CN105232396A - Biologically-ultraviolet-proof blusher cosmetic composition and preparation method thereof - Google Patents
Biologically-ultraviolet-proof blusher cosmetic composition and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/08—Preparations containing skin colorants, e.g. pigments for cheeks, e.g. rouge
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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Abstract
The invention provides a biologically-ultraviolet-proof blusher cosmetic composition. The biologically-ultraviolet-proof blusher cosmetic composition is prepared from the following components in parts by weight: 20-35 parts of mycosporine-like amino acid, 0.5-5 parts of an ultraviolet light absorber, and 60-70 parts of camellia haematochrome. The invention further provides a preparation method of the biologically-ultraviolet-proof blusher cosmetic composition. The biologically-ultraviolet-proof blusher cosmetic composition has the beneficial effects of the biologically-ultraviolet-proof function and the skin-brightening function without chemical stimulation.
Description
Technical field
The present invention relates to rouge cosmetic technical field.More particularly, the present invention relates to and there is biological anti-ultraviolet and skin is played to the biological anti-ultraviolet rouge cosmetic composition highlighting excellent specific property.
Background technology
When Ozone hole problem is day by day serious, the ultraviolet radiation (especially UVB) arriving ground and water body is more and more stronger.The effect of the ultraviolet radiation that all aquatiles all may be strengthened day by day, these effects comprise the change of the macromolecular substances such as protein and DNA structure, and the chronic suppression of reacting some key physiological and acute injury etc.
Class mycetocyte element aminoacid be a kind of have uv-protection, with the pure natural anti-ultraviolet biologic artifact of Cutaneous permeation compatibility effect, it exists in a large number in Thallus Porphyrae, and its non-stimulated anti-ultraviolet function be applied in cosmetics exists important value.And in prior art, the rouge with biological anti-ultraviolet function does not but exist, along with the irradiation of intense UV rays, multilamellar protection is carried out to skin quite important.
Summary of the invention
As the result of various extensive and careful research and experiment, the present inventor has been found that, when adding the pure-natural biological composition containing specific anti-ultraviolet and highlight the natural plant extract of skin in biological sun care preparations, described bio-extract component contributes to improving the anti-ultraviolet of sun care preparations and highlighting the performance of skin.Based on this discovery, complete the present invention.
An object of the present invention is to solve at least the problems referred to above or defect, and the advantage will illustrated at least is below provided.
A further object of the invention is to provide a kind of biological rouge cosmetics with anti-ultraviolet, and it by adding the composition of the anti-ultraviolet of biological pure natural, can prevent the damage of outer bound pair skin, to skin without any stimulation, using natural gentleness.
A further object of the invention is by adding by extracting the biological pigment of red pigment from camellia japonica as rouge from Flos Camelliae Japonicae in biological rouge cosmetics; improve containing the utilization rate of various effective ingredient plant, highlight to obtain better to play skin, moisten and the pure natural plant ingredients of protective effect.
In order to realize according to these objects of the present invention and other advantage, provide a kind of biological anti-ultraviolet rouge cosmetic composition, described compositions comprises following component by weight: 20 ~ 35 parts, class mycetocyte element sample aminoacid, UV absorbent 0.5 ~ 5 part, red pigment from camellia japonica 60-70 part.
Preferably, wherein, described UV absorbent is one or more of plant Anthraquinones, Flavonoids and plant polyphenol apoplexy due to endogenous wind.
Preferably, wherein, described plant Anthraquinones is one or more of sequestered Anthraquinones, reduced form Anthraquinones and quinone glycoside apoplexy due to endogenous wind.
Preferably, wherein, described compositions comprises following component by weight: 30 parts, class mycetocyte element sample aminoacid, UV absorbent 2.5 parts, red pigment from camellia japonica 65 parts.
