CN105410038A - Holotrichia parallela sex pheromone synergist and preparation method - Google Patents
Holotrichia parallela sex pheromone synergist and preparation method Download PDFInfo
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- CN105410038A CN105410038A CN201510789391.4A CN201510789391A CN105410038A CN 105410038 A CN105410038 A CN 105410038A CN 201510789391 A CN201510789391 A CN 201510789391A CN 105410038 A CN105410038 A CN 105410038A
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- synergist
- holotrichia parallela
- sex pheromone
- holotrichia
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N49/00—Biocides, pest repellants or attractants, or plant growth regulators, containing compounds containing the group, wherein m+n>=1, both X together may also mean —Y— or a direct carbon-to-carbon bond, and the carbon atoms marked with an asterisk are not part of any ring system other than that which may be formed by the atoms X, the carbon atoms in square brackets being part of any acyclic or cyclic structure, or the group, wherein A means a carbon atom or Y, n>=0, and not more than one of these carbon atoms being a member of the same ring system, e.g. juvenile insect hormones or mimics thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
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Abstract
The invention provides a holotrichia parallela sex pheromone synergist and a preparation method and belongs to the technical field of comprehensive prevention and control of holotrichia parallela. The holotrichia parallela sex pheromone synergist is characterized by being prepared from holotrichia parallela sex pheromone, a synergist and an organic solvent. The holotrichia parallela sex pheromone is prepared from L-isoleucine methyl ester, (R)-(-)-linalool and 1-aminocyclohexanecarboxylic acid, the synergist is prepared from cis-9, trans-11-tetradecadien acetate, cis-5, trans-7-dodecadien acetate, honey and mustard oil, and the organic solvent is prepared from dichloroethane, cyclohexane and fatty acid methyl ester. The synergist has the advantages of being sensitive, specific, high in efficiency, long in lasting period, biodegradable, good in biological compatibility, free of environmental pollution, low in cost and the like, can be used for population monitoring of the holotrichia parallela, prevention and control of trapping and killing of a large number of holotrichia parallela and accurate prediction of the density of a next generation of insect populations and has very good economic benefits and ecological benefits.
Description
Technical field
A kind of Holotrichia parallela sex pheromone synergist and preparation method, belong to peanut insect Holotrichia parallela biological control method technical field.
Background technology
Grub endangers the maximum insect of peanut at present.Grub mainly takes food peanut pod and root, peanut pod and root can be eaten up in flakes, have a strong impact on output when worm amount is many.Some place is due to the harm of grub, and the peanut underproduction reaches more than 50%, even has no harvest.Grub is the main soil insect of harm peanut, large, the difficult control of harm, and easily out in the cold.Grub take food when starting to endanger the firm rudiment of peanut seed, bite seedling rhizome broken, causing is short of seedling is completely cured; Later growth moth food pod, forms hole, causes peanut ghost.Grub stings food peanut always, until harvest, not only causes the peanut underproduction, but also greatly reduces its commodity value.Grub is owing to being soil insect, and harm is large, difficult to be prevented and treated, and easily out in the cold.Present stage is still based on chemical control.In addition, residue of pesticide, the problems such as environmental pollution exist, and make us carry out pest control in the urgent need to a kind of novel approach of green non-pollution.Holotrichia parallela (Holotrichiaparallela) belongs to coleoptera (Coleoptera) scarab beetle Superfamily (Scarabaeoidea) Melolonthidae (Melolonthidae), is the adult of grub.The use of insect sex pheromone in recent years provides a new approach for control of insect.The sex pheromone of Shandong Peanut Inst. to China's Holotrichia parallela is studied, independent research holotrichia parallela sex pheromone core and supporting trapper, and achieves in field and good lure worm effect (Brockerhoffetal., 2006; Zhouetal., 2009; Li Xiao etc., 2012).But there are problem (ReddyandGuerrero, 2004 such as specific attractant male worm, consumption time be short in gyplure;
etal., 2005).Gathering effect need the problems such as raising.
Summary of the invention
In order to solve problems of the prior art, the object of the present invention is to provide a kind of Holotrichia parallela sex pheromone synergist and preparation method, to improve the attractant effect of gyplure to prevent and treat Holotrichia parallela.
