CN105349906A - Centrifugal casting method of super duplex stainless steel horizontal screw centrifugal separator drum - Google Patents

Centrifugal casting method of super duplex stainless steel horizontal screw centrifugal separator drum Download PDF

Info

Publication number
CN105349906A
CN105349906A CN201510724807.4A CN201510724807A CN105349906A CN 105349906 A CN105349906 A CN 105349906A CN 201510724807 A CN201510724807 A CN 201510724807A CN 105349906 A CN105349906 A CN 105349906A
Authority
CN
China
Prior art keywords
stainless steel
duplex stainless
super
centrifugal casting
separator drum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201510724807.4A
Other languages
Chinese (zh)
Other versions
CN105349906B (en
Inventor
屈志
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SICHUAN WEIZHEN PETROCHEMICAL EQUIPMENT Co Ltd
Original Assignee
SICHUAN WEIZHEN PETROCHEMICAL EQUIPMENT Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SICHUAN WEIZHEN PETROCHEMICAL EQUIPMENT Co Ltd filed Critical SICHUAN WEIZHEN PETROCHEMICAL EQUIPMENT Co Ltd
Priority to CN201510724807.4A priority Critical patent/CN105349906B/en
Publication of CN105349906A publication Critical patent/CN105349906A/en
Application granted granted Critical
Publication of CN105349906B publication Critical patent/CN105349906B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/58Ferrous alloys, e.g. steel alloys containing chromium with nickel with more than 1.5% by weight of manganese
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22DCASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
    • B22D13/00Centrifugal casting; Casting by using centrifugal force
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/0068Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for particular articles not mentioned below
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C33/00Making ferrous alloys
    • C22C33/04Making ferrous alloys by melting
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/42Ferrous alloys, e.g. steel alloys containing chromium with nickel with copper
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/44Ferrous alloys, e.g. steel alloys containing chromium with nickel with molybdenum or tungsten
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/001Austenite
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/005Ferrite
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

Abstract

The invention discloses a centrifugal casting method of a super duplex stainless steel horizontal screw centrifugal separator drum. The method comprises the following steps that a, the ratio of specific chemical components of a super duplex stainless steel material is designed according to the requirement for the strength of the drum; b, materials are selected; c, refining is performed; d, centrifugal casting is performed; e, heat treatment is performed; f, detection is performed; g, finished products are machined; and h, inspection is performed. Compared with the prior art, the corrosion resistance and mechanical strength of the material are improved, and the material cost is greatly lowered; due to the high-strength of the material, the wall thickness of the product can be decreased by about one third, and the material is saved; meanwhile, due to the fact that drum parts are used on the condition that the rotating speed reaches over 3000 r/min, the equipment energy consumption is greatly lowered after the weight of the parts is decreased, and more energy is saved during equipment operation. Due to the fact that the material is improved, the overall performance of a horizontal screw centrifugal separator is greatly improved, the manufacturing cost of the equipment is lowered, and maximization of the cost performance of the horizontal screw centrifugal machine parts is achieved.

