CN105343918B - A kind of deodorizer containing conch meal - Google Patents
A kind of deodorizer containing conch meal Download PDFInfo
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- CN105343918B CN105343918B CN201510897699.0A CN201510897699A CN105343918B CN 105343918 B CN105343918 B CN 105343918B CN 201510897699 A CN201510897699 A CN 201510897699A CN 105343918 B CN105343918 B CN 105343918B
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- 235000012054 meals Nutrition 0.000 title claims abstract description 36
- 239000002086 nanomaterial Substances 0.000 claims abstract description 12
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 15
- 238000001354 calcination Methods 0.000 claims description 12
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims description 6
- 238000010791 quenching Methods 0.000 claims description 6
- 230000000171 quenching effect Effects 0.000 claims description 6
- 241000237509 Patinopecten sp. Species 0.000 claims description 5
- 239000005543 nano-size silicon particle Substances 0.000 claims description 5
- 235000020637 scallop Nutrition 0.000 claims description 5
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 claims description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical group [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 4
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 150000007524 organic acids Chemical class 0.000 claims description 4
- 159000000000 sodium salts Chemical class 0.000 claims description 4
- -1 sucrose fatty acid ester Chemical class 0.000 claims description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 229930006000 Sucrose Natural products 0.000 claims description 3
- 238000013019 agitation Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 3
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 3
- 239000000194 fatty acid Substances 0.000 claims description 3
- 229930195729 fatty acid Natural products 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 229910052814 silicon oxide Inorganic materials 0.000 claims description 3
- 239000005720 sucrose Substances 0.000 claims description 3
- 239000005711 Benzoic acid Substances 0.000 claims description 2
- 239000002202 Polyethylene glycol Substances 0.000 claims description 2
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims description 2
- 235000010233 benzoic acid Nutrition 0.000 claims description 2
- 239000001530 fumaric acid Substances 0.000 claims description 2
- 229920001223 polyethylene glycol Polymers 0.000 claims description 2
- 239000001632 sodium acetate Substances 0.000 claims description 2
- 235000017281 sodium acetate Nutrition 0.000 claims description 2
- 239000011780 sodium chloride Substances 0.000 claims description 2
- 239000001509 sodium citrate Substances 0.000 claims description 2
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 2
- 230000001877 deodorizing effect Effects 0.000 abstract description 9
- 239000004615 ingredient Substances 0.000 abstract description 4
- 239000000463 material Substances 0.000 abstract description 3
- 230000002195 synergetic effect Effects 0.000 abstract description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 6
- 238000004332 deodorization Methods 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 239000002781 deodorant agent Substances 0.000 description 4
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 3
- 229910021529 ammonia Inorganic materials 0.000 description 3
- DNJIEGIFACGWOD-UHFFFAOYSA-N ethanethiol Chemical compound CCS DNJIEGIFACGWOD-UHFFFAOYSA-N 0.000 description 3
- 239000010794 food waste Substances 0.000 description 3
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000010813 municipal solid waste Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- AEQDJSLRWYMAQI-UHFFFAOYSA-N 2,3,9,10-tetramethoxy-6,8,13,13a-tetrahydro-5H-isoquinolino[2,1-b]isoquinoline Chemical compound C1CN2CC(C(=C(OC)C=C3)OC)=C3CC2C2=C1C=C(OC)C(OC)=C2 AEQDJSLRWYMAQI-UHFFFAOYSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 241001597008 Nomeidae Species 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- HRKQOINLCJTGBK-UHFFFAOYSA-N dihydroxidosulfur Chemical compound OSO HRKQOINLCJTGBK-UHFFFAOYSA-N 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000005189 flocculation Methods 0.000 description 1
- 230000016615 flocculation Effects 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 150000008282 halocarbons Chemical class 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 229960003511 macrogol Drugs 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000003641 microbiacidal effect Effects 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 210000000697 sensory organ Anatomy 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 239000000176 sodium gluconate Substances 0.000 description 1
- 235000012207 sodium gluconate Nutrition 0.000 description 1
- 229940005574 sodium gluconate Drugs 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
Landscapes
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The invention discloses a kind of deodorizer containing conch meal, it is characterised in that described deodorizer contains the nano-material modified conch meal of 1-2 weight portion。Modified by various ingredients and material of deodorizer of the present invention, and the selection collocation of specific components, so that played synergistic function between each component, and then make obtained deodorizer have good deodorizing effect and few residual, there is good application potential and market value widely。
Description
Technical field
The invention belongs to cosmetics of everyday use technical field, be specifically related to a kind of deodorizer containing conch meal。
Background technology
