CN104000275B - Spearmint essential oil microemulsion formula used for beverage anticorrosion and preparation method thereof - Google Patents
Spearmint essential oil microemulsion formula used for beverage anticorrosion and preparation method thereof Download PDFInfo
- Publication number
- CN104000275B CN104000275B CN201410206374.9A CN201410206374A CN104000275B CN 104000275 B CN104000275 B CN 104000275B CN 201410206374 A CN201410206374 A CN 201410206374A CN 104000275 B CN104000275 B CN 104000275B
- Authority
- CN
- China
- Prior art keywords
- essential oil
- food
- spearmint essential
- grade
- potassium sorbate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000341 volatile oil Substances 0.000 title claims abstract description 90
- 235000014749 Mentha crispa Nutrition 0.000 title claims abstract description 89
- 239000004530 micro-emulsion Substances 0.000 title claims abstract description 69
- 235000013361 beverage Nutrition 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 244000024873 Mentha crispa Species 0.000 title claims description 76
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 74
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 50
- 235000010241 potassium sorbate Nutrition 0.000 claims abstract description 47
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims abstract description 44
- 239000004302 potassium sorbate Substances 0.000 claims abstract description 44
- 229940069338 potassium sorbate Drugs 0.000 claims abstract description 44
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 36
- 239000012153 distilled water Substances 0.000 claims abstract description 27
- 244000078639 Mentha spicata Species 0.000 claims abstract 13
- 239000000203 mixture Substances 0.000 claims description 50
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 30
- 229920000053 polysorbate 80 Polymers 0.000 claims description 30
- 239000011259 mixed solution Substances 0.000 claims description 29
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 27
- 238000004321 preservation Methods 0.000 claims description 20
- 239000002994 raw material Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 5
- 230000008569 process Effects 0.000 claims description 4
- 235000013305 food Nutrition 0.000 abstract description 9
- 230000008901 benefit Effects 0.000 abstract description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 abstract 2
- 239000002211 L-ascorbic acid Substances 0.000 abstract 1
- 235000000069 L-ascorbic acid Nutrition 0.000 abstract 1
- 229960005070 ascorbic acid Drugs 0.000 abstract 1
- 238000003860 storage Methods 0.000 description 17
- 239000003795 chemical substances by application Substances 0.000 description 11
- 239000002245 particle Substances 0.000 description 10
- 239000006185 dispersion Substances 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- 235000019249 food preservative Nutrition 0.000 description 4
- 239000005452 food preservative Substances 0.000 description 4
- 230000036541 health Effects 0.000 description 4
- 230000000845 anti-microbial effect Effects 0.000 description 3
- 244000005700 microbiome Species 0.000 description 3
- CHHHXKFHOYLYRE-STWYSWDKSA-M potassium sorbate Chemical class [K+].C\C=C\C=C\C([O-])=O CHHHXKFHOYLYRE-STWYSWDKSA-M 0.000 description 3
- 239000003755 preservative agent Substances 0.000 description 3
- 230000002335 preservative effect Effects 0.000 description 3
- 238000001228 spectrum Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 239000008346 aqueous phase Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000004064 cosurfactant Substances 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 230000002269 spontaneous effect Effects 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- 235000019640 taste Nutrition 0.000 description 2
- FRXSZNDVFUDTIR-UHFFFAOYSA-N 6-methoxy-1,2,3,4-tetrahydroquinoline Chemical compound N1CCCC2=CC(OC)=CC=C21 FRXSZNDVFUDTIR-UHFFFAOYSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- YAEIKOFIOLLMBE-UHFFFAOYSA-L C(C=CC=CC)(=O)[O-].[K+].C([O-])(O)=O.[Na+] Chemical compound C(C=CC=CC)(=O)[O-].[K+].C([O-])(O)=O.[Na+] YAEIKOFIOLLMBE-UHFFFAOYSA-L 0.000 description 1
- 241001070941 Castanea Species 0.000 description 1
- 235000014036 Castanea Nutrition 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 206010016952 Food poisoning Diseases 0.000 description 1
- 208000019331 Foodborne disease Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 241000235648 Pichia Species 0.000 description 1
- 238000012356 Product development Methods 0.000 description 1
- 241000235342 Saccharomycetes Species 0.000 description 1
- 241000235346 Schizosaccharomyces Species 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000001857 anti-mycotic effect Effects 0.000 description 1
