CN105348938A - Ecological jade interior wall paint and preparation method thereof - Google Patents
Ecological jade interior wall paint and preparation method thereof Download PDFInfo
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- CN105348938A CN105348938A CN201510910454.7A CN201510910454A CN105348938A CN 105348938 A CN105348938 A CN 105348938A CN 201510910454 A CN201510910454 A CN 201510910454A CN 105348938 A CN105348938 A CN 105348938A
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Abstract
The invention discloses ecological jade interior wall paint and a preparation method thereof and belongs to the field of building ornament materials. The paint is prepared from, by weight, 18-22 parts of water, 0.01-0.2 part of cellulose ether, 0.2-0.5 part of pH modifier, 0.1-0.2 part of wetting agent, 0.5-0.7 part of dispersing agent, 0.3-0.5 part of antifoaming agent, 8-14 parts of titanium dioxide, 6-15 parts of kaolin, 32-42 parts of jade powder, 14-22 parts of styrene-acrylic emulsion, 1.5-2.0 parts of coalescing agent and 0.1-0.15 part of antibacterial preservative. The ecological jade interior wall paint reduces emission of VOC and the content of soluble heavy metal, has the effects of desulfuration and air purification, and comprehensively increases the total value of decoration engineering to create a healthy indoor environment.
Description
Technical field
The invention belongs to the interior wall paint product in building coating, specifically a kind of ecological jade interior wall paint and preparation method thereof.
Background technology
Building coating refers to the various coating products being applied in building aspect, the development in its market is closely bound up in building trade, the development of urbanization in recent years brings the huge market space to building coating, especially along with the develop rapidly of dwelling construction, the people, to the pursuit of comfortable living environment, greatly stimulate the exploitation of all kinds of building coating, promotion and application.Interior wall paint is as the main force of building coating, and the fast development along with national economy has had swift and violent development.
As everyone knows, building coating is an important branch of material of construction, and according to investigations, interior wall paint decorations effect occupies the weight of 80% in room Integral decoration finishing effect.For one family, if room takes up an area 100 square metres, according to industry standard, the fraction of coverage of coating should 8.6mm greatly, probably needs decorative paint quantity 25.24 liters.This shows, the development of real estate and people, to the increase of the demand of house, promote interior wall paint market to a great extent.In addition along with the transformation in national shanty town and the dynamics of Housing Guarantee continue to increase, have the house of oneself future by having more and more resident, furniture building materials market will present prosperity scene.
Interior wall paint is exactly the said emulsion paints of people, is for one of main decorating and renovating material of indoor wall in decoration design for residence engineering.Along with the further raising that the people require for household living--room decoration, environmental protection, low-carbon (LC) life become the main flow in epoch.The developing direction of building coating trends towards middle and high end, and inner wall of building paint is more outstanding, not only requires to have good scrub resistance, the texture of coating, color and environmental-protecting performance are had higher requirement simultaneously, as low VOC, color is naturally soft, absorption VOC etc.
The source of pollution of coating mainly come from the objectionable impurities contained in its composition.The organic solvent used in modern coatings, various auxiliary agent, sanitas and containing the pigment of heavy metal and filler, produce objectionable impurities in production with in using, cause the pollution to environment, affect HUMAN HEALTH.
The harm of coating is mainly derived from three aspects, first is the total organic volatile in coating, namely usually said VOC, volatile organic compounds is discharged in air, can be combined with solid particulate matter, under the effect of light, form PM2.5 particle with the oxygen reaction in air, be the important sources of haze simultaneously; Second is formaldehyde.Formaldehyde is a kind of colourless, and the gas of irritant smell, has volatile, that toxicity is high feature.Formaldehyde toxicity is higher, to protein have very strong solidify important, can and the amino of nucleic acid and hydroxy combining make it be out of shape, the effect of gastric enzyme and pancreatin can be hindered, affect the metabolic function of health.The steam of formaldehyde has carcinogenesis to rodent; 3rd is soluble heavy metal, and namely density is greater than 4.5g/cm
3metal, as lead, cadmium, chromium, mercury etc.The main source of heavy metal is dark pigment, and Long Term Contact heavy metal can cause slight neurasthenic syndrome and indigestion symptom, and comparatively anaemia and plumbous paralysis then appear in severe one.
