CN1054370A - A kind of manufacture method of kidney-tonifying health-care medicament - Google Patents
A kind of manufacture method of kidney-tonifying health-care medicament Download PDFInfo
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- CN1054370A CN1054370A CN91102061A CN91102061A CN1054370A CN 1054370 A CN1054370 A CN 1054370A CN 91102061 A CN91102061 A CN 91102061A CN 91102061 A CN91102061 A CN 91102061A CN 1054370 A CN1054370 A CN 1054370A
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Abstract
The present invention relates to a kind of manufacture method of kidney-tonifying health-care medicament, be raw material mainly with Chinese crude drugs such as Fructus Cnidii, Semen Cuscutae, Herba Epimedii, the Radix Astragali, Fructus Lycii, Radix Polygoni Multiflori Preparata and sucrose, through weighing and burden, processing steps such as alcohol extraction percolation, water extract-alcohol precipitation, dosing adjustment, check fill are made Chinese materia medica syrup.The Chinese materia medica syrup of producing with this method has that cost is low, and sugar content is low, and is anticorrosion, the mildew-resistant ability is strong, characteristics such as good stability, also tool significantly tonify Qi of the kidney, the effect of enhancing body premunition.
Description
The invention belongs to a kind of manufacture method of medical preparation, relate in particular to a kind of kidney-tonifying health-care Chinese materia medica syrup manufacture method of low sugar.
In " pharmaceutics " teaching material, to the sugar content general provision of syrup about 50% even higher.Its theoretical foundation is that the sugar content height not only can flavoring, and also the big relative density ambassador's drug microparticles that can suppress growth of microorganism, breeding and medicinal liquid of osmotic pressure because of medicinal liquid keeps suspended state, is difficult for precipitation.In brief, the sucrose of Chinese materia medica syrup middle and high concentration exists as correctives, antibacterial and stabilizing agent.But the syrup of high sugar content makes the user take in a large amount of sugar parts, and modern medicine has proved that this can produce many harmful effects to health, makes many users produce the psychology of fear.It is 89105826.5 to be called the patent application document of " a kind of manufacture method of medicine of enhancing body function " that Patent Office of the People's Republic of China once disclosed a application number, wherein having proposed a kind of is primary raw material with Chinese crude drug such as Radix Ginseng, Herba Epimedii, Fructus Lycii, the Radix Astragali, Semen Cuscutae, Fructus Rosae Laevigatae and Mel, through raw material handle, batching, extract, concentrate, precipitate with ethanol and filtration, decolouring take off the method that processing steps such as charcoal, dosing, cold preservation, the inspection of semifinished product, fill are made Chinese medicine preparation.This method processing step is more, technological process is longer.Especially adding Mel can only be as correctives, and the protein of also perishable because of containing, easy flocculation sediment, fat etc. influence anti-corrosive properties, the stability of medicament.In addition, owing to add valuable medicinals such as Mel, Radix Ginseng, its production cost is also higher.
The objective of the invention is to overcome above-mentioned deficiency of the prior art and the kidney-tonifying health-care Chinese materia medica syrup that a kind of production technology is simple, flow process is short, sugar content is low manufacture method is provided, that its product has is anticorrosion preferably, fungicidal properties and stability, can be accepted by fearing sugared patient again.