Description

Super-duplex stainless steel crouches spiral shell centrifugal separator drum centrifugal casting process
Technical field
The present invention relates to a kind of centrifugal casting process, particularly relate to a kind of super-duplex stainless steel and to crouch spiral shell centrifugal separator drum centrifugal casting process.
Background technology
Sleeping spiral shell separating centrifuge manufacturing wishes constantly to promote the anti-deep-etching of key components and parts, physical strength and dynamic balance performance always, obtains high performance material.
Summary of the invention
Object of the present invention is just to provide one to solve the problems referred to above super-duplex stainless steel and crouches spiral shell centrifugal separator drum centrifugal casting process.
To achieve these goals, the technical solution used in the present invention is: a kind of super-duplex stainless steel crouches spiral shell centrifugal separator drum centrifugal casting process, and method steps is as follows,
A. the specific chemical composition proportion design to super-duplex stainless steel material is required according to barrate strength
According to Cr equivalent Creq, Ni equivalent Nieq experimental formula 1-1,1-2, primary design chemical composition,
Creq=Cr%+Mo%+1.5Si%+0.5Nb+0.5W formula 1-1
Nieq=Ni%+0.3Mn%+0.3Cu%+16 (C+N) formula 1-2
Carry out calculation level corrosion equivalent value PREw by formula 1-3, tentatively judge the corrosion resistance nature of material according to pitting attack value,
PREN=Cr%+3.3 (Mo%+0.5W)+16N formula 1-3
According to the chemical composition of above primary design referring again to the WRC-1992 phase component figure in Stainless Steel Alloy system, chemical composition component is finely tuned, make it final completely satisfied wherein α (ferrite) Phase Proportion to require to control 50% ~ 60%, other is γ (austenite) phase, and reaches the corrosion-resistant requirement of similar super-duplex stainless steel S32750 (SAF2507) same level of expection;
B. selection
Rationally prepared burden by the iron alloy of the carbon steel scrap and high-quality of selecting high-quality, and iron alloy is baked to more than 800 DEG C, guarantee crystal water to dry;
C. refining
Metallic substance in step b is smelted into molten steel through electric arc furnace or medium-frequency induction furnace, after tentatively reaching the chemical composition ranges in step a and tapping temperature arrive 1450 DEG C ~ 1700 DEG C after tapping, molten steel is blended into AOD furnace to be blown into oxygen and to carry out decarburization, desiliconization, and be heated to 1500 DEG C ~ 1700 DEG C temperature ranges, add lime again, fluorite is also blown into argon gas or nitrogen carries out refining, through slag making, skim, remove the S in molten steel, Si, inclusion and nitrogen, oxygen, obnoxious flavour, should again finely tune chemical composition in the process, refining reduction is carried out 1600 DEG C ~ 1700 DEG C temperature ranges, add reductive agent and carry out final deoxygenation by chromium in steel, the metallic reducings such as molybdenum are returned, finally adjust the material requirements of chemical composition to step a, according to the liquidus line calculating of this steel grade and the temperature losses of the process after tapping, and the centrifugal pipe weight of casting, specification size, calculate the best tapping temperature of refining furnace, tap after more qualified liquid steel temperature being adjusted to optimum temps,
D. rotational casting
By mechanical dimension's requirement of sleeping spiral shell centrifugal separator drum, design the type tube of centrifugal casting machine, by molten steel good for refining through centrifugal casting machine cast molding;
E. thermal treatment
Rotational casting shell heat treatment step through being up to the standards is heat-treated, and promotes material corrosion resistant and mechanical property;
F. detect;
G. processed finished products;
H. check.
