CN105287689A - Preparation method of semen trichosanthis - Google Patents
Preparation method of semen trichosanthis Download PDFInfo
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- CN105287689A CN105287689A CN201510779536.2A CN201510779536A CN105287689A CN 105287689 A CN105287689 A CN 105287689A CN 201510779536 A CN201510779536 A CN 201510779536A CN 105287689 A CN105287689 A CN 105287689A
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- fructus trichosanthis
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Abstract
The invention relates to a preparation method of semen trichosanthis, and belongs to the field of medicine production processing. Unsaturated fatty acid content of semen trichosanthis prepared via the preparation method is higher. The preparation method comprises following steps: trichosanthes kirilowii Maxim pulp is removed via biological enzyme-assisted removing, and obtained semen trichosanthis is washed and dried; wherein semen trichosanthis is heated to 90 to 100 DEG C for 30 to 40min of drying, and is cooled to 50 to 70 DEG C for 8 to 10h of drying. The preparation method is capable of shortening washing time and drying time at the same time, and is capable of increasing unsaturated fatty acid content of semen trichosanthis.
Description
Technical field
The present invention relates to a kind of preparation method of Fructus Trichosanthis seed, belong to drug manufacture manufacture field.
Background technology
Fructus Trichosanthis is the perennial dioecism liana of Cucurbitaceae, and the large traditional Chinese medicinal materials assortment of dietotherapeutic, applicating history is long, and medical value is high, at home and abroad has long enjoyed a good reputation.Fructus Trichosanthis not only has very high medical value; and there is higher nutrition and health care value; its peel, kernel; root is all done medicinal, and normal food Fructus Trichosanthis seed is to protection breathing and cardiovascular system, anticancer, treatment diabetes, treatment " three-hypers " and improve body immune function, adjustment endocrine has good effect.
That is familiar with Fructus Trichosanthis along with people gos deep into, it is worth the accreditation more and more obtaining everybody, Fructus Trichosanthis seed demand on edible, medicinal increases, and in Sichuan, Anhui, Zhejiang, the ground cultivated area such as Shandong be also more and more wider, but the technique be stripped out from snake gourd fruit pulp by Fructus Trichosanthis seed is but very loaded down with trivial details.Seed is tightly bundled together by snake gourd fruit pulp, and after peelling off Pericarpium Trichosanthis, snake gourd fruit pulp is wrapped in Fructus Trichosanthis seed tightly, and the many fleshes of seed are hard, and seed is embedded very dark, therefore wants successfully to peel off Fructus Trichosanthis seed fast and is not easy very much.In production practices, the Fructus Trichosanthis seed with snake gourd fruit pulp is put into and is sealed in woven bag or covered with plastic sheeting by medicinal herb growers usually, then water is watered, make its snake gourd fruit pulp corrupt, then after 12 ~ 14 days, by snake gourd fruit pulp eluting, obtain Fructus Trichosanthis seed, usually adopt and hand-launder or stir the disengaging of help snake gourd fruit pulp with waddy in container; In cleaning process, snake gourd fruit pulp gives out strong pungent odor, and turn one's stomach vomiting, and a lot of people is difficult to stand, and therefore Fructus Trichosanthis also has a popular name " dung melon seed ".Even if but through above-mentioned process, snake gourd fruit pulp still not easily eluting; Usually cleaning is also needed 6 ~ 10 times, could by Fructus Trichosanthis seed eluting out, if hand-laundered, the injury of opponent is very large.Therefore the method for traditional eluting Fructus Trichosanthis seed, consumes a large amount of manpower and materials, brings great puzzlement to the melon grower of a large amount of plantation.
