CN105399501A - Trunk-injection medicament for controlling branch and trunk diseases of fruit trees, and preparation method for trunk-injection medicament - Google Patents

Trunk-injection medicament for controlling branch and trunk diseases of fruit trees, and preparation method for trunk-injection medicament Download PDF

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Publication number
CN105399501A
CN105399501A CN201510823693.9A CN201510823693A CN105399501A CN 105399501 A CN105399501 A CN 105399501A CN 201510823693 A CN201510823693 A CN 201510823693A CN 105399501 A CN105399501 A CN 105399501A
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CN
China
Prior art keywords
trunk
fruit trees
substance
dry medicament
branches
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Pending
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CN201510823693.9A
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Chinese (zh)
Inventor
马瑜
朱海云
柯杨
李勃
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Microbiology Institute Of Shaanxi
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Microbiology Institute Of Shaanxi
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Priority to CN201510823693.9A priority Critical patent/CN105399501A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/20Liquid fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B1/00Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • C05B1/02Superphosphates

Abstract

The invention discloses a trunk-injection medicament for controlling branch and trunk diseases of fruit trees. The trunk-injection medicament is prepared from the following components by volume percentage: 0.5-10% of a bactericidal substance, 0.025-0.1% of a surfactant, 0.1-2% of a nutrient substance, 0.01-0.1% of a penetrating agent and 89-99% of water, wherein the total content of the components is 100%. The invention further discloses a preparation method for the trunk-injection medicament, and the preparation method comprises the following steps: weighing the raw materials, adding all of the weighed components into water separately, and stirring to enable the mixture to be mixed uniformly to prepare a stock solution of medical liquid; filling and sealing to obtain the trunk-injection medicament. The trunk-injection medicament allows nutrient required for the growth of plants to be organically combined, so that not only are pathogenic fungi killed, but also the plant wound healing is accelerated to speed up recovery of the trees; meanwhile, the trunk-injection medicament has the characteristics of being safe, nontoxic and wide in raw material source, and is suitable for large-sized popularization and application, easy to use, excellent in effect, and suitable for large-scale popularization and application.