As preferably, in step a, the chemical composition per-cent of described super-duplex stainless steel material is Cr20.0-27.0%, Ni0.5-3.00%, Mn5.0-13.00%, Mo0.5-4.0%, N0.20-0.70%, C≤0.03%, Si≤1.00%, Cu0.5-1.5%, P≤0.035%, S≤0.030%, W0.5-4.0%, surplus are Fe, by improving cheap element M n, N content, and significantly reduce the noble metal content such as Ni, W, Mo, Cu, the excellent properties basis reaching super-duplex stainless steel reduces material cost.
As preferably, in step b, high-quality iron alloy is ferrochrome, molybdenum-iron, metal nickel plate, metallic copper and tungsten.
As preferably, in step c, when carrying out refining reduction, the reductive agent added is ferrosilicon, silico-calcium or aluminium block.
As preferably, in step c, be ensure molten steel performance, the best tapping temperature of refining furnace is 1550 DEG C ~ 1800 DEG C.
As preferably, in steps d, the processing method of centrifugal casting machine cast molding is as follows, centrifugal casting machine type tube is toasted, opening centrifugal casting machine makes type tube reach 400r/min ~ 600r/min rotating speed, again type tube inwall is evenly sprayed into coating, allow its seasoning, then progressively improve centrifuge speed, then ladle molten steel is injected baked water bucket, and flow into type tube by water bucket, further adjustment rotating speed, to 700r/min ~ 2000r/min, after molten steel has watered, more progressively reduces rotating speed, until the complete cooling forming of foundry goods, then by the foundry goods demoulding.
As preferably, be 200 ~ 300 DEG C by the temperature of centrifugal casting machine type tube baking, now storing temperature the best.
As preferably, described in the paint thickness that sprays into control between 1mm ~ 3mm.
As preferably, in step e, under the temperature condition of 1030-1200 DEG C, carry out solution treatment.
As preferably, carry out cooling fast after solid solution with the precipitation reducing γ, π, χ second-phase.
Compared with prior art, the invention has the advantages that: the present invention is promoting the anticorrosive and physical strength of material, compare conventional stainless material as 316L, 2205, Novel super duplex stainless steel significantly reduces material cost, due to the high strength of material, makes product wall thickness can reduce about 1/3, save material, simultaneously because rotary drum component use under up to more than 3000r/min operating mode, after parts loss of weight, equipment energy consumption is significantly declined, equipment runs more energy-conservation.By the progress of material, promote increasing substantially of sleeping spiral shell centrifuge apparatus overall performance, reduced the manufacturing cost of equipment, achieved the maximization of horizontal screw centrifuge component cost performance.
Accompanying drawing explanation
Fig. 1 is the WRC-1992 phase component figure in Stainless Steel Alloy system.
Embodiment
The invention will be further described below.
Embodiment: a kind of super-duplex stainless steel crouches spiral shell centrifugal separator drum centrifugal casting process, and method steps is as follows,
A. the specific chemical composition proportion design to super-duplex stainless steel material is required according to barrate strength
For obtaining the best structure property of material, according to Cr equivalent (Creq), Ni equivalent (Nieq) experimental formula 1-1,1-2, primary design chemical composition,
Creq=Cr%+Mo%+1.5Si%+0.5Nb+0.5W formula 1-1
Nieq=Ni%+0.3Mn%+0.3Cu%+16 (C+N) formula 1-2
Carry out calculation level corrosion equivalent value PREw by formula 1-3, tentatively judge the corrosion resistance nature of material according to pitting attack value,
PREN=Cr%+3.3 (Mo%+0.5W)+16N formula 1-3
According to the chemical composition of above primary design referring again to the WRC-1992 phase component figure in Stainless Steel Alloy system as Fig. 1, chemical composition component is finely tuned, make it final completely satisfied wherein α (ferrite) Phase Proportion to require to control 50% ~ 60%, other is γ (austenite) phase, and reaches the corrosion-resistant requirement of similar super-duplex stainless steel S32750 (SAF2507) same level of expection;
This patent discloses a kind of chemical composition of Novel super two-phase stainless steel first at China, enterprise's steel grade code is: WZ-SX06, and it is as shown in table 1 that its chemical composition forms (%):
