CN105326755A - Additive-free acne-removal nourishing mung bean paper mask and green production method thereof - Google Patents
Additive-free acne-removal nourishing mung bean paper mask and green production method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
Abstract
The invention relates to an additive-free acne-removal nourishing mung bean paper mask and a green production method thereof, belonging to a cosmetic processing technology. The paper mask is prepared elaborately by the processes of continuous activation, disintegration at high pressure, supercritical extraction and the like through adopting the food grade or medicinal and edible raw materials of mung beans, pearls, pine pollen, lily, tremella fuciformis, honeysuckle, dried rose flowers, lemon slices and dried tangerine or orange peel; a product is free of essence, pigment and preservative. The product is good in organoleptic quality and has the functions of clearing away heat and toxic materials and diminishing inflammation and resisting bacteria. The product is suitable for people needing facial skin and beauty care, as well as treatment or remission of skin disease patients with acnes (whelks). A production process of the product is free of generation of pollution, waste residue, waste steam and harmful substances, so that green production is realized; the product is fresh and cool and delicate in fragrance, safe and nontoxic. The product is a novel food grade paper mask. In the production process of the paper mask, no chemical reagent is adopted, no medicine is added, no hormone is added, and thus the paper mask is safe and free of any toxic and side effects.
Description
Technical field
The invention belongs to cosmetics processing technique field, refer in particular to a kind of Semen phaseoli radiati anti-acne maintenance face paper and production method thereof.
Background technology
Facial film is a kind of carrier of skin of face maintenance or cosmetics, applied or be attached to and kept certain hour on the face, when the benefit materials in maintenance or cosmetics is absorbed by the skin, or after in epidermis face, the material of harmful skin health is adsorbed by facial film, removed by cleaning or peeling off, reach the maintenance of facial skin quality or beautify object.Current facial film goods kind and dosage form more, as unguentum, powder, cream, emulsion and with the materials such as non-woven fabrics, silkworm silk, biological fiber for rely on tearing type wet paper towel facial film etc.Beauty treatment or the maintenance principle of facial film utilize it to cover face's certain hour exactly, that skin is temporarily isolated with extraneous air and pollution, improve skin temperature, the pore expansion of skin, promotes sweat gland secretion and metabolism, makes the oxygen content of skin increase, get rid of epidermis cell metabolism product and accumulation oil substances, moisture simultaneously in facial film and beneficiating ingredient infiltrate the horny layer of epidermis, and skin becomes soft, and light is flexible naturally.Generally facial film is divided into mud cream type, tear-pull, gel-type, wet paper towel type four kinds of forms.Especially wet tissue formula face paper, easy to use, effective, be easy to deposit, the people deeply liked to be beautiful likes, occupies very big share rapidly in cosmetics industry.Owing to storing and transporting convenience, cost of transportation is low, and also deeply praise highly by manufacturer, therefore its consumption figure is very big.In many facial skin diseases, the sickness rate of acne is higher, and also known as acne, skin sore, the traditional Chinese medical science claims acne vulgaris ancient times, is dermatology common disease, frequently-occurring disease, and the juvenile onset rate being especially in adolescence is higher, is referred to as " comedo ".According to statistics, have 95% at Adolescent male, women has 85% to suffer from acne in various degree.If treatment not in time or blindly treatment can cause maxillofacial disease more serious, extend the course of disease, even leave the cicatrix being difficult to eradicate, unhealthful and vivid, bring psychological shade to teenager.Acne is that one betides pilosebaceous chronic dermatosis, is mainly in the position that the sebaceous gland such as Head And Face, cervical region, shirtfront back are abundant.Traditional medicine think the main cause of bringing out acne be due to the thick greasy so that taste of surfeit delicious food warm in accumulate upper steaming, or lung meridian intrinsic heat, outward by ailment said due to cold or exposure, or excessive thinking, excited, dysphoria, QI and blood pent up heat-transformation, or digestive tract function disorder, constipation, appoint and rush uncomfortable stagnating in face and cause.Doctor trained in Western medicine thinks that acne is high with Serum Testosterone Levels in human body, sebum secretion is too vigorous, sebaceous gland duct epidermis dyskeratosis blocks hair follicle hole, sebum local accumulation drainage difficulty, corynebacterium acnes (also claiming propionibacterium) infect and make that skin of face tissue produces inflammation and the factors such as edema are relevant.
Patients with acne is except employing Drug therapy, reasonable diet conditioning are lived, and some have the cosmetics of acne-removal function, especially facial film series products due to treatment maintenance have concurrently, easy to use, also deeply welcome by the personage that likes to be beautiful of patients with acne and facial.But the current overwhelming majority alleviates or the facial film goods of Acne treatment all add the medicines such as dexamethasone, chloromycetin, metronidazole, aspirin, clindamycin, erythromycin, chloromycetin, even adds hormones, antibiotic; Or add the additives such as imidazolidinyl urea, Polyethylene Glycol, zinc oxide, propylene glycol, Kaolin.And nearly all add antiseptic, make skin produce drug dependence on the one hand, life-time service develops immunity to drugs; Simultaneously also can, because skin is to the taken in excess of medicine or additive, health be made to produce untoward reaction.
Summary of the invention
The invention provides a kind of additive-free Semen phaseoli radiati anti-acne maintenance face paper and Green production method thereof, this product with Semen phaseoli radiati, Margarita, Pollen Pini, Bulbus Lilii, Flos Lonicerae, Rose Blume Getrocknete, Fructus Citri Limoniae, Pericarpium Citri Reticulatae for primary raw material, do not add any medicine, do not add any chemical addition agent, namely all use food stage or dietotherapeutic raw material, adopt the techniques such as activation, high pressure disintegrate, supercritical extraction, low temperature immersion meticulously to process; Product is not containing essence, pigment, antiseptic, and have heat-clearing and toxic substances removing, antiphlogistic antibacterial effect, product is applicable to each stratum, the treatment of each age group needs facial acne (comedo) or the skin patient of alleviation, also can meet the beauty treatment needs carrying out skin of face maintenance.Process of producing product is pollution-free, produces without waste residue, waste vapour and harmful substance, realizes green production, the salubrious delicate fragrance of product special flavour, safety non-toxic.