Purpose of the present invention can adopt following processing step to realize:
A. weighing and burden (by weight)
Fructus Cnidii 4～7 Radix Polygoni Multiflori Preparata 14～16 Radix Glycyrrhizae Preparatas 2～5
Rhizoma Dioscoreae 8～10 Semen Cuscutae 12～15 Radix Rehmanniaes Preparata 17～21
Rhizoma Chuanxiong 5～8 Semen Trigonellaes 17～21 Poria 5～7
Fructus Lycii 11～15 Fructus Psoraleaes 5～8 Herba Cistanches 8～11
Fructus Rosae Laevigatae 17～21 Herba Epimedii 17～21 Fructus Schisandrae Chinensis 6～8
Sucrose 30～50 Radix Angelicae Sinensis 8～11 Radixs Astragali 9～11
Fructus Rubi 6～7 antiseptic 0.2～0.4
Make the syrup medicinal liquid of 150～250 weight portions altogether;
B. alcohol extraction percolation is got Fructus Cnidii, Herba Epimedii, Radix Angelicae Sinensis, Rhizoma Chuanxiong and is broken into coarse powder, with slow percolation after 60～90% alcohol dipping, concentrates, filters percolate standby;
C. water extract-alcohol precipitation is suitably cataclasm with all the other medical materials, decocts with water, and decoction liquor adds 2～4 times ethanol precipitation after filtering, being concentrated into thick paste, standby after the supernatant concentration;
D. dosing adjustment is carried standby medicinal liquid with alcohol extraction, water and is mixed, and adds sucrose and boils 10～30 minutes, adds antiseptic, adjusts medicinal liquid and to ormal weight and with alkali compoundss such as NaOH, trisodium citrates the pH value of medicinal liquid is transferred to 4.0～6.0;
E. check fill, will filter, check, the medicinal liquid of relative density (heat is surveyed) greater than 1.08 carried out the fill warehouse-in through adjusted medicinal liquid.
The present invention also can adopt following measure to reach better effect:
(1) in alcohol extraction percolation medicinal raw material, adds the Fructus Foeniculi of 2～4 weight portions; In water extract-alcohol precipitation medicine village raw material, add the Semen Plantaginis of 2～5 weight portions and the Rhizoma Atractylodis Macrocephalae of 2～4 weight portions; The edge strip Radix Ginseng Rubra that other gets 3～5 weight portions is broken into coarse powder, with 15～30% alcohol dipping, backflow, again with backflow through filtering, concentrate, in the medicinal liquid that adding was boiled when dosing is adjusted;
(2) when dosing is adjusted, the most handy trisodium citrate is adjusted the pH value to 4.5 of medicinal liquid, makes mouthfeel the best of medicinal liquid, stability best;
(3) when dosing is adjusted, the medicament antiseptic of available routine, the ethyl hydroxybenzoate of the sodium benzoate of the most handy 0.2 weight portion and 0.1 weight portion matches, its antiseptic effect the best.
Embodiment 1:
A. according to following prescription batching:
Fructus Cnidii 28.9 is restrained the Radix Polygoni Multiflori 75.3 gram Radix Glycyrrhizae Preparatas 15.1 grams
Rhizoma Dioscoreae 47.2 gram Semen Cuscutae 66.9 gram Radix Rehmanniaes Preparata 94.9 grams
River glutinous rehmannia 29.2 gram Semen Trigonellaes 94.9 gram Poria 30.9 grams
Fructus Lycii 66.9 gram Fructus Psoraleaes 29.4 gram Herba Cistanches 48.2 grams
Fructus Rosae Laevigatae 95.5 gram Herba Epimedii 95.5 gram Fructus Schisandrae Chinensis 36.9 grams
The sucrose 200 gram Radix Angelicae Sinensis 47.7 gram Radixs Astragali 52.3 grams
Fructus Rubi 33.8 gram sodium benzoate 1 gram ethyl hydroxybenzoate 0.5 gram
Make 1000 milliliters syrup medicinal liquid altogether;
B. Fructus Cnidii, Herba Epimedii, Radix Angelicae Sinensis, Rhizoma Chuanxiong power are broken into the powder about 12 orders, in percolator, do solvent dipping 36 hours with 80% ethanol, with the slow percolation of per kilogram crude drug 1～3 ml/min speed, reclaiming ethanol from percolate, medicinal liquid is concentrated into relative density is 1.10, filters standby;
C. it is suitably cataclasm to get all the other medical materials, decoct with water 2 times, and each 2 hours, merge decoction liquor and filter, filtrate is concentrated into the thick paste shape, add duple 95% ethanol precipitation 72 hours, to get supernatant and reclaim ethanol, it is 1.10 standby that medicinal liquid is concentrated into relative density.
