CN105251031B - A kind of air purifying preparation and preparation method thereof - Google Patents
A kind of air purifying preparation and preparation method thereof Download PDFInfo
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- CN105251031B CN105251031B CN201510827841.4A CN201510827841A CN105251031B CN 105251031 B CN105251031 B CN 105251031B CN 201510827841 A CN201510827841 A CN 201510827841A CN 105251031 B CN105251031 B CN 105251031B
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- 238000002360 preparation method Methods 0.000 title claims abstract description 35
- 241000411851 herbal medicine Species 0.000 claims abstract description 33
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000000341 volatile oil Substances 0.000 claims abstract description 16
- 235000009051 Ambrosia paniculata var. peruviana Nutrition 0.000 claims abstract description 9
- 235000003097 Artemisia absinthium Nutrition 0.000 claims abstract description 9
- 240000001851 Artemisia dracunculus Species 0.000 claims abstract description 9
- 235000017731 Artemisia dracunculus ssp. dracunculus Nutrition 0.000 claims abstract description 9
- 235000003261 Artemisia vulgaris Nutrition 0.000 claims abstract description 9
- 239000001138 artemisia absinthium Substances 0.000 claims abstract description 9
- 239000000463 material Substances 0.000 claims abstract description 9
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000011148 porous material Substances 0.000 claims abstract description 8
- 239000000843 powder Substances 0.000 claims abstract description 7
- 241000432824 Asparagus densiflorus Species 0.000 claims abstract description 6
- 235000009008 Eriobotrya japonica Nutrition 0.000 claims abstract description 6
- 235000008708 Morus alba Nutrition 0.000 claims abstract description 6
- 240000000249 Morus alba Species 0.000 claims abstract description 6
- 235000016639 Syzygium aromaticum Nutrition 0.000 claims abstract description 6
- 244000223014 Syzygium aromaticum Species 0.000 claims abstract description 6
- 239000002904 solvent Substances 0.000 claims abstract description 6
- 241001116389 Aloe Species 0.000 claims abstract description 3
- 235000011399 aloe vera Nutrition 0.000 claims abstract description 3
- 244000061508 Eriobotrya japonica Species 0.000 claims abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
- 239000012141 concentrate Substances 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 239000011521 glass Substances 0.000 claims description 5
- 238000007654 immersion Methods 0.000 claims description 5
- 238000002386 leaching Methods 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 2
- 238000005292 vacuum distillation Methods 0.000 claims description 2
- 241000219780 Pueraria Species 0.000 claims 1
- 238000010521 absorption reaction Methods 0.000 claims 1
- 239000003921 oil Substances 0.000 claims 1
- 238000002604 ultrasonography Methods 0.000 claims 1
- 241000700605 Viruses Species 0.000 abstract description 8
- 244000052616 bacterial pathogen Species 0.000 abstract description 6
- 239000005416 organic matter Substances 0.000 abstract description 6
- 235000010575 Pueraria lobata Nutrition 0.000 abstract description 5
- 244000046146 Pueraria lobata Species 0.000 abstract description 5
- BCNBMSZKALBQEF-UHFFFAOYSA-N 1,3-dimethylpyrrolidin-2-one Chemical class CC1CCN(C)C1=O BCNBMSZKALBQEF-UHFFFAOYSA-N 0.000 abstract description 4
- 125000003118 aryl group Chemical group 0.000 abstract description 2
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 5
- 241001092070 Eriobotrya Species 0.000 description 4
- 239000002689 soil Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 235000014676 Phragmites communis Nutrition 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 239000003344 environmental pollutant Substances 0.000 description 2
- 231100000719 pollutant Toxicity 0.000 description 2
- 235000010894 Artemisia argyi Nutrition 0.000 description 1
- 206010057190 Respiratory tract infections Diseases 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 238000004887 air purification Methods 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 230000000840 anti-viral effect Effects 0.000 description 1
- 244000030166 artemisia Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 206010022000 influenza Diseases 0.000 description 1
- 230000002147 killing effect Effects 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002594 sorbent Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
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- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of air purifying preparation, including following components in percentage by weight：Chinese herbal medicine 10 15%, wormwood essential oil 2 6%, diatomite 25 35%, pore creating material 3 6%, remaining is solvent.The Chinese herbal medicine include following weight than component：White 25 parts of the palm, 46 parts of cloves, 6 14 parts of aloe, 13 parts of asparagus fern, 25 parts of loquat, 6 12 parts of folium isatidis, 13 parts of mulberry leaf, 25 parts of kudzu-vine root powder.The solvent is N, N dimethyl pyrrolidones.Diatomite effectively adsorbs pathogenic bacteria, virus and volatile organic matter in air；Chinese herbal medicine active component and the collaboration of wormwood essential oil remove virus, pathogenic bacteria and volatile organic matter, and the aromatic odor of essential oil creates pure and fresh, pleasant, healthy space to people；Membranaceous air purifying preparation can be attached to the idle spaces such as indoor wall, considerably increase the convenience used.
