63—Arthropods
    • A61K35/64—Insects, e.g. bees, wasps or fleas
    • A61K35/644—Beeswax; Propolis; Royal jelly; Honey
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/288—Taraxacum (dandelion)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/34—Campanulaceae (Bellflower family)
    • A61K36/346—Platycodon
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/481—Astragalus (milkvetch)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
    • A61K36/718—Coptis (goldthread)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/74—Rubiaceae (Madder family)
    • A61K36/744—Gardenia
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/75—Rutaceae (Rue family)
    • A61K36/754—Evodia
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
    • A61K47/08—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing oxygen, e.g. ethers, acetals, ketones, quinones, aldehydes, peroxides
    • A61K47/12—Carboxylic acids; Salts or anhydrides thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/0012—Galenical forms characterised by the site of application
    • A61K9/0053—Mouth and digestive tract, i.e. intraoral and peroral administration
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/08—Solutions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30—Extraction of the material
    • A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30—Extraction of the material
    • A61K2236/35—Extraction with lipophilic solvents, e.g. Hexane or petrol ether
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50—Methods involving additional extraction steps
    • A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50—Methods involving additional extraction steps
    • A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Epidemiology (AREA)
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  • Pharmacology & Pharmacy (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Veterinary Medicine (AREA)
  • Engineering & Computer Science (AREA)
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  • Alternative & Traditional Medicine (AREA)
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  • Insects & Arthropods (AREA)
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  • Nutrition Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
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Abstract

The invention discloses a dental ulcer oral solution and a preparation method of the dental ulcer oral solution. The dental ulcer oral solution is mainly prepared from the following components of kawazure, astragalus membranaceus, fructus evodiae, cortex moutan, cape jasmine, platycodon grandiflorum, dandelion and royal jelly. The preparation method comprises the steps of respectively weighing raw materials according to the components; extracting effective components of the kawazure, astragalus membranaceus, fructus evodiae and cape jasmine by utilizing a reflux method, a decocting method, an ethanol extracting method and an ethyl acetate extracting method; extracting effective components of the cortex moutan, platycodon grandiflorum and dandelion by utilizing the decocting method; then merging extracting solutions, obtaining a refined solution by utilizing an alcohol deposition method, and adding the royal jelly in the refined solution; finally obtaining the dental ulcer oral solution by sub-packaging the refined solution in bottles. The dental ulcer oral solution disclosed by the invention has the advantages of small side effect and simple preparation technology.