With regard to building trade, the organic compound discharged in the production of building coating, use procedure is one of main environmental pollutant.Therefore how reducing VOC content, make product reach the requirement of coating environmental protection standard, is one of pursuing a goal of domestic and international building coating manufacturer.The product structure of building coating answers meeting the market requirement, in the middle of constantly adjusting, does, increase value-added content of product from environmental protection, low-carbon (LC), green concept.Therefore the environment-friendly coating such as ecological jade interior wall paint arises at the historic moment.
Summary of the invention
The object of the present invention is to provide a kind of ecological jade interior wall paint and preparation method thereof, it not only can reduce the discharge of VOC, use natural jade to do pigment simultaneously, decrease the content of the soluble heavy metal in interior wall paint, improve spreading rate, the effect that there is desulfurization simultaneously and purify air, the overall value of General Promotion Decorating Project.
A kind of ecological jade interior wall paint it be made up of the starting material of following weight proportioning:
18 ~ 22 parts, water
Ether of cellulose 0.01 ~ 0.2 part
PH adjusting agent 0.2 ~ 0.5 part
Wetting agent 0.1 ~ 0.2 part
Dispersion agent 0.5 ~ 0.7 part
Defoamer agent 0.3 ~ 0.5 part
Titanium dioxide 8 ~ 14 parts
Kaolin 6 ~ 15 parts
Jade powder 32 ~ 42 parts
Benzene emulsion 14 ~ 22 parts
Film coalescence aid 1.5 ~ 2.0 parts
Fungicidal preservative 0.1 ~ 0.15 part
For the preparation of a preparation method for ecological jade interior wall paint, comprise the following steps:
1) add in dispersion cylinder by 18 ~ 22 parts of water, start agitator, control rotating speed at 300 ~ 500rpm, slowly add 0.01 ~ 0.2 part of ether of cellulose, ether of cellulose adds 0.2 ~ 0.5 part of pH adjusting agent after adding, the dissolving of accelerating fibers element ether;
2) rotating speed to the 800 ~ 1000rpm of agitator is improved, after adding 0.1 ~ 0.2 part of wetting agent, 0.5 ~ 0.7 part of dispersion agent, 0.2 ~ 0.4 part of defoamer agent, 8 ~ 14 parts of titanium dioxides, 6 ~ 15 parts of kaolin, 32 ~ 42 parts of jade powder successively, again improve rotating speed to 1800 ~ 2000rpm, time length is 40 ~ 60min, detect fineness and whether be less than 60um, as fineness is greater than 60um, then stir appropriate time again, until fineness is less than 60um;
3) reduce rotating speed to 1000 ~ 1200rpm, add 14 ~ 22 parts of benzene emulsions, 1.5 ~ 2.0 parts of film coalescence aid and 0.1 ~ 0.15 part of fungicidal preservative successively, 0.1 ~ 0.2 part of defoamer, disperse 30 ~ 40 minutes, until mix.
Described ether of cellulose is the hydroxypropyl methyl cellulose ether, hydroxyethyl ethylcellulose ether, TYLOSE 30000, Hydroxypropyl ethyl cellulose ether, hydroxyethyl ether cellulose etc. of water miscible non-ionic different molecular weight.It is as the thickening material of interior wall paint, makes interior wall paint have a suitable working viscosity, ensures that pigment has good dispersion in interior wall paint, the not sedimentation when storing simultaneously.Preferably viscosity is the hydroxyethyl ether cellulose of 15000 ~ 30000.
Described pH adjusting agent can be ammoniacal liquor, sodium carbonate solution, caustic soda soln, 2-amino-2-methyl-1-propanol, and it is mainly used to regulate potential of hydrogen, for the use of various auxiliary agent improves alkaline environment, prevents interior wall paint rotten change in storage process from going bad.Preferably caustic soda soln.
Described dispersion agent is water-based, can be the ammonium salt etc. of polyacrylic acid sodium salt or ammonium salt, polycarboxylate sodium or ammonium salt or acrylic copolymer, is beneficial to color stuffing and is uniformly dispersed and stable storing in system.Preferably ammonium polyacrylate salt dispersion agent.