Description

A kind of for note dry medicament preventing and treating diseases of branches of fruit trees and preparation method thereof
Technical field
The invention belongs to fruit diseases Prevention Technique field, being specifically related to a kind of note dry medicament for preventing and treating diseases of branches of fruit trees, the invention still further relates to the preparation method of above-mentioned note dry medicament.
Background technology
Trunk disease is a class disease the most common in cultivation of fruit tree process, mainly through harm branches of fruit trees, causes fruit tree cortical necrosis, and severe patient can cause tree body dead.According to the difference of pathogenic bacteria, fungal disease (as canker of apple fruit, Walnut Canker, Dothiorella Gregaria Sacc etc.) and bacterial disease (as kiwi berry bacterial canker) can be divided into, wherein comparatively common with fungal disease.Also canker, Peptic Ulcers, blight, gummosis etc. can be divided into according to its symptom difference.These trunk diseases usually cause deadwood, extremely set, and serious even causes the garden of ruining; In addition, the tree vigo(u)r caused owing to falling ill is weak often has a strong impact on output and fruit quality.
Due to remarkable in economical benefits, fruit industry is the important agriculture mainstay industry of China always.But, for many years due to big area contiguous plant, kind is single, partially to fertilize and local climate disaster the problem such as to take place frequently, result in the diseases of branches of fruit trees such as canker, Peptic Ulcers and continue big area generation, as canker of apple fruit, kiwi berry bacterial canker etc., become the subject matter having had a strong impact on industry Sustainable development.At present, the method striking off administration of antibiotics (as Streptomycin sulphate, kasugamycin etc.) and broad spectrum chemical bactericide (as octicin solution, tebuconazole etc.) after tree body focus is still mainly adopted to the prevention and therapy of such disease both at home and abroad.But chemical bactericide exists the problems such as drug effect difference, residual quantity be large, and excessive abuse causes environmental pollution, Pesticide Residues in Fruit exceeds standard, degradation problem worsens increasingly under quality.In addition, antibiotic excessive use also makes the drug resistance problems of pathogenic bacteria day by day remarkable.And after tree body lesion scraping, wound healing is slow, and tree vigo(u)r is difficult to reply in a short time, thus has a strong impact on generation of bearing fruit.Therefore, the demand for nontoxic, efficient, eco-friendly novel pesticide control is further urgent.
Ozone (O 3) be oxygen (O 2) allotropic substance, there is extremely strong oxidisability, ozone molecule can produce oxidizing reaction with the tryptophan residue in different kinds of proteins aminoacid sequence in bacterial cell membrane and the carbon-carbon double bond in unsaturated fatty acids and destroy its structure, thus plays germicidal action.Research in recent years finds, containing unsaturated fatty acidss (65-90%) such as abundant oleic acid and linolic acid in vegetables oil, its grease has significant killing action for all kinds of pathogenic micro-organisms such as bacterium, fungi and viruses after ozonation treatment.
Secondly, the active oxygen be rich in saturated ozonize vegetables oil is as peroxidized anion free radical (O 2-), hydroxy radical qiao (OH), hydrogen peroxide (H 2o 2) etc. material be the important component part of cell signaling and regulation and control, the signal transduction path of plant cell defense reaction and the expression of resistance related gene can be started.Meanwhile, active oxygen by the growth of inducing the formation of secondary cell wall to accelerate callus, thus can also promote the fruit tree wound healing after striking off focus.
But, existing saturated ozonize vegetables oil composition is comparatively single, plant is only played to the effect of sterilization, and plant needs a large amount of nutrients can only to be obtained by additive methods such as fertilisings when wound healing, plant cannot obtain nutrient in the very first time, this reduces the speed of plant wound heeling.
Summary of the invention