Application number be 201410116545.9 Chinese patent application disclose a kind of enzyme and assist the method for sloughing snake gourd fruit pulp, and specifically disclose the Fructus Trichosanthis seed of band flesh put into enzyme solution, after Fructus Trichosanthis seed is separated with flesh, get Fructus Trichosanthis seed, washing, dry, obtain Fructus Trichosanthis seed.But it only adopts conventional drying means, there is the problem that in short or Fructus Trichosanthis seed drying time, unsaturated fatty acid content is lower.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of preparation method of Fructus Trichosanthis seed, and in Fructus Trichosanthis seed prepared by the method, unsaturated fatty acid content is higher.
The preparation method of Fructus Trichosanthis seed of the present invention, comprises the steps: to assist the snake gourd fruit pulp of sloughing band flesh Fructus Trichosanthis seed with enzyme, gets Fructus Trichosanthis seed, washing, dry, obtains Fructus Trichosanthis seed;
Wherein, described drying means is: be first warming up to 90 ~ 100 DEG C of drying 30 ~ 40min, is then cooled to 50 ~ 70 DEG C of drying 8 ~ 10h.
The preparation method of Fructus Trichosanthis seed of the present invention, adopts above-mentioned two sections of intensification drying meanss, compares room temperature or cold drying, effectively can shorten drying time, enhance productivity; Compare and only adopt one section of high temperature drying, the decomposition of unsaturated fatty acid can be prevented, well retain unsaturated fatty acid content in Fructus Trichosanthis seed.First be warming up to 90 ~ 100 DEG C of drying 30 ~ 40min, Fructus Trichosanthis seed surface temperature can be made to raise rapidly, evaporate a large amount of free moistures; Then 50 ~ 70 DEG C of drying 8 ~ 10h are cooled to, over-drying and the excess shrinkage produced due to too fast surface evaporation can be avoided, meanwhile, avoid continuous high temperature to make unsaturated fatty acids acid degradation, thus unsaturated fatty acid content in Fructus Trichosanthis seed is kept.
Further, preferably, described drying means is: first heat up as 95 DEG C of dry 35min, is then cooled to 60 DEG C of dry 9h.
Further, in order to take into account cost and snake gourd fruit pulp sloughs effect, described enzyme assists the method for sloughing snake gourd fruit pulp, comprises the steps:
A, the enzyme solution that band flesh Fructus Trichosanthis seed is put into, wherein, the solid-liquid ratio of band flesh Fructus Trichosanthis seed and enzyme solution is 3 ~ 8:3 ~ 8g/ml, and enzyme solution temperature is 25 ~ 35 DEG C;
B, maintenance enzyme solution temperature 25 ~ 35 DEG C, leave standstill 60 ~ 120h;
C, get Fructus Trichosanthis seed, washing, dry, to obtain final product.
Further, in order to reduce production cost, ensure that snake gourd fruit pulp can be efficiently separated, described enzyme solution concentration is preferably 0.05 ~ 0.75wt%, is more preferably 0.15 ~ 0.65wt%, most preferably is 0.25wt% simultaneously.
Further, in order to enhance productivity, enzyme of the present invention is assisted and is sloughed the enzyme adopted in the method for snake gourd fruit pulp and be preferably at least one in amylase, cellulase; Further, described amylase is preferably α-amylase; At least one in the preferred endoglucanase of described cellulase, exoglucanase, beta glucan glycosides enzyme.
Further, enzymatic solution consumption too much can cause the waste of raw material, consumption is crossed and can be affected snake gourd fruit pulp at least and slough effect, in order to accelerate snake gourd fruit pulp decomposition rate, allow the eluting of Fructus Trichosanthis seed cleaner simultaneously, preferably, the solid-liquid ratio with flesh Fructus Trichosanthis seed and enzyme solution in a step is 4 ~ 7:4 ~ 7g/ml, is preferably 5:6g/ml.
Further, under above-mentioned steps parameter, in order to make Fructus Trichosanthis seed better be separated with flesh, in a and b step, enzyme solution temperature is preferably 30 DEG C; In described b step, time of repose is preferably 65 ~ 84h, is more preferably 72h; Washing times preferably 2 or 3 times in described step c.