Object of the present invention still further provides the preparation method of biological anti-ultraviolet rouge cosmetic composition, and described method comprises:
Step one, choose Thallus Porphyrae as class mycetocyte element sample amino acid whose extraction source, the silt in cleaning Thallus Porphyrae, in vacuum freeze drier, carry out drying, baking temperature is-10 ~-30 DEG C, and drying time is 15 ~ 20h; Secondly, get dried Thallus Porphyrae 10g, be dissolved in the methanol of 500mL, 2 ~ 2.5h is heated with 50 ~ 60 DEG C, cooling, high speed centrifugation, centrifugal rotating speed is 3000 ~ 3500 revs/min, time is 5 ~ 6min, filter, add wherein in the dichloromethane of 800mL, high speed centrifugation, centrifugal rotating speed is 3000 ~ 3500 revs/min, time is 5 ~ 6min, obtains transparent supernatant, when noble gas, evaporative removal solvent, the deionized water dissolving adding 50mL is prepared into high performance liquid chromatography sample; Finally, carry out high performance liquid chromatography separation and draw pure class mycetocyte element sample aminoacid, wherein, high performance liquid chromatography separation condition is: column temperature: 30 DEG C, mobile phase 0.2% glacial acetic acid aqueous solution, and flow velocity is 0.5mL/min, mensuration wavelength is 330nm, and sample size is 20 μ L, sample introduction 30min analysis time;
Step 2, choose Flos Camelliae Japonicae and as the extraction source of red pigment from camellia japonica, red pigment from camellia japonica is extracted, specifically comprise: the citric acid-sodium citrate buffer of preparation pH=4.50, after the fragmentation of fresh Flos Camelliae Japonicae petal, under 40 ~ 65 DEG C of temperature conditions, the citric acid-sodium citrate buffer of 15 ~ 30 milliliters of preparation pH=4.75 is used, soak extraction 9 ~ 12h by every gram of fresh Flos Camelliae Japonicae petal; Soak is filtered rear absorption with macroporous adsorbent resin; With the ethanol water eluting macroporous adsorbent resin that mass ratio is 75%, elution flow rate is 12 ~ 15BV/h, collects eluent; Red pigment from camellia japonica is obtained after eluent being adopted vacuum rotary evaporator spin concentration, vacuum lyophilization;
The preparation of step 3, biological anti-ultraviolet rouge cosmetic composition: one or more of selection plant Anthraquinones, Flavonoids and plant polyphenol apoplexy due to endogenous wind are as UV absorbent, in UV absorbent described in 0.5 ~ 5 weight portion, add class mycetocyte element sample aminoacid 20 ~ 35 parts of weight portions that described step one obtains and the red pigment from camellia japonica 60-70 weight portion that described step 2 obtains, carry out ultramicronising by dry pulverization process technology or waterproof pulverization technology and obtain biological sun care preparations.
Preferably, wherein, in described step one, the baking temperature of vacuum lyophilization is-20 DEG C, and drying time is 18h.
Preferably, wherein, in step 2, the baking temperature of vacuum lyophilization is-20 ~-30 DEG C, and drying time is 15 ~ 18h.
Preferably, wherein, what the ultramicronising in described step 3 adopted is dynamic high-pressure microjet ultramicronising technology, concrete steps: shearing, broken and homogenizing, wherein operating pressure is 150 ~ 180MPa, and operating temperature is 20 ~ 25 DEG C.
The present invention at least comprises following beneficial effect:
The present invention's biological anti-ultraviolet rouge cosmetics overcome the defect of the effect in traditional rouge without anti-ultraviolet, and add harsh chemicals and defect that is carcinogenic or toxic chemical in a large number in traditional rouge, the present invention adopts Pure natural cosmetic composition, the composition of biological preventing ultraviolet effect is added in the rouge of pure natural components, therefore, it is possible to effective protection skin is not by the damage of the foul such as extraneous various ray and grieshoch, biological anti-ultraviolet composition and biology is adopted to highlight skin composition, to skin without any stimulation, total care is carried out to skin and has highlighted, the crowd of sensitive skin can be widely used in, owing to taking, active component extracting method is carried out to the pure natural plant containing effective ingredient, therefore, it is possible to improve the utilization rate of plant, without adding any toxic chemical solvent in whole leaching process, and ultramicronising has been carried out to the biological anti-ultraviolet rouge cosmetics formed, skin can be absorbed better.
Part is embodied by explanation below by other advantage of the present invention, target and feature, part also will by research and practice of the present invention by those skilled in the art is understood.
Detailed description of the invention
Below in conjunction with the present invention is described in further detail, can implement according to this with reference to description word to make those skilled in the art.
Should be appreciated that used hereinly such as " to have ", other element one or more do not allotted in " comprising " and " comprising " term or the existence of its combination or interpolation.
< example 1>
A kind of biological anti-ultraviolet rouge cosmetic composition, described compositions comprises following component by weight: 30 parts, class mycetocyte element sample aminoacid, UV absorbent 2.5 parts, red pigment from camellia japonica 65 parts.