Odor pollution is extensively subject to the attention of various countries, is thought one of six big public hazards being only second to noise by many countries。Particularly have a strong impact on environment especially at the stench on the ground such as resident lavatory and drain of kitchen, garbage disposal plant, plant, public lavatory。The chemical substance distributing foul odour is broadly divided into five classes by chemical composition: sulfur-containing compound is hydrogen sulfide, thio-alcohol, thioether etc. such as；Nitrogen-containing compound is ammonia, amide etc. such as；Halogen and derivant thereof be chlorine, halogenated hydrocarbons such as；Hydro carbons is alkane, alkene, aromatic hydrocarbon etc. such as；Oxygen-containing organic compound is alcohol, phenol, aldehyde, ketone etc. such as。
Deodorizer is used for alleviating offending abnormal smells from the patient, and comfortable life is played an important role。Deodorizer mainly has following several types: physical deodorization agent, chemical deodorizing agent, microbiocidal deodorizer etc.。Current international and domestic conventional deodorizer mainly has: several big series products such as natural plant liquid deodorizer, biological deodorant, fragrant and deodorizing agent, macromolecular deodorizer, activated charcoal deodorants。Wherein natural plant liquid deodorizer, fragrant and deodorizing agent, activated charcoal deodorants belong to spreadability deodorizer, namely do not eliminate stink, but add in spice in stink and stink, so as to reduce the impact of stink from sense organ。Biological deodorant is reactive deodorizer, principle is biological bacteria and the combination of deodorization molecule, reacts to reach deodorizing effect, but this deodorizer needs to concentrate gas extraction system, and ambient temperature is required by microorganism fungus kind, when temperature is relatively low in the winter time, activity reduces, and deodorizing effect declines。Macromolecular deodorizer is absorption degradation type deodorizer, its principle is dependent on flocculation ability by after deodorization Molecular Adsorption, effective ingredient degraded odorant pollutant in recycling deodorizer is to reach the purpose of deodorization, but environment can be produced to pollute by general macromolecular deodorizer again。
Therefore, how obtaining a kind of good deodorization effect, will not produce the deodorizer of secondary pollution is those skilled in the art's technical problems urgently to be resolved hurrily。
Summary of the invention
The invention aims to provide a kind of deodorizer, can effectively remove the stench on the ground such as resident lavatory and drain of kitchen, garbage disposal plant, plant, public lavatory, and secondary pollution will not be produced, this is conducted in-depth research by the present inventor, having paid substantial amounts of creative work and after further investigation is explored, thus completing the present invention。In order to realize the purpose of the present invention, intend adopting the following technical scheme that
One aspect of the present invention relates to a kind of deodorizer containing conch meal, it is characterised in that described deodorizer contains the nano-material modified conch meal of 1-2 weight portion, it is preferred that described conch meal is deep-sea scallop conch meal。
In a preferred embodiment of the present invention, described nano-material modified conch meal is made up of the nano aluminium oxide of 5-10% percentage by weight, the nano silicon of 5-10% and the conch meal of surplus。
In another preferred embodiment of the present invention, described nano-material modified conch meal is prepared by method and prepares:
(1) being calcined 60-80 minute at 750-850 DEG C by clean deep-sea scallop shell, be then naturally cooling to room temperature, after calcining, shell is pulverized, is ground, and crosses 200-300 mesh sieve, obtains conch meal, be separately added into nano aluminium oxide and nano silicon oxide, mix homogeneously；
(2) gradient calcining and quenching it are sequentially carried out, concrete operations are: carry out calcining 10-15 minute at 380-420 DEG C, then it is warmed up to 480-520 DEG C with the heating rate of 8-12 DEG C/min, and insulation is calcined 20-25 minute at such a temperature, it is placed in the ethanol water of 15-25% volumetric concentration while hot and lowers the temperature quenches；Filtering after quenching, filtering residue is warmed up to 680-720 DEG C with the heating rate of 3-7 DEG C/min, and insulation is calcined 30-40 minute at such a temperature；Calcining naturally cools to room temperature after terminating, and is again pulverized by conch meal, grinds, crosses 200-300 mesh sieve, obtain nano-material modified conch meal。
In a preferred embodiment of the present invention, possibly together with Polyethylene Glycol 2-5 part in described deodorizer, sucrose fatty acid ester 4-10 part, sodium salt 1-2 part, essence 2-4 part, organic acid 2-4 part, water 50-60 part。
In a preferred embodiment of the present invention, described deodorizer is prepared by method and prepares: above-mentioned component be in addition to water sequentially added under agitation in water, and after mix homogeneously, the mixing speed with 1500-2500rpm prepares for high-speed stirred 1-3 hour。
In a preferred embodiment of the present invention, described deodorizer does not contain other component。
In a preferred embodiment of the present invention, described organic acid is fumaric acid or citric acid or benzoic acid。
In a preferred embodiment of the present invention, described sodium salt is sodium chloride or sodium citrate or sodium acetate。
Modified by various ingredients and material of deodorizer of the present invention, and the selection collocation of specific components, so that played synergistic function between each component, and then make obtained deodorizer have good deodorizing effect and few residual, there is good application potential and market value widely。
Detailed description of the invention