The present invention adopts biological enzyme hydrolysis principle to realize, and utilizes enzyme to the hydrolysis property of the organic principle such as starch, saccharide, and the organic principle in snake gourd fruit pulp is decomposed, thus its flesh seed is separated.
Beneficial effect of the present invention:
1, the preparation method of Fructus Trichosanthis seed of the present invention in shortening elution time and while drying time, can retain the unsaturated fatty acid in Fructus Trichosanthis seed, improves its content greatly.
2, obtained Fructus Trichosanthis seed bright color is attractive in appearance, avoids the loss of effective ingredient, can ensure the quality of Fructus Trichosanthis seed.
3, adopt the preparation method of a kind of Fructus Trichosanthis seed of the present invention, have simple to operate, energy-conservation, the benefit that cost is low, can complete processing and the preparation of Fructus Trichosanthis seed without the need to a large amount of manpower.
4, adopt two sections of intensification seasonings to prepare Fructus Trichosanthis seed, effectively can shorten drying time, enhance productivity; Meanwhile, unsaturated fatty acid content in Fructus Trichosanthis seed can well be retained.
Detailed description of the invention
The preparation method of Fructus Trichosanthis seed of the present invention, comprises the steps: to assist the snake gourd fruit pulp of sloughing band flesh Fructus Trichosanthis seed with enzyme, gets Fructus Trichosanthis seed, washing, dry, obtains Fructus Trichosanthis seed;
Wherein, described drying means is: be first warming up to 90 ~ 100 DEG C of drying 30 ~ 40min, is then cooled to 50 ~ 70 DEG C of drying 8 ~ 10h.
The preparation method of Fructus Trichosanthis seed of the present invention, adopts above-mentioned two sections of intensification drying meanss, compares room temperature or cold drying, effectively can shorten drying time, enhance productivity; Compare and only adopt one section of high temperature drying, the decomposition of unsaturated fatty acid can be prevented, well retain unsaturated fatty acid content in Fructus Trichosanthis seed.First be warming up to 90 ~ 100 DEG C of drying 30 ~ 40min, Fructus Trichosanthis seed surface temperature can be made to raise rapidly, evaporate a large amount of free moistures; Then 50 ~ 70 DEG C of drying 8 ~ 10h are cooled to, over-drying and the excess shrinkage produced due to too fast surface evaporation can be avoided, meanwhile, avoid continuous high temperature to make unsaturated fatty acids acid degradation, thus unsaturated fatty acid content in Fructus Trichosanthis seed is kept.
Further, preferably, described drying means is: first heat up as 95 DEG C of dry 35min, is then cooled to 60 DEG C of dry 9h.
Further, in order to take into account cost and snake gourd fruit pulp sloughs effect, described enzyme assists the method for sloughing snake gourd fruit pulp, comprises the steps:
A, the enzyme solution that band flesh Fructus Trichosanthis seed is put into, wherein, the solid-liquid ratio of band flesh Fructus Trichosanthis seed and enzyme solution is 3 ~ 8:3 ~ 8g/ml, and enzyme solution temperature is 25 ~ 35 DEG C;
B, maintenance enzyme solution temperature 25 ~ 35 DEG C, leave standstill 60 ~ 120h;
C, get Fructus Trichosanthis seed, washing, dry, to obtain final product.
Further, in order to reduce production cost, ensure that snake gourd fruit pulp can be efficiently separated, described enzyme solution concentration is preferably 0.05 ~ 0.75wt%, is more preferably 0.15 ~ 0.65wt%, most preferably is 0.25wt% simultaneously.
Further, in order to enhance productivity, enzyme of the present invention is assisted and is sloughed the enzyme adopted in the method for snake gourd fruit pulp and be preferably at least one in amylase, cellulase; Further, described amylase is preferably α-amylase; At least one in the preferred endoglucanase of described cellulase, exoglucanase, beta glucan glycosides enzyme.