Element Cr Ni Mn Mo N C
Composition 20.0-27.0 0.5-2.0 5.0-13.0 0.5-2.0 0.20-0.70 ≤0.03
Element Si Cu P S W Fe
Composition ≤1.00 0.5-1.5 ≤0.035 ≤0.030 0.5-2.0 Surplus
Table 1 chemical composition is formed
This steel grade is compared to the traditional duplex stainless steel announced and other stainless steel trade mark, owing to having saved Ni, the precious metals such as Mo, material cost is declined to a great extent, to contrast with traditional stainless material 022cr17Ni14Mo2 (hereinafter referred to as 316L), material cost can save 20% ~ 40%, its corrosion resisting property especially resistance to Cl+ ion etching performance is much more excellent than 316L and intermediate duplex stainless steel 022cr25Ni5Mo3N (hereinafter referred to as 2205), its corrosion resistance value PREN >=40 are equal to S32750 (SAF2507), all be better than intermediate duplex stainless steel 2205 and austenitic stainless steel 316 L under many circumstances, its mechanical performance indexs etc., also much larger than above two steel grades, therefore can reduce wall thickness, alleviate weight of equipment, also greatly save material cost in producing apparatus process.In a word, this steel grade is the Novel super two-phase stainless steel that a kind of comprehensive cost performance is very high.
B. selection
Again by selecting high-quality carbon steel scrap, and high-quality iron alloy is as ferrochrome, molybdenum-iron, metal nickel plate, metallic copper and tungsten etc., rationally prepares burden.Polluting molten steel for preventing the crystal water in alloy from entering in molten steel, iron alloy must be baked to more than 800 DEG C, and guarantee crystal water to dry;
C. refining
Metallic substance in step b is smelted into molten steel through electric arc furnace or medium-frequency induction furnace and tentatively reaches chemical composition ranges and tap after adjusting molten steel tapping temperature, best tapping temperature is at 1450 DEG C ~ 1700 DEG C, molten steel is blended into AOD furnace (argon oxygen decarburizing furnace) to be blown into oxygen and to carry out decarburization, desiliconization etc., and by chemical heat heating molten steel to 1500 DEG C ~ 1700 DEG C temperature ranges, add lime, fluorite is also blown into argon gas or nitrogen etc. and carries out refining, through repeatedly slag making, skim, remove S in steel, the inclusiones such as Si and nitrogen, the obnoxious flavoures such as oxygen, should again finely tune chemical composition in the process, guarantee that the chemical composition after reducing reaches design requirements, refining reduction is carried out 1600 DEG C ~ 1700 DEG C temperature ranges, add ferrosilicon or silico-calcium, also aluminium block can be added or other reductive agent carries out final deoxygenation by chromium in steel, the metallic reducings such as molybdenum are returned, finally adjust chemical composition to material requirements, according to the liquidus line calculating of this steel grade and the temperature losses of the process after tapping, and the centrifugal pipe weight of casting, specification size, calculate the best tapping temperature of refining furnace, qualified liquid steel temperature is adjusted to optimum temps (1550 DEG C ~ 1800 DEG C) to tap afterwards and carry out rotational casting,
D. rotational casting
By mechanical dimension's requirement of sleeping spiral shell centrifugal separator drum, design the type tube of centrifugal casting machine, by molten steel good for refining through centrifugal casting machine cast molding, the processing method of centrifugal casting machine cast molding is as follows: centrifugal casting machine type tube is baked to 200 ~ 300 DEG C, opening centrifugal casting machine makes type tube reach 400r/min ~ 600r/min rotating speed, again type tube inwall is evenly sprayed into coating, conservative control paint thickness is between 1mm ~ 3mm, allow its seasoning certain hour, improve centrifuge speed to certain value, then ladle molten steel is injected baked water bucket, and flow into type tube by water bucket, according to product needed, further adjustment rotating speed is to 700r/min ~ 2000r/min, after molten steel has watered, progressively rotating speed is reduced again according to foundry goods cooling situation, until the complete cooling forming of foundry goods, then by the foundry goods demoulding,
