CN105238138A - Strawberry fragrance oil-based varnish for pencil and preparation method of oil-based varnish - Google Patents
Strawberry fragrance oil-based varnish for pencil and preparation method of oil-based varnish Download PDFInfo
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- CN105238138A CN105238138A CN201510672263.1A CN201510672263A CN105238138A CN 105238138 A CN105238138 A CN 105238138A CN 201510672263 A CN201510672263 A CN 201510672263A CN 105238138 A CN105238138 A CN 105238138A
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- strawberry
- oil varnish
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Abstract
The invention provides strawberry fragrance oil-based varnish for a pencil. The oil-based varnish is prepared from, by weight, 1%-10% of microcapsule strawberry essence and 90%-99% of oil-based varnish bodies. The invention further provides a preparation method of the strawberry fragrance oil-based varnish for the pencil. The preparation method includes the steps that the oil-based varnish bodies and the microcapsule strawberry essence are weighed by mass; the oil-based varnish bodies are added into a reaction container and stirred; the microcapsule strawberry essence is added to the oil-based varnish bodies and stirred continuously till strawberry essence microcapsules are evenly dispersed, the strawberry fragrance oil-based varnish for the pencil is obtained, the oil-based varnish with the strawberry fragrance is arranged on the surface of the pencil in a covering mode, and the pencil with the fragrance special to strawberries can be obtained. The strawberry fragrance oil-based varnish for the pencil is stable in mass, light and elegant in fragrance, natural, life-like and durable in fragrance and has the fragrance special to strawberries.
Description
Technical field
The invention belongs to chemical field, relate to a kind of fragrant Oil varnish, particularly a kind of strawberry fragrance pencil Oil varnish and preparation method thereof.
Background technology
Along with the development of modern economy society, the raising of people's living standard, fragrance varnish, relative to traditional varnish, with the fragrance of certain feature, to greatly improve added value and the result of use of varnish, meet the continuous demand of people to material life, so the development of fragrant Oil varnish has market outlook and important using value widely.And a kind of fruit aroma that strawberry aroma is people generally to be liked, she gives off a strong fragrance, and therefore, the development with the pencil Oil varnish of strawberry aroma feature has very important significance.
Summary of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of strawberry fragrance pencil Oil varnish and preparation method thereof, described this strawberry fragrance pencil Oil varnish and preparation method thereof solves pencil Oil varnish of the prior art and layering, system instability easily occurs, and the technical problem that fragrance is pure not, fragrance remaining time is not grown.
The invention provides a kind of strawberry fragrance pencil Oil varnish, count by weight percentage, composition and the content of its raw material are as follows:
Microcapsule strawberry flavour 1%-10%,
Oil varnish 90%-99%.
Described microcapsule strawberry flavour counts by weight percentage, its composition and content as follows:
Strawberry flavour 5%-20%,
Maltodextrin 50%-80%,
Octyl succinic acid starch sodium 5%-30%.
Described Oil varnish counts by weight percentage, its composition and content as follows:
Surplus is the mixed solution of ethyl acetate and Virahol, and in described mixed solution, the mass ratio of ethyl acetate and Virahol is 2:8 ~ 8:2; In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
Present invention also offers the preparation method of above-mentioned a kind of strawberry fragrance pencil Oil varnish, comprise the steps:
1) Oil varnish and microcapsule strawberry flavour is taken according to mass percent;
2) in a reaction vessel, add Oil varnish, open and stir;
3) by microcapsule strawberry flavour, join in the Oil varnish described in step (2), continue to stir, strawberry flavour microcapsule are uniformly dispersed, obtain strawberry fragrance pencil Oil varnish.
Further, the preparation process of described microcapsule strawberry flavour comprises the steps:
1) strawberry flavour, maltodextrin and octyl succinic acid starch sodium is taken according to mass percent;
2) in a reaction vessel, maltodextrin and starch Sodium Octenyl Succinate is added, then deionized water is added, described deionized quality equals maltodextrin and octyl succinic acid starch sodium amount sum, and heated and stirred, until become settled solution system completely;
3) by strawberry flavour, join in the settled solution that step (2) obtains, continue to stir, essence is uniformly dispersed, shear 5-15min with 5000-8000r/min;
4) homogeneous solution that step (3) obtains is carried out spraying dry, the inlet temperature of spray-drying tower is 150-200 DEG C, and temperature out is 80-120 DEG C, obtains microcapsule strawberry flavour from meal outlet.