- 239000002543 antimycotic Substances 0.000 description 1
- 238000005842 biochemical reaction Methods 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000004033 diameter control Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000014105 formulated food Nutrition 0.000 description 1
- 235000015203 fruit juice Nutrition 0.000 description 1
- 239000007970 homogeneous dispersion Substances 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 239000003845 household chemical Substances 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 230000003362 replicative effect Effects 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 235000014214 soft drink Nutrition 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/42—Preservation of non-alcoholic beverages
- A23L2/44—Preservation of non-alcoholic beverages by adding preservatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
Description
Density | pH | Particle diameter | |
Control group | 1.0192 | 7.02 | 24.50 |
Storage 30d | 1.0254 | 6.66 | 20.05 |
Density | pH | Particle diameter (nm) | |
Control group | 1.012 | 8.56 | 1972 |
Storage 30d | 1.015 | 8.44 | 1711 |
Density | pH | Particle diameter (nm) | |
Control group | 0.998 | 8.89 | 1942 |
Storage 30d | 1.0621 | 8.55 | 1856 |
Density | pH | Particle diameter (nm) | |
Control group | 1.0327 | 7.47 | 25.63 |
Storage 30d | 1.0464 | 7.43 | 24.90 |
Density | pH | Particle diameter (nm) | |
Control group | 0.9982 | 8.29 | 54.23 |
Storage 30d | 1.0025 | 8.27 | 48.29 |
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201410206374.9A CN104000275B (en) | 2014-05-16 | 2014-05-16 | Spearmint essential oil microemulsion formula used for beverage anticorrosion and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201410206374.9A CN104000275B (en) | 2014-05-16 | 2014-05-16 | Spearmint essential oil microemulsion formula used for beverage anticorrosion and preparation method thereof |
Publications (2)
Publication Number | Publication Date |
---|---|
CN104000275A CN104000275A (en) | 2014-08-27 |
CN104000275B true CN104000275B (en) | 2015-07-22 |
Family
ID=51361399
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201410206374.9A Active CN104000275B (en) | 2014-05-16 | 2014-05-16 | Spearmint essential oil microemulsion formula used for beverage anticorrosion and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN104000275B (en) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108391768A (en) * | 2017-02-07 | 2018-08-14 | 三得利控股株式会社 | Transparent beverage containing spearmint extract |
CN107897870A (en) * | 2017-11-23 | 2018-04-13 | 广东工业大学 | A kind of plants essential oil microemulsion and preparation method thereof |
CN108029753A (en) * | 2017-12-20 | 2018-05-15 | 上海应用技术大学 | A kind of clove oil microemulsion fresh-keeping for fresh-cut fruit and vegetable and preparation method |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106070202A (en) * | 2006-02-15 | 2016-11-09 | 博塔诺凯普有限公司 | The application of microencapsulated essential oils |
CN101810361A (en) * | 2010-01-05 | 2010-08-25 | 江南大学 | Microemulsion edible antistaling agent product and preparation method |
CN102166254A (en) * | 2011-04-06 | 2011-08-31 | 西北农林科技大学 | Oil-in-water type spearmint oil nano emulsion and method for preparing same |
CN102511511B (en) * | 2011-12-09 | 2014-07-09 | 江南大学 | Nano-antibacterial emulsion containing mint oil and preparation method thereof |
-
2014
- 2014-05-16 CN CN201410206374.9A patent/CN104000275B/en active Active
Also Published As
Publication number | Publication date |
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CN104000275A (en) | 2014-08-27 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CP03 | Change of name, title or address |
Address after: 200000 No. 120-121, Xuhui District, Shanghai, Caobao Road Patentee after: Shanghai Institute of Technology Address before: 200235 Xuhui District, Caobao Road, No. 120, Patentee before: Shanghai Institute of Technology |
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CP03 | Change of name, title or address | ||
TR01 | Transfer of patent right |
Effective date of registration: 20170927 Address after: 215100 Taiping Road, Taiping Street, Suzhou, Jiangsu, Xiangcheng District (Taiping Industrial Park) Patentee after: Suzhou Qingxin Health Technology Co. Ltd. Address before: 200000 No. 120-121, Xuhui District, Shanghai, Caobao Road Patentee before: Shanghai Institute of Technology |
|
TR01 | Transfer of patent right | ||
CB03 | Change of inventor or designer information |
Inventor after: Mao Jianlin Inventor before: Wang Yifei Inventor before: Chen Shuo Inventor before: Zhang Binbin Inventor before: He Yan Inventor before: Liu Zhuzhen Inventor before: Liu Xiaoyu |
|
CB03 | Change of inventor or designer information |