E. thermal treatment
Rotational casting shell heat treatment step through being up to the standards is heat-treated, and promotes material corrosion resistant and mechanical property; This material carries out solution treatment under the temperature condition of 1030-1200 DEG C, to obtain the thermal treatment of supersaturated solid solution, after solid solution, suggestion carries out cooling fast with the precipitation reducing the second-phases such as γ, π, χ, and second-phase precipitation may have a negative impact to the performance of material.
F. detect
Mechanical property and corrosive nature detection are carried out to rotational casting shell;
G. processed finished products
Detect that qualified rotational casting shell is machined again reaches separation machinery stainless steel cylinder desired size through thermal treatment;
H. check
The stainless steel cylinder processed can mark packaging and dispatch from the factory after the testing proceduress such as nondestructive testing are qualified.
Rotational casting of the present invention become stainless steel cylinder blank as: the shape such as cylindrical tube, conic tube, is made into horizontal screw centrifuge component after machining and thermal treatment, as cone section rotary drum, straight-section rotary drum, spiral axis etc.
The sleeping spiral shell centrifugal separator drum that Novel super two-phase stainless steel of the present invention goes out through rotational casting explained hereafter, its mechanical property and other material contrast as shown in table 2:
The mechanical property of table 2 part centrifugal casting stainless material
Novel super duplex stainless steel material corrosion resistance of the present invention and other material contrast as follows:
1. stress corrosion fission (SCC) is as shown in table 3,
Table 3 stress corrosion fission (SCC) is compared
2. anti-spot corrosion and crevice corrosion performance
WZ-SX06 is according to ASTMG48A requirement, and in water bath with thermostatic control (22 ± 2 DEG C), soak 72h, weight loss is at 0.2 ~ 0.3mg; Corrosion rate is 0mpy.
3., for anti-local corrosion performance, such as spot corrosion and crevice corrosion, make it be improved by with the addition of elemental chromium, molybdenum and nitrogen.The corrosion of these modes usually occurs in the environment of chloride.In the white liquid of simulation, Novel super duplex stainless steel is tested.The results are shown in Table shown in 4 ~ table 8.
Table 4 testing liquid
The trade mark Weight loss, mg Corrosion rate, mpy
WZ-SX06 0.2,0.3 0.000,0.000
RA2205 0.3,0.7 0.000,0.000
304L 1.3,1.0 0.000,0.000
316L 4.5,3.4 0.002,0.002
2304 0.6,0.3 0.000,0.000
Liquid phase experiments under table 5 (90 DEG C) condition, 21 days
Table 61.5%FeCl36H2O+3%NaCl+20ml/LHACPh=2,24h
Solution Concentration WZ-SX04 316L RA2205
HCL 1% 55 30 85
H2SO4 10% 75 50 60
H2SO4 96.4% 30 45 25
The critical temperature that in table 7 sulfuric acid and hydrochloric acid, 0.127mm (millimeter/year) corrodes, DEG C
Solution Concentration WZ-SX06 316L RA2205
H3PO4 83% 35 65 50
HF 2%
WPA1 75% 30 <10 45
WPA2 75% <15 <10 60
The critical temperature that table 8 phosphoric acid 0.127mm (millimeter/year) corrodes, DEG C
Above exhaustive presentation is carried out to the super-duplex stainless steel provided by the present invention spiral shell centrifugal separator drum centrifugal casting process that crouches, apply specific case herein to set forth principle of the present invention and embodiment, the explanation of above embodiment just understands method of the present invention and core concept thereof for helping; Simultaneously, for one of ordinary skill in the art, according to thought of the present invention, all will change in specific embodiments and applications, to change of the present invention and improve will be possible, and design and the scope of accessory claim defined can not be exceeded, in sum, this description should not be construed as limitation of the present invention.