Further, the preparation process of described Oil varnish comprises the steps:
1) mixed solution of nitrocellulose acetic acid ethyl fluid, Synolac isopropyl alcohol liquid, propyl acetate, toughner, ethyl acetate and Virahol is taken according to mass percent;
2) nitrocellulose acetic acid ethyl fluid, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and a certain proportion of ethyl acetate and Virahol after 20 ~ 50 minutes while stirring, stir 5 ~ 20 minutes again after adding, through filtration after Oil varnish.
Microcapsule strawberry flavour joins in Oil varnish by the present invention by a certain percentage, and constantly stirs, and makes it be dispersed in Oil varnish, namely obtains the Oil varnish with strawberry aroma feature.
A kind of strawberry fragrance pencil Oil varnish of the present invention, has the fragrance of strawberry, thus improves added value and the result of use of Oil varnish.There is not layering, stable system in this strawberry fragrance pencil Oil varnish.Strawberry fragrance Oil varnish is covered with paint, lacquer, colour wash, etc. in pencil surface, the pencil with strawberry characteristic perfume can be obtained.
The present invention compares with prior art, and its technical progress is significant.The invention provides a kind of fragrance remaining time long, pencil Oil varnish with strawberry aroma feature and preparation method thereof.Strawberry fragrance pencil Oil varnish steady quality of the present invention, fragrance is simple and elegant, natural true to nature, and lasting is lasting, has the characteristic perfume of strawberry.
Embodiment
Below by embodiment, the present invention is further described, but does not affect protection scope of the present invention.
Embodiment 1
A kind of strawberry fragrance pencil Oil varnish, count by weight percentage, composition and the content of its raw material are as follows:
Microcapsule strawberry flavour 10%
Oil varnish 90%
Above-mentioned a kind of strawberry fragrance pencil Oil varnish is prepared by the following method, and this preparation process comprises the steps:
(1), in beaker, add 90g Oil varnish, open and stir;
(2), by 10g microcapsule strawberry flavour, be added in the Oil varnish described in step (1), continue to stir, strawberry flavour slow-release microcapsule is uniformly dispersed, obtains the stay-in-grade Oil varnish with strawberry characteristic perfume.
(3), fragrant strawberry Oil varnish is covered with paint, lacquer, colour wash, etc. in pencil surface, the pencil with strawberry characteristic perfume can be obtained.
Above-mentioned microcapsule strawberry flavour, counts by weight percentage, and composition and the content of its raw material are as follows:
Strawberry flavour 5%
Maltodextrin 80%
Starch Sodium Octenyl Succinate 15%
Above-mentioned microcapsule strawberry flavour is prepared by the following method, and this preparation process comprises the steps:
(1), in 250ml beaker, add 80g maltodextrin and 15g starch Sodium Octenyl Succinate, then add the water of 95g, heated and stirred, until hydration becomes settled solution system completely.
(2), by 5g strawberry flavour, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shear 15min with 5000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 180 DEG C, and temperature out is 100 DEG C.Fragrant aroma, strawberry powdered flavor true to nature can be obtained from meal outlet.
Above-mentioned Oil varnish, counts by weight percentage, and composition and the content of its raw material are as follows:
In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
Above-mentioned Oil varnish is prepared by the following method, and this preparation process comprises the steps:
After the title in formula, ratio precise, nitrocellulose acetic acid ethyl fluid in formula, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and a certain proportion of ethyl acetate and Virahol after 30 minutes while stirring, stir 10 minutes again after adding, through filtration after Oil varnish.
The strawberry fragrance pencil Oil varnish steady quality of above-mentioned gained, fragrance is simple and elegant, natural true to nature, and lasting is lasting, has the characteristic perfume of strawberry.
Embodiment 2
A kind of strawberry fragrance pencil Oil varnish, count by weight percentage, composition and the content of its raw material are as follows:
Microcapsule strawberry flavour 1%
Oil varnish 99%
Above-mentioned a kind of strawberry fragrance pencil Oil varnish is prepared by the following method, and this preparation process comprises the steps:
(1), in beaker, add 99g Oil varnish, open and stir;
(2), by 1g microcapsule strawberry flavour, be added drop-wise in the Oil varnish described in step (1), continue to stir, strawberry flavour slow-release microcapsule is uniformly dispersed, obtains the stay-in-grade Oil varnish with strawberry characteristic perfume.
