CN105277395A - Garlic source hydrogen sulfide real-time rapid gatherer - Google Patents

Garlic source hydrogen sulfide real-time rapid gatherer Download PDF

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Publication number
CN105277395A
CN105277395A CN201410319724.2A CN201410319724A CN105277395A CN 105277395 A CN105277395 A CN 105277395A CN 201410319724 A CN201410319724 A CN 201410319724A CN 105277395 A CN105277395 A CN 105277395A
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China
Prior art keywords
gas
real
sulfide
garlic
gatherer
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Application number
CN201410319724.2A
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Chinese (zh)
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CN105277395B (en
Inventor
苏彦斌
程瑛琨
李正强
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Jilin Institute of Chemical Technology
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Jilin Institute of Chemical Technology
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Priority to CN201410319724.2A priority Critical patent/CN105277395B/en
Publication of CN105277395A publication Critical patent/CN105277395A/en
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Publication of CN105277395B publication Critical patent/CN105277395B/en
Expired - Fee Related legal-status Critical Current
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Abstract

The invention relates to a garlic source hydrogen sulfide real-time rapid gatherer and belongs to the technical field of biophysics; the garlic source hydrogen sulfide real-time rapid gatherer has characteristics of instantaneous, quickness, trace amount and safety. The gatherer is sealed at the upper part, and three holes are left on the sealed upper part. A spoon for containing reactant sulfide is inserted in the first hole; a glass tubule, containing reagent for reacting with the sulfide to produce H<2>S, is inserted in the second hole; another glass tubule is inserted in the third hole and a detecting reagent is added to the bottom of the glass container via the glass tubule. During determination, the reactant sulfide is added in the spoon, the detecting reagent is added through the glass tubule in the third hole, and the reactant reagent is added through the glass tubule in the second hole, so that trace of H<2>S is generated, free exchange of the H<2>S occurs, the H<2>S reacts with the detecting reagent at the bottom of the glass container; an accurate trace amount of reaction liquid is generated in real time rapidly; and the reaction liquid is collected and H<2>S concentration is determined. The garlic source hydrogen sulfide real-time rapid gatherer is suitable for biomass source H<2>S detection of the biophysics field, research on trace gas production and regulation and control, and research on pharmaceutical application.

Description

Garlic source sulfuretted hydrogen collector real-time
Technical field
The invention belongs to biological micro gas collector technical field, change sulfuretted hydrogen (Hydrogensulfide, H into mainly for detection garlic source sulfide 2s) need to detect real-time to design, belong to micro detecting device category.
Background technology
Detect biological micro H 2s is colourimetry and electrode method mainly, but accurately collects micro-H 2s gas is a difficult problem for biological research fields always, and at present, this difficult problem is not effectively solved.
Summary of the invention
According to biological micro H 2s Cleaning Principle, invention design garlic source H 2s is collector real-time, the advantage of the design: adopt double-layer transparent glass structure, airtight outer bed device, the open inner-layer device of mesh, ectonexine device free exchange, and Real-time Collection is produced by inner-layer device and comes from garlic trace H 2s gas, this device effectively have collected the micro-H that garlic source generates after testing 2s gas, collects fast, accurate and detectability is low, and the outer good airproof performance of this device, internal layer permeability are strong, the research of appropriate biological technical field.
This device adopts sealing double-layer transparent glass container suitable for reading, and vessel volume adopts a series of different specification, to facilitate different amount H 2s measures, and above container, reserve three apertures, first hole is garlic source H 2s holds spoon; Second Kong Weixiang garlic source H 2s holds in spoon to pass into react with sulfide and produces H 2the glass tubule of S gas detect material (chemical reagent, i.e. reactive material); The glass tubule detecting reagent is passed at the bottom of 3rd Kong Weixiang bottle.
Accompanying drawing explanation
Fig. 1 is apparatus of the present invention structural drawing; Fig. 2 is apparatus of the present invention three-view diagrams.In Fig. 1,1. pass into reactive material glass tubule; 2. garlic source H 2s holds spoon; 3. pass into and detect reagent glass tubule; 4. device gland bonnet; 5. device vial.
embodiment
Operate by Fig. 1, the a certain amount of garlic P.E containing sulfide is added in 2., by 1., 2., 3. according in accompanying drawing order insert in the aperture 4. gone up successively, 5. the above-mentioned part installed is gone up by being arranged on shown in accompanying drawing and covering tightly, detection reagent is passed in 3., in 1., pass into reactive material more afterwards, garlic source sulfide and reactive material react in semisphere bucket 2., produce H 2s gas, produces H 2s gas free exchange, flows to full bottle, reacts with detection reagent, after question response is complete, takes out solution in bottle and detects.