Description

A kind of oral ulcer oral liquid and preparation method thereof
Technical field
The present invention relates to field of traditional Chinese medicine formula, particularly relate to formula of a kind of oral ulcer oral liquid and preparation method thereof.
Background technology
Oral ulcer is one of common at present oral disease, also has person for " aphtha ", is a kind of shallow and little, circular or avette ulcer.In oral ulcer, modal one is " recurrent oral ulceration ", usually raw on lip, tongue or other positions in oral cavity, and can often recurrence.
Summary of the invention
One of technical problem to be solved by this invention is to provide a kind of oral ulcer oral liquid, and the component of described oral ulcer oral liquid comprises Chinese crude drug, and side effect is little.
The technical scheme that the present invention solves the problems of the technologies described above is as follows:
A kind of oral ulcer oral liquid, its component formation mainly comprises Rhizoma Coptidis, the Radix Astragali, Fructus Evodiae, Cortex Moutan, Fructus Gardeniae, Radix Platycodonis, Herba Taraxaci, Lac regis apis; Its parts by weight are: Rhizoma Coptidis 3-5 part, Radix Astragali 10-20 part, Fructus Evodiae 5-10 part, Cortex Moutan 3-5 part, Fructus Gardeniae 3-5 part, Radix Platycodonis 3-5 part, Herba Taraxaci 3-5 part, Lac regis apis 15-20 part.
Rhizoma Coptidis has effect of pathogenic fire purging, dampness, removing toxic substances.
The Radix Astragali has the effect of expelling pus and promoting granulation.
Fructus Evodiae has effect of dispersing cold for relieving pain, external treatment aphtha.
Cortex Moutan has effect of clearing away heat and cooling blood.
Fructus Gardeniae has effect of pathogenic fire purging relieving restlessness, clearing away heat-damp and promoting diuresis, removing pathogenic heat from blood and toxic substance from the body.
Radix Platycodonis has the effect for the treatment of aphtha of the mouth and tongue.
Herba Taraxaci has effect of heat-clearing and toxic substances removing.
Two of technical problem to be solved by this invention is to provide the preparation method of described oral liquid, and described preparation method technique is simple.
The technical scheme that the present invention solves the problems of the technologies described above comprises the following steps:
Raw material is taken according to component;
Rhizoma Coptidis is pulverized, uses reflux extraction effective component extracting, extracting liquid filtering is after sterilizing for subsequent use;
The Radix Astragali is pulverized, uses decocting method effective component extracting, extracting liquid filtering is after sterilizing for subsequent use;
Fructus Evodiae is pulverized, uses ethanol extraction method effective component extracting, extracting liquid filtering is after sterilizing for subsequent use;
Fructus Gardeniae is pulverized, with ethyl acetate extraction method effective component extracting, extracting liquid filtering is for subsequent use after sterilizing;
Cortex Moutan, Radix Platycodonis, Herba Taraxaci are pulverized, uses decocting method effective component extracting, extracting liquid filtering is after sterilizing for subsequent use;
Merge extractive liquid, integral filter is also for subsequent use after sterilizing;
Concentrated by extracting solution, after medicinal liquid places 1 hour, add ethanol, airtight cold preservation, reclaims ethanol after filtration, namely obtains refined liquid;
In refined liquid, add Lac regis apis, filter after mix homogeneously and use vinegar acid for adjusting pH.Acetic acid effectively can promote the performance of Fructus Evodiae effective ingredient;
Be sub-packed in bottle.
Further, described pH is 5.0-6.0.
Further, the addition of described ethanol makes alcohol content reach 50-60%, effectively can remove the impurity such as starch.
Further, described concentration ratio is 1:1.The consumption of ethanol can be reduced after concentration of liquid medicine.
Further, the time of described airtight cold preservation is 2 hours, can effectively prevent ethanol from volatilizing, and promotes the sedimentation of separating out precipitation.
Beneficial effect of the present invention: the beneficial effect of the oral ulcer oral liquid described in (1) is that its component comprises Chinese crude drug, and side effect is little, and effectively can treat the recurrent exerbation with preventing canker sore.(2) beneficial effect of the preparation method described in is that preparation technology is simple, and patient is easy to use.
Detailed description of the invention
Be described principle of the present invention and feature below in conjunction with example, example, only for explaining the present invention, is not intended to limit scope of the present invention.
The oral ulcer oral liquid of embodiment 1, its component formation mainly comprises Rhizoma Coptidis 5g, Radix Astragali 20g, Fructus Evodiae 10g, Cortex Moutan 5g, Fructus Gardeniae 5g, Radix Platycodonis 5g, Herba Taraxaci 5g, Lac regis apis 20g.
The preparation method of the oral ulcer oral liquid of embodiment 2: 5g Rhizoma Coptidis is pulverized, uses reflux extraction effective component extracting, extracting liquid filtering is for subsequent use after sterilizing; Radix Astragali 20g is pulverized, use decocting method effective component extracting, extracting liquid filtering is for subsequent use after sterilizing; Fructus Evodiae 10g is pulverized, use ethanol extraction method effective component extracting, extracting liquid filtering is for subsequent use after sterilizing; Fructus Gardeniae 5g is pulverized, with ethyl acetate extraction method effective component extracting, extracting liquid filtering is for subsequent use after sterilizing; Cortex Moutan 5g, Radix Platycodonis 5g, Herba Taraxaci 5g are pulverized, use decocting method effective component extracting, extracting liquid filtering is for subsequent use after sterilizing; Merge extractive liquid, integral filter is also for subsequent use after sterilizing; Concentrated by extracting solution, after medicinal liquid places 1 hour, add ethanol, airtight cold preservation, reclaims ethanol after filtration, namely obtains refined liquid; In refined liquid, add Lac regis apis 20g, filter after mix homogeneously and use vinegar acid for adjusting pH to 5.0; Be sub-packed in bottle.
The preparation method of the oral ulcer oral liquid of embodiment 3: 3g Rhizoma Coptidis is pulverized, uses reflux extraction effective component extracting, extracting liquid filtering is for subsequent use after sterilizing; Radix Astragali 10g is pulverized, use decocting method effective component extracting, extracting liquid filtering is for subsequent use after sterilizing; Fructus Evodiae 5g is pulverized, use ethanol extraction method effective component extracting, extracting liquid filtering is for subsequent use after sterilizing; Fructus Gardeniae 3g is pulverized, with ethyl acetate extraction method effective component extracting, extracting liquid filtering is for subsequent use after sterilizing; Cortex Moutan 3g, Radix Platycodonis 3g, Herba Taraxaci 3g are pulverized, use decocting method effective component extracting, extracting liquid filtering is for subsequent use after sterilizing; Merge extractive liquid, integral filter is also for subsequent use after sterilizing; Concentrated by extracting solution, after medicinal liquid places 1 hour, add ethanol, airtight cold preservation, reclaims ethanol after filtration, namely obtains refined liquid; In refined liquid, add Lac regis apis 15g, filter after mix homogeneously and use vinegar acid for adjusting pH to 5.0; Be sub-packed in bottle.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.