(3), fragrant strawberry Oil varnish is covered with paint, lacquer, colour wash, etc. in pencil surface, the pencil with strawberry characteristic perfume can be obtained.
Above-mentioned microcapsule strawberry flavour, counts by weight percentage, and composition and the content of its raw material are as follows:
Strawberry flavour 20%
Maltodextrin 50%
Starch Sodium Octenyl Succinate 30%
Above-mentioned microcapsule strawberry flavour is prepared by the following method, and this preparation process comprises the steps:
(1), in 250ml beaker, add 50g maltodextrin and 30g starch Sodium Octenyl Succinate, then add the water of 80g, heated and stirred, until hydration becomes settled solution system completely.
(2), by 20g strawberry flavour, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shear 5min with 8000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 180 DEG C, and temperature out is 100 DEG C.Fragrant aroma, strawberry powdered flavor true to nature can be obtained from meal outlet.
Above-mentioned Oil varnish, counts by weight percentage, and composition and the content of its raw material are as follows:
In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
Above-mentioned Oil varnish is prepared by the following method, and this preparation process comprises the steps:
After the title in formula, ratio precise, nitrocellulose acetic acid ethyl fluid in formula, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and a certain proportion of ethyl acetate and Virahol after 30 minutes while stirring, stir 10 minutes again after adding, through filtration after Oil varnish.
The strawberry fragrance pencil Oil varnish steady quality of above-mentioned gained, fragrance is more weak, natural true to nature, and lasting is lasting, has the characteristic perfume of strawberry.
Embodiment 3
A kind of strawberry fragrance pencil Oil varnish, count by weight percentage, composition and the content of its raw material are as follows:
Microcapsule strawberry flavour 10%
Oil varnish 90%
Above-mentioned a kind of strawberry fragrance pencil Oil varnish is prepared by the following method, and this preparation process comprises the steps:
(1), in beaker, add 90g Oil varnish, open and stir;
(2), by 10g microcapsule strawberry flavour, be added drop-wise in the Oil varnish described in step (1), continue to stir, strawberry flavour slow releasing capsule is uniformly dispersed, obtains the stay-in-grade Oil varnish with strawberry characteristic perfume.
(3), fragrant strawberry Oil varnish is covered with paint, lacquer, colour wash, etc. in pencil surface, the pencil with strawberry characteristic perfume can be obtained.
Above-mentioned microcapsule strawberry flavour, counts by weight percentage, and composition and the content of its raw material are as follows:
Strawberry flavour 10%
Maltodextrin 70%
Starch Sodium Octenyl Succinate 20%
Above-mentioned microcapsule strawberry flavour is prepared by the following method, and this preparation process comprises the steps:
(1), in 250ml beaker, add 70g maltodextrin and 20g starch Sodium Octenyl Succinate, then add the water of 90g, heated and stirred, until hydration becomes settled solution system completely.
(2), by 10g strawberry flavour, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shear 10min with 6000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 180 DEG C, and temperature out is 100 DEG C.Fragrant aroma, strawberry powdered flavor true to nature can be obtained from meal outlet.
Above-mentioned Oil varnish, counts by weight percentage, and composition and the content of its raw material are as follows:
In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
Above-mentioned Oil varnish is prepared by the following method, and this preparation process comprises the steps:
After the title in formula, ratio precise, nitrocellulose acetic acid ethyl fluid in formula, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and a certain proportion of ethyl acetate and Virahol after 30 minutes while stirring, stir 10 minutes again after adding, through filtration after Oil varnish.
The strawberry fragrance pencil Oil varnish steady quality of above-mentioned gained, give off a strong fragrance, natural true to nature, lasting is lasting, has the characteristic perfume of strawberry.
Embodiment 4
A kind of strawberry fragrance pencil Oil varnish, count by weight percentage, composition and the content of its raw material are as follows:
Microcapsule strawberry flavour 1%
Oil varnish 99%
Above-mentioned a kind of strawberry fragrance pencil Oil varnish is prepared by the following method, and this preparation process comprises the steps:
(1), in beaker, add 99g Oil varnish, open and stir;
(2), by 1g microcapsule strawberry flavour, be added drop-wise in the Oil varnish described in step (1), continue to stir, strawberry flavour slow-release microcapsule is uniformly dispersed, obtains the stay-in-grade Oil varnish with strawberry characteristic perfume.