Wherein, described UV absorbent is plant Anthraquinones and Flavonoids mixture, and described plant Anthraquinones is one or more of sequestered Anthraquinones, reduced form Anthraquinones and quinone glycoside apoplexy due to endogenous wind.
The preparation method of described biological anti-ultraviolet rouge cosmetic composition, described method comprises:
Step one, choose Thallus Porphyrae as class mycetocyte element sample amino acid whose extraction source, the silt in cleaning Thallus Porphyrae, in vacuum freeze drier, carry out drying, baking temperature is-10 ~-30 DEG C, and drying time is 15 ~ 20h; Secondly, get dried Thallus Porphyrae 10g, be dissolved in the methanol of 500mL, 2 ~ 2.5h is heated with 50 ~ 60 DEG C, cooling, high speed centrifugation, centrifugal rotating speed is 3000 ~ 3500 revs/min, time is 5 ~ 6min, filter, add wherein in the dichloromethane of 800mL, high speed centrifugation, centrifugal rotating speed is 3000 ~ 3500 revs/min, time is 5 ~ 6min, obtains transparent supernatant, when noble gas, evaporative removal solvent, the deionized water dissolving adding 50mL is prepared into high performance liquid chromatography sample; Finally, carry out high performance liquid chromatography separation and draw pure class mycetocyte element sample aminoacid, wherein, high performance liquid chromatography separation condition is: column temperature: 30 DEG C, mobile phase 0.2% glacial acetic acid aqueous solution, flow velocity is 0.5mL/min, and mensuration wavelength is 330nm, and sample size is 20 μ L, sample introduction 30min analysis time, wherein, the baking temperature of vacuum lyophilization is-20 DEG C, and drying time is 18h;
Step 2, choose Flos Camelliae Japonicae and as the extraction source of red pigment from camellia japonica, red pigment from camellia japonica is extracted, specifically comprise: the citric acid-sodium citrate buffer of preparation pH=4.50, after the fragmentation of fresh Flos Camelliae Japonicae petal, under 40 ~ 65 DEG C of temperature conditions, the citric acid-sodium citrate buffer of 15 ~ 30 milliliters of preparation pH=4.75 is used, soak extraction 9 ~ 12h by every gram of fresh Flos Camelliae Japonicae petal; Soak is filtered rear absorption with macroporous adsorbent resin; With the ethanol water eluting macroporous adsorbent resin that mass ratio is 75%, elution flow rate is 12 ~ 15BV/h, collects eluent; Obtain red pigment from camellia japonica after eluent being adopted vacuum rotary evaporator spin concentration, vacuum lyophilization, wherein, the baking temperature of vacuum lyophilization is-25 DEG C, and drying time is 16h;
Step 3, the preparation of biological anti-ultraviolet rouge cosmetic composition: select plant Anthraquinones and Flavonoids mixture as UV absorbent, class mycetocyte element sample aminoacid 30 parts of weight portions that described step one obtains and red pigment from camellia japonica 65 weight portion that described step 2 obtains is added in UV absorbent described in 2.5 weight portions, carry out ultramicronising by dry pulverization process technology or waterproof pulverization technology and obtain biological sun care preparations, wherein, what ultramicronising adopted is dynamic high-pressure microjet ultramicronising technology, concrete steps: shear, fragmentation and homogenizing, wherein operating pressure is 160MPa, operating temperature is 25 DEG C.
Obtained biological anti-ultraviolet rouge cosmetics are through system destructive testing, and to skin without any damage, and the every sense index of product, physical and chemical index, sanitary index all meet corresponding national standard.
< example 2>
A kind of biological anti-ultraviolet rouge cosmetic composition, described compositions comprises following component by weight: 20 parts, class mycetocyte element sample aminoacid, UV absorbent 0.5 part, red pigment from camellia japonica 60 parts.
Wherein, described UV absorbent is plant Anthraquinones and plant polyphenol kind mixture, and described plant Anthraquinones is one or more of sequestered Anthraquinones, reduced form Anthraquinones and quinone glycoside apoplexy due to endogenous wind.