D. merge alcohol extraction, water is carried standby medicinal liquid, adds sucrose and boils 10 minutes, filters, and adds sodium benzoate and ethyl hydroxybenzoate again, adjusts medicinal liquid to ormal weight, and adjusts pH value to 5.0 with NaOH;
E. with adjusted medical filtration, check is put relative density in storage greater than 1.08 liquid medicine filling.
Embodiment 2:
A. by following prescription batching:
Fructus Cnidii 28 is restrained the Radix Polygoni Multiflori 74.4 gram Rhizoma Chuanxiongs 28.3 grams
Semen Plantaginis 16.5 gram Semen Cuscutae 66 gram Radix Rehmanniaes Preparata 94 grams
Fructus Psoraleae 28.5 Keshan medicines 46.3 gram Poria 30 grams
Fructus Lycii 66 gram edge strip Radix Ginseng Rubra 20 gram Semen Trigonellaes 94 grams
Fructus Foeniculi 14.4 gram Herba Epimedii 94.6 gram Fructus Schisandrae Chinensis 36 grams
The Herba Cistanches 47.3 gram Fructus Rosae Laevigatae 94.6 gram Radixs Astragali 51.4 grams
The Rhizoma Atractylodis Macrocephalae 14.2 gram sucrose 200 gram Radix Angelicae Sinensis 46.8 grams
Radix Glycyrrhizae Preparata 14.2 gram Fructus Rubies 32.9 gram sodium benzoate 1 gram
Ethyl hydroxybenzoate 0.5 gram
Make 1000 milliliters syrup medicinal liquid altogether;
B. Fructus Cnidii, Herba Epimedii, Radix Angelicae Sinensis, Rhizoma Chuanxiong, Fructus Foeniculi are ground into the powder about 14 orders, in percolator, do solvent dipping 48 hours with 70% ethanol, with the slow percolation of per kilogram crude drug 1～3 ml/min speed, reclaiming ethanol from percolate, medicinal liquid is concentrated into relative density is 1.10, filters standby;
C. the edge strip red ginseng powder is broken into about 15 purpose powder, reflux 2 times in the vessel in heating of taking back the stream device with 20% alcohol dipping 8 hours, each each 2 hours, merge backflow and filter, reclaim 1/2 standby to crude drug weight of ethanol and cryoconcentration from filtrate, medicinal residues are sneaked into Chinese crude drug to be decocted;
D. with the suitable cataclasm edge strip Radix Ginseng Rubra backflow medicinal residues of sneaking into of all the other medical materials, decoct with water 2 times, each each 2 hours, merge decoction liquor and filter, be concentrated into the thick paste shape, add three times of 95% ethanol precipitation 48 hours, supernatant reclaims ethanol, and to be concentrated into relative density be 1.10 standby;
E. merge alcohol extraction, water is carried standby medicinal liquid, adds sucrose and boils 15 minutes, filters and adds edge strip Radix Ginseng Rubra reflux standby medicinal liquid, sodium benzoate and ethyl hydroxybenzoate, adjust medicinal liquid to ormal weight, and adjust pH value to 4.5 with trisodium citrate;
F. adjusted medicinal liquid is filtered, checks, relative density is put in storage greater than 1.08 liquid medicine filling.
The present invention has following characteristics compared with prior art:
(1) production technology is simple, and flow process is short, particularly adopts alcohol extraction percolation technology, can more effectively extract the medicine active ingredient;
(2) the medicament sugar content of Sheng Chaning is lower, more useful user's physical and mental health;
(3) medicament of Sheng Chaning is anticorrosion, the mildew-resistant ability is strong, good stability, not perishable during storage, precipitation;
(4) the medicament pharmaceutical characteristic of Sheng Chaning is good, the energy kidney-tonifying health-care, and clinical practice is evident in efficacy.