Claims (10)

1. super-duplex stainless steel crouches a spiral shell centrifugal separator drum centrifugal casting process, it is characterized in that: method steps is as follows,
A. the specific chemical composition proportion design to super-duplex stainless steel material is required according to barrate strength
According to Cr equivalent Creq, Ni equivalent Nieq experimental formula 1-1,1-2, primary design chemical composition,
Creq=Cr%+Mo%+1.5Si%+0.5Nb+0.5W formula 1-1
Nieq=Ni%+0.3Mn%+0.3Cu%+16 (C+N) formula 1-2
Carry out calculation level corrosion equivalent value PREw by formula 1-3, tentatively judge the corrosion resistance nature of material according to pitting attack value,
PREN=Cr%+3.3 (Mo%+0.5W)+16N formula 1-3
According to the chemical composition of above primary design referring again to the WRC-1992 phase component figure in Stainless Steel Alloy system, chemical composition component is finely tuned, make it finally to meet completely this proportion requirement of alpha ferrite phase and γ austenite phase, and corrosion-resistant requirement;
B. selection
Rationally prepared burden by the iron alloy of the carbon steel scrap and high-quality of selecting high-quality, and iron alloy is baked to more than 800 DEG C, guarantee crystal water to dry;
C. refining
Metallic substance in step b is smelted into molten steel through electric arc furnace or medium-frequency induction furnace, after tentatively reaching the chemical composition ranges in step a and tapping temperature arrive 1450 DEG C ~ 1700 DEG C after tapping, molten steel is blended into AOD furnace to be blown into oxygen and to carry out decarburization, desiliconization, and be heated to 1500 DEG C ~ 1700 DEG C temperature ranges, add lime again, fluorite is also blown into argon gas or nitrogen carries out refining, through slag making, skim, remove the S in molten steel, Si, inclusion and nitrogen, oxygen, obnoxious flavour, should again finely tune chemical composition in the process, refining reduction is carried out 1600 DEG C ~ 1700 DEG C temperature ranges, add reductive agent and carry out final deoxygenation by chromium in steel, the metallic reducings such as molybdenum are returned, finally adjust the material requirements of chemical composition to step a, according to the liquidus line calculating of this steel grade and the temperature losses of the process after tapping, and the centrifugal pipe weight of casting, specification size, calculate the best tapping temperature of refining furnace, tap after more qualified liquid steel temperature being adjusted to optimum temps,
D. rotational casting
By mechanical dimension's requirement of sleeping spiral shell centrifugal separator drum, design the type tube of centrifugal casting machine, by molten steel good for refining through centrifugal casting machine cast molding;
E. thermal treatment
Rotational casting shell heat treatment step through being up to the standards is heat-treated, and promotes material corrosion resistant and mechanical property;
F. detect;
G. processed finished products;
H. check.
2. super-duplex stainless steel according to claim 1 crouches spiral shell centrifugal separator drum centrifugal casting process, it is characterized in that: in step a, the chemical composition per-cent of described super-duplex stainless steel material is Cr20.0-27.0%, Ni0.5-2.0%, Mn5.0-13.00%, Mo0.5-2.0%, N0.20-0.70%, C≤0.03%, Si≤1.00%, Cu0.5-1.5%, P≤0.035%, S≤0.030%, W0.5-2.0%, surplus be Fe.
3. super-duplex stainless steel according to claim 1 crouches spiral shell centrifugal separator drum centrifugal casting process, and it is characterized in that: in step b, high-quality iron alloy is ferrochrome, molybdenum-iron, metal nickel plate, metallic copper and tungsten.
4. super-duplex stainless steel according to claim 1 crouches spiral shell centrifugal separator drum centrifugal casting process, and it is characterized in that: in step c, when carrying out refining reduction, the reductive agent added is ferrosilicon, silico-calcium or aluminium block.
5. super-duplex stainless steel according to claim 1 crouches spiral shell centrifugal separator drum centrifugal casting process, and it is characterized in that: in step c, the best tapping temperature of refining furnace is 1550 DEG C ~ 1800 DEG C.
6. super-duplex stainless steel according to claim 1 crouches spiral shell centrifugal separator drum centrifugal casting process, it is characterized in that: in steps d, the processing method of centrifugal casting machine cast molding is as follows, centrifugal casting machine type tube is toasted, opening centrifugal casting machine makes type tube reach 400r/min ~ 600r/min rotating speed, again type tube inwall is evenly sprayed into coating, allow its seasoning, then progressively centrifuge speed is improved, then ladle molten steel is injected baked water bucket, and flow into type tube by water bucket, further adjustment rotating speed is to 700r/min ~ 2000r/min, after molten steel has watered, progressively reduce rotating speed again, until the complete cooling forming of foundry goods, then by the foundry goods demoulding.
7. super-duplex stainless steel according to claim 6 crouches spiral shell centrifugal separator drum centrifugal casting process, it is characterized in that: the temperature of being toasted by centrifugal casting machine type tube is 200 ~ 300 DEG C.
8. super-duplex stainless steel according to claim 6 crouches spiral shell centrifugal separator drum centrifugal casting process, it is characterized in that: described in the paint thickness that sprays into control between 1mm ~ 3mm.
9. super-duplex stainless steel according to claim 1 crouches spiral shell centrifugal separator drum centrifugal casting process, it is characterized in that: in step e, under the temperature condition of 1030-1200 DEG C, carries out solution treatment.
10. super-duplex stainless steel according to claim 9 crouches spiral shell centrifugal separator drum centrifugal casting process, it is characterized in that: carry out cooling fast after solid solution with the precipitation reducing γ, π, χ second-phase.
CN201510724807.4A 2015-11-02 2015-11-02 The sleeping spiral shell centrifugal separator drum centrifugal casting process of super-duplex stainless steel Active CN105349906B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510724807.4A CN105349906B (en) 2015-11-02 2015-11-02 The sleeping spiral shell centrifugal separator drum centrifugal casting process of super-duplex stainless steel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510724807.4A CN105349906B (en) 2015-11-02 2015-11-02 The sleeping spiral shell centrifugal separator drum centrifugal casting process of super-duplex stainless steel