The technical scheme that the present invention takes is, is to be obtained by the raw material of following weight portion and step:
25 ~ 35 parts, Semen phaseoli radiati, Margarita 3 ~ 5 parts, Pollen Pini 2 ~ 3 parts, Getrocknete Blumen 1 ~ 3 part, Rose Blume Getrocknete 2 ~ 3 parts, dried lily bulb 1 ~ 2 part, lemon tablet 1 ~ 2 part, dry 1 ~ 2 part of Pericarpium Citri Reticulatae, 0.1 ~ 0.5 part, Tremella;
(1) Semen phaseoli radiati activates continuously and pulverizes
Get and remove impurity when producing the screening of ripe Semen phaseoli radiati seed per year, 8 ~ 15 DEG C of cold water spray washings are clean, send into the boiling hot groove of eddy current leaching in 80 ~ 90 DEG C of water, soak boiling hot 3 ~ 5s, carry out first time activation, then pull rapidly aerobic reciprocating vibration in input 29 ~ 35 DEG C of water out and soak 5 ~ 9h, carry out second time activation processing, frequency of oscillation is 30 ~ 80r/min, it is 1 ~ 3L/h that Xiang Shuizhong passes into air capacity, then circulating water cleaning showers, drain surface moisture, in 40 ~ 45 DEG C, 3 ~ 5min microwave oscillation carries out third time activation processing, then lyophilization is to water content 18 ~ 25%, being crushed to can all by the active Semen phaseoli radiati powder of 60 ~ 100 order aperture sieve, aseptic storage, for subsequent use,
(2) Semen phaseoli radiati, Pollen Pini, the disintegrate of Margarita powder associating high pressure
Crushing pearl to 80 ~ 100 object Margarita powder is for subsequent use, then active Semen phaseoli radiati powder Margarita powder and step () obtained and Pollen Pini are mixed homogeneously, adjustment water content mass percent is 24 ~ 30%, utilize screw extruder rotary extrusion under the condition of pressure 18 ~ 20MPa, temperature 102 ~ 120 DEG C, the macromolecular substances in raw material and hard plant material composition is made at high temperature under high pressure disintegrate to occur, be conducive to the stripping of effective ingredient, extrudate cold drying is to moisture 6 ~ 8%, it is 80 ~ 100 object powder that pulverizing obtains granularity, aseptic storage, for subsequent use;
(3) Tremella, respectively spend dry, lemon tablet and working of Pericarpium Citri Reticulatae and pulverize
Tremella, dried lily bulb are respectively at the process of 8 ~ 15 DEG C of cold water soak 5 ~ 10h rehydrations, then washes clean, the clean surface moisture of drop, in 40 ~ 45 DEG C, 5 ~ 8min microwave oscillation carries out activation processing, then lyophilization is to water content 6 ~ 8%, Bulbus Lilii powder is broken to can all by the powder of 60 ~ 100 order aperture sieve, and aseptic storage is for subsequent use; Tremella powder is broken to can all by the powder of 240 ~ 500 order aperture sieve, and aseptic storage is for subsequent use;
Rose Blume Getrocknete, Getrocknete Blumen, lemon tablet, Pericarpium Citri Reticulatae dry cleaning remove impurity, being crushed to can all by the powder of 40 ~ 100 order aperture sieve, add pure water adjustment water content 30 ~ 35%, in 40 ~ 45 DEG C, 5 ~ 8min microwave oscillation carries out activation processing, then lyophilization is to water content 6 ~ 8%, being crushed to can all by the powder of 60 ~ 100 order aperture sieve, and aseptic storage is for subsequent use;
(4) supercritical extraction
Get the material powder prepared by above-mentioned steps, mix homogeneously, add effective ingredient extraction and guide and support agent, adjustment mixture moisture content is 28 ~ 40%, guide and support the edible ethanol 2% that agent consists of pure water 96%, food stage 3 ° of white vinegars 2%, concentration 30%, then stir, in 45 ~ 60 DEG C, 25 ~ 45MPa, time 60 ~ 120min, CO
2flow 19 ~ 26L/h carries out CO
2supercritical fluid extraction, extract aseptic storage, for subsequent use;
(5) alternating temperature lixiviate
The raffinate of step (four) is taken out from extraction kettle, adds its quality
5 ~ 15deionized water doubly, stirs, and floods 1 ~ 3d, is then separated, filters that obtain can all by the extracting solution of 5 ~ 10 μm of bore filter films, aseptic storage under 15 ~ 30 DEG C of conditions, for subsequent use; Dregs after being separated are added by its mass ratio
4 ~ 6deionized water doubly, stirs, lixiviate 30 ~ 60min under 40 ~ 60 DEG C of conditions, lixiviate 20 ~ 40min under 60 ~ 90 DEG C of conditions, is then separated, filters that obtain can all by the lixiviating solution of 5 ~ 10 μm of bore filter films, aseptic storage, for subsequent use;
(6) allocate, sterilize, flood
Mix homogeneously under the lixiviating solution cleaning condition that the supercritical extract obtain step (four) and step (five) obtain, add Tremella powder, continue to stir, then in 130 ~ 135 DEG C, 4 ~ 9s ultra high temperature short time sterilization, be cooled to 22 ~ 30 DEG C, obtaining the natural Semen phaseoli radiati curing fluid capable of skin of face deposits in aseptic tank, natural silk face paper through aseptic process is put into above-mentioned Semen phaseoli radiati curing fluid capable, in 25 ~ 30 DEG C, 2 ~ 6h is flooded under aseptic condition, take out, smooth, aseptic packaging is in waterproof, in air-locked airtight package bag, be Semen phaseoli radiati anti-acne maintenance face paper product.
Product of the present invention is drug containing and chemical addition agent not, is all made up of food material, and have the safety of food grade products, life-time service has no side effect, and does not produce drug dependence.Additive-free Semen phaseoli radiati anti-acne maintenance face paper, spreads on face during use, peels off after 10 ~ 25min, to wash one's face portion with clear water.Life-time service has skin of face to be removed dirt, beautifies skin of face, antiphlogistic antibacterial, alleviate the effect of acne, desalination comedo cicatrix, skin of face can be made careful, glossy simultaneously.