(3), fragrant strawberry Oil varnish is covered with paint, lacquer, colour wash, etc. in pencil surface, the pencil with strawberry characteristic perfume can be obtained.
Above-mentioned microcapsule strawberry flavour, counts by weight percentage, and composition and the content of its raw material are as follows:
Strawberry flavour 10%
Maltodextrin 70%
Starch Sodium Octenyl Succinate 20%
Above-mentioned microcapsule strawberry flavour is prepared by the following method, and this preparation process comprises the steps:
(1), in 250ml beaker, add 70g maltodextrin and 20g starch Sodium Octenyl Succinate, then add the water of 90g, heated and stirred, until hydration becomes settled solution system completely.
(2), by 10g strawberry flavour, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shear 5min with 8000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 180 DEG C, and temperature out is 100 DEG C.Fragrant aroma, strawberry powdered flavor true to nature can be obtained from meal outlet.
Above-mentioned Oil varnish, counts by weight percentage, and composition and the content of its raw material are as follows:
In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
Above-mentioned Oil varnish is prepared by the following method, and this preparation process comprises the steps:
After the title in formula, ratio precise, nitrocellulose acetic acid ethyl fluid in formula, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and a certain proportion of ethyl acetate and Virahol after 30 minutes while stirring, stir 10 minutes again after adding, through filtration after Oil varnish.
The strawberry fragrance pencil Oil varnish steady quality of above-mentioned gained, fragrance is faint, natural true to nature, and lasting is lasting, has the characteristic perfume of strawberry.
Embodiment 5
A kind of strawberry fragrance pencil Oil varnish, count by weight percentage, composition and the content of its raw material are as follows:
Microcapsule strawberry flavour 5%
Oil varnish 95%
Above-mentioned a kind of strawberry fragrance pencil Oil varnish is prepared by the following method, and this preparation process comprises the steps:
(1), in beaker, add 95g Oil varnish, open and stir;
(2), by 5g strawberry flavour microcapsule, be added drop-wise in the Oil varnish described in step (1), continue to stir, strawberry flavour slow-release microcapsule is uniformly dispersed, obtains the stay-in-grade Oil varnish with strawberry characteristic perfume.
(3), fragrant strawberry Oil varnish is covered with paint, lacquer, colour wash, etc. in pencil surface, the pencil with strawberry characteristic perfume can be obtained.
Above-mentioned microcapsule strawberry flavour, counts by weight percentage, and composition and the content of its raw material are as follows:
Strawberry flavour 10%
Maltodextrin 70%
Starch Sodium Octenyl Succinate 20%
Above-mentioned microcapsule strawberry flavour is prepared by the following method, and this preparation process comprises the steps:
(1), in 250ml beaker, add 70g maltodextrin and 20g starch Sodium Octenyl Succinate, then add the water of 90g, heated and stirred, until hydration becomes settled solution system completely.
(2), by 10g strawberry flavour, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shear 10min with 6000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 180 DEG C, and temperature out is 100 DEG C.Fragrant aroma, strawberry powdered flavor true to nature can be obtained from meal outlet.
Above-mentioned Oil varnish, counts by weight percentage, and composition and the content of its raw material are as follows:
In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
Above-mentioned Oil varnish is prepared by the following method, and this preparation process comprises the steps:
After the title in formula, ratio precise, nitrocellulose acetic acid ethyl fluid in formula, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and a certain proportion of ethyl acetate and Virahol after 30 minutes while stirring, stir 10 minutes again after adding, through filtration after Oil varnish.
Claims (4)
1. a strawberry fragrance pencil Oil varnish, it is characterized in that counting by weight percentage, composition and the content of its raw material are as follows:
Microcapsule strawberry flavour 1%-10%,
Oil varnish 90%-99%.
Described microcapsule strawberry flavour counts by weight percentage, its composition and content as follows:
Strawberry flavour 5%-20%,
Maltodextrin 50%-80%,
Octyl succinic acid starch sodium 5%-30%.