Publications (2)

Publication Number Publication Date
CN105349906A true CN105349906A (en) 2016-02-24
CN105349906B CN105349906B (en) 2018-08-10

Family

ID=55325965

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510724807.4A Active CN105349906B (en) 2015-11-02 2015-11-02 The sleeping spiral shell centrifugal separator drum centrifugal casting process of super-duplex stainless steel

Country Status (1)

Country Link
CN (1) CN105349906B (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105834390A (en) * 2016-06-14 2016-08-10 四川维珍石化设备有限公司 Method for carrying out vertical centrifugal casting on annular part of centrifugal machine through metal mold
CN107829029A (en) * 2017-11-10 2018-03-23 洛阳双瑞特种装备有限公司 A kind of ZG022Cr22Ni5Mo3N materials two phase stainless steel smelting process method
CN107900612A (en) * 2017-11-02 2018-04-13 江苏巨能机械有限公司 The processing technology of large-scale two phase stainless steel rotary drum disk
CN109468522A (en) * 2018-12-26 2019-03-15 无锡市优工精密阀门有限公司 The full form casting process of super-duplex stainless steel pump case

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101003115A (en) * 2006-12-22 2007-07-25 成都天保机械制造有限公司 Method for fabricating rotary drum
CN102027147A (en) * 2008-05-16 2011-04-20 奥托库姆普联合股份公司 Stainless steel product, use of the product and method of its manufacture
CN102248147A (en) * 2011-07-01 2011-11-23 屈志 Novel stainless steel centrifuge revolving drum and manufacturing method thereof
CN102732808A (en) * 2012-07-12 2012-10-17 屈志 Dual-phase stainless-steel cylinder in separator industry and centrifugal casting process thereof
CN103857816A (en) * 2011-10-21 2014-06-11 新日铁住金不锈钢株式会社 Duplex stainless steel, duplex stainless steel slab, and duplex stainless steel material

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101003115A (en) * 2006-12-22 2007-07-25 成都天保机械制造有限公司 Method for fabricating rotary drum
CN102027147A (en) * 2008-05-16 2011-04-20 奥托库姆普联合股份公司 Stainless steel product, use of the product and method of its manufacture
CN102248147A (en) * 2011-07-01 2011-11-23 屈志 Novel stainless steel centrifuge revolving drum and manufacturing method thereof
CN103857816A (en) * 2011-10-21 2014-06-11 新日铁住金不锈钢株式会社 Duplex stainless steel, duplex stainless steel slab, and duplex stainless steel material
CN102732808A (en) * 2012-07-12 2012-10-17 屈志 Dual-phase stainless-steel cylinder in separator industry and centrifugal casting process thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105834390A (en) * 2016-06-14 2016-08-10 四川维珍石化设备有限公司 Method for carrying out vertical centrifugal casting on annular part of centrifugal machine through metal mold
CN107900612A (en) * 2017-11-02 2018-04-13 江苏巨能机械有限公司 The processing technology of large-scale two phase stainless steel rotary drum disk
CN107900612B (en) * 2017-11-02 2019-10-18 江苏巨能机械有限公司 The processing technology of large-scale two phase stainless steel rotary drum disk
CN107829029A (en) * 2017-11-10 2018-03-23 洛阳双瑞特种装备有限公司 A kind of ZG022Cr22Ni5Mo3N materials two phase stainless steel smelting process method
CN109468522A (en) * 2018-12-26 2019-03-15 无锡市优工精密阀门有限公司 The full form casting process of super-duplex stainless steel pump case