Raw materials used being of the present invention has heat-clearing and toxic substances removing, the food stage of antiinflammatory antiinflammatory antivirus action or the raw material of dietotherapeutic, and life-time service is without any side effects, specific as follows:
Semen phaseoli radiati (Vignaradiata (Linn.) Wilczek.) belongs to pulse family, has another name called Semen phaseoli radiati, the cultivation history in China's existing 2 over thousands of years, and present East Asia various countries generally plant, and also there are a small amount of plantation in Africa, Europe, the U.S..China is one of main exported country of Semen phaseoli radiati.Every 100g Semen phaseoli radiati is containing 21.6 grams, protein, 0.8 gram, fat, carbohydrate 55.6 grams, dietary fiber 6.4 grams, calcium 81 milligrams, ferrum 6.5 milligrams, 2.18 milligrams, zinc, vitamin e1 0.95 milligram after testing.Modern study shows that Semen phaseoli radiati contains the bioactive ingredients such as flavonoid, tannin, Saponin, alkaloid, plant sterol, coumarin, cardiac glycoside.According to clinical experiment, Semen phaseoli radiati has anti-allergic effects, has inhibitory action to staphylococcus and some virus, energy heat-clearing and toxic substances removing; Semen phaseoli radiati has the effect of the liver protecting, kidney." Kaibao Bencao " is recorded: " Semen phaseoli radiati, sweet, cold, nontoxic.Enter the heart, stomach warp." Compendium of Material Medica record: " Semen phaseoli radiati though the merit of detumescence treatment of smallpox is same as Semen Phaseoli, and presses the power of thermal detoxification to cross it.And QI invigorating, thick the intestines and stomach, qualcomm meridian, without taking avoiding of withered people for a long time.Surgery controls carbuncle, and have expelling the toxic substance from the body with tonic to protect the heart and fall apart, pole says that it is imitated." and " metal and stone, arsenicum, all poison of vegetation can be separated ".Chinese medicine thinks Semen phaseoli radiati sweet in the mouth, cold in nature; Enter the heart, stomach warp; Have heat-clearing and toxic substances removing, relieve summer heat, diuresis, anti-acne effect.
Pericarpium Citri Reticulatae: be the peel of the multiple Citrus chachiensis Hort. classes (CitruschachiensisHort.) such as rutaceae Citrus reticulata Blanco cv. Chachiensis or bowl Citrus chachiensis Hort., containing hesperidin (Hesperidin), Nobiletin (Nobiletin) and volatile oil.Acrid in the mouth, sweet, cold in nature, enter spleen, stomach warp.Have the therapeutic method to keep the adverse QI flowing downwards, adjust in, reduce phlegm, alcoholic intoxication effect.Cure mainly full vexed, the abdominal distention of drinking and eating irregularly, retention of dampness due to stagnation of QI, chest and diaphragm, the disease such as thirsty of getting sick from drinking too much wine.Modern medicine study Citrus chachiensis Hort. C. Suavissima Tanaka contains hesperidin and Citrin, has antiinflammatory, anti-allergic effects.
Fructus Citri Limoniae: the fruit of the evergreen dungarunga Fructus Citri Limoniae (CitrunLimoniaOsbeck) of Rutaceae both citrus.Fructus Citri Limoniae is rich in the multiple nutritional components such as citric acid, malic acid, saccharide, hesperidin, naringin, vitamin C, vitamin B1, vitamin B2, nicotinic acid, calcium, phosphorus, ferrum.Fructus Citri Limoniae sour in the mouth, micro-sweet, property is flat to be slightly cold, and enters liver, stomach warp.There is preventing phlegm from forming and stopping coughing, promote the production of body fluid, the effects such as spleen invigorating, sharp liver, anti-sclerosis, Vitamin C, antibiotic and sterilizing, increase immunity.The diseases such as mainly treating bronchitis, vitamin C deficiency, excessive thirst, inappetence, poor appetite.Modern medicine, Nutritional studies show that Fructus Citri Limoniae is high alka food, have very strong antioxidation, have the effect such as metabolism, promotion liver and expelling toxin, slow down aging, scavenging free radicals, suppression cutaneous pigmentation promoting body.
Bulbus Lilii: edible lily is the underground bulb of Bulbus Lilii, the compositions such as rich in starch and protein, fat, alkaloid, calcium, phosphorus, ferrum and Bulbus Lilii Saponin, removes the functional component such as acyl Bulbus Lilii Saponin, β-D-glucopyanoside.Bulbus Lilii sweet in the mouth, micro-hardship, cold nature, nontoxic, enter the heart, lung meridian.There is the effects such as nourishing the lung to arrest cough, replenishing YIN and removing heat, clearing away heart-fire for tranquillization, sharp defecation.Be usually used in the treatment of the diseases such as chronic cough of deficiency lung, chronic cough spitting of blood, calentura waste heat are clear, fidgets due to deficiency palpitation with fear, insomnia and dreamful sleep.
Margarita powder: Margarita is medicinal in China's history of existing more than 2000 years.The medical ancient books such as the period of Three Kingdoms " Mingyi Bielu ", beam generation " book on Chinese herbal medicine is through collection ", the Tang Dynasty " Haiyao Bencao, Oversea Materia Medica ", Song dynasty " Kaibao Bencao ", Ming Dynasty's Compendium of Material Medica, Qing Dynasty's Leigon's Nature of Drugs in Songs, all have clear and definite record to the curative effect of Margarita.Compendium of Material Medica is recorded, and " Margarita salty in the mouth is sweet cold nontoxic, relieving palpitation point order; Margarita is coated with face, makes us moist good color.------except speckle, antidiarrheal; Except children's's fever (of children) accompanied by fear, peace soul; Only to pass out semen nebulousurine, separate pox and treat poison.Make gloss pure white " etc.Also record in Compendium of Material Medica, Margarita has the effect of desalination freckle, chloasma.Modern medicine study finds, containing a large amount of trace element in Margarita, has antioxidation, strengthens the effects such as skin activity, heat clearing away toxin expelling, whitening, anti-acne, desalination mottle.The Pharmacopoeia of the People's Republic of China and " Chinese medicine voluminous dictionary " are recorded Margarita and are had the effects such as arresting convulsion of calming the nerves, improving eyesight removing nebula, removing toxic substances and promoting granulation.Modern medicine study shows that Margarita powder is improving the effect all in body immunity, slow down aging, freckle removing and whitening, supplement calcium etc. with uniqueness.
Pollen Pini: Pollen Pini is the spermatid of pinaster pistil, having another name called pine yellow, is pure, the dry pollen that pick up from China indigenous tree pinaceae plant Pinus massoniana Lamb (PinusMassonianaLamb.) and Pinus tabuliformis (PinustabulaeformisCarr.).Chinese history just there is the record about " pine is yellow " in first pharmacopeia Shennong's Herbal.Ancient doctor's nationality claims Pollen Pini " sweet, warm, nontoxic ", has functions such as " profit cardiopulmonary, QI invigorating, hemostasis of dispeling the wind, strong Yan Yizhi ".Bright Li Shizhen (1518-1593 A.D.) Compendium of Material Medica: Flos pini, sweet, warm, nontoxic.Profit cardiopulmonary, QI invigorating, hemostasis of dispeling the wind, also can make wine.Pollen Pini is nontoxic, have no side effect, and it does not have the allergen material of sensitization, can not cause pollen allergy yet." dietetic therapy " that China ancient books in the pre-Qin days " Zhou Li " records has established the theory of medicine of Chinese medicine " preventive treatment of disease ", and " Treatise on Dietetic Therapy " that descendant compiles, and all useful Pollen Pini does the record of soup, filling processed, cake, wine brewing.Modern medicine independent studies result also proves that Pollen Pini is nontoxic.