Further, enzymatic solution consumption too much can cause the waste of raw material, consumption is crossed and can be affected snake gourd fruit pulp at least and slough effect, in order to accelerate snake gourd fruit pulp decomposition rate, allow the eluting of Fructus Trichosanthis seed cleaner simultaneously, preferably, the solid-liquid ratio with flesh Fructus Trichosanthis seed and enzyme solution in a step is 4 ~ 7:4 ~ 7g/ml, is preferably 5:6g/ml.
Further, under above-mentioned steps parameter, in order to make Fructus Trichosanthis seed better be separated with flesh, in a and b step, enzyme solution temperature is preferably 30 DEG C; In described b step, time of repose is preferably 65 ~ 84h, is more preferably 72h; Washing times preferably 2 or 3 times in described step c.
The present invention adopts biological enzyme hydrolysis principle to realize, and utilizes enzyme to the hydrolysis property of the organic principle such as starch, saccharide, and the organic principle in snake gourd fruit pulp is decomposed, thus its flesh seed is separated.
Below in conjunction with embodiment, the specific embodiment of the present invention is further described, does not therefore limit the present invention among described scope of embodiments.
Embodiment 1
A, fresh Fructus Trichosanthis vertical profile is removed Pericarpium Trichosanthis, obtain band flesh Fructus Trichosanthis seed;
B, 50g is put into flesh Fructus Trichosanthis seed the enzymatic solution that 60ml concentration is 0.15wt%, wherein, in enzymatic solution, enzyme is mixed formed by α-amylase, endoglucanase, exoglucanase, beta glucan glycosides enzyme, and enzymatic solution temperature is 30 DEG C;
C, maintenance enzymatic solution temperature 30 DEG C, leave standstill 72h;
D, with washing the band flesh Fructus Trichosanthis seed and solution mixture that seed floatation equipment eluting obtains through step C process, obtain Fructus Trichosanthis seed;
E, the Fructus Trichosanthis seed drying equipment obtained through D step process are dried Fructus Trichosanthis seed, are first warming up to 90 DEG C of dry 40min, are then cooled to 50 DEG C and carry out dry 10h, obtain dry Fructus Trichosanthis seed;
F, the Fructus Trichosanthis seed fork screening machine of drying through E step carry out selected, obtained.
After measured, in obtained Fructus Trichosanthis seed, unsaturated fatty acid content is 87.35%.
Embodiment 2
A, fresh Fructus Trichosanthis vertical profile is removed Pericarpium Trichosanthis, obtain band flesh Fructus Trichosanthis seed;
B, 50g is put into flesh Fructus Trichosanthis seed the endo-glucanase enzymatic solution that 60ml concentration is 0.25wt%, wherein, enzymatic solution temperature is 30 DEG C;
C, maintenance enzymatic solution temperature 30 DEG C, leave standstill 72h;
D, with washing the band flesh Fructus Trichosanthis seed and solution mixture that seed floatation equipment eluting obtains through step C process, obtain Fructus Trichosanthis seed;
E, the Fructus Trichosanthis seed drying equipment obtained through D step process are dried Fructus Trichosanthis seed, are first warming up to 95 DEG C of dry 35min, are then cooled to 60 DEG C and carry out dry 9h, obtain dry Fructus Trichosanthis seed;
F, the Fructus Trichosanthis seed fork screening machine of drying through E step carry out selected, obtained.
After measured, in obtained Fructus Trichosanthis seed, unsaturated fatty acid content is 89.62%.