If not specified, that technological means used in embodiment is well known to those skilled in the art conventional means。
Embodiment 1:
(1) being calcined 60-80 minute at 800 DEG C by clean deep-sea scallop shell, be then naturally cooling to room temperature, after calcining, shell is pulverized, is ground, cross 200-300 mesh sieve, obtain conch meal, be separately added into the nano aluminium oxide and nano silicon oxide that account for conch meal weight 10%, mix homogeneously。
(2) gradient calcining and quenching it are sequentially carried out, concrete operations are: carry out calcining 10-15 minute at 400 DEG C, then it is warmed up to 500 DEG C with the heating rate of 8-12 DEG C/min, and insulation is calcined 20-25 minute at such a temperature, it is placed in the ethanol water of 20% volumetric concentration while hot and lowers the temperature quenches；Filtering after quenching, filtering residue is warmed up to 700 DEG C with the heating rate of 3-7 DEG C/min, and insulation is calcined 30-40 minute at such a temperature；Calcining naturally cools to room temperature after terminating, and is again pulverized by conch meal, grinds, crosses 200-300 mesh sieve, obtain nano-material modified conch meal。
(3) nano-material modified conch meal 1-2 part is weighed, Macrogol 2000 2-5 part, sucrose fatty acid ester 4-10 part, sodium gluconate 1-2 part, essence 2-4 part, citric acid 2-4 part, water 50-60 part, above-mentioned component being in addition to water sequentially added under agitation in water, after mix homogeneously, the mixing speed high-speed stirred with 2000rpm obtains deodorizer in 2 hours。Being added without nano-material modified conch meal in matched group adopts same recipe and preparation method to obtain deodorizer。
In order to further illustrate the deodorizing effect of deodorizer involved by the application, this deodorizer is used for changing food waste by inventor。In the 5L wide mouthed bottle of the changing food waste highly rotted equipped with 1000g, add the deodorizer 20g containing conch meal and changing food waste mix homogeneously, use rubber stopper seal bottleneck；Being not added with deodorizer matched group, often group Setup Experiments 3 is parallel simultaneously, detects stench intensity, ammonia concentration, concentration of hydrogen sulfide and TVOC concentration after 24h, and measurement result is as shown in the table。
| Testing index | Matched group | Experimental group | Reduction rate |
| Odor strength (OU) | 650000 | 250000 | 61.5% |
| Ammonia concentration (mg/m3) | 49.6 | 23.6 | 52.4% |
| Concentration of hydrogen sulfide (mg/m3) | 180.6 | 57.8 | 68.0% |
| TVOC concentration (mg/m3) | 45.7 | 15.3 | 66.5% |
Can be seen that from testing result above, modified by various ingredients and material of deodorizer of the present invention, and specific components selection collocation and specific preparation method, so that played synergistic function between each component, and then make obtained deodorizer have good deodorizing effect and few residual, there is good application potential and market value widely。
The above is the preferred embodiments of the present invention; it should be pointed out that, for those skilled in the art, under the premise without departing from principle of the present invention; can also making some improvements and modifications, these improvements and modifications also should be regarded as protection scope of the present invention。
Claims (5)
1. the deodorizer containing conch meal, it is characterised in that described deodorizer contains the nano-material modified conch meal of 1-2 weight portion, possibly together with Polyethylene Glycol 2-5 part in described deodorizer, sucrose fatty acid ester 4-10 part, sodium salt 1-2 part, essence 2-4 part, organic acid 2-4 part, water 50-60 part；Described deodorizer does not contain other component；Described nano-material modified conch meal is made up of the nano aluminium oxide of 5-10% percentage by weight, the nano silicon of 5-10% and the conch meal of surplus；Described nano-material modified conch meal is prepared by method and prepares:
(1) being calcined 60-80 minute at 750-850 DEG C by clean deep-sea scallop shell, be then naturally cooling to room temperature, after calcining, shell is pulverized, is ground, and crosses 200-300 mesh sieve, obtains conch meal, be separately added into nano aluminium oxide and nano silicon oxide, mix homogeneously；
(2) gradient calcining and quenching it are sequentially carried out, concrete operations are: carry out calcining 10-15 minute at 380-420 DEG C, then it is warmed up to 480-520 DEG C with the heating rate of 8-12 DEG C/min, and insulation is calcined 20-25 minute at such a temperature, it is placed in the ethanol water of 15-25% volumetric concentration while hot and lowers the temperature quenches；Filtering after quenching, filtering residue is warmed up to 680-720 DEG C with the heating rate of 3-7 DEG C/min, and insulation is calcined 30-40 minute at such a temperature；Calcining naturally cools to room temperature after terminating, and is again pulverized by conch meal, grinds, crosses 200-300 mesh sieve, obtain nano-material modified conch meal。
2. the deodorizer containing conch meal according to claim 1, described conch meal is deep-sea scallop conch meal。
3. the deodorizer containing conch meal according to claim 1, described organic acid is fumaric acid or citric acid or benzoic acid。
4. the deodorizer containing conch meal according to claim 1, described sodium salt is sodium chloride or sodium citrate or sodium acetate。
5. the deodorizer containing conch meal according to claim 1-4 any one, described deodorizer is prepared by method and prepares: above-mentioned component be in addition to water sequentially added under agitation in water, and after mix homogeneously, the mixing speed with 1500-2500rpm prepares for high-speed stirred 1-3 hour。
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