Pollen Pini contains the whole active nutritional compositions needed for life entity, comprising multiple proteins, aminoacid, mineral, enzyme and coenzyme, nucleic acid, monosaccharide, polysaccharide, biotin, cellulose, unsaturated fatty acid, flavone, rutin isoreactivity material, total content reaches more than 200 and plants, and collocation rationally, can supplement, nutrition needed for balancing human body comprehensively.Pollen Pini contains abundant nutrition and functional component, can strengthen skin metabolism, increases skin elasticity, delay skin aging, activating cell, scavenging free radicals, block the generation of chloasma, butterfly spot, eliminate dermal melanin, reduce, remove comedo, make the pure white beauty of skin.
Flos Lonicerae:
flosLonicerae(drawing), the flower that Caprifoliaceae woodbine Radix Ophiopogonis and congener dry flower or band are just opened, originates in China, distribution each province." Flos Lonicerae " one comes from Compendium of Material Medica, owing to opening as white at the beginning of Flos Lonicerae, after transfer yellow to, hence obtain one's name Flos Lonicerae, is described as the good medicine of heat-clearing and toxic substances removing from ancient times.Shennong's Herbal carries: " Flos Lonicerae sweet in the mouth cold in nature, has effect of heat-clearing and toxic substances removing, removing heat from bloodization silt, cure mainly affection due to external wind and heat, pestilence from the beginning of, skin infection furunculosis, red and swollen heat pain, passing stool with blood and pus " etc.Flos Lonicerae is discussed in detail and has the effect of " for a long time clothes make light of one's life by commiting suicide, life lengthening " in Compendium of Material Medica.Flos Lonicerae property sweet cold fragrance, clearing away heat with drugs sweet in flavor and cold in nature and not injuring one's stomach, fragrance thoroughly reaches and can be eliminating evil, can dispelling wind-heat, also kind removing summer-heat blood poison, for various febrile disease, as fever of the body, dermexanthesis, sends out the cards such as speckle, pyretic toxicity carbuncle sore, laryngopharynx swelling and pain.Flos Lonicerae is cold in nature, sweet in the mouth, enters lung, the heart, stomach warp, has heat-clearing and toxic substances removing, antiinflammatory antiinflammatory, tonify deficiency treat effect of wind, cures mainly disease under distension, epidemic febrile disease heating, the diseases such as pyretic toxicity carbuncle and ulcer and tumor.All certain curative effect is had for diseases such as enteritis, measles, pneumonia, epidemic encephalitis, septicemia, skin infection, carbuncle furuncle, erysipelas, parotitis, suppurative tonsillitiss.Flos Lonicerae is just extensive and famous with its medical value since ancient times.
Rose Blume Getrocknete: Flos Rosae Rugosae originates in China, cultivation history is long, it is a kind of Rosaceae chamiso (Rosarugosa), rose hip is edible, be rich in vitamin C, conventional what vanilla tea, fruit jam, fruit jelly, fruit juice and bread etc., Yi You Sweden soup (Nyponsoppa), hydromel (Rhodomel).Flos Rosae Rugosae contains Flos Rosae Rugosae quintessence oil, and main component is that left-handed perfume (or spice) is fragrant and mellow, edible and used for cosmetic, and petal can cake filling processed, cider, rose in syrup, can make tea after drying.Flos Rosae Rugosae sweet in the mouth warm in nature, micro-hardship, return liver, spleen channel.There is circulation of qi promoting soothing liver-QI for relieving depression and the effect such as blood, pain relieving.Cure mainly chest and diaphragm full vexed, the diseases such as gastral cavilty, the side of body rib, menoxenia, traumatic injury, carbuncle." food book on Chinese herbal medicine " calls it, and " main sharp lung spleen, the liver benefiting gallbladder, the fragrance of food is sweet and refreshing, makes us refreshing refreshing." long-term taking, can anti-inflammation and sterilization, allaying tiredness, improve body constitution, moist skin, effectively scavenging free radicals, eliminate pigmentation, beauty treatment etc.
Tremella: another name Tremella, white ear, Mulberry goose, five ancient cooking vessel sesames, the white ears or side handles of a utensil.Property flat, sweet in the mouth, light, nontoxic.Return lung, stomach, kidney channel.The foster lung yin of energy, Ji kidney are dry, QI invigorating of refreshing oneself.Have that nourishing is promoted the production of body fluid, essence strengthening and the kidney invigorating, replenishing YIN and removing heat lung moistening, nourishing the stomach clearing away heat and moistening the bowels, QI replenishing and blood harmonizing, heart tonifying strengthen body, the effect such as supplementing the brain is refreshed oneself, facial beautification and skin rejuvenation function.Tremella also has alleviation muscle fatigue, prevents radiation injury, increases the effects such as immunity of organisms.The tremella polysaccharide contained in Tremella and tremella polysaccharide spore have antiulcer, antiinflammatory action.
The invention provides a kind of additive-free Semen phaseoli radiati anti-acne maintenance face paper with heat-clearing and toxic substances removing, antiphlogistic antibacterial, this product with Semen phaseoli radiati, Margarita, Pollen Pini, Bulbus Lilii, Flos Lonicerae, Flos Rosae Rugosae, lemon tablet, Pericarpium Citri Reticulatae, Tremella for raw material, do not add any medicine, additive, namely all by food stage or dietotherapeutic raw material, the techniques such as activation, high pressure disintegrate, supercritical extraction are adopted meticulously to process; Product is not containing essence, pigment, antiseptic.Product is applicable to each stratum, each age group needs facial care cosmetic needs, and the treatment of acne (comedo) or the skin patient of alleviation.Process of producing product is pollution-free, produces without waste residue, waste vapour and harmful substance, realizes green production; The salubrious delicate fragrance of product special flavour, safety non-toxic, external flush coat is a kind of food stage facial film of new type of safe.Production process of the present invention does not adopt any chemical reagent, and do not add any medicine, do not add any hormone, have the advantages such as nontoxic, pollution-free, easy to operate, life-time service is without any side effects.