The object of this invention is to provide a kind of note dry medicament for preventing and treating diseases of branches of fruit trees, solving the problem that drug effect is poor, residual quantity is large that existing note dry medicament exists because using chemical bactericide, can fruit tree wound healing be promoted simultaneously, accelerate tree vigo(u)r and recover; Another object of the present invention is to provide the preparation method of above-mentioned note dry medicament, solves the problem of existing note dry medicament only containing single bacteriocidal substance.
The technical solution adopted in the present invention is: a kind of note dry medicament for preventing and treating diseases of branches of fruit trees, by volume per-cent is than composed of the following components: bacteriocidal substance 0.5% ~ 10%, tensio-active agent 0.025% ~ 0.1%, nutritive substance 0.1% ~ 2%, permeate agent 0.01% ~ 0.1%, water 89% ~ 99%, the content summation of above component is 100%.
Feature of the present invention is also,
Nutritive substance is the mixture of Repone K, potassium primary phosphate, bicarbonate of ammonia and calcium superphosphate composition, and Repone K, potassium primary phosphate, mass ratio between bicarbonate of ammonia and calcium superphosphate are 1:1 ~ 3:2 ~ 8:0.1 ~ 0.5.
Bacteriocidal substance is ozonize plant-sourced unsaturated fatty acids.
The IP value (amount containing active oxygen in per kilogram vegetables oil) of ozonize plant-sourced unsaturated fatty acids is 750 ~ 850mmolKg -1, viscosity is 300 ~ 450mPas, and acid number (in and the milligram number of potassium hydroxide needed for 1mg sample be 1U) is not less than 35U.
Plant-sourced unsaturated fatty acids is mixture or oleic acid, linolic acid, the linolenic mixture of a kind of in oleic acid, linolic acid, linolenic acid or any two kinds.
In mixture, the quality of unsaturated fatty acids is not less than 75% of grease total mass.
Another technical scheme of the present invention is: the preparation method of above-mentioned note dry medicament, specifically carries out according to following steps:
Step 1, takes raw material,
By volume per-cent takes following component: bacteriocidal substance 0.5% ~ 10%, tensio-active agent 0.025% ~ 0.1%, nutritive substance 0.1% ~ 2%, permeate agent 0.01% ~ 0.1%, water 89% ~ 99%, and the content summation of above component is 100%;
Step 2, raw material mixes,
Bacteriocidal substance step 1 taken, tensio-active agent, nutritive substance, permeate agent are added to the water respectively, constantly stir until each component is dissolved completely and mixed, obtained liquid stoste;
Step 3, packing liquid,
The liquid stoste that step 2 is obtained is filled in the Plastic Bottle or plastics bag that capacity is 100 ~ 2000mL, sealing, obtained note dry medicament.
The invention has the beneficial effects as follows,
1) a kind of note dry medicament for preventing and treating diseases of branches of fruit trees, using the product of plant-sourced unsaturated fatty acids after saturated ozonation treatment as active sterilization component, and the nutritive substance needed for supplementary plant materials growth is organically combined, plant wound heeling can be promoted while killing pathogenic bacteria, accelerate tree vigo(u)r to recover, further, this note dry medicament has safety non-toxic, raw material sources feature widely, and suit large area to popularize application.
2) a kind of preparation method of the note dry medicament for preventing and treating diseases of branches of fruit trees, by bacteriocidal substance, tensio-active agent, nutritive substance, permeate agent being added to the water respectively and mixing, after encapsulation, plurality of active ingredients is fully merged, various raw material sources is extensive, obtained note dry medicament using method is easy, and drug effect is remarkable, is applicable to large-scale promotion and uses.
Embodiment
Below in conjunction with embodiment, the present invention is described in detail:
A kind of note dry medicament for preventing and treating diseases of branches of fruit trees of the present invention, by volume per-cent is than composed of the following components: bacteriocidal substance 0.5% ~ 10%, tensio-active agent 0.025% ~ 0.1%, nutritive substance 0.1% ~ 2%, permeate agent 0.01% ~ 0.1%, water 89% ~ 99%, the content summation of above component is 100%, wherein, nutritive substance is the mixture of Repone K, potassium primary phosphate, bicarbonate of ammonia and calcium superphosphate composition, and Repone K, potassium primary phosphate, mass ratio between bicarbonate of ammonia and calcium superphosphate are 1:1 ~ 3:2 ~ 8:0.1 ~ 0.5; Bacteriocidal substance is ozonize plant-sourced unsaturated fatty acids, and IP value is 750 ~ 850mmolKg -1viscosity is 300 ~ 450mPas, acid number is not less than 35U, further, plant-sourced unsaturated fatty acids is mixture or oleic acid, linolic acid, the linolenic mixture of a kind of in oleic acid, linolic acid, linolenic acid or any two kinds, and the quality of unsaturated fatty acids is not less than 75% of grease total mass.