Described wetting agent is the nonionic emulsifying agent of water-based, not containing APEO, formaldehyde content is extremely low, soak for people's interior wall paint, reduce the beating consistency of color stuffing, improve the consistency of color stuffing and polymer emulsion, the wetting aid as color stuffing dispersion has excellent seepage force and reduces capillary effect, improves the cohesive force of interior wall paint and basic unit.Preferred wetting agent is the polyoxyethylene ether of C7 ~ C12 alcohol, and the polymerization degree is 15 ~ 20.
Described defoamer is non-ionic type defoamer, mineral oil defoaming agent, silicone antifoam agent, hybrid molecule defoamer etc.Usually in formula system, use two kinds of defoamers, use in the making beating stage and press down the good defoamer of bubble effect, prevent from system, producing a large amount of bubbles; The stronger defoamer of defoaming capacity is added, micro-bubble remaining in removal system in the final stage of coating.
Described titanium dioxide is anatase thpe white powder or Rutile type Titanium Dioxide, provides hiding rare and the contrast ratio of interior wall paint film in formula.In order to obtain good cost performance, select anatase thpe white powder.
Described kaolin adopts calcined kaolin, and in formula, occupy the contrast ratio providing interior wall paint film, prevent coating system sedimentation in storage process, after interior wall drying varniss, paint film has certain hiding rare.
Described jade powder is ground by the natural soapstone of shades of colour to form, and not containing harmful material, the obnoxious flavour in adsorbable air, long-term releasing negative oxygen ion, color is naturally lively, permanent as new.
Described benzene emulsion is formed by vinylbenzene and various vinylformic acid (ester) monomer copolymerization, is a kind of aqueous polymer emulsion of anionic.As the filmogen of interior wall paint, can be the cohesive force that film provides good.In the preparation of ecological interior wall paint, the selection of benzene emulsion is very important, requires it not contain or slightly containing VOC and formaldehyde, does not use APEO class emulsifying agent.In order to the scrub resistance providing film good, the second-order transition temperature of benzene emulsion is more high better, but at room temperature film forming properties is poor for the high benzene emulsion of second-order transition temperature, needs to add more film coalescence aid.Also to pay attention to the viscosity of benzene emulsion and solid content in addition.Preferred benzene emulsion should be solid content is 47 ~ 49%, and viscosity is 3000 ~ 6000cps(3# rotor/12rpm, 25 DEG C), particle diameter is 0.1 ~ 0.5um.
At normal atmospheric pressure, boiling point more than 250 DEG C, not for the VOC of interior wall paint contributes, should not have smell simultaneously, interior wall paint can be helped more than 5 DEG C can to form a continuous print film described filmogen.Optional filmogen is ethylene glycol monobutyl ether, phenylcarbinol, propylene glycol monobutyl ether, 2,2,4-trimethylammonium-1,3-pentanediol mono isobutyrate, propylene glycol dibenzoate, ethylene glycol bisthioglycolate benzoic ether etc., preferably 2,2,4-trimethylammonium-1,3-pentanediol mono isobutyrate, propylene glycol dibenzoate, ethylene glycol bisthioglycolate phenylformic acid and their mixture thereof.
Described sanitas adopts conventional isothiazolinone biocide agent, has sterilization and anticorrosion effect, ensures that interior wall paint does not become morally degenerate in the process of storage, transport.
The present invention adopts technique scheme to have following beneficial effect:
The selected various Material cladding collocation of the present invention, especially adopts natural jade powder as filler and pigment, determines each component and part by weight thereof in interior wall paint, develop a kind of ecological jade interior wall paint by Multitest.Interior wall paint provided by the present invention is compared with traditional building coating, has the following advantages:
(1) production unit of interior wall paint provided by the present invention, detecting instrument, coating process are identical with traditional building coating, do not need to increase new facility investment;
(2) ecological jade interior wall paint provided by the present invention not only reduces VOC discharge, improves coating efficiency, has saved labor cost, decreased trucking costs;
(3) ecological jade interior wall paint provided by the present invention take natural jade powder as filler and pigment, not containing harmful soluble heavy metal, and the obnoxious flavour in adsorbable air, long-term releasing negative oxygen ion, color is naturally lively, permanent as new;
(4) ecological jade interior wall paint provided by the present invention is on the basis keeping traditional architecture coating advantage, and also can improve solid content, dilute with water can directly not constructed, 1.5 times of traditional architecture coating during the coating thickness of an application.
Embodiment
Below in conjunction with specific embodiment, the present invention will be further described.