Detailed description of the invention
Embodiment 1
Obtained by the raw material of following weight portion and step:
25 parts, Semen phaseoli radiati, Margarita 3 parts, Pollen Pini 2 parts, Getrocknete Blumen 1 part, Rose Blume Getrocknete 2 parts, dried lily bulb 1 part, lemon tablet 1 part, dry 1 part of Pericarpium Citri Reticulatae, 0.1 part, Tremella;
(1) Semen phaseoli radiati activates continuously and pulverizes
Get and remove impurity when producing the screening of ripe Semen phaseoli radiati seed per year, 8 DEG C of cold water spray washings are clean, send into the boiling hot groove of eddy current leaching in 80 DEG C of water, soak boiling hot 5s, carry out first time activation, then pull rapidly aerobic reciprocating vibration in input 29 DEG C of water out and soak 9h, carry out second time activation processing, frequency of oscillation is 30r/min, it is 1L/h that Xiang Shuizhong passes into air capacity, then circulating water cleaning showers, drain surface moisture, in 40 DEG C, 5min microwave oscillation carries out third time activation processing, then lyophilization is to water content 18%, being crushed to can all by the active Semen phaseoli radiati powder of 60 order aperture sieve, aseptic storage, for subsequent use,
(2) Semen phaseoli radiati, Pollen Pini, the disintegrate of Margarita powder associating high pressure
Crushing pearl to 80 object Margarita powder is for subsequent use, then active Semen phaseoli radiati powder Margarita powder and step () obtained and Pollen Pini are mixed homogeneously, adjustment water content mass percent is 24%, utilize screw extruder rotary extrusion under the condition of pressure 18MPa, temperature 102 DEG C, the macromolecular substances in raw material and hard plant material composition is made at high temperature under high pressure disintegrate to occur, be conducive to the stripping of effective ingredient, extrudate cold drying is to moisture 6%, it is 80 object powder that pulverizing obtains granularity, aseptic storage, for subsequent use;
(3) Tremella, respectively spend dry, lemon tablet and working of Pericarpium Citri Reticulatae and pulverize
Tremella, dried lily bulb respectively at the process of 8 DEG C of cold water soak 10h rehydrations, then washes clean, the clean surface moisture of drop, in 40 DEG C, 8min microwave oscillation carries out activation processing, then lyophilization is to water content 6%, and Bulbus Lilii powder is broken to can all by the powder of 60 order aperture sieve, aseptic storage, for subsequent use; Tremella powder is broken to can all by the powder of 240 order aperture sieve, and aseptic storage is for subsequent use;
Rose Blume Getrocknete, Getrocknete Blumen, lemon tablet, Pericarpium Citri Reticulatae dry cleaning remove impurity, being crushed to can all by the powder of 40 order aperture sieve, add pure water adjustment water content 30%, in 40 DEG C, 8min microwave oscillation carries out activation processing, then lyophilization is to water content 6%, being crushed to can all by the powder of 60 order aperture sieve, and aseptic storage is for subsequent use;
(4) supercritical extraction
Get the material powder prepared by above-mentioned steps, mix homogeneously, add effective ingredient extraction and guide and support agent, adjustment mixture moisture content is 28%, guide and support the edible ethanol 2% that agent consists of pure water 96%, food stage 3 ° of white vinegars 2%, concentration 30%, then stir, in 45 DEG C, 25MPa, the time 120min, CO
2flow 19L/h carries out CO
2supercritical fluid extraction, extract aseptic storage, for subsequent use;
(5) alternating temperature lixiviate
The raffinate of step (four) is taken out from extraction kettle, adds its quality
5deionized water doubly, stirs, floods 3d, be then separated under 15 DEG C of conditions, filters that obtain can all by the extracting solution of 5 μm of bore filter films, aseptic storage, for subsequent use; Dregs after being separated are added by its mass ratio
4deionized water doubly, stirs, lixiviate 60min under 40 DEG C of conditions, lixiviate 40min under 60 DEG C of conditions, the lixiviating solution of 5 μm of bore filter films, and aseptic storage is for subsequent use;
(6) allocate, sterilize, flood
Mix homogeneously under the lixiviating solution cleaning condition that the supercritical extract obtain step (four) and step (five) obtain, add Tremella powder, continue to stir, then in 130 DEG C, 9s ultra high temperature short time sterilization, be cooled to 22 DEG C, obtaining the natural Semen phaseoli radiati curing fluid capable of skin of face deposits in aseptic tank, natural silk face paper through aseptic process is put into above-mentioned Semen phaseoli radiati curing fluid capable, in 25 DEG C, flood 6h under aseptic condition, take out, smooth, aseptic packaging in waterproof, air-locked airtight package bag, be Semen phaseoli radiati anti-acne maintenance face paper product.