" renal aid " bran slurry agent that method constructed in accordance is produced, press the pertinent regulations of Ministry of Public Health and " pharmacy of Chinese materia medica " through the institute for drug control, Jiangxi Province, under room temperature (5～16 ℃), constant temperature acceleration (40 ℃), three kinds of situations of cold preservation (0～5 ℃), preserve respectively and tested in three months, the results are shown in following table:
| Resting period (moon) | Color and luster | Clarity | Relative density | PH value | |
| Room temperature | 0 1.5 3 | Quite the same with standard color solution Y-6 | Basic clarification is the same | 1.120 1.118 1.120 | 4.5 4.4 4.4 |
| Constant temperature | 0 1.5 3 | With standard color solution Y-6 number quite the same | Basic clarification is the same | 1.120 1.120 1.120 | 4.5 4.4 4.4 |
| Cold preservation | 0 1.5 3 | With standard color solution Y-6 number quite the same | Basic clarification is the same | 1.120 1.119 1.120 | 4.5 4.4 4.3 |
The hygiene inspection of this medicament ties up to and carries out when depositing 0,1.5,3 months in 37 ℃ of incubators, and its result is: assorted bacterium, mycete number average＜10/milliliter, escherichia coli all do not detect.
Through 421 routine deficiency of kidney-YANG syndrome patients being carried out the research statistics of clinical taking " renal aid ", the total effective rate of two courses of treatment (28 days) reaches 86.4%, and wherein the clinical recovery rate is 25.0%, and obvious effective rate is 40.0%, and improvement rate is 21.4%.Attached Yueyang doctor Wang Huaming of hospital of Shanghai College of Traditional Chinese Medicine once write articles " clinical practice of renal aid " on " Chinese patent medicine " 89 years the 5th phases, point out because the merit of renal aid tool kidney warming and yang invigorating, improving inspiration by invigorating kidney-QI Dingchuan, invigorating the spleen and benefiting QI, strengthening the body resistance, clinically be widely used in sexual impotence, seminal emission, soreness of waist pain, fear of cold is afraid of cold, nocturia, spiritlessness and weakness, alopecia tinnitus, the women leucorrhea, diseases such as menorrhagia also do to have good alleviating and preventive effect frequently to asthma due to failure of the kidney in receiving QI.Diseases such as author's clinical practice renal aid treatment bronchial asthma, frequent micturition, sexual impotence, odontoseisis, soreness of waist pain, obtained gratifying effect, and sum up: renal aid has the merit and the enhancing body premunition of obviously tonifying Qi of the kidney, all have a deficiency of suffering from a deficiency of the kidney, the disease of deficiency of both QI and blood, all available renal aid Zhi Qiben.
Claims (4)
1, a kind of manufacture method of kidney-tonifying health-care Chinese formulated products, primary raw material comprises Semen Cuscutae, Fructus Rosae Laevigatae, Fructus Lycii, Herba Epimedii, the Radix Astragali, Radix Glycyrrhizae Preparata Chinese crude drug, make product through batching, extraction, dosing, check, fill operation, it is characterized in that adopting following process steps:
A. weighing and burden (by weight)
Fructus Cnidii 4～7 Radix Polygoni Multiflori Preparata 14～16 Radix Glycyrrhizae Preparatas 2～5
Rhizoma Dioscoreae 8～10 Semen Cuscutae 12～15 Radix Rehmanniaes Preparata 17～21
Rhizoma Chuanxiong 5～8 Semen Trigonellaes 17～21 Poria 5～7
Fructus Lycii 11～15 Fructus Psoraleaes 5～8 Herba Cistanches 8～11
Fructus Rosae Laevigatae 17～21 Herba Epimedii 17～21 Fructus Schisandrae Chinensis 6～8
Sucrose 30～50 Radix Angelicae Sinensis 8～11 Radixs Astragali 9～11
Fructus Rubi 6～7 antiseptic 0.2～0.4
Make the syrup medicinal liquid of 150～250 weight portions altogether;
B. the alcohol extraction percolation is got Fructus Cnidii, Herba Epimedii, Radix Angelicae Sinensis, Rhizoma Chuanxiong pulverizing, with slow percolation after 60～90% alcohol dipping, concentrates, filters standby then;
C. water extract-alcohol precipitation is cataclasm with all the other medical materials, decocts with water, and adds 2～4 times ethanol precipitation after filtering, concentrating again, and supernatant concentration is standby;
D. dosing adjustment, merging alcohol extraction, water are carried reserve liquid, after adding sucrose boils, add antiseptic, adjust medicinal liquid and adjust pH value to 4.0～6.0 to ormal weight and with alkali compounds;
E. check fill, the medicinal liquid through adjusting is filtered, checks, relative density is put in storage greater than 1.08 liquid medicine filling.