Also Published As

Publication number Publication date
CN105349906B (en) 2018-08-10

Similar Documents

Publication Publication Date Title
CN106636858B (en) A kind of method for producing high anti-corrosion high-nitrogen super austenitic stainless steel
CN111575588B (en) Martensite precipitation hardening stainless steel and preparation method and application thereof
CN104651754B (en) Low alloy steel for high-pressure boiler tube and preparation method thereof
CN109440009A (en) A kind of TMCP state ship VOC storage tank low-temperature steel plate and manufacturing method
CN101429630B (en) Novel austenite cold-heading stainless steel and its steel wire production method
CN105200349A (en) Method for producing sulfuric acid dew-point corrosion-resistant round steel 09CrCuSb
CN105349906A (en) Centrifugal casting method of super duplex stainless steel horizontal screw centrifugal separator drum
CN109468522B (en) Investment casting process of super duplex stainless steel pump shell
CN103447348A (en) Manufacturing method of stainless steel wire
CN101070582A (en) Austenite cold-forged stainless-steel and steel wire making method
CN104089109B (en) A kind of 625MPa grades of UOE welded tube and its manufacture method
CN104357756B (en) A kind of anti-H 2 S stress corrosion straight seam welding petroleum casing pipe and manufacture method thereof
CN106756559B (en) A kind of Resistance to Concentrated Sulfuric Acid Corrosion high-silicon austenite stainless steel and preparation method thereof
CN104131237A (en) Economic type diphasic stainless steel with good toughness and weldability and manufacturing method thereof
JP6259336B2 (en) Ni-based alloy and method for producing the same
CN108286025A (en) A kind of resistance to marine corrosion reinforcing bar
CN102776442A (en) Hot rolled steel used for stirrer in automotive stirring tank and production method thereof
Song et al. Development of Chinese duplex stainless steel in recent years
CN107747027A (en) High resistivity, high magnetic permeability 1Cr12Mo martensitic stain less steel rotating shaft process for manufacturing forging
KR20120076392A (en) Duplex stainless steel having excellent alkali resistance
CN106555124A (en) Gao Ge, the stainless preparation method of high molybdenum-iron ferritic
CN114164376A (en) Low-carbon peritectic steel continuous casting round billet for high-pressure boiler and manufacturing method thereof
CN102732808A (en) Dual-phase stainless-steel cylinder in separator industry and centrifugal casting process thereof
CN105256254A (en) Preparation method of stripping tube material for preparing urea by means of CO2 gas stripping method
CN111020381B (en) Austenitic stainless steel and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
CB02 Change of applicant information

Address after: 643000 No. 3 Golden North Road, Qingbaijiang District, Sichuan, Chengdu

Applicant after: Sichuan virgin hi tech Material Co., Ltd.

Address before: 643000 No. 3 Golden North Road, Qingbaijiang District, Sichuan, Chengdu

Applicant before: SICHUAN WEIZHEN PETROCHEMICAL EQUIPMENT CO., LTD.

COR Change of bibliographic data
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CP02 Change in the address of a patent holder

Address after: 643000 No. 939, Tianxing Avenue, Qingbaijiang District, Chengdu, Sichuan

Patentee after: SICHUAN WEIZHEN HI-TECH MATERIAL CO.,LTD.

Address before: 643000 No. 3, Huangjin North Road, Qingbaijiang District, Chengdu, Sichuan

Patentee before: SICHUAN WEIZHEN HI-TECH MATERIAL CO.,LTD.

CP02 Change in the address of a patent holder