Embodiment 2
Obtained by the raw material of following weight portion and step:
35 parts, Semen phaseoli radiati, Margarita 5 parts, Pollen Pini 3 parts, Getrocknete Blumen 3 parts, Rose Blume Getrocknete 3 parts, dried lily bulb 2 parts, lemon tablet 2 parts, dry 2 parts of Pericarpium Citri Reticulatae, 0.5 part, Tremella;
(1) Semen phaseoli radiati activates continuously and pulverizes
Get and remove impurity when producing the screening of ripe Semen phaseoli radiati seed per year, 15 DEG C of cold water spray washings are clean, send into the boiling hot groove of eddy current leaching in 90 DEG C of water, soak boiling hot 3s, carry out first time activation, then pull rapidly aerobic reciprocating vibration in input 35 DEG C of water out and soak 5h, carry out second time activation processing, frequency of oscillation is 80r/min, it is 3L/h that Xiang Shuizhong passes into air capacity, then circulating water cleaning showers, drain surface moisture, in 45 DEG C, 3min microwave oscillation carries out third time activation processing, then lyophilization is to water content 25%, being crushed to can all by the active Semen phaseoli radiati powder of 100 order aperture sieve, aseptic storage, for subsequent use,
(2) Semen phaseoli radiati, Pollen Pini, the disintegrate of Margarita powder associating high pressure
Crushing pearl to 100 object Margarita powder is for subsequent use, then active Semen phaseoli radiati powder Margarita powder and step () obtained and Pollen Pini are mixed homogeneously, adjustment water content mass percent is 30%, utilize screw extruder rotary extrusion under the condition of pressure 20MPa, temperature 120 DEG C, the macromolecular substances in raw material and hard plant material composition is made at high temperature under high pressure disintegrate to occur, be conducive to the stripping of effective ingredient, extrudate cold drying is to moisture 8%, it is 100 object powder that pulverizing obtains granularity, aseptic storage, for subsequent use;
(3) Tremella, respectively spend dry, lemon tablet and working of Pericarpium Citri Reticulatae and pulverize
Tremella, dried lily bulb respectively at the process of 15 DEG C of cold water soak 5h rehydrations, then washes clean, the clean surface moisture of drop, in 45 DEG C, 5min microwave oscillation carries out activation processing, then lyophilization is to water content 8%, and Bulbus Lilii powder is broken to can all by the powder of 100 order aperture sieve, aseptic storage, for subsequent use; Tremella powder is broken to can all by the powder of 500 order aperture sieve, and aseptic storage is for subsequent use;
Rose Blume Getrocknete, Getrocknete Blumen, lemon tablet, Pericarpium Citri Reticulatae dry cleaning remove impurity, being crushed to can all by the powder of 100 order aperture sieve, add pure water adjustment water content 35%, in 45 DEG C, 5min microwave oscillation carries out activation processing, then lyophilization is to water content 8%, being crushed to can all by the powder of 100 order aperture sieve, and aseptic storage is for subsequent use;
(4) supercritical extraction
Get the material powder prepared by above-mentioned steps, mix homogeneously, add effective ingredient extraction and guide and support agent, adjustment mixture moisture content is 40%, guide and support the edible ethanol 2% that agent consists of pure water 96%, food stage 3 ° of white vinegars 2%, concentration 30%, then stir, in 60 DEG C, 45MPa, the time 60min, CO
2flow 26L/h carries out CO
2supercritical fluid extraction, extract aseptic storage, for subsequent use;
(5) alternating temperature lixiviate
The raffinate of step (four) is taken out from extraction kettle, adds its quality
15deionized water doubly, stirs, floods 1d, be then separated under 30 DEG C of conditions, filters that obtain can all by the extracting solution of 10 μm of bore filter films, aseptic storage, for subsequent use; Dregs after being separated are added by its mass ratio
6deionized water doubly, stirs, lixiviate 30min under 60 DEG C of conditions, lixiviate 20min under 90 DEG C of conditions, is then separated, filters that obtain can all by the lixiviating solution of 10 μm of bore filter films, aseptic storage, for subsequent use;
(6) allocate, sterilize, flood
Mix homogeneously under the lixiviating solution cleaning condition that the supercritical extract obtain step (four) and step (five) obtain, add Tremella powder, continue to stir, then in 135 DEG C, 4s ultra high temperature short time sterilization, be cooled to 30 DEG C, obtaining the natural Semen phaseoli radiati curing fluid capable of skin of face deposits in aseptic tank, natural silk face paper through aseptic process is put into above-mentioned Semen phaseoli radiati curing fluid capable, in 30 DEG C, flood 2h under aseptic condition, take out, smooth, aseptic packaging in waterproof, air-locked airtight package bag, be Semen phaseoli radiati anti-acne maintenance face paper product.
Embodiment 3
Obtained by the raw material of following weight portion and step:
30 parts, Semen phaseoli radiati, Margarita 4 parts, Pollen Pini 2.5 parts, Getrocknete Blumen 2 parts, Rose Blume Getrocknete 2.5 parts, dried lily bulb 1.5 parts, lemon tablet 1.5 parts, dry 1.5 parts of Pericarpium Citri Reticulatae, 0.3 part, Tremella;
(1) Semen phaseoli radiati activates continuously and pulverizes
Get and remove impurity when producing the screening of ripe Semen phaseoli radiati seed per year, 11 DEG C of cold water spray washings are clean, send into the boiling hot groove of eddy current leaching in 85 DEG C of water, soak boiling hot 4s, carry out first time activation, then pull rapidly aerobic reciprocating vibration in input 32 DEG C of water out and soak 7h, carry out second time activation processing, frequency of oscillation is 55r/min, it is 2L/h that Xiang Shuizhong passes into air capacity, then circulating water cleaning showers, drain surface moisture, in 42.5 DEG C, 4min microwave oscillation carries out third time activation processing, then lyophilization is to water content 22%, being crushed to can all by the active Semen phaseoli radiati powder of 80 order aperture sieve, aseptic storage, for subsequent use,
(2) Semen phaseoli radiati, Pollen Pini, the disintegrate of Margarita powder associating high pressure
Crushing pearl to 90 object Margarita powder is for subsequent use, then active Semen phaseoli radiati powder Margarita powder and step () obtained and Pollen Pini are mixed homogeneously, adjustment water content mass percent is 27%, utilize screw extruder rotary extrusion under the condition of pressure 19MPa, temperature 111 DEG C, the macromolecular substances in raw material and hard plant material composition is made at high temperature under high pressure disintegrate to occur, be conducive to the stripping of effective ingredient, extrudate cold drying is to moisture 7%, it is 90 object powder that pulverizing obtains granularity, aseptic storage, for subsequent use;
(3) Tremella, respectively spend dry, lemon tablet and working of Pericarpium Citri Reticulatae and pulverize
Tremella, dried lily bulb respectively at the process of 11 DEG C of cold water soak 8h rehydrations, then washes clean, the clean surface moisture of drop, in 42.5 DEG C, 7min microwave oscillation carries out activation processing, then lyophilization is to water content 7%, and Bulbus Lilii powder is broken to can all by the powder of 80 order aperture sieve, aseptic storage, for subsequent use; Tremella powder is broken to can all by the powder of 380 order aperture sieve, and aseptic storage is for subsequent use;
Rose Blume Getrocknete, Getrocknete Blumen, lemon tablet, Pericarpium Citri Reticulatae dry cleaning remove impurity, being crushed to can all by the powder of 60 order aperture sieve, add pure water adjustment water content 33%, in 42.5 DEG C, 7min microwave oscillation carries out activation processing, then lyophilization is to water content 7%, being crushed to can all by the powder of 80 order aperture sieve, and aseptic storage is for subsequent use;
(4) supercritical extraction
Get the material powder prepared by above-mentioned steps, mix homogeneously, add effective ingredient extraction and guide and support agent, adjustment mixture moisture content is 34%, guide and support the edible ethanol 2% that agent consists of pure water 96%, food stage 3 ° of white vinegars 2%, concentration 30%, then stir, in 52 DEG C, 35MPa, the time 90min, CO
2flow 23L/h carries out CO
2supercritical fluid extraction, extract aseptic storage, for subsequent use;
(5) alternating temperature lixiviate
The raffinate of step (four) is taken out from extraction kettle, adds its quality
10deionized water doubly, stirs, floods 2d, be then separated under 23 DEG C of conditions, filters that obtain can all by the extracting solution of 8 μm of bore filter films, aseptic storage, for subsequent use; Dregs after being separated are added by its mass ratio
5deionized water doubly, stirs, lixiviate 45min under 50 DEG C of conditions, lixiviate 30min under 75 DEG C of conditions, is then separated, filters that obtain can all by the lixiviating solution of 8 μm of bore filter films, aseptic storage, for subsequent use;
(6) allocate, sterilize, flood
Mix homogeneously under the lixiviating solution cleaning condition that the supercritical extract obtain step (four) and step (five) obtain, add Tremella powder, continue to stir, then in 133 DEG C, 6s ultra high temperature short time sterilization, be cooled to 26 DEG C, obtaining the natural Semen phaseoli radiati curing fluid capable of skin of face deposits in aseptic tank, natural silk face paper through aseptic process is put into above-mentioned Semen phaseoli radiati curing fluid capable, in 27 DEG C, flood 4h under aseptic condition, take out, smooth, aseptic packaging in waterproof, air-locked airtight package bag, be Semen phaseoli radiati anti-acne maintenance face paper product.