2, Chinese formulated products manufacture method according to claim 1, it is characterized in that also can when batching, adding edge strip Radix Ginseng Rubra 3～5 by weight, Fructus Foeniculi 2～4, Semen Plantaginis 2～5, the Rhizoma Atractylodis Macrocephalae 2～4 Chinese crude drugs, wherein Fructus Foeniculi is with alcohol extraction percolation medical material pulverization process, and Semen Plantaginis, the Rhizoma Atractylodis Macrocephalae are with the cataclasm processing of water extract-alcohol precipitation medical material, the edge strip Radix Ginseng Rubra is pulverized the back with 15～30% alcohol dipping, backflow, backflow is added in the medicinal liquid that boiled when dosing is adjusted after filtering, concentrating again.
3, Chinese formulated products manufacture method according to claim 1 and 2, used alkali compounds is a trisodium citrate when it is characterized in that the dosing adjustment, optimal pH is 4.5.
4, Chinese formulated products manufacture method according to claim 3 is characterized in that dosing adjustment time institute's adding preservative agent and consumption thereof are sodium benzoate 0.2 and ethyl hydroxybenzoate 0.1 weight portion.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN91102061A CN1054370A (en) | 1991-03-30 | 1991-03-30 | A kind of manufacture method of kidney-tonifying health-care medicament |
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| Application Number | Priority Date | Filing Date | Title |
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| CN91102061A CN1054370A (en) | 1991-03-30 | 1991-03-30 | A kind of manufacture method of kidney-tonifying health-care medicament |
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| CN1054370A true CN1054370A (en) | 1991-09-11 |
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| CN91102061A Pending CN1054370A (en) | 1991-03-30 | 1991-03-30 | A kind of manufacture method of kidney-tonifying health-care medicament |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1093764C (en) * | 1998-08-28 | 2002-11-06 | 王欢 | Medical liquor for nourishing kidney |
| WO2003037246A2 (en) * | 2001-07-17 | 2003-05-08 | Integrated Chinese Medicine Holdings Ltd. | Compositions and methods for prostate and kidney health and disorders, an herbal preparation |
| US7449202B1 (en) | 2003-07-10 | 2008-11-11 | Integrated Chinese Medicine Holdings, Ltd. | Compositions and methods for prostate and kidney health and disorders, an herbal preparation |
| CN101343606B (en) * | 2008-08-25 | 2011-07-20 | 甘海龙 | Life prolonging wine and preparation |
| CN103041282A (en) * | 2013-01-29 | 2013-04-17 | 王鹤成 | Traditional Chinese medicine for treating deficiency of spleen and kidney and preparation method of medicine |
| CN103768214A (en) * | 2014-02-12 | 2014-05-07 | 蒋保珍 | Traditional Chinese medicinal composition for treating kidney-yang deficiency type rhinitis |
| CN103933449A (en) * | 2014-04-23 | 2014-07-23 | 宁佐兰 | Traditional Chinese medicine composition for treating lumbago and preparation method of traditional Chinese medicine composition |
| CN103933448A (en) * | 2014-04-17 | 2014-07-23 | 丁亚朋 | Traditional Chinese medicine bath for nourishing yuan and reinforcing kidneys |
| CN104522652A (en) * | 2014-12-19 | 2015-04-22 | 赵俊辉 | Formula of nutrient solution for children and preparation method of nutrient solution for children |
| CN105434960A (en) * | 2015-12-30 | 2016-03-30 | 俞成莲 | Medicine for treating alopecia caused by liver blood deficiency and hair nourishment loss |