The preparation method of described biological anti-ultraviolet rouge cosmetic composition, described method comprises:
Step one, choose Thallus Porphyrae as class mycetocyte element sample amino acid whose extraction source, the silt in cleaning Thallus Porphyrae, in vacuum freeze drier, carry out drying, baking temperature is-10 ~-30 DEG C, and drying time is 15 ~ 20h; Secondly, get dried Thallus Porphyrae 10g, be dissolved in the methanol of 500mL, 2 ~ 2.5h is heated with 50 ~ 60 DEG C, cooling, high speed centrifugation, centrifugal rotating speed is 3000 ~ 3500 revs/min, time is 5 ~ 6min, filter, add wherein in the dichloromethane of 800mL, high speed centrifugation, centrifugal rotating speed is 3000 ~ 3500 revs/min, time is 5 ~ 6min, obtains transparent supernatant, when noble gas, evaporative removal solvent, the deionized water dissolving adding 50mL is prepared into high performance liquid chromatography sample; Finally, carry out high performance liquid chromatography separation and draw pure class mycetocyte element sample aminoacid, wherein, high performance liquid chromatography separation condition is: column temperature: 30 DEG C, mobile phase 0.2% glacial acetic acid aqueous solution, flow velocity is 0.5mL/min, and mensuration wavelength is 330nm, and sample size is 20 μ L, sample introduction 30min analysis time, wherein, the baking temperature of vacuum lyophilization is-20 DEG C, and drying time is 18h;
Step 2, choose Flos Camelliae Japonicae and as the extraction source of red pigment from camellia japonica, red pigment from camellia japonica is extracted, specifically comprise: the citric acid-sodium citrate buffer of preparation pH=4.50, after the fragmentation of fresh Flos Camelliae Japonicae petal, under 40 ~ 65 DEG C of temperature conditions, the citric acid-sodium citrate buffer of 15 ~ 30 milliliters of preparation pH=4.75 is used, soak extraction 9 ~ 12h by every gram of fresh Flos Camelliae Japonicae petal; Soak is filtered rear absorption with macroporous adsorbent resin; With the ethanol water eluting macroporous adsorbent resin that mass ratio is 75%, elution flow rate is 12 ~ 15BV/h, collects eluent; Obtain red pigment from camellia japonica after eluent being adopted vacuum rotary evaporator spin concentration, vacuum lyophilization, wherein, the baking temperature of vacuum lyophilization is-20 DEG C, and drying time is 18h;
Step 3, the preparation of biological anti-ultraviolet rouge cosmetic composition: select plant Anthraquinones and plant polyphenol kind mixture as UV absorbent, class mycetocyte element sample aminoacid 20 parts of weight portions that described step one obtains and red pigment from camellia japonica 60 weight portion that described step 2 obtains is added in UV absorbent described in 0.5 weight portion, carry out ultramicronising by dry pulverization process technology or waterproof pulverization technology and obtain biological sun care preparations, wherein, what ultramicronising adopted is dynamic high-pressure microjet ultramicronising technology, concrete steps: shear, fragmentation and homogenizing, wherein operating pressure is 150MPa, operating temperature is 20 DEG C.
Obtained biological anti-ultraviolet rouge cosmetics are through system destructive testing, and to skin without any damage, and the every sense index of product, physical and chemical index, sanitary index all meet corresponding national standard.
< example 3>
A kind of biological anti-ultraviolet rouge cosmetic composition, described compositions comprises following component by weight: 35 parts, class mycetocyte element sample aminoacid, UV absorbent 5 parts, red pigment from camellia japonica 70 parts.
Wherein, described UV absorbent is plant Anthraquinones, and described plant Anthraquinones is one or more of sequestered Anthraquinones, reduced form Anthraquinones and quinone glycoside apoplexy due to endogenous wind.