The present invention tests respond well through crowd, result is as following table:
Table 1 additive-free Semen phaseoli radiati anti-acne maintenance face paper result of use test result
Claims (2)
1. an additive-free Semen phaseoli radiati anti-acne maintenance face paper, it is characterized in that being obtained by the raw material of following weight portion and step:
25 ~ 35 parts, Semen phaseoli radiati, Margarita 3 ~ 5 parts, Pollen Pini 2 ~ 3 parts, Getrocknete Blumen 1 ~ 3 part, Rose Blume Getrocknete 2 ~ 3 parts, dried lily bulb 1 ~ 2 part, lemon tablet 1 ~ 2 part, dry 1 ~ 2 part of Pericarpium Citri Reticulatae, 0.1 ~ 0.5 part, Tremella;
(1) Semen phaseoli radiati activates continuously and pulverizes
Get and remove impurity when producing the screening of ripe Semen phaseoli radiati seed per year, 8 ~ 15 DEG C of cold water spray washings are clean, send into the boiling hot groove of eddy current leaching in 80 ~ 90 DEG C of water, soak boiling hot 3 ~ 5s, carry out first time activation, then pull rapidly aerobic reciprocating vibration in input 29 ~ 35 DEG C of water out and soak 5 ~ 9h, carry out second time activation processing, frequency of oscillation is 30 ~ 80r/min, it is 1 ~ 3L/h that Xiang Shuizhong passes into air capacity, then circulating water cleaning showers, drain surface moisture, in 40 ~ 45 DEG C, 3 ~ 5min microwave oscillation carries out third time activation processing, then lyophilization is to water content 18 ~ 25%, being crushed to can all by the active Semen phaseoli radiati powder of 60 ~ 100 order aperture sieve, aseptic storage, for subsequent use,
(2) Semen phaseoli radiati, Pollen Pini, the disintegrate of Margarita powder associating high pressure
Crushing pearl to 80 ~ 100 object Margarita powder is for subsequent use, then active Semen phaseoli radiati powder Margarita powder and step () obtained and Pollen Pini are mixed homogeneously, adjustment water content mass percent is 24 ~ 30%, utilize screw extruder rotary extrusion under the condition of pressure 18 ~ 20MPa, temperature 102 ~ 120 DEG C, the macromolecular substances in raw material and hard plant material composition is made at high temperature under high pressure disintegrate to occur, be conducive to the stripping of effective ingredient, extrudate cold drying is to moisture 6 ~ 8%, it is 80 ~ 100 object powder that pulverizing obtains granularity, aseptic storage, for subsequent use;
(3) Tremella, respectively spend dry, lemon tablet and working of Pericarpium Citri Reticulatae and pulverize
Tremella, dried lily bulb are respectively at the process of 8 ~ 15 DEG C of cold water soak 5 ~ 10h rehydrations, then washes clean, the clean surface moisture of drop, in 40 ~ 45 DEG C, 5 ~ 8min microwave oscillation carries out activation processing, then lyophilization is to water content 6 ~ 8%, Bulbus Lilii powder is broken to can all by the powder of 60 ~ 100 order aperture sieve, and aseptic storage is for subsequent use; Tremella powder is broken to can all by the powder of 240 ~ 500 order aperture sieve, and aseptic storage is for subsequent use;
Rose Blume Getrocknete, Getrocknete Blumen, lemon tablet, Pericarpium Citri Reticulatae dry cleaning remove impurity, being crushed to can all by the powder of 40 ~ 100 order aperture sieve, add pure water adjustment water content 30 ~ 35%, in 40 ~ 45 DEG C, 5 ~ 8min microwave oscillation carries out activation processing, then lyophilization is to water content 6 ~ 8%, being crushed to can all by the powder of 60 ~ 100 order aperture sieve, and aseptic storage is for subsequent use;
(4) supercritical extraction
Get the material powder prepared by above-mentioned steps, mix homogeneously, add effective ingredient extraction and guide and support agent, adjustment mixture moisture content is 28 ~ 40%, guide and support the edible ethanol 2% that agent consists of pure water 96%, food stage 3 ° of white vinegars 2%, concentration 30%, then stir, in 45 ~ 60 DEG C, 25 ~ 45MPa, time 60 ~ 120min, CO
2flow 19 ~ 26L/h carries out CO
2supercritical fluid extraction, extract aseptic storage, for subsequent use;
(5) alternating temperature lixiviate
The raffinate of step (four) is taken out from extraction kettle, adds its quality
5 ~ 15deionized water doubly, stirs, and floods 1 ~ 3d, is then separated, filters that obtain can all by the extracting solution of 5 ~ 10 μm of bore filter films, aseptic storage under 15 ~ 30 DEG C of conditions, for subsequent use; Dregs after being separated are added by its mass ratio
4 ~ 6deionized water doubly, stirs, lixiviate 30 ~ 60min under 40 ~ 60 DEG C of conditions, lixiviate 20 ~ 40min under 60 ~ 90 DEG C of conditions, is then separated, filters that obtain can all by the lixiviating solution of 5 ~ 10 μm of bore filter films, aseptic storage, for subsequent use;
(6) allocate, sterilize, flood
Mix homogeneously under the lixiviating solution cleaning condition that the supercritical extract obtain step (four) and step (five) obtain, add Tremella powder, continue to stir, then in 130 ~ 135 DEG C, 4 ~ 9s ultra high temperature short time sterilization, be cooled to 22 ~ 30 DEG C, obtaining the natural Semen phaseoli radiati curing fluid capable of skin of face deposits in aseptic tank, natural silk face paper through aseptic process is put into above-mentioned Semen phaseoli radiati curing fluid capable, in 25 ~ 30 DEG C, 2 ~ 6h is flooded under aseptic condition, take out, smooth, aseptic packaging is in waterproof, in air-locked airtight package bag, be Semen phaseoli radiati anti-acne maintenance face paper product.