Claims (4)

1. one kind gathers H real-time 2the device of S gas, holds H in a device 2s gas detect reagent, then by H 2the agent of S gas detect passes in device, it is characterized in that: adopt double-layer transparent glass structure, airtight outer bed device, the open inner-layer device of mesh, ectonexine device free exchange, the micro-H coming from garlic that Real-time Collection is produced by inner-layer device 2s gas, reserves three apertures above container, and first hole is that garlic source sulfide holds spoon; Second Kong Weixiang garlic source sulfide holds in spoon to pass into react with sulfide and produces H 2the glass tubule of S gas detect material (chemical reagent, i.e. reactive material); The glass tubule detecting reagent is passed at the bottom of 3rd Kong Weixiang bottle.
2. according to claim 1ly gather H real-time 2the device of S gas, is characterized in that: device is airtight, the H produced in device 2s gas can not outflow, and, at H 2s gas will be detected agent absorbent while producing, thus reaches the object implementing Quick Acquisition, and meanwhile, because device is airtight, thus test result can be more accurate.
3. according to claim 1ly gather H real-time 2the device of S gas, is characterized in that: according to different demands, can produce the device of not co-content, different size, to facilitate different amount H 2the mensuration of S.
4. according to claim 1ly gather H real-time 2the device of S gas, is characterized in that: device adopts glass apparatus, thus can not the chemical substance used with experiment react, thus not to can experimental result impact.
CN201410319724.2A 2014-07-08 2014-07-08 The real-time collector of garlic source hydrogen sulfide Expired - Fee Related CN105277395B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410319724.2A CN105277395B (en) 2014-07-08 2014-07-08 The real-time collector of garlic source hydrogen sulfide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410319724.2A CN105277395B (en) 2014-07-08 2014-07-08 The real-time collector of garlic source hydrogen sulfide

Publications (2)

Publication Number Publication Date
CN105277395A true CN105277395A (en) 2016-01-27
CN105277395B CN105277395B (en) 2018-04-06

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Family Applications (1)

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CN201410319724.2A Expired - Fee Related CN105277395B (en) 2014-07-08 2014-07-08 The real-time collector of garlic source hydrogen sulfide

Country Status (1)

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CN (1) CN105277395B (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3997296A (en) * 1975-02-06 1976-12-14 Spex Industries Inc. Primary standards
CN2740285Y (en) * 2004-11-17 2005-11-16 樊红艳 Experimental device for metal reacting with concentrated sulfuric acid
EP2482068A2 (en) * 2010-11-02 2012-08-01 Picarro Inc. Sample preparation for gas analysis using inductive heating
US20130149788A1 (en) * 2011-12-09 2013-06-13 Cornell University Assay for quantifying elemental sulfur levels in a sample

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3997296A (en) * 1975-02-06 1976-12-14 Spex Industries Inc. Primary standards
CN2740285Y (en) * 2004-11-17 2005-11-16 樊红艳 Experimental device for metal reacting with concentrated sulfuric acid
EP2482068A2 (en) * 2010-11-02 2012-08-01 Picarro Inc. Sample preparation for gas analysis using inductive heating
US20130149788A1 (en) * 2011-12-09 2013-06-13 Cornell University Assay for quantifying elemental sulfur levels in a sample

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
SJM20991: "0906朝阳区化学二模练习及答案", 《豆丁网WWW.DOCIN.COM/P-612917841.HTML》 *

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