A kind of ecological jade interior wall paint it be made up of the starting material of following weight proportioning:
18 ~ 22 parts, water
Ether of cellulose 0.01 ~ 0.2 part
PH adjusting agent 0.2 ~ 0.5 part
Wetting agent 0.1 ~ 0.2 part
Dispersion agent 0.5 ~ 0.7 part
Defoamer agent 0.3 ~ 0.5 part
Titanium dioxide 8 ~ 14 parts
Kaolin 6 ~ 15 parts
Jade powder 32 ~ 42 parts
Benzene emulsion 14 ~ 22 parts
Film coalescence aid 1.5 ~ 2.0 parts
Fungicidal preservative 0.1 ~ 0.15 part
For the preparation of a preparation method for ecological jade interior wall paint, comprise the following steps:
1) add in dispersion cylinder by 18 ~ 22 parts of water, start agitator, control rotating speed at 300 ~ 500rpm, slowly add 0.01 ~ 0.2 part of ether of cellulose, ether of cellulose adds 0.2 ~ 0.5 part of pH adjusting agent after adding, the dissolving of accelerating fibers element ether;
2) rotating speed to the 800 ~ 1000rpm of agitator is improved, after adding 0.1 ~ 0.2 part of wetting agent, 0.5 ~ 0.7 part of dispersion agent, 0.2 ~ 0.4 part of defoamer agent, 8 ~ 14 parts of titanium dioxides, 6 ~ 15 parts of kaolin, 32 ~ 42 parts of jade powder successively, again improve rotating speed to 1800 ~ 2000rpm, time length is 40 ~ 60min, detect fineness and whether be less than 60um, as fineness is greater than 60um, then stir appropriate time again, until fineness is less than 60um;
3) reduce rotating speed to 1000 ~ 1200rpm, add 14 ~ 22 parts of benzene emulsions, 1.5 ~ 2.0 parts of film coalescence aid and 0.1 ~ 0.15 part of fungicidal preservative successively, 0.1 ~ 0.2 part of defoamer, disperse 30 ~ 40 minutes, until mix.
Embodiment 1
A preparation method for ecological jade interior wall paint, comprises the following steps:
1) 18.5 parts of water are added in dispersion cylinder, start agitator, control rotating speed at 300 ~ 500rpm, slowly add 0.15 part of hydroxyethyl ether cellulose 250HBR, ether of cellulose adds the caustic soda soln of 0.3 part of pH adjusting agent 0.1% after adding, the dissolving of accelerating fibers element ether.
2) rotating speed to the 800 ~ 1000rpm of agitator is improved, after adding 0.15 part of wetting agent EH-9,0.6 part of dispersion agent SN5040,0.3 part of defoamer agent NXZ, 10 parts of titanium dioxide BLR-699,8 part of 1250 order kaolin, 39.8 part of 1000 medamaite powder successively, again improve rotating speed to 1800 ~ 2000rpm, the time length is 40min.Detect fineness, be less than 60um.
3) reduce rotating speed to 1000 ~ 1200rpm, add 20 parts of benzene emulsion PX7035Xap, 2.0 parts of film coalescence aid B-50 and 0.1 part of fungicidal preservative LXE successively, 0.1 part of defoamer agent A-10, dispersion 40 minutes, mix.
Embodiment 2
A preparation method for ecological jade interior wall paint, comprises the following steps:
(1) 20 parts of water are added in dispersion cylinder, start agitator, control rotating speed at 300 ~ 500rpm, slowly add 0.18 part of hydroxyethyl ether cellulose 250HBR, ether of cellulose adds the caustic soda soln of 0.3 part of pH adjusting agent 0.1% after adding, the dissolving of accelerating fibers element ether.
(2) rotating speed to the 800 ~ 1000rpm of agitator is improved, after adding 0.15 part of wetting agent EH-9,0.55 part of dispersion agent SN5040,0.3 part of defoamer agent NXZ, 8.5 parts of titanium dioxide BLR-699,10 part of 1250 order kaolin, 40.0 part of 1000 medamaite powder successively, again improve rotating speed to 1800 ~ 2000rpm, the time length is 50min.Detect fineness, be less than 60um.
(3) reduce rotating speed to 1000 ~ 1200rpm, add 18 parts of benzene emulsion PX7035Xap, 1.8 parts of film coalescence aid B-50 and 0.12 part of fungicidal preservative LXE successively, 0.1 part of defoamer agent A-10, dispersion 35 minutes, mix.