2. the Green production method of a kind of additive-free Semen phaseoli radiati anti-acne maintenance face paper as claimed in claim 1, is characterized in that the raw material and the step that comprise following weight portion:
25 ~ 35 parts, Semen phaseoli radiati, Margarita 3 ~ 5 parts, Pollen Pini 2 ~ 3 parts, Getrocknete Blumen 1 ~ 3 part, Rose Blume Getrocknete 2 ~ 3 parts, dried lily bulb 1 ~ 2 part, lemon tablet 1 ~ 2 part, dry 1 ~ 2 part of Pericarpium Citri Reticulatae, 0.1 ~ 0.5 part, Tremella;
(1) Semen phaseoli radiati activates continuously and pulverizes
Get and remove impurity when producing the screening of ripe Semen phaseoli radiati seed per year, 8 ~ 15 DEG C of cold water spray washings are clean, send into the boiling hot groove of eddy current leaching in 80 ~ 90 DEG C of water, soak boiling hot 3 ~ 5s, carry out first time activation, then pull rapidly aerobic reciprocating vibration in input 29 ~ 35 DEG C of water out and soak 5 ~ 9h, carry out second time activation processing, frequency of oscillation is 30 ~ 80r/min, it is 1 ~ 3L/h that Xiang Shuizhong passes into air capacity, then circulating water cleaning showers, drain surface moisture, in 40 ~ 45 DEG C, 3 ~ 5min microwave oscillation carries out third time activation processing, then lyophilization is to water content 18 ~ 25%, being crushed to can all by the active Semen phaseoli radiati powder of 60 ~ 100 order aperture sieve, aseptic storage, for subsequent use,
(2) Semen phaseoli radiati, Pollen Pini, the disintegrate of Margarita powder associating high pressure
Crushing pearl to 80 ~ 100 object Margarita powder is for subsequent use, then active Semen phaseoli radiati powder Margarita powder and step () obtained and Pollen Pini are mixed homogeneously, adjustment water content mass percent is 24 ~ 30%, utilize screw extruder rotary extrusion under the condition of pressure 18 ~ 20MPa, temperature 102 ~ 120 DEG C, the macromolecular substances in raw material and hard plant material composition is made at high temperature under high pressure disintegrate to occur, be conducive to the stripping of effective ingredient, extrudate cold drying is to moisture 6 ~ 8%, it is 80 ~ 100 object powder that pulverizing obtains granularity, aseptic storage, for subsequent use;
(3) Tremella, respectively spend dry, lemon tablet and working of Pericarpium Citri Reticulatae and pulverize
Tremella, dried lily bulb are respectively at the process of 8 ~ 15 DEG C of cold water soak 5 ~ 10h rehydrations, then washes clean, the clean surface moisture of drop, in 40 ~ 45 DEG C, 5 ~ 8min microwave oscillation carries out activation processing, then lyophilization is to water content 6 ~ 8%, Bulbus Lilii powder is broken to can all by the powder of 60 ~ 100 order aperture sieve, and aseptic storage is for subsequent use; Tremella powder is broken to can all by the powder of 240 ~ 500 order aperture sieve, and aseptic storage is for subsequent use;
Rose Blume Getrocknete, Getrocknete Blumen, lemon tablet, Pericarpium Citri Reticulatae dry cleaning remove impurity, being crushed to can all by the powder of 40 ~ 100 order aperture sieve, add pure water adjustment water content 30 ~ 35%, in 40 ~ 45 DEG C, 5 ~ 8min microwave oscillation carries out activation processing, then lyophilization is to water content 6 ~ 8%, being crushed to can all by the powder of 60 ~ 100 order aperture sieve, and aseptic storage is for subsequent use;
(4) supercritical extraction
Get the material powder prepared by above-mentioned steps, mix homogeneously, add effective ingredient extraction and guide and support agent, adjustment mixture moisture content is 28 ~ 40%, guide and support the edible ethanol 2% that agent consists of pure water 96%, food stage 3 ° of white vinegars 2%, concentration 30%, then stir, in 45 ~ 60 DEG C, 25 ~ 45MPa, time 60 ~ 120min, CO
2flow 19 ~ 26L/h carries out CO
2supercritical fluid extraction, extract aseptic storage, for subsequent use;
(5) alternating temperature lixiviate
The raffinate of step (four) is taken out from extraction kettle, adds its quality
5 ~ 15deionized water doubly, stirs, and floods 1 ~ 3d, is then separated, filters that obtain can all by the extracting solution of 5 ~ 10 μm of bore filter films, aseptic storage under 15 ~ 30 DEG C of conditions, for subsequent use; Dregs after being separated are added by its mass ratio
4 ~ 6deionized water doubly, stirs, lixiviate 30 ~ 60min under 40 ~ 60 DEG C of conditions, lixiviate 20 ~ 40min under 60 ~ 90 DEG C of conditions, is then separated, filters that obtain can all by the lixiviating solution of 5 ~ 10 μm of bore filter films, aseptic storage, for subsequent use;
(6) allocate, sterilize, flood
Mix homogeneously under the lixiviating solution cleaning condition that the supercritical extract obtain step (four) and step (five) obtain, add Tremella powder, continue to stir, then in 130 ~ 135 DEG C, 4 ~ 9s ultra high temperature short time sterilization, be cooled to 22 ~ 30 DEG C, obtaining the natural Semen phaseoli radiati curing fluid capable of skin of face deposits in aseptic tank, natural silk face paper through aseptic process is put into above-mentioned Semen phaseoli radiati curing fluid capable, in 25 ~ 30 DEG C, 2 ~ 6h is flooded under aseptic condition, take out, smooth, aseptic packaging is in waterproof, in air-locked airtight package bag, be Semen phaseoli radiati anti-acne maintenance face paper product.
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