Claims (6)

1. an oral ulcer oral liquid, is characterized in that, its component formation mainly comprises Rhizoma Coptidis, the Radix Astragali, Fructus Evodiae, Cortex Moutan, Fructus Gardeniae, Radix Platycodonis, Herba Taraxaci, Lac regis apis; Its parts by weight are: Rhizoma Coptidis 3-5 part, Radix Astragali 10-20 part, Fructus Evodiae 5-10 part, Cortex Moutan 3-5 part, Fructus Gardeniae 3-5 part, Radix Platycodonis 3-5 part, Herba Taraxaci 3-5 part, Lac regis apis 15-20 part.
2. a preparation method for oral liquid as described in the appended claim 1, comprises the following steps:
Raw material is taken according to component;
Rhizoma Coptidis is pulverized, uses reflux extraction effective component extracting, extracting liquid filtering is after sterilizing for subsequent use;
The Radix Astragali is pulverized, uses decocting method effective component extracting, extracting liquid filtering is after sterilizing for subsequent use;
Fructus Evodiae is pulverized, uses ethanol extraction method effective component extracting, extracting liquid filtering is after sterilizing for subsequent use;
Fructus Gardeniae is pulverized, with ethyl acetate extraction method effective component extracting, extracting liquid filtering is for subsequent use after sterilizing;
Cortex Moutan, Radix Platycodonis, Herba Taraxaci are pulverized, uses decocting method effective component extracting, extracting liquid filtering is after sterilizing for subsequent use;
Merge extractive liquid, integral filter is also for subsequent use after sterilizing;
Concentrated by extracting solution, after medicinal liquid places 1 hour, add ethanol, airtight cold preservation, reclaims ethanol after filtration, namely obtains refined liquid;
In refined liquid, add Lac regis apis, filter after mix homogeneously and use vinegar acid for adjusting pH;
Be sub-packed in bottle.
3. according to the preparation method described in claim 2, it is characterized in that, described pH is 5.0-6.0.
4. according to the preparation method described in claim 2, it is characterized in that, the addition of described ethanol makes alcohol content reach 50-60%.
5. according to the preparation method described in claim 2, it is characterized in that, described concentration ratio is 1:1.
6. according to the preparation method described in claim 2, it is characterized in that, the time of described airtight cold preservation is 2 hours.
CN201510980887.XA 2015-12-23 2015-12-23 Dental ulcer oral solution and preparation method thereof Pending CN105456456A (en)

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Application Number Priority Date Filing Date Title
CN201510980887.XA CN105456456A (en) 2015-12-23 2015-12-23 Dental ulcer oral solution and preparation method thereof

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111686085A (en) * 2020-06-30 2020-09-22 贵州益佰女子大药厂有限责任公司 Preparation method of throat-clearing preparation

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111686085A (en) * 2020-06-30 2020-09-22 贵州益佰女子大药厂有限责任公司 Preparation method of throat-clearing preparation
CN111686085B (en) * 2020-06-30 2022-09-06 贵州益佰女子大药厂有限责任公司 Preparation method of throat clearing preparation

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