The technical scheme that the present invention takes is: a kind of Holotrichia parallela sex pheromone synergist is made up of Holotrichia parallela pheromones, synergist and organic solvent.Holotrichia parallela pheromones is made up of ILE methyl esters, (R)-(-)-linalool and 1-cyclohexane-carboxylic acid, synergist is by suitable 9, anti-11-tetradecadienyl acetate, suitable 5, anti-7-12 carbon diene acetic acid esters, honey and mustard oil form, and organic solvent is made up of dichloroethane, cyclohexane and fatty acid methyl ester.
The mass ratio of Holotrichia parallela pheromones, synergist and organic solvent is 1:5-10:50-100.
Holotrichia parallela pheromones ILE methyl esters, (R)-(-)-linalool and 1-cyclohexane-carboxylic acid mass ratio are 5:4:1.
Synergist is along 9, and anti-11-tetradecadienyl acetate, suitable 5, anti-7-12 carbon diene acetic acid esters, honey and mustard oil mass ratio are 1:1:8:10.
Organic solvent dichloroethane, cyclohexane and fatty acid methyl ester mass ratio are 1:2:2.
Beneficial effect of the present invention is: by the basis of traditional lure, adds synergist and reaches the effect continuing efficiently to lure, and reach the stability of storage, economic benefit and ecological benefits remarkable.
Embodiment
Below in conjunction with specific embodiment, the present invention will be further described, but these examples do not limit the scope of the invention.In addition any change of doing the present invention of those of ordinary skill in the related art, only otherwise depart from essence of the present invention, all drops on equivalence in claims of the present invention limited range.
Embodiment 1
ILE methyl esters 5 grams, (R)-(-)-linalool 4 grams, 1-cyclohexane-carboxylic acid 1 gram, 9, anti-11-tetradecadienyl acetate 2.5 grams, suitable 5, anti-7-12 carbon diene acetic acid esters 2.5 grams, honey 20 grams, mustard oil 25 grams, dichloroethane 100 grams, cyclohexane 200 grams, fatty acid methyl ester 200 grams.Obtain the Holotrichia parallela gyplure adding synergist, (do not add the anti-11-tetradecadienyl acetate of synergist, along 5 compared with the control, anti-7-12 carbon diene acetic acid esters, honey and mustard oil), 1 evening traped quantity and adds 1580, added 52%.
Embodiment 2
ILE methyl esters 5 grams, (R)-(-)-linalool 4 grams, 1-cyclohexane-carboxylic acid 1 gram, 9, anti-11-tetradecadienyl acetate 3.5 grams, suitable 5, anti-7-12 carbon diene acetic acid esters 3.5 grams, honey 28 grams, mustard oil 35 grams, dichloroethane 140 grams, cyclohexane 280 grams, fatty acid methyl ester 280 grams.Obtain the Holotrichia parallela gyplure adding synergist, (do not add the anti-11-tetradecadienyl acetate of synergist, along 5 compared with the control, anti-7-12 carbon diene acetic acid esters, honey and mustard oil), 1 evening traped quantity and adds 2352, added 85%.
Embodiment 3
ILE methyl esters 5 grams, (R)-(-)-linalool 4 grams, 1-cyclohexane-carboxylic acid 1 gram, 9, anti-11-tetradecadienyl acetate 5 grams, suitable 5, anti-7-12 carbon diene acetic acid esters 5 grams, honey 40 grams, mustard oil 50 grams, dichloroethane 200 grams, cyclohexane 400 grams, fatty acid methyl ester 400 grams.Obtain the Holotrichia parallela gyplure adding synergist, (do not add the anti-11-tetradecadienyl acetate of synergist, along 5 compared with the control, anti-7-12 carbon diene acetic acid esters, honey and mustard oil), 1 evening traped quantity and adds 1976, added 73%.
Claims (5)
1. Holotrichia parallela sex pheromone synergist and a preparation method, is characterized in that it forms by by Holotrichia parallela pheromones, synergist and organic solvent; Holotrichia parallela pheromones is made up of ILE methyl esters, (R)-(-)-linalool and 1-cyclohexane-carboxylic acid, synergist is by suitable 9, anti-11-tetradecadienyl acetate, suitable 5, anti-7-12 carbon diene acetic acid esters, honey and mustard oil form, and organic solvent is made up of dichloroethane, cyclohexane and fatty acid methyl ester.
