CN105371981A - Inner wall-silver plated and liquid crystal-filled hollow optical fiber surface plasmon resonance temperature sensor - Google Patents
Inner wall-silver plated and liquid crystal-filled hollow optical fiber surface plasmon resonance temperature sensor Download PDFInfo
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- CN105371981A CN105371981A CN201510817418.6A CN201510817418A CN105371981A CN 105371981 A CN105371981 A CN 105371981A CN 201510817418 A CN201510817418 A CN 201510817418A CN 105371981 A CN105371981 A CN 105371981A
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Abstract
The invention provides an inner wall-silver plated and liquid crystal-filled hollow optical fiber surface plasmon resonance temperature sensor and belongs to the optical fiber sensing technical field. According to the structure of the sensor, the interior of a hollow glass optical fiber is plated with silver, and the silver-plated hollow glass optical fiber is filled with liquid crystal; the inner diameter of the hollow glass optical fiber ranges from 300 microns to 500 microns, the numerical aperture of the hollow glass optical fiber is not lower than 0.27, and the length of the hollow glass optical fiber ranges from 30 mm to 50 mm; sensitization treatment is performed on the inner wall of the hollow glass optical fiber, and a 45nm-to 80nm uniform silver film is formed in the optical fiber through adopting a liquid phase chemical deposition method, and therefore, a sensing layer of surface plasmon resonance can be formed; and the hollow optical fiber is filled with thermotropic nematic liquid crystal, and plastic-clad multimode optical fibers are coupled to the ports of the optical fiber respectively, and end sealing processing is realized. With the inner wall-silver plated and liquid crystal-filled hollow optical fiber surface plasmon resonance temperature sensor adopted, subtle temperature changes can be dynamically monitored in real time. The inner wall-silver plated and liquid crystal-filled hollow optical fiber surface plasmon resonance temperature sensor is suitable for long-distance transmission. According to the inner wall-silver plated and liquid crystal-filled hollow optical fiber surface plasmon resonance temperature sensor, special inner wall silver plating technology is adopted, and the hollow optical fiber is filled with the thermotropic liquid crystal, and therefore, the oxidation of the external silver layer of the solid optical fiber surface plasma resonance sensor can be avoided.
Description
Technical field
The invention belongs to technical field of optical fiber sensing, the liquid crystal relating to the silver-plated formula of a kind of inwall fills hollow optic fibre surface plasma body resonant vibration temperature sensor.
Background technology
Current temperature sensor many employings thermistor and thermopair are as sensing element, and such transducer sensitivity is low, measuring error large, be subject to environmental interference, is difficult in field widespread uses such as biochemistry; And fibre optic temperature sensor relies on other sensitive elements to realize modulation function mostly, there is optical fiber and sensing head coupled problem in such sensor, and complex structure is too responsive to disturbances such as mechanical vibration; Though there is at present the fibre optic temperature sensor based on Surface Plasmon Resonance Technology, but adopt the reflective probe structure of solid core fibres, complex structure, response time are long, and the degree of accuracy of detection is also poor more; And though filling liquid crystal photonic crystal fiber temperature sensor has report, but due to the inner aperture of photonic crystal fiber narrow and small, it is large to fill difficulty, and the impact of the factors such as cost of manufacture is high is difficult to widespread use.
Summary of the invention
The liquid crystal that the object of this invention is to provide the silver-plated formula of a kind of inwall fills hollow optic fibre surface plasma body resonant vibration temperature sensor, can realize the change of real-time dynamic monitoring slight temperature, be applicable to long range propagation; Adopt the silver-plated technical matters of special inwall and thermotropic liquid crystal is packed into hollow glass optical fiber, avoiding the oxidation of the outside silver layer of solid core fibres surface plasma resonance sensor; Adopt optical patchcord signal transmission, avoid the labyrinth of prism coupled type surface plasma resonance sensor, realize long apart from anti-interference transmission; By the characteristic that liquid-crystal refractive-index responds temperature variation, realize the real-time response process of sensor for temperature.