Embodiment 3
A, fresh Fructus Trichosanthis vertical profile is removed Pericarpium Trichosanthis, obtain band flesh Fructus Trichosanthis seed;
B, 30g is put into flesh Fructus Trichosanthis seed the α-amylase solution that 30ml concentration is 0.75wt%, wherein, enzymatic solution temperature is 30 DEG C;
C, maintenance enzymatic solution temperature 30 DEG C, leave standstill 96h;
D, with washing the band flesh Fructus Trichosanthis seed and solution mixture that seed floatation equipment eluting obtains through step C process, obtain Fructus Trichosanthis seed;
E, the Fructus Trichosanthis seed drying equipment obtained through D step process are dried Fructus Trichosanthis seed, are first warming up to 100 DEG C of dry 40min, are then cooled to 70 DEG C and carry out dry 8h, obtain dry Fructus Trichosanthis seed;
F, the Fructus Trichosanthis seed fork screening machine of drying through E step carry out selected, obtained.
After measured, in obtained Fructus Trichosanthis seed, unsaturated fatty acid content is 87.57%.
Comparative example
Adopt the method in embodiment 2 to prepare Fructus Trichosanthis seed, just drying steps is different, and in design parameter and the Fructus Trichosanthis seed for preparing, unsaturated fatty acid content sees the following form:
Table 1
| Baking temperature | Drying time | Unsaturated fatty acid content |
| 25℃ | 18h | 88.63％ |
| 50℃ | 14h | 88.75％ |
| 70℃ | 10h | 86.92％ |
| 90℃ | 8h | 79.49％ |
| 100℃ | 6h | 73.21％ |
As can be seen from the above table, adopt cold drying, drying time used is long; Adopt continuous high temperature seasoning, used short, but the loss of unsaturated fatty acid content can not be avoided.This is because in dry run, dry rate is first high rear low, and moisture evaporation rate is directly proportional to dry temperature, and temperature is higher, and moisture evaporation rate is larger, and the cold drying continued makes moisture evaporation rate greatly reduce, thus drying time lengthens.In the high-temperature drying procedures continued, reduce the skin resistance of Fructus Trichosanthis seed shell, promote inner hygroscopic water transfer rate, so dry rate promotes greatly, drying time is short simultaneously; After free hygroscopic water is got rid of, because baking temperature is higher, Fructus Trichosanthis seed inside is made to produce very large moist gradient to surface, too fast surface evaporation will cause significant to shrink and over-drying, simultaneously, excessive temperature easily makes unsaturated fatty acid decompose, and causes the unsaturated fatty acid content in Fructus Trichosanthis seed to reduce.
The present invention adopts two sections of continuous drying legal systems for Fructus Trichosanthis seed, and dry run is first warming up to 90 ~ 100 DEG C of drying 30 ~ 40min, is then cooled to 50 ~ 70 DEG C of drying 8 ~ 10h.First adopt high temperature drying, destroy Fructus Trichosanthis seed shell surface texture, reduce the skin resistance of Fructus Trichosanthis seed shell, evaporate a large amount of Free water; Rear reduction temperature, reduces Fructus Trichosanthis seed inside to surface moisture gradient, avoids the loss of over-drying brought unsaturated fatty acid, remain the content of unsaturated fatty acid in Fructus Trichosanthis seed.
Claims (10)
1. the preparation method of Fructus Trichosanthis seed, is characterized in that comprising the steps: to assist the snake gourd fruit pulp of sloughing band flesh Fructus Trichosanthis seed with enzyme, gets Fructus Trichosanthis seed, washing, dry, obtains Fructus Trichosanthis seed; Wherein, described drying means is: be first warming up to 90 ~ 100 DEG C of drying 30 ~ 40min, is then cooled to 50 ~ 70 DEG C of drying 8 ~ 10h.
2. the preparation method of Fructus Trichosanthis seed according to claim 1, is characterized in that described drying means is: first heat up as 95 DEG C of dry 35min, is then cooled to 60 DEG C of dry 9h.