| CN106306966A (en) * | 2016-08-19 | 2017-01-11 | 上海世道健康科技有限公司 | Preparation method of medicinal and edible plant compound functional beverage |
| CN106310082A (en) * | 2016-09-23 | 2017-01-11 | 路杨景 | Kidney-tonifying traditional Chinese medicine composition and preparation method thereof |
| CN111686230A (en) * | 2020-07-15 | 2020-09-22 | 徐文华 | Yang-tonifying hair-growing composition, preparation method and application |
-
1991
- 1991-03-30 CN CN91102061A patent/CN1054370A/en active Pending
Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1093764C (en) * | 1998-08-28 | 2002-11-06 | 王欢 | Medical liquor for nourishing kidney |
| WO2003037246A2 (en) * | 2001-07-17 | 2003-05-08 | Integrated Chinese Medicine Holdings Ltd. | Compositions and methods for prostate and kidney health and disorders, an herbal preparation |
| WO2003037246A3 (en) * | 2001-07-17 | 2003-10-30 | Integrated Chinese Medicine Ho | Compositions and methods for prostate and kidney health and disorders, an herbal preparation |
| US6855344B2 (en) | 2001-07-17 | 2005-02-15 | Integrated Chinese Medicine Holdings, Ltd. | Compositions and methods for prostate and kidney health and disorders, an herbal preparation |
| US7223424B2 (en) | 2001-07-17 | 2007-05-29 | Integrated Chinese Medicine Holdings, Ltd. | Compositions and methods for prostate and kidney health and disorders, an herbal preparation |
| US7465466B2 (en) | 2001-07-17 | 2008-12-16 | Integrated Chinese Medicine Holdings, Ltd. | Compositions and methods for prostate and kidney health and disorders, an herbal preparation |
| US7449202B1 (en) | 2003-07-10 | 2008-11-11 | Integrated Chinese Medicine Holdings, Ltd. | Compositions and methods for prostate and kidney health and disorders, an herbal preparation |
| CN101343606B (en) * | 2008-08-25 | 2011-07-20 | 甘海龙 | Life prolonging wine and preparation |
| CN103041282A (en) * | 2013-01-29 | 2013-04-17 | 王鹤成 | Traditional Chinese medicine for treating deficiency of spleen and kidney and preparation method of medicine |
| CN103041282B (en) * | 2013-01-29 | 2014-08-13 | 王鹤成 | Traditional Chinese medicine for treating deficiency of spleen and kidney and preparation method of medicine |
| CN103768214A (en) * | 2014-02-12 | 2014-05-07 | 蒋保珍 | Traditional Chinese medicinal composition for treating kidney-yang deficiency type rhinitis |
| CN103933448A (en) * | 2014-04-17 | 2014-07-23 | 丁亚朋 | Traditional Chinese medicine bath for nourishing yuan and reinforcing kidneys |
| CN103933449A (en) * | 2014-04-23 | 2014-07-23 | 宁佐兰 | Traditional Chinese medicine composition for treating lumbago and preparation method of traditional Chinese medicine composition |
| CN104522652A (en) * | 2014-12-19 | 2015-04-22 | 赵俊辉 | Formula of nutrient solution for children and preparation method of nutrient solution for children |
| CN105434960A (en) * | 2015-12-30 | 2016-03-30 | 俞成莲 | Medicine for treating alopecia caused by liver blood deficiency and hair nourishment loss |
| CN106306966A (en) * | 2016-08-19 | 2017-01-11 | 上海世道健康科技有限公司 | Preparation method of medicinal and edible plant compound functional beverage |
| CN106310082A (en) * | 2016-09-23 | 2017-01-11 | 路杨景 | Kidney-tonifying traditional Chinese medicine composition and preparation method thereof |
| CN111686230A (en) * | 2020-07-15 | 2020-09-22 | 徐文华 | Yang-tonifying hair-growing composition, preparation method and application |
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