The technical solution adopted in the present invention is:
The silver-plated liquid crystal of a kind of inwall fills hollow optic fibre surface plasma body resonant vibration temperature sensor, and this sensor adopts hollow glass optical fiber structure, and the inside of hollow glass optical fiber is silver-plated, at silver-plated hollow glass inside of optical fibre filling liquid crystal; Adopt the hollow glass inside of optical fibre deposition 45-80nm silverskin of liquid-phase chemistry deposition technique after inwall sensitized treatment, form the sensing layer of surface plasma body resonant vibration; Again thermic nematic liquid crystal is packed in hollow glass optical fiber, at two port coupling plastic envelope multimode optical fibers of hollow glass optical fiber, to two-port termination process; Wherein the core diameter of plastic envelope multimode optical fiber is consistent with hollow glass optical fiber internal diameter; The internal diameter of hollow glass optical fiber is 300 μm-500 μm, numerical aperture be not less than 0.27 and length be 30mm-50mm.
Multimode optical fiber wire jumper is adopted to carry out the coupled transfer of signal.The wide spectrum optical that optical fiber source is launched fills hollow optic fibre surface plasma body resonant vibration temperature sensor through a liquid crystal entering the silver-plated formula of inwall of optical patchcord, with inwall silver plating film interface excitation surface plasma body resonant vibration in sensing passage liquid crystal, transducing signal is transferred to the sensor other end by inside liquid crystal, is coupled on spectrometer CCD detects through wire jumper one.
Effect of the present invention and benefit are:
Adopt comparatively simple liquid-phase chemistry deposition technique to achieve the silver-plated technology of inwall of hollow optic fibre, changed by regulating and controlling temperature, realize the response of liquid-crystal refractive-index for temperature, thus realize the quick response of surface plasma body resonant vibration signal.Small and exquisite simple, the stable performance of this sensor construction, technique is simple, easy to make and cost is lower, and has higher sensitivity to sensing detection.Adopt liquid crystal temperature sensing, the environmental interference factor impacts such as magnetic field can be got rid of, realize the temperature-responsive real-time of long distance.
Accompanying drawing explanation
Accompanying drawing is that the liquid crystal of the silver-plated formula of inwall fills hollow optic fibre surface plasma body resonant vibration arrangement of temperature sensor schematic diagram.
In figure: 1 plastic envelope multimode optical fiber; 2 silverskin; 3 liquid crystal; 4 hollow glass optical fiber.
Embodiment
The specific embodiment of the present invention is described in detail below in conjunction with technical scheme and accompanying drawing.
The present invention is using surface plasma body resonant vibration as sensing principle, and the generation of this effect depends on wide spectrum light source, and object is the sensing detection realizing wavelength-modulated mode in a fiber.Liquid crystal, as sensor information, has the temperature variant characteristic of refractive index; By the response of surface plasmon resonance effect for refractive index, the situation of change of temperature of reaction.In order to strengthen signal intensity, optimize sensing capabilities, the hollow optic fibre making sensor selects large diameter kapillary.Hollow optic fibre optical fiber internal diameter 500 μm, external diameter 700 μm, numerical aperture 0.37 that the present invention adopts.Plastic envelope multimode optical fiber fibre core, covering, coat diameter are respectively 500 μm, 530 μm, 830 μm, numerical aperture 0.37.Liquid crystal adopts row to thermotropic liquid crystal 4'-n-pentyl-4-cyanobiphenyl (5CB).
Preparation process of the present invention is as follows:
(1) first get the hollow glass optical fiber of one section of 50mm, polished by two of hollow glass optical fiber end face sand paper, after the cleaning of ethanol, acetone, dichloromethane solution successively repeated ultrasonic, nitrogen dries up for subsequent use.
(2) by hollow glass Fiber connection on peristaltic pump, pass into sensitizing solution and deionized water successively; Liquid deposition film plating process is adopted silverskin to be deposited on hollow glass optical fiber inwall; Time and the temperature of accurate control silver mirror reaction ensure that coating film thickness is about 50nm.
(3) get two sections of 80mm plastic envelope multimode optical fibers, peel off two ends respectively and obtain coat, then polished by the end face sand paper of optical fiber, after the cleaning of ethanol, acetone, dichloromethane solution successively repeated ultrasonic, nitrogen dries up for subsequent use.
(4) liquid crystal is packed into by peristaltic pump and is coated with in the hollow glass optical fiber of silverskin, the plastic envelope multimode optical fiber handled well is accessed respectively termination process after two-port, prevents liquid crystal from flowing out.