3. the preparation method of Fructus Trichosanthis seed according to claim 1 and 2, is characterized in that: described enzyme assists the method for the snake gourd fruit pulp of sloughing band flesh Fructus Trichosanthis seed to comprise the steps:
A, the enzyme solution that band flesh Fructus Trichosanthis seed is put into, wherein, described enzyme is at least one in amylase, cellulase, the concentration of enzyme solution is 0.05 ~ 0.75wt%, solid-liquid ratio with flesh Fructus Trichosanthis seed and enzyme solution is 3 ~ 8:3 ~ 8g/ml, and enzyme solution temperature is 25 ~ 35 DEG C;
B, maintenance enzyme solution temperature 25 ~ 35 DEG C, leave standstill 60 ~ 120h;
C, get Fructus Trichosanthis seed, washing, dry, to obtain final product.
4. the preparation method of Fructus Trichosanthis seed according to claim 3, is characterized in that: described amylase is α-amylase, and described cellulase is at least one in endoglucanase, exoglucanase, beta glucan glycosides enzyme.
5. the preparation method of Fructus Trichosanthis seed according to claim 3, is characterized in that: the concentration of described enzyme solution is 0.25wt%.
6. the preparation method of Fructus Trichosanthis seed according to claim 3, is characterized in that: the solid-liquid ratio with flesh Fructus Trichosanthis seed and enzyme solution in a step is 4 ~ 7:4 ~ 7g/ml.
7. the preparation method of Fructus Trichosanthis seed according to claim 3, is characterized in that: the solid-liquid ratio with flesh Fructus Trichosanthis seed and enzyme solution in a step is 5:6g/ml.
8. the preparation method of Fructus Trichosanthis seed according to claim 3, is characterized in that: in a and b step, enzyme solution temperature is 30 DEG C.
9. the preparation method of Fructus Trichosanthis seed according to claim 3, is characterized in that: in b step, time of repose is 65 ~ 84h.
10. the preparation method of Fructus Trichosanthis seed according to claim 3, is characterized in that: in b step, time of repose is 72h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510779536.2A CN105287689B (en) | 2015-11-13 | 2015-11-13 | The preparation method of Snakegourd Fruit seed |
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| CN201510779536.2A CN105287689B (en) | 2015-11-13 | 2015-11-13 | The preparation method of Snakegourd Fruit seed |
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| CN105287689A true CN105287689A (en) | 2016-02-03 |
| CN105287689B CN105287689B (en) | 2019-10-18 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106233872A (en) * | 2016-08-04 | 2016-12-21 | 安徽徽大农业有限公司 | A kind of cucumber seeds extracting method |
| CN107549748A (en) * | 2017-08-12 | 2018-01-09 | 安徽廷龙食品有限公司 | A kind of method for processing Snakegourd Fruit seed |
| CN110016346A (en) * | 2019-03-25 | 2019-07-16 | 北京林业大学 | A kind of desert afforestation water-retaining agent, preparation method and applications |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101889698A (en) * | 2010-06-21 | 2010-11-24 | 衢州市衢天食品有限公司 | Trichosantheskirilowiimaxim seed processing method |
| CN103860624A (en) * | 2014-03-26 | 2014-06-18 | 成都理工大学 | Method for removing fructus trichosanthis pulp by assist of biological enzyme |
-
2015
- 2015-11-13 CN CN201510779536.2A patent/CN105287689B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101889698A (en) * | 2010-06-21 | 2010-11-24 | 衢州市衢天食品有限公司 | Trichosantheskirilowiimaxim seed processing method |
| CN103860624A (en) * | 2014-03-26 | 2014-06-18 | 成都理工大学 | Method for removing fructus trichosanthis pulp by assist of biological enzyme |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106233872A (en) * | 2016-08-04 | 2016-12-21 | 安徽徽大农业有限公司 | A kind of cucumber seeds extracting method |
| CN107549748A (en) * | 2017-08-12 | 2018-01-09 | 安徽廷龙食品有限公司 | A kind of method for processing Snakegourd Fruit seed |
| CN110016346A (en) * | 2019-03-25 | 2019-07-16 | 北京林业大学 | A kind of desert afforestation water-retaining agent, preparation method and applications |
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| CN105287689B (en) | 2019-10-18 |
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