2. the mass ratio of Holotrichia parallela pheromones, synergist and organic solvent is 1:5-10:50-100 as claimed in claim 1.
3. as claimed in claim 1, Holotrichia parallela pheromones is made up of ILE methyl esters, (R)-(-)-linalool and 1-cyclohexane-carboxylic acid, and its mass ratio is 5:4:1.
4. as claimed in claim 1, synergist is by suitable 9, and anti-11-tetradecadienyl acetate, suitable 5, anti-7-12 carbon diene acetic acid esters, honey and mustard oil form, and its mass ratio is 1:1:8:10.
5. as claimed in claim 1, organic solvent is made up of dichloroethane, cyclohexane and fatty acid methyl ester, and phase mass ratio is 1:2:2.
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| CN201510789391.4A CN105410038B (en) | 2015-11-17 | 2015-11-17 | A kind of Holotrichia parallela sex pheromone synergist and preparation method |
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| CN201510789391.4A CN105410038B (en) | 2015-11-17 | 2015-11-17 | A kind of Holotrichia parallela sex pheromone synergist and preparation method |
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| CN105410038A true CN105410038A (en) | 2016-03-23 |
| CN105410038B CN105410038B (en) | 2018-04-10 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1520724A (en) * | 2003-01-30 | 2004-08-18 | 中国科学院动物研究所 | Red bordered white moth exohormone induction core and its uses |
| CN101627757A (en) * | 2009-08-03 | 2010-01-20 | 山东省花生研究所 | Dark melolonthidae sex pheromone and sex attractant |
| CN104041490A (en) * | 2014-06-13 | 2014-09-17 | 山东省花生研究所 | Granular holotrichia parallela slow-releasing sex attractant and preparation method thereof |
| CN104738034A (en) * | 2015-04-01 | 2015-07-01 | 山东省花生研究所 | Acetic acid cis-3-hexenyl ester synergistic holotrichia parallela sex attractant |
| CN104839191A (en) * | 2015-04-01 | 2015-08-19 | 山东省花生研究所 | Holotrichia parallela sex attractant synergized by using trans-2-vinyl acetate |
-
2015
- 2015-11-17 CN CN201510789391.4A patent/CN105410038B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1520724A (en) * | 2003-01-30 | 2004-08-18 | 中国科学院动物研究所 | Red bordered white moth exohormone induction core and its uses |
| CN101627757A (en) * | 2009-08-03 | 2010-01-20 | 山东省花生研究所 | Dark melolonthidae sex pheromone and sex attractant |
| CN104041490A (en) * | 2014-06-13 | 2014-09-17 | 山东省花生研究所 | Granular holotrichia parallela slow-releasing sex attractant and preparation method thereof |
| CN104738034A (en) * | 2015-04-01 | 2015-07-01 | 山东省花生研究所 | Acetic acid cis-3-hexenyl ester synergistic holotrichia parallela sex attractant |
| CN104839191A (en) * | 2015-04-01 | 2015-08-19 | 山东省花生研究所 | Holotrichia parallela sex attractant synergized by using trans-2-vinyl acetate |
Non-Patent Citations (4)
| Title |
|---|
| ZHOU LI-MEI等: "EAG and behavioral responses of the large black chafer，Holotrichia parallela(Coleoptera：Scarabaeidae)to its sex pheromone", 《ACTA ENTOMOLOGICA SINICA》 * |
| 李晓等: "利用性诱剂防治花生田暗黑鳃金龟的研究", 《植物保护》 * |
| 王萌长 主编: "《昆虫生物化学》", 28 February 2001 * |
| 龚恒亮等: "金龟甲诱剂的研究与应用状况", 《广东农业科》 * |
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| CN105410038B (en) | 2018-04-10 |
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Effective date of registration: 20221124 Address after: Room 211, Block D, Lanhua Institute, No. 36, Jinshui Road, Laoshan District, Qingdao City, Shandong Province, 266000 Patentee after: QINGDAO RUSSELL IPM BIOTECH CO.,LTD. Address before: Licang District 266000 years Springs Road No. 126, Shandong city of Qingdao Province Patentee before: SHANDONG PEANUT Research Institute |