Embodiment 3
A preparation method for ecological jade interior wall paint, comprises the following steps:
(1) 22 parts of water are added in dispersion cylinder, start agitator, control rotating speed at 300 ~ 500rpm, slowly add 0.2 part of hydroxyethyl ether cellulose 250HBR, ether of cellulose adds the caustic soda soln of 0.3 part of pH adjusting agent 0.1% after adding, the dissolving of accelerating fibers element ether.
(2) rotating speed to the 800 ~ 1000rpm of agitator is improved, after adding 0.15 part of wetting agent EH-9,0.50 part of dispersion agent SN5040,0.3 part of defoamer agent NXZ, 12 parts of titanium dioxide BLR-699,14 part of 1250 order kaolin, 33.8 part of 1000 medamaite powder successively, again improve rotating speed to 1800 ~ 2000rpm, the time length is 40min.Detect fineness, be less than 60um.
(3) reduce rotating speed to 1000 ~ 1200rpm, add 15 parts of benzene emulsion PX7035Xap, 1.5 parts of film coalescence aid B-50 and 0.15 part of fungicidal preservative LXE successively, 0.1 part of defoamer agent A-10, dispersion 30 minutes, mix.
Interior wall paint product performance in each embodiment of ecological jade interior wall paint prepared by the present invention are carried out according to the regulation of GB/T9756-2009 " resin latex dope "; The environmental-protecting performance of product detects according to the regulation of HJ2537-2014 " environmental labelling product technical requirements interior wall coating ".
The product performance of ecological jade interior wall paint prepared in each embodiment of the present invention meet the technical requirements of standard GB/T/T9756-2009 " resin latex dope "; The environmental-protecting performance of product meets the requirements of environmental standard HJ2537-2014 " environmental labelling product technical requirements interior wall coating ".
The result that the sample sample presentation produced detects is as follows:
Ecological jade interior wall paint provided by the present invention take natural jade powder as filler and pigment, not containing harmful soluble heavy metal, color is naturally lively, permanent as new, and decrease VOC discharge, obnoxious flavour in adsorbable air, long-term releasing negative oxygen ion, is conducive to HUMAN HEALTH.Ecological jade interior wall paint provided by the present invention is on the basis keeping traditional architecture coating advantage, and also can improve solid content, dilute with water can directly not constructed, 1.5 times of traditional architecture coating during the coating thickness of an application.
Above-mentioned embodiment just carries out detailed explanation to technical scheme of the present invention; the present invention has more than and is only confined to above-described embodiment; those skilled in the art it should be understood that every according to the improvement of above-mentioned principle on basis of the present invention, substitute many should in protection scope of the present invention.
Claims (8)
1. ecological jade interior wall paint and preparation method thereof, is characterized in that:
It is made up of the starting material of following weight proportioning:
18 ~ 22 parts, water
Ether of cellulose 0.01 ~ 0.2 part
PH adjusting agent 0.2 ~ 0.5 part
Wetting agent 0.1 ~ 0.2 part
Dispersion agent 0.5 ~ 0.7 part
Defoamer agent 0.3 ~ 0.5 part
Titanium dioxide 8 ~ 14 parts
Kaolin 6 ~ 15 parts
Jade powder 32 ~ 42 parts
Benzene emulsion 14 ~ 22 parts
Film coalescence aid 1.5 ~ 2.0 parts
Fungicidal preservative 0.1 ~ 0.15 part.
2. ecological jade interior wall paint of one according to claim 1 and preparation method thereof, is characterized in that: described ether of cellulose is water miscible non-ionic viscosity is the hydroxyethyl ether cellulose of 15000 ~ 30000.
3. ecological jade interior wall paint of one according to claim 1 and preparation method thereof, is characterized in that: described pH adjusting agent is caustic soda soln.
4. ecological jade interior wall paint of one according to claim 1 and preparation method thereof, is characterized in that: described dispersion agent is ammonium polyacrylate salt dispersion agent.
5. ecological jade interior wall paint of one according to claim 1 and preparation method thereof, is characterized in that: described wetting agent is the nonionic emulsifying agent of water-based, the C not containing APEO
7~ C
12the polyoxyethylene ether of alcohol, the polymerization degree is 15 ~ 20.