Described Oil varnish counts by weight percentage, its composition and content as follows:
Surplus is the mixed solution of ethyl acetate and Virahol, and in described mixed solution, the mass ratio of ethyl acetate and Virahol is 2:8 ~ 8:2; In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
2. the preparation method of a kind of strawberry fragrance pencil Oil varnish according to claim 1, is characterized in that comprising the steps:
1) Oil varnish and microcapsule strawberry flavour is taken according to mass percent;
2) in a reaction vessel, add Oil varnish, open and stir;
3) by microcapsule strawberry flavour, join in the Oil varnish described in step (2), continue to stir, strawberry flavour microcapsule are uniformly dispersed, obtain strawberry fragrance pencil Oil varnish.
3. the preparation method of a kind of strawberry fragrance pencil Oil varnish according to claim 2, is characterized in that: the preparation process of described microcapsule strawberry flavour comprises the steps:
1) strawberry flavour, maltodextrin and octyl succinic acid starch sodium is taken according to mass percent;
2) in a reaction vessel, maltodextrin and starch Sodium Octenyl Succinate is added, then deionized water is added, described deionized quality equals maltodextrin and octyl succinic acid starch sodium amount sum, and heated and stirred, until become settled solution system completely;
3) by strawberry flavour, join in the settled solution that step (2) obtains, continue to stir, essence is uniformly dispersed, shear 5-15min with 5000-8000r/min;
4) homogeneous solution that step (3) obtains is carried out spraying dry, the inlet temperature of spray-drying tower is 150-200 DEG C, and temperature out is 80-120 DEG C, obtains microcapsule strawberry flavour from meal outlet.
4. the preparation method of a kind of strawberry fragrance pencil Oil varnish according to claim 2, is characterized in that: the preparation process of described Oil varnish comprises the steps:
1) mixed solution of nitrocellulose acetic acid ethyl fluid, Synolac isopropyl alcohol liquid, propyl acetate, toughner, ethyl acetate and Virahol is taken according to mass percent;
2) nitrocellulose acetic acid ethyl fluid, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and ethyl acetate and Virahol after 20 ~ 50 minutes while stirring, stir 5 ~ 20 minutes again after adding, through filtration after Oil varnish.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510672263.1A CN105238138A (en) | 2015-10-16 | 2015-10-16 | Strawberry fragrance oil-based varnish for pencil and preparation method of oil-based varnish |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510672263.1A CN105238138A (en) | 2015-10-16 | 2015-10-16 | Strawberry fragrance oil-based varnish for pencil and preparation method of oil-based varnish |
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| CN105238138A true CN105238138A (en) | 2016-01-13 |
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| CN201510672263.1A Pending CN105238138A (en) | 2015-10-16 | 2015-10-16 | Strawberry fragrance oil-based varnish for pencil and preparation method of oil-based varnish |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB651855A (en) * | 1946-11-29 | 1951-04-11 | British Celanese | A process for coating cellulose propionate articles and materials |
| CN103695177A (en) * | 2013-12-27 | 2014-04-02 | 广东江大和风香精香料有限公司 | Red jujube flavor and preparation method thereof |
| CN103952036A (en) * | 2014-05-16 | 2014-07-30 | 安硕文教用品（上海）股份有限公司 | Technical method for paint decoration on surface of pencil |
| CN104921047A (en) * | 2015-05-20 | 2015-09-23 | 增城华栋调味品有限公司 | Microcapsule mustard essence and preparation method thereof |
-
2015
- 2015-10-16 CN CN201510672263.1A patent/CN105238138A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB651855A (en) * | 1946-11-29 | 1951-04-11 | British Celanese | A process for coating cellulose propionate articles and materials |
| CN103695177A (en) * | 2013-12-27 | 2014-04-02 | 广东江大和风香精香料有限公司 | Red jujube flavor and preparation method thereof |
| CN103952036A (en) * | 2014-05-16 | 2014-07-30 | 安硕文教用品（上海）股份有限公司 | Technical method for paint decoration on surface of pencil |
| CN104921047A (en) * | 2015-05-20 | 2015-09-23 | 增城华栋调味品有限公司 | Microcapsule mustard essence and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 化学工业部产品销售公司编: "《化工产品手册（统配部管产品）》", 28 February 1982 * |
| 卫秦芝等: "香味文具对中小学生健康的影响", 《现代预防医学》 * |
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Application publication date: 20160113 |