The surfactant that the present invention is used, as long as the nonionic surfactant that can use in common gardening preparation is just not particularly limited.Comprising sugar ester type tensio-active agents such as act sorbitan-fatty acid ester (C12-18), sucrose fatty esters; The fatty acid ester type tensio-active agents such as POE fatty acid ester (C12-18), POE resin acid esters, POE fatty acid diesters (C12-18); The alcohol type tensio-active agents such as POE alkyl oxide (C12-18); The alkylbenzene phenolic tensio-active agents such as POE alkyl (C8-12) phenyl ether, POE dialkyl group (C8-12) phenyl ether; The multi-aromatic ring type tensio-active agents such as POA benzyl phenyl (or phenyl) ether, POA styryl phenyl (or phenyl) ether; POE ether and the silicon system such as ester type silicon and fluorine system tensio-active agent, fluorine system tensio-active agent etc.
The surfactant that the present invention is used, as long as the pesticide penetrating agent that can use in common gardening preparation is just not particularly limited.Such as, polysiloxane polyoxyethylene ethers, poly alkyl alcohol oxyalkyl ethers, alcohol ether succsinic acid salt etc.
The preparation method of a kind of note dry medicament for preventing and treating diseases of branches of fruit trees of the present invention, specifically carry out according to following steps: by volume per-cent takes following component: bacteriocidal substance 0.5% ~ 10%, tensio-active agent 0.025% ~ 0.1%, nutritive substance 0.1% ~ 2%, permeate agent 0.01% ~ 0.1%, water 89% ~ 99%, the content summation of above component is 100%; The bacteriocidal substance taken, tensio-active agent, nutritive substance, permeate agent are added to the water respectively, constantly stir until each component is dissolved completely and mixed, obtained liquid stoste; Obtained liquid stoste is filled in the Plastic Bottle or plastics bag that capacity is 100 ~ 2000mL, sealing, obtained note dry medicament.
Embodiment 1
By volume per-cent takes following component: bacteriocidal substance 0.5%, tensio-active agent 0.025%, nutritive substance 0.465%, permeate agent 0.01%, water 99%, and the content summation of above component is 100%; The bacteriocidal substance taken, tensio-active agent, nutritive substance, permeate agent are added to the water respectively, constantly stir until each component is dissolved completely and mixed, obtained liquid stoste; Obtained liquid stoste is filled in the Plastic Bottle or plastics bag that capacity is 100mL, sealing, obtained note dry medicament.
Embodiment 2
By volume per-cent takes following component: bacteriocidal substance 10%, tensio-active agent 0.1%, nutritive substance 0.8%, permeate agent 0.1%, water 89%, and the content summation of above component is 100%; The bacteriocidal substance taken, tensio-active agent, nutritive substance, permeate agent are added to the water respectively, constantly stir until each component is dissolved completely and mixed, obtained liquid stoste; Obtained liquid stoste is filled in the Plastic Bottle or plastics bag that capacity is 500mL, sealing, obtained note dry medicament.
Embodiment 3
By volume per-cent takes following component: bacteriocidal substance 4.8%, tensio-active agent 0.05%, nutritive substance 0.1%, permeate agent 0.05%, water 95%, and the content summation of above component is 100%; The bacteriocidal substance taken, tensio-active agent, nutritive substance, permeate agent are added to the water respectively, constantly stir until each component is dissolved completely and mixed, obtained liquid stoste; Obtained liquid stoste is filled in the Plastic Bottle or plastics bag that capacity is 1000mL, sealing, obtained note dry medicament.
Embodiment 4
By volume per-cent takes following component: bacteriocidal substance 6.9%, tensio-active agent 0.05%, nutritive substance 2%, permeate agent 0.05%, water 97%, and the content summation of above component is 100%; The bacteriocidal substance taken, tensio-active agent, nutritive substance, permeate agent are added to the water respectively, constantly stir until each component is dissolved completely and mixed, obtained liquid stoste; Obtained liquid stoste is filled in the Plastic Bottle or plastics bag that capacity is 2000mL, sealing, obtained note dry medicament.