6. ecological jade interior wall paint of one according to claim 1 and preparation method thereof, it is characterized in that: described benzene emulsion is formed by vinylbenzene and various Acrylic Acid Monomer copolymerization, its solid content is 47 ~ 49%, viscosity is 3000 ~ 6000cps(3# rotor/12rpm, 25 DEG C), particle diameter is 0.1 ~ 0.5um.
7. ecological jade interior wall paint of one according to claim 1 and preparation method thereof, it is characterized in that: described filmogen is 2,2,4-trimethylammonium-1,3-pentanediol mono isobutyrate, propylene glycol dibenzoate, ethylene glycol bisthioglycolate phenylformic acid and their mixture thereof.
8. ecological jade interior wall paint of the one according to any one of claim 1-7 and preparation method thereof, is characterized in that: comprise the following steps:
1) add in dispersion cylinder by 18 ~ 22 parts of water, start agitator, control rotating speed at 300 ~ 500rpm, slowly add 0.01 ~ 0.2 part of ether of cellulose, ether of cellulose adds 0.2 ~ 0.5 part of pH adjusting agent after adding, the dissolving of accelerating fibers element ether;
2) rotating speed to the 800 ~ 1000rpm of agitator is improved, after adding 0.1 ~ 0.2 part of wetting agent, 0.5 ~ 0.7 part of dispersion agent, 0.2 ~ 0.4 part of defoamer agent, 8 ~ 14 parts of titanium dioxides, 6 ~ 15 parts of kaolin, 32 ~ 42 parts of jade powder successively, again improve rotating speed to 1800 ~ 2000rpm, time length is 40 ~ 60min, detect fineness and whether be less than 60um, as fineness is greater than 60um, then stir appropriate time again, until fineness is less than 60um;
3) reduce rotating speed to 1000 ~ 1200rpm, add 14 ~ 22 parts of benzene emulsions, 1.5 ~ 2.0 parts of film coalescence aid and 0.1 ~ 0.15 part of fungicidal preservative successively, 0.1 ~ 0.2 part of defoamer, disperse 30 ~ 40 minutes, until mix.
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| CN106222776A (en) * | 2016-07-27 | 2016-12-14 | 恒天海龙（潍坊）新材料有限责任公司 | A kind of jade is felt nice and cool regenerated celulose fibre and preparation method thereof |
| CN109503076A (en) * | 2018-12-17 | 2019-03-22 | 北京未来空间美居科技有限公司 | A kind of preparation method of ornament materials and its dalle with releasing negative oxygen ion environmental protection health-preserving function |
| CN109593406A (en) * | 2018-12-14 | 2019-04-09 | 沈阳美佳奥硅藻新材料科技有限公司 | One kind having damping, sterilization, release anion diatom base coating and emulsified material inner wall decoration wall material and preparation method |
| CN109627834A (en) * | 2018-12-14 | 2019-04-16 | 沈阳美佳奥硅藻新材料科技有限公司 | One kind having ventilative damping, sterilization, release anion keeps in good health interior wall diatom base coloured silk white background material and fabric and preparation method thereof |
| CN111848102A (en) * | 2020-07-21 | 2020-10-30 | 北京莱恩斯新材料科技有限公司 | Efficient mildew-proof, bactericidal and fireproof interior wall paint and preparation method thereof |
| CN114687458A (en) * | 2022-03-19 | 2022-07-01 | 北京工业大学 | Assembled ecological inner wall and floor slab self-tapping nail cluster and post-cast strip combined connection structure and manufacturing method |
| CN115160861A (en) * | 2022-05-10 | 2022-10-11 | 沈阳化工大学 | Preparation method of water-based emulsion paint by replacing heavy calcium carbonate with waste jade powder |
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| CN111848102B (en) * | 2020-07-21 | 2021-12-28 | 北京莱恩斯新材料科技有限公司 | Efficient mildew-proof, bactericidal and fireproof interior wall paint and preparation method thereof |
| CN114687458A (en) * | 2022-03-19 | 2022-07-01 | 北京工业大学 | Assembled ecological inner wall and floor slab self-tapping nail cluster and post-cast strip combined connection structure and manufacturing method |
| CN115160861A (en) * | 2022-05-10 | 2022-10-11 | 沈阳化工大学 | Preparation method of water-based emulsion paint by replacing heavy calcium carbonate with waste jade powder |
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