Description
Technical field
The invention belongs to technical field of air purification, and in particular to a kind of air purifying preparation and preparation method thereof.
Background technology
The most of the time is to spend indoors in human life, and substantial amounts of volatile organic matter, cause are contained in room air
The pollutants such as germ.Research shows that the concentration of the material such as formaldehyde, benzene,toluene,xylene in China resident room will be significantly larger than
International standard.Indoor a large amount of virus and pathogenic bacteria are to cause respiratory tract infection simultaneously, the main reason for the disease such as influenza.
Therefore, conventional holding cleanser with fresh air can not meet many demands of people.It is a kind of with drop to be badly in need of exploitation
Solution volatile organic matter in air, and removal virus, pathogenic bacteria etc. are multi-functional, and air that is nuisanceless, having no toxic side effect is net
Agent.
Chinese herbal medicine is a kind of antiviral natural medicine, containing various active composition, while to the killing action of virus and bacteria
Mechanism is various.Existing air purifying preparation typically has liquid, or is supported on solid absorbent and is fabricated to block (or powder
Shape) adsorbent, so far without the membranaceous air purifying preparation of appearance.
The content of the invention
An object of the present invention provides a kind of air purifying preparation, and the volatility that it can be effectively removed in air is organic
Thing, virus and bacterium.The second purpose is to provide a kind of method of air purifying preparation, Chinese herbal medicine and essential oil is effectively loaded
A kind of membranaceous air purifying preparation is formed on the sorbent, adds the convenience that air purifying preparation uses.
The invention provides a kind of air purifying preparation, including following components in percentage by weight：Chinese herbal medicine 10-15%, Chinese mugwort
Careless essential oil 2-6%, diatomite 25-35%, pore creating material 3-6%, remaining is solvent.
The Chinese herbal medicine include following weight than component：White palm 2-5 parts, cloves 4-6 parts, aloe 6-14 parts, asparagus fern 1-3
Part, loquat 2-5 parts, folium isatidis 6-12 parts, mulberry leaf 1-3 parts, kudzu-vine root powder 2-5 parts.
The solvent is N, N- dimethyl pyrrolidones.
Further, the diatomite is the hydrochloric acid immersion treatment of use quality fraction 10%, the diatom through ultrasonic washing
Soil, filter opening remain intact.
The preparation method of above-mentioned air purifying preparation, comprises the following steps：
(1) Chinese herbal medicine is weighed according to above-mentioned weight ratio, by Chinese herbal medicine co-grinding, adds 15-25 times of weight of Chinese herbal medicine
Ethanol leaches 12h at 65 DEG C, is filtrated to get leaching liquid, and then vacuum distillation obtains concentrate；
(2) concentrate in step (1), wormwood essential oil, diatomite and pore creating material are added to N, N- dimethyl pyrroles
In alkanone, 6-12 hours are stirred at 40-65 DEG C, then standing and defoaming 12 hours, form homogeneous phase solution；
(3) solution obtained by step (2) is cast on a glass, knifing, is then immersed in deionized water, forms Chinese herbal medicine
Membranaceous air purifying preparation over celite is loaded and adsorbed with essential oil.
The beneficial effect that the present invention is compared with the prior art is：
Diatomite effectively adsorbs pathogenic bacteria, virus and volatile organic matter in air；Chinese herbal medicine active component and
Wormwood essential oil synergy removes virus, pathogenic bacteria and volatile organic matter, and the aromatic odor of essential oil brings one
Pure and fresh, pleasant, healthy atmosphere；Membranaceous air purifying preparation can be attached to the idle spaces such as indoor wall, considerably increased
The convenience used.