(5) said structure is accessed the coupled transfer that multimode optical fiber wire jumper carries out signal, one end connects wide spectrum light source, and other end connection spectrometer CCD detects.
Claims (3)
1. liquid crystal fills the silver-plated hollow optic fibre surface plasma body resonant vibration temperature sensor of inwall, it is characterized in that, this sensor adopts hollow glass optical fiber structure, and the inside of hollow glass optical fiber is silver-plated, at silver-plated hollow glass inside of optical fibre filling liquid crystal.
2. a kind of liquid crystal according to claim 1 fills the silver-plated hollow optic fibre surface plasma body resonant vibration temperature sensor of inwall, it is characterized in that, adopt the hollow glass inside of optical fibre deposition 45-80nm silverskin of liquid-phase chemistry deposition technique after inwall sensitized treatment, form the sensing layer of surface plasma body resonant vibration; Again thermic nematic liquid crystal is packed in hollow glass optical fiber, at two port coupling plastic envelope multimode optical fibers of hollow glass optical fiber, to two-port termination process; Wherein the core diameter of plastic envelope multimode optical fiber is consistent with hollow glass optical fiber internal diameter.
3. a kind of liquid crystal according to claim 1 and 2 fills the silver-plated hollow optic fibre surface plasma body resonant vibration temperature sensor of inwall, it is characterized in that, the internal diameter of hollow glass optical fiber is 300 μm-500 μm, the numerical aperture of hollow glass optical fiber is not less than 0.27, and the length of hollow glass optical fiber is 30mm-50mm.
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CN106052903A (en) * | 2016-08-24 | 2016-10-26 | 哈尔滨工业大学(威海) | Ultra-small-size optical fiber temperature sensing probe and preparation method thereof |
CN106679846A (en) * | 2016-12-29 | 2017-05-17 | 中国农业大学 | Side-polished polymer temperature sensing fiber and manufacturing method thereof |
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CN107255532A (en) * | 2017-05-08 | 2017-10-17 | 东南大学 | A kind of SMD luminance temperature of metal phasmon and infrared ray sensor |
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CN111006716A (en) * | 2019-11-14 | 2020-04-14 | 东北大学 | Biomolecule and temperature double-parameter optical fiber sensor and manufacturing method and application thereof |
CN111220296A (en) * | 2020-01-21 | 2020-06-02 | 金华伏安光电科技有限公司 | Microcavity type temperature sensor and system |
CN112432715A (en) * | 2020-11-19 | 2021-03-02 | 哈尔滨理工大学 | SPR (surface plasmon resonance) -based D-type photonic crystal fiber temperature sensing device and method |
JP2021131263A (en) * | 2020-02-18 | 2021-09-09 | 公立大学法人大阪 | Sensor, manufacturing method of sensor, measurement system and measurement method of pressure or temperature |
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CN106052903A (en) * | 2016-08-24 | 2016-10-26 | 哈尔滨工业大学(威海) | Ultra-small-size optical fiber temperature sensing probe and preparation method thereof |
CN106679846A (en) * | 2016-12-29 | 2017-05-17 | 中国农业大学 | Side-polished polymer temperature sensing fiber and manufacturing method thereof |
CN106840410A (en) * | 2017-01-23 | 2017-06-13 | 京东方科技集团股份有限公司 | A kind of temperature sensor and its temperature checking method |
CN107255532B (en) * | 2017-05-08 | 2019-04-30 | 东南大学 | A kind of metal phasmon patch type luminance temperature and infrared sensor |
CN107238448A (en) * | 2017-05-08 | 2017-10-10 | 东南大学 | A kind of SMD temperature of metal phasmon and infrared ray sensor |
CN107255532A (en) * | 2017-05-08 | 2017-10-17 | 东南大学 | A kind of SMD luminance temperature of metal phasmon and infrared ray sensor |
CN107238448B (en) * | 2017-05-08 | 2019-06-21 | 东南大学 | A kind of metal phasmon patch type temperature and infrared sensor |
CN107525605A (en) * | 2017-10-26 | 2017-12-29 | 深圳大学 | A kind of temperature sensor based on surface plasma body resonant vibration and preparation method thereof |
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CN109115363A (en) * | 2018-10-15 | 2019-01-01 | 辽宁省计量科学研究院 | A kind of fibre optic temperature sensor based on surface plasma body resonant vibration and strain compensation |
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Application publication date: 20160302 |