Claims (7)

1. one kind for preventing and treating the note dry medicament of diseases of branches of fruit trees, it is characterized in that, by volume per-cent is than composed of the following components: bacteriocidal substance 0.5% ~ 10%, tensio-active agent 0.025% ~ 0.1%, nutritive substance 0.1% ~ 2%, permeate agent 0.01% ~ 0.1%, water 89% ~ 99%, the content summation of above component is 100%.
2. a kind of note dry medicament for preventing and treating diseases of branches of fruit trees according to claim 1, it is characterized in that, described nutritive substance is the mixture of Repone K, potassium primary phosphate, bicarbonate of ammonia and calcium superphosphate composition, and Repone K, potassium primary phosphate, mass ratio between bicarbonate of ammonia and calcium superphosphate are 1:1 ~ 3:2 ~ 8:0.1 ~ 0.5.
3. a kind of note dry medicament for preventing and treating diseases of branches of fruit trees according to claim 1 and 2, is characterized in that, described bacteriocidal substance is ozonize plant-sourced unsaturated fatty acids.
4. a kind of note dry medicament for preventing and treating diseases of branches of fruit trees according to claim 3, is characterized in that, the IP value of described ozonize plant-sourced unsaturated fatty acids is 750 ~ 850mmolKg -1, viscosity is 300 ~ 450mPas, and acid number is not less than 35U.
5. a kind of note dry medicament for preventing and treating diseases of branches of fruit trees according to claim 3, it is characterized in that, described plant-sourced unsaturated fatty acids is mixture or oleic acid, linolic acid, the linolenic mixture of a kind of in oleic acid, linolic acid, linolenic acid or any two kinds.
6. a kind of note dry medicament for preventing and treating diseases of branches of fruit trees according to claim 5, is characterized in that, in described mixture, the quality of unsaturated fatty acids is not less than 75% of grease total mass.
7. for preventing and treating a preparation method for the note dry medicament of diseases of branches of fruit trees, it is characterized in that, specifically carrying out according to following steps:
Step 1, takes raw material,
By volume per-cent takes following component: bacteriocidal substance 0.5% ~ 10%, tensio-active agent 0.025% ~ 0.1%, nutritive substance 0.1% ~ 2%, permeate agent 0.01% ~ 0.1%, water 89% ~ 99%, and the content summation of above component is 100%;
Step 2, raw material mixes,
Bacteriocidal substance step 1 taken, tensio-active agent, nutritive substance, permeate agent are added to the water respectively, constantly stir until each component is dissolved completely and mixed, obtained liquid stoste;
Step 3, packing liquid,
The liquid stoste that step 2 is obtained is filled in the Plastic Bottle or plastics bag that capacity is 100 ~ 2000mL, sealing, obtained note dry medicament.
CN201510823693.9A 2015-11-24 2015-11-24 Trunk-injection medicament for controlling branch and trunk diseases of fruit trees, and preparation method for trunk-injection medicament Pending CN105399501A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06305921A (en) * 1993-04-27 1994-11-01 Bisuta:Kk Plant growth regulator treated with active oxygen group and production and use thereof
CN101218927A (en) * 2007-12-13 2008-07-16 泰安市泰山林业科学研究院 Medicament for preventing and controlling jujube witches broom
CN101616579A (en) * 2007-02-23 2009-12-30 考格尼斯知识产权管理有限责任公司 At least comprise a kind of Biocidal composition based on oleic acid or linoleic dialkyl amide
CN101743989A (en) * 2009-12-30 2010-06-23 北京富力特农业科技有限责任公司 Insecticide injection composition
CN103430797A (en) * 2013-08-13 2013-12-11 陕西省微生物研究所 Method for preventing and controlling fungal diseases of cucumbers

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06305921A (en) * 1993-04-27 1994-11-01 Bisuta:Kk Plant growth regulator treated with active oxygen group and production and use thereof
CN101616579A (en) * 2007-02-23 2009-12-30 考格尼斯知识产权管理有限责任公司 At least comprise a kind of Biocidal composition based on oleic acid or linoleic dialkyl amide
CN101218927A (en) * 2007-12-13 2008-07-16 泰安市泰山林业科学研究院 Medicament for preventing and controlling jujube witches broom
CN101743989A (en) * 2009-12-30 2010-06-23 北京富力特农业科技有限责任公司 Insecticide injection composition
CN103430797A (en) * 2013-08-13 2013-12-11 陕西省微生物研究所 Method for preventing and controlling fungal diseases of cucumbers

Non-Patent Citations (5)

* Cited by examiner, † Cited by third party
Title
李勃等: "臭氧化葵花油对植物病原真菌的抗性研究", 《中国生物防治学报》 *
李勃等: "臭氧防治苹果树腐烂病技术", 《西北园艺》 *
杨烨: "臭氧化油制备及其对苹果树腐烂病的防治效果研究", 《河北农业大学学报》 *
柯杨 等: "臭氧化植物油防治苹果腐烂病的研究简报", 《陕西农业科学》 *
马瑜等: "利用臭氧化油防治猕猴桃溃疡病新技术", 《果农之友》 *

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Application publication date: 20160316