Embodiment
With reference to embodiment, the invention will be further described.
Embodiment 1
A kind of preparation method of air purifying preparation, comprises the following steps：
(1) Chinese herbal medicine 10g is weighed.The weight ratio of each component is wherein in Chinese herbal medicine：White palm 2-5 parts, cloves 4-6 parts, reed
Luxuriant growth 6-14 parts, asparagus fern 1-3 parts, loquat 2-5 parts, folium isatidis 6-12 parts, mulberry leaf 1-3 parts, kudzu-vine root powder 2-5 parts.Chinese herbal medicine is mixed
Crush, add the ethanol of 15-25 times of weight of Chinese herbal medicine, leach 12h at 65 DEG C, be filtrated to get leaching liquid, be then evaporated in vacuo
Obtain concentrate；
(2) concentrate in step (1), wormwood essential oil 2g, diatomite 25g and pore creating material 3g are added to 60gN, N-
In dimethyl pyrrolidone, 6-12 hours are stirred at 40-65 DEG C, then standing and defoaming 12 hours, form homogeneous phase solution；
(3) solution obtained by step (2) is cast on a glass, knifing, is then immersed in deionized water, forms Chinese herbal medicine
With the membranaceous air purifying preparation of essential oil load over celite.
Further, the diatomite is the hydrochloric acid immersion treatment of use quality fraction 10%, the diatom through ultrasonic washing
Soil, filter opening remain intact.
Embodiment 2
A kind of preparation method of air purifying preparation, comprises the following steps：
(1) Chinese herbal medicine 15g is weighed.The weight ratio of each component is wherein in Chinese herbal medicine：White palm 2-5 parts, cloves 4-6 parts, reed
Luxuriant growth 6-14 parts, asparagus fern 1-3 parts, loquat 2-5 parts, folium isatidis 6-12 parts, mulberry leaf 1-3 parts, kudzu-vine root powder 2-5 parts.Chinese herbal medicine is mixed
Crush, add the ethanol of 15-25 times of weight of Chinese herbal medicine, leach 12h at 65 DEG C, be filtrated to get leaching liquid, be then evaporated in vacuo
Obtain concentrate；
(2) concentrate in step (1), wormwood essential oil 6g, diatomite 35g and pore creating material 6g are added to 38gN, N-
In dimethyl pyrrolidone, 6-12 hours are stirred at 40-65 DEG C, then standing and defoaming 12 hours, form homogeneous phase solution；
(3) solution obtained by step (2) is cast on a glass, knifing, is then immersed in deionized water, forms Chinese herbal medicine
With the membranaceous air purifying preparation of essential oil load over celite.
Further, the diatomite is the hydrochloric acid immersion treatment of use quality fraction 10%, the diatom through ultrasonic washing
Soil, filter opening remain intact.
Embodiment 3
A kind of preparation method of air purifying preparation, comprises the following steps：
(1) Chinese herbal medicine 12g is weighed：The weight ratio of each component is wherein in Chinese herbal medicine：White palm 2-5 parts, cloves 4-6 parts, reed
Luxuriant growth 6-14 parts, asparagus fern 1-3 parts, loquat 2-5 parts, folium isatidis 6-12 parts, mulberry leaf 1-3 parts, kudzu-vine root powder 2-5 parts, Chinese herbal medicine is mixed
Crush, the ethanol for adding 15-25 times of weight of Chinese herbal medicine leaches 12h at 65 DEG C, is filtrated to get leaching liquid, is then distilled in vacuum to give
To concentrate；
(2) concentrate in step (1), wormwood essential oil 4g, diatomite 30g and pore creating material 5g are added to 49gN, N-
In dimethyl pyrrolidone, 6-12 hours are stirred at 40-65 DEG C, then standing and defoaming 12 hours, form homogeneous phase solution；
(3) solution obtained by step (2) is cast on a glass, knifing, is then immersed in deionized water, forms Chinese herbal medicine
With the membranaceous air purifying preparation of essential oil load over celite.