The preparation method of described biological anti-ultraviolet rouge cosmetic composition, described method comprises:
Step one, choose Thallus Porphyrae as class mycetocyte element sample amino acid whose extraction source, the silt in cleaning Thallus Porphyrae, in vacuum freeze drier, carry out drying, baking temperature is-10 ~-30 DEG C, and drying time is 15 ~ 20h; Secondly, get dried Thallus Porphyrae 10g, be dissolved in the methanol of 500mL, 2 ~ 2.5h is heated with 50 ~ 60 DEG C, cooling, high speed centrifugation, centrifugal rotating speed is 3000 ~ 3500 revs/min, time is 5 ~ 6min, filter, add wherein in the dichloromethane of 800mL, high speed centrifugation, centrifugal rotating speed is 3000 ~ 3500 revs/min, time is 5 ~ 6min, obtains transparent supernatant, when noble gas, evaporative removal solvent, the deionized water dissolving adding 50mL is prepared into high performance liquid chromatography sample; Finally, carry out high performance liquid chromatography separation and draw pure class mycetocyte element sample aminoacid, wherein, high performance liquid chromatography separation condition is: column temperature: 30 DEG C, mobile phase 0.2% glacial acetic acid aqueous solution, flow velocity is 0.5mL/min, and mensuration wavelength is 330nm, and sample size is 20 μ L, sample introduction 30min analysis time, wherein, the baking temperature of vacuum lyophilization is-20 DEG C, and drying time is 18h;
Step 2, choose Flos Camelliae Japonicae and as the extraction source of red pigment from camellia japonica, red pigment from camellia japonica is extracted, specifically comprise: the citric acid-sodium citrate buffer of preparation pH=4.50, after the fragmentation of fresh Flos Camelliae Japonicae petal, under 40 ~ 65 DEG C of temperature conditions, the citric acid-sodium citrate buffer of 15 ~ 30 milliliters of preparation pH=4.75 is used, soak extraction 9 ~ 12h by every gram of fresh Flos Camelliae Japonicae petal; Soak is filtered rear absorption with macroporous adsorbent resin; With the ethanol water eluting macroporous adsorbent resin that mass ratio is 75%, elution flow rate is 12 ~ 15BV/h, collects eluent; Obtain red pigment from camellia japonica after eluent being adopted vacuum rotary evaporator spin concentration, vacuum lyophilization, wherein, the baking temperature of vacuum lyophilization is-30 DEG C, and drying time is 15h;
Step 3, the preparation of biological anti-ultraviolet rouge cosmetic composition: select plant Anthraquinones as UV absorbent, class mycetocyte element sample aminoacid 35 parts of weight portions that described step one obtains and red pigment from camellia japonica 70 weight portion that described step 2 obtains is added in UV absorbent described in 5 weight portions, carry out ultramicronising by dry pulverization process technology or waterproof pulverization technology and obtain biological sun care preparations, wherein, what ultramicronising adopted is dynamic high-pressure microjet ultramicronising technology, concrete steps: shear, fragmentation and homogenizing, wherein operating pressure is 180MPa, operating temperature is 25 DEG C.
Obtained biological anti-ultraviolet rouge cosmetics are through system destructive testing, and to skin without any damage, and the every sense index of product, physical and chemical index, sanitary index all meet corresponding national standard.
Visible, the present invention's biological anti-ultraviolet rouge cosmetics overcome the defect of the effect in traditional rouge without anti-ultraviolet, and add harsh chemicals and defect that is carcinogenic or toxic chemical in a large number in traditional rouge, the present invention adopts Pure natural cosmetic composition, the composition of biological preventing ultraviolet effect is added in the rouge of pure natural components, therefore, it is possible to effective protection skin is not by the damage of the foul such as extraneous various ray and grieshoch, biological anti-ultraviolet composition and biology is adopted to highlight skin composition, to skin without any stimulation, total care is carried out to skin and has highlighted, the crowd of sensitive skin can be widely used in, owing to taking, active component extracting method is carried out to the pure natural plant containing effective ingredient, therefore, it is possible to improve the utilization rate of plant, without adding any toxic chemical solvent in whole leaching process, and ultramicronising has been carried out to the biological anti-ultraviolet rouge cosmetics formed, skin can be absorbed better.
Although embodiment of the present invention are open as above, it is not restricted to listed in description and embodiment utilization.It can be applied to various applicable the field of the invention completely.For those skilled in the art, can easily realize other amendment.Therefore do not deviating under the general concept that claim and equivalency range limit, the present invention is not limited to specific details and illustrates here and the legend described.
Claims (8)
1. a biological anti-ultraviolet rouge cosmetic composition, described compositions comprises following component by weight: 20 ~ 35 parts, class mycetocyte element sample aminoacid, UV absorbent 0.5 ~ 5 part, red pigment from camellia japonica 60-70 part.
2. biological anti-ultraviolet rouge cosmetic composition as claimed in claim 1, wherein, described UV absorbent is one or more of plant Anthraquinones, Flavonoids and plant polyphenol apoplexy due to endogenous wind.
3. biological anti-ultraviolet rouge cosmetic composition as claimed in claim 2, wherein, described plant Anthraquinones is one or more of sequestered Anthraquinones, reduced form Anthraquinones and quinone glycoside apoplexy due to endogenous wind.
4. biological anti-ultraviolet rouge cosmetic composition as claimed in claim 1, