CN105238137A - Coconut fragrant oil varnish for pencil and preparing method thereof - Google Patents
Coconut fragrant oil varnish for pencil and preparing method thereof Download PDFInfo
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- CN105238137A CN105238137A CN201510672253.8A CN201510672253A CN105238137A CN 105238137 A CN105238137 A CN 105238137A CN 201510672253 A CN201510672253 A CN 201510672253A CN 105238137 A CN105238137 A CN 105238137A
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- coconut
- oil varnish
- essence
- pencil
- microcapsule
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Abstract
The invention provides coconut fragrant oil varnish for a pencil. The coconut fragrant oil varnish is prepared from, by weight, 1-10% of micro-capsule coconut essence and 90-99% of oil varnish. The invention further provides a preparing method for the coconut fragrant oil varnish for the pencil. According to the method, the micro-capsule coconut essence and the oil varnish are weighed according to the mass percentage; the oil varnish is added into a reactor, and stirring is started; the micro-capsule coconut essence is added into the oil varnish, stirring continues to be carried out, and therefore the micro-capsule coconut essence can be dispersed uniformly to obtain the coconut fragrant oil varnish for the pencil. The coconut fragrant oil varnish for the pencil has coconut fragrance, so that an additional value and a use effect of the oil varnish are improved; layering of the coconut fragrant oil varnish for the pencil is avoided, and a system is stable; the surface of the pencil is coated with the coconut fragrant oil varnish to obtain the pencil with coconut characteristic fragrance.
Description
Technical field
The invention belongs to chemical field, relate to a kind of fragrant Oil varnish, specifically in particular to a kind of coconut fragrance pencil Oil varnish and preparation method thereof.
Background technology
Along with the development of modern economy society, the raising of people's living standard, fragrance varnish, relative to traditional varnish, with the fragrance of certain feature, to greatly improve added value and the result of use of varnish, meet the continuous demand of people to material life, so the development of fragrant Oil varnish has market outlook and important using value widely.And a kind of fruit aroma that coconut fragrance is people generally to be liked, her fragrance is strong, and therefore, the development with the pencil Oil varnish of coconut odour characteristics has very important significance.
Summary of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of coconut fragrance pencil Oil varnish and preparation method thereof, described this coconut fragrance pencil Oil varnish and preparation method thereof solves pencil Oil varnish of the prior art and layering, system instability easily occurs, and the technical problem that fragrance is pure not, fragrance remaining time is not grown.
A kind of coconut fragrance of the present invention pencil Oil varnish, count by weight percentage, composition and the content of its raw material are as follows:
Microcapsule coconut essence 1%-10%,
Oil varnish 90%-99%,
Described microcapsule coconut essence counts by weight percentage, its composition and content as follows:
Coconut essence 5%-20%,
Maltodextrin 50%-80%,
Octyl succinic acid starch sodium 5%-30%,
Described Oil varnish formula counts by weight percentage, its composition and content as follows:
Surplus is the mixed solution of ethyl acetate and Virahol, and in described mixed solution, the mass ratio of ethyl acetate and Virahol is 2:8 ~ 8:2; In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
Present invention also offers the preparation method of above-mentioned a kind of coconut fragrance pencil Oil varnish, comprise the steps:
1) microcapsule coconut essence, Oil varnish is taken according to mass percent;
2) in a reaction vessel, add Oil varnish, open and stir;
3) by microcapsule coconut essence, join in the Oil varnish described in step (1), continue to stir, coconut essence microcapsule are uniformly dispersed, obtain coconut fragrance pencil Oil varnish.
Further, described microcapsule coconut essence is prepared by the following method:
1) coconut essence, maltodextrin and starch Sodium Octenyl Succinate is taken according to mass percent;
2) in a reaction vessel, maltodextrin and starch Sodium Octenyl Succinate is added, then deionized water is added, described deionized quality equals the quality sum of maltodextrin and octyl succinic acid starch sodium, heated and stirred, until become settled solution system completely;
3) by coconut essence, join in the settled solution that step (2) obtains, continue to stir, essence is uniformly dispersed, shear 5-15min with 5000-8000r/min;
4) homogeneous solution that step (3) obtains is carried out spraying dry, the inlet temperature of spray-drying tower is 150-200 DEG C, and temperature out is 80-120 DEG C, obtains microcapsule coconut essence from meal outlet.
Further, described microcapsule coconut essence is prepared by the following method:
1) mixed solution of nitrocellulose acetic acid ethyl fluid, Synolac isopropyl alcohol liquid, propyl acetate, toughner, ethyl acetate and Virahol is taken according to mass percent;
2) nitrocellulose acetic acid ethyl fluid, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and a certain proportion of ethyl acetate and Virahol after 20 ~ 50 minutes while stirring, stir 5 ~ 20 minutes again after adding, through filtration after Oil varnish.
Microcapsule coconut essence joins in Oil varnish by the present invention by a certain percentage, and constantly stirs, and makes it be dispersed in Oil varnish, namely obtains the Oil varnish with coconut odour characteristics.
The present invention compares with prior art, and its technical progress is significant.The invention provides a kind of fragrance remaining time long, there is the pencil Oil varnish of coconut odour characteristics.A kind of coconut fragrance pencil Oil varnish of the present invention, has the fragrance of coconut, thus improves added value and the result of use of Oil varnish.There is not layering, stable system in this coconut fragrance pencil Oil varnish.Coconut fragrance Oil varnish is covered with paint, lacquer, colour wash, etc. in pencil surface, the pencil with coconut characteristic perfume can be obtained.
Embodiment
Below by embodiment, the present invention is further described, but does not affect protection scope of the present invention.
Embodiment 1
A kind of coconut fragrance pencil Oil varnish, count by weight percentage, composition and the content of its raw material are as follows:
Microcapsule coconut essence 10%
Oil varnish 90%
Above-mentioned a kind of coconut fragrance pencil Oil varnish is prepared by the following method, and this preparation process comprises the steps:
(1), in beaker, add 90g Oil varnish, open and stir;
(2), by 10g microcapsule coconut essence, be added in the Oil varnish described in step (1), continue to stir, coconut essence slow-release microcapsule is uniformly dispersed, obtains the stay-in-grade Oil varnish with coconut characteristic perfume.
(3), fragrant coconut Oil varnish is covered with paint, lacquer, colour wash, etc. in pencil surface, the pencil with coconut characteristic perfume can be obtained.
Above-mentioned microcapsule coconut essence, counts by weight percentage, and composition and the content of its raw material are as follows:
Coconut essence 5%
Maltodextrin 80%
Starch Sodium Octenyl Succinate 15%
Above-mentioned microcapsule coconut essence is prepared by the following method, and this preparation process comprises the steps:
(1), in 250ml beaker, add 80g maltodextrin and 15g starch Sodium Octenyl Succinate, then add the water of 95g, heated and stirred, until hydration becomes settled solution system completely.
(2), by 5g coconut essence, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shear 15min with 5000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 180 DEG C, and temperature out is 100 DEG C.Fragrant aroma, coconut powdered flavor true to nature can be obtained from meal outlet.
Above-mentioned Oil varnish, counts by weight percentage, and composition and the content of its raw material are as follows:
In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
Above-mentioned Oil varnish is prepared by the following method, and this preparation process comprises the steps:
After the title in formula, ratio precise, nitrocellulose acetic acid ethyl fluid in formula, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and a certain proportion of ethyl acetate and Virahol after 30 minutes while stirring, stir 10 minutes again after adding, through filtration after Oil varnish.
The coconut fragrance pencil Oil varnish steady quality of above-mentioned gained, fragrance is simple and elegant, natural true to nature, and lasting is lasting, has the characteristic perfume of coconut.
Embodiment 2
A kind of coconut fragrance pencil Oil varnish, count by weight percentage, composition and the content of its raw material are as follows:
Microcapsule coconut essence 1%
Oil varnish 99%
Above-mentioned a kind of coconut fragrance pencil Oil varnish is prepared by the following method, and this preparation process comprises the steps:
(1), in beaker, add 99g Oil varnish, open and stir;
(2), by 1g microcapsule coconut essence, be added drop-wise in the Oil varnish described in step (1), continue to stir, coconut essence slow-release microcapsule is uniformly dispersed, obtains the stay-in-grade Oil varnish with coconut characteristic perfume.
(3), fragrant coconut Oil varnish is covered with paint, lacquer, colour wash, etc. in pencil surface, the pencil with coconut characteristic perfume can be obtained.
Above-mentioned microcapsule coconut essence, counts by weight percentage, and composition and the content of its raw material are as follows:
Coconut essence 20%
Maltodextrin 50%
Starch Sodium Octenyl Succinate 30%
Above-mentioned microcapsule coconut essence is prepared by the following method, and this preparation process comprises the steps:
(1), in 250ml beaker, add 50g maltodextrin and 30g starch Sodium Octenyl Succinate, then add the water of 80g, heated and stirred, until hydration becomes settled solution system completely.
(2), by 20g coconut essence, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shear 5min with 8000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 180 DEG C, and temperature out is 100 DEG C.Fragrant aroma, coconut powdered flavor true to nature can be obtained from meal outlet.
Above-mentioned Oil varnish, counts by weight percentage, and composition and the content of its raw material are as follows:
In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
Above-mentioned Oil varnish is prepared by the following method, and this preparation process comprises the steps:
After the title in formula, ratio precise, nitrocellulose acetic acid ethyl fluid in formula, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and a certain proportion of ethyl acetate and Virahol after 30 minutes while stirring, stir 10 minutes again after adding, through filtration after Oil varnish.
The coconut fragrance pencil Oil varnish steady quality of above-mentioned gained, fragrance is more weak, natural true to nature, has the characteristic perfume of coconut.
Embodiment 3
A kind of coconut fragrance pencil Oil varnish, count by weight percentage, composition and the content of its raw material are as follows:
Microcapsule coconut essence 10%
Oil varnish 90%
Above-mentioned a kind of coconut fragrance pencil Oil varnish is prepared by the following method, and this preparation process comprises the steps:
(1), in beaker, add 90g Oil varnish, open and stir;
(2), by 10g microcapsule coconut essence, be added drop-wise in the Oil varnish described in step (1), continue to stir, coconut essence slow releasing capsule is uniformly dispersed, obtains the stay-in-grade Oil varnish with coconut characteristic perfume.
(3), fragrant coconut Oil varnish is covered with paint, lacquer, colour wash, etc. in pencil surface, the pencil with coconut characteristic perfume can be obtained.
Above-mentioned microcapsule coconut essence, counts by weight percentage, and composition and the content of its raw material are as follows:
Coconut essence 10%
Maltodextrin 70%
Starch Sodium Octenyl Succinate 20%
Above-mentioned microcapsule coconut essence is prepared by the following method, and this preparation process comprises the steps:
(1), in 250ml beaker, add 70g maltodextrin and 20g starch Sodium Octenyl Succinate, then add the water of 90g, heated and stirred, until hydration becomes settled solution system completely.
(2), by 10g coconut essence, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shear 10min with 6000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 180 DEG C, and temperature out is 100 DEG C.Fragrant aroma, coconut powdered flavor true to nature can be obtained from meal outlet.
Above-mentioned Oil varnish, counts by weight percentage, and composition and the content of its raw material are as follows:
In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
Above-mentioned Oil varnish is prepared by the following method, and this preparation process comprises the steps:
After the title in formula, ratio precise, nitrocellulose acetic acid ethyl fluid in formula, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and a certain proportion of ethyl acetate and Virahol after 30 minutes while stirring, stir 10 minutes again after adding, through filtration after Oil varnish.
The coconut fragrance pencil Oil varnish steady quality of above-mentioned gained, fragrance is strong, natural true to nature, and lasting is lasting, has the characteristic perfume of coconut.
Embodiment 4
A kind of coconut fragrance pencil Oil varnish, count by weight percentage, composition and the content of its raw material are as follows:
Microcapsule coconut essence 1%
Oil varnish 99%
Above-mentioned a kind of coconut fragrance pencil Oil varnish is prepared by the following method, and this preparation process comprises the steps:
(1), in beaker, add 99g Oil varnish, open and stir;
(2), by 1g microcapsule coconut essence, be added drop-wise in the Oil varnish described in step (1), continue to stir, coconut essence slow-release microcapsule is uniformly dispersed, obtains the stay-in-grade Oil varnish with coconut characteristic perfume.
(3), fragrant coconut Oil varnish is covered with paint, lacquer, colour wash, etc. in pencil surface, the pencil with coconut characteristic perfume can be obtained.
Above-mentioned microcapsule coconut essence, counts by weight percentage, and composition and the content of its raw material are as follows:
Coconut essence 10%
Maltodextrin 70%
Starch Sodium Octenyl Succinate 20%
Above-mentioned microcapsule coconut essence is prepared by the following method, and this preparation process comprises the steps:
(1), in 250ml beaker, add 70g maltodextrin and 20g starch Sodium Octenyl Succinate, then add the water of 90g, heated and stirred, until hydration becomes settled solution system completely.
(2), by 10g coconut essence, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shear 5min with 8000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 180 DEG C, and temperature out is 100 DEG C.Fragrant aroma, coconut powdered flavor true to nature can be obtained from meal outlet.
Above-mentioned Oil varnish, counts by weight percentage, and composition and the content of its raw material are as follows:
In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
Above-mentioned Oil varnish is prepared by the following method, and this preparation process comprises the steps:
After the title in formula, ratio precise, nitrocellulose acetic acid ethyl fluid in formula, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and a certain proportion of ethyl acetate and Virahol after 30 minutes while stirring, stir 10 minutes again after adding, through filtration after Oil varnish.
The coconut fragrance pencil Oil varnish steady quality of above-mentioned gained, fragrance is faint, natural true to nature, has the characteristic perfume of coconut.
Embodiment 5
A kind of coconut fragrance pencil Oil varnish, count by weight percentage, composition and the content of its raw material are as follows:
Microcapsule coconut essence 5%
Oil varnish 95%
Above-mentioned a kind of coconut fragrance pencil Oil varnish is prepared by the following method, and this preparation process comprises the steps:
(1), in beaker, add 95g Oil varnish, open and stir;
(2), by 5g coconut essence microcapsule, be added drop-wise in the Oil varnish described in step (1), continue to stir, coconut essence slow-release microcapsule is uniformly dispersed, obtains the stay-in-grade Oil varnish with coconut characteristic perfume.
(3), fragrant coconut Oil varnish is covered with paint, lacquer, colour wash, etc. in pencil surface, the pencil with coconut characteristic perfume can be obtained.
Above-mentioned microcapsule coconut essence, counts by weight percentage, and composition and the content of its raw material are as follows:
Coconut essence 10%
Maltodextrin 70%
Starch Sodium Octenyl Succinate 20%
Above-mentioned microcapsule coconut essence is prepared by the following method, and this preparation process comprises the steps:
(1), in 250ml beaker, add 70g maltodextrin and 20g starch Sodium Octenyl Succinate, then add the water of 90g, heated and stirred, until hydration becomes settled solution system completely.
(2), by 10g coconut essence, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shear 10min with 6000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 180 DEG C, and temperature out is 100 DEG C.Fragrant aroma, coconut powdered flavor true to nature can be obtained from meal outlet.
Above-mentioned Oil varnish, counts by weight percentage, and composition and the content of its raw material are as follows:
In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
Above-mentioned Oil varnish is prepared by the following method, and this preparation process comprises the steps:
After the title in formula, ratio precise, nitrocellulose acetic acid ethyl fluid in formula, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and a certain proportion of ethyl acetate and Virahol after 30 minutes while stirring, stir 10 minutes again after adding, through filtration after Oil varnish.
The coconut fragrance pencil Oil varnish steady quality of above-mentioned gained, fragrance is simple and elegant, natural true to nature, and lasting is lasting, has the characteristic perfume of coconut.
Claims (4)
1. a coconut fragrance pencil Oil varnish, it is characterized in that counting by weight percentage, composition and the content of its raw material are as follows:
Microcapsule coconut essence 1%-10%,
Oil varnish 90%-99%,
Described microcapsule coconut essence counts by weight percentage, its composition and content as follows:
Coconut essence 5%-20%,
Maltodextrin 50%-80%,
Octyl succinic acid starch sodium 5%-30%,
Described Oil varnish formula counts by weight percentage, its composition and content as follows:
Surplus is the mixed solution of ethyl acetate and Virahol, and in described mixed solution, the mass ratio of ethyl acetate and Virahol is 2:8 ~ 8:2; In described nitrocellulose acetic acid ethyl fluid, the mass percent concentration of nitrocellulose is 20% ~ 80%; In described Synolac isopropyl alcohol liquid, the mass percent concentration of Synolac is 20% ~ 80%.
2. the preparation method of a kind of coconut fragrance pencil Oil varnish according to claim 1, is characterized in that comprising the steps:
1) microcapsule coconut essence, Oil varnish is taken according to mass percent;
2) in a reaction vessel, add Oil varnish, open and stir;
3) by microcapsule coconut essence, join in the Oil varnish described in step (1), continue to stir, coconut essence microcapsule are uniformly dispersed, obtain coconut fragrance pencil Oil varnish.
3. the preparation method of a kind of coconut fragrance pencil Oil varnish according to claim 2, is characterized in that described microcapsule coconut essence is prepared by the following method:
1) coconut essence, maltodextrin and starch Sodium Octenyl Succinate is taken according to mass percent;
2) in a reaction vessel, maltodextrin and starch Sodium Octenyl Succinate is added, then deionized water is added, described deionized quality equals the quality sum of maltodextrin and octyl succinic acid starch sodium, heated and stirred, until become settled solution system completely;
3) by coconut essence, join in the settled solution that step (2) obtains, continue to stir, essence is uniformly dispersed, shear 5-15min with 5000-8000r/min;
4) homogeneous solution that step (3) obtains is carried out spraying dry, the inlet temperature of spray-drying tower is 150-200 DEG C, and temperature out is 80-120 DEG C, obtains microcapsule coconut essence from meal outlet.
4. the preparation method of a kind of coconut fragrance pencil Oil varnish according to claim 2, is characterized in that described microcapsule coconut essence is prepared by the following method:
1) mixed solution of nitrocellulose acetic acid ethyl fluid, Synolac isopropyl alcohol liquid, propyl acetate, toughner, ethyl acetate and Virahol is taken according to mass percent;
2) nitrocellulose acetic acid ethyl fluid, Synolac isopropyl alcohol liquid are put into mould wash mixer and stirred, stir the mixed solution adding propyl acetate, toughner and ethyl acetate and Virahol after 20 ~ 50 minutes while stirring, stir 5 ~ 20 minutes again after adding, through filtration after Oil varnish.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510672253.8A CN105238137A (en) | 2015-10-16 | 2015-10-16 | Coconut fragrant oil varnish for pencil and preparing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510672253.8A CN105238137A (en) | 2015-10-16 | 2015-10-16 | Coconut fragrant oil varnish for pencil and preparing method thereof |
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| CN105238137A true CN105238137A (en) | 2016-01-13 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB651855A (en) * | 1946-11-29 | 1951-04-11 | British Celanese | A process for coating cellulose propionate articles and materials |
| CN103695177A (en) * | 2013-12-27 | 2014-04-02 | 广东江大和风香精香料有限公司 | Red jujube flavor and preparation method thereof |
| CN103952036A (en) * | 2014-05-16 | 2014-07-30 | 安硕文教用品（上海）股份有限公司 | Technical method for paint decoration on surface of pencil |
| CN104921047A (en) * | 2015-05-20 | 2015-09-23 | 增城华栋调味品有限公司 | Microcapsule mustard essence and preparation method thereof |
-
2015
- 2015-10-16 CN CN201510672253.8A patent/CN105238137A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB651855A (en) * | 1946-11-29 | 1951-04-11 | British Celanese | A process for coating cellulose propionate articles and materials |
| CN103695177A (en) * | 2013-12-27 | 2014-04-02 | 广东江大和风香精香料有限公司 | Red jujube flavor and preparation method thereof |
| CN103952036A (en) * | 2014-05-16 | 2014-07-30 | 安硕文教用品（上海）股份有限公司 | Technical method for paint decoration on surface of pencil |
| CN104921047A (en) * | 2015-05-20 | 2015-09-23 | 增城华栋调味品有限公司 | Microcapsule mustard essence and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 化学工业部产品销售公司编: "《化工产品手册（统配部管产品）》", 28 February 1982 * |
| 卫秦芝等: "香味文具对中小学生健康的影响", 《现代预防医学》 * |
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Application publication date: 20160113 |