Further, the diatomite is the hydrochloric acid immersion treatment of use quality fraction 10%, the diatom through ultrasonic washing
Soil, filter opening remain intact.
Air purifying preparation diaphragm (4cm*4cm) prepared by embodiment 1-3, is respectively put into a closed container, in container
The formaldehyde and dimethylbenzene that initial concentration is 120mg/L are filled with, the concentration of chromatographic pollutant is used after 120 minutes.
The antibacterial of the membranaceous air purifying preparations of embodiment 1-3 is determined according to the anti-microbial property test method of QB/T2591-2003 antibiotic plastics
Performance.As a result shown in table 1 below：
Table 1
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Formaldehyde clearance (%) | 53 | 66 | 52 |
| Dimethylbenzene clearance (%) | 49 | 57 | 43 |
| Antibiotic rate (%) | 69 | 71 | 65 |
Claims (2)
1. a kind of air purifying preparation, it is characterised in that including following components in percentage by weight：Chinese herbal medicine 10-15%, wormwood essence
Oily 2-6%, diatomite 25-35%, pore creating material 3-6%, remaining is solvent；The Chinese herbal medicine include following weight than component：
White palm 2-5 parts, cloves 4-6 parts, aloe 6-14 parts, asparagus fern 1-3 parts, loquat 2-5 parts, folium isatidis 6-12 parts, mulberry leaf 1-3 parts, Pueraria lobota
Root powder 2-5 parts；The solvent is N, N- dimethyl pyrrolidones, and the preparation method of the air purifying preparation specifically includes following step
Suddenly：
(1) Chinese herbal medicine is weighed according to above-mentioned weight ratio, by Chinese herbal medicine co-grinding, the ethanol of addition 15-25 times of weight of Chinese herbal medicine
12h is leached at 65 DEG C, is filtrated to get leaching liquid, then vacuum distillation obtains concentrate；
(2) concentrate in step (1), wormwood essential oil, diatomite and pore creating material are added to N, N- dimethyl pyrrolidones
In, 6-12 hours are stirred at 40-65 DEG C, then standing and defoaming 12 hours, form homogeneous phase solution；
(3) solution obtained by step (2) is cast on a glass, knifing, is then immersed in deionized water, forms Chinese herbal medicine and essence
The membranaceous air purifying preparation of oil load and absorption over celite.
2. air purifying preparation according to claim 1, it is characterised in that the diatomite is use quality fraction 10%
Hydrochloric acid immersion treatment, the diatomite through ultrasound washing.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510827841.4A CN105251031B (en) | 2015-11-24 | 2015-11-24 | A kind of air purifying preparation and preparation method thereof |
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| CN201510827841.4A CN105251031B (en) | 2015-11-24 | 2015-11-24 | A kind of air purifying preparation and preparation method thereof |
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| CN105251031A CN105251031A (en) | 2016-01-20 |
| CN105251031B true CN105251031B (en) | 2017-12-12 |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106268257A (en) * | 2016-08-31 | 2017-01-04 | 苏州华泰空气过滤器有限公司 | A kind of green air cleanser and preparation method thereof |
| CN106512724A (en) * | 2016-11-22 | 2017-03-22 | 广西南宁益土生物科技有限责任公司 | Plant source deodorant containing folium mori |
| CN108607340A (en) * | 2018-04-30 | 2018-10-02 | 段宝荣 | A kind of air purifying preparation and preparation method thereof |
| CN115895320A (en) * | 2022-11-25 | 2023-04-04 | 鹿寨美源新型涂料科技有限公司 | Antiviral formaldehyde-removing dry powder type coating and preparation method thereof |
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| KR20110000216A (en) * | 2009-06-26 | 2011-01-03 | 주식회사 코즈 | Composition for aromatic containing extracts of pine needlesand, artemisia, green tea leaves and the manufacturing method thereof |
| CN104857545A (en) * | 2014-02-24 | 2015-08-26 | 唐瑜燕 | Incense used for life cultivation and health preservation, and preparation method thereof |
| CN104258441A (en) * | 2014-09-03 | 2015-01-07 | 王晓伟 | Solid air purifying agent and preparation method thereof |
| CN104815544A (en) * | 2015-04-22 | 2015-08-05 | 上海中科昆虫生物技术开发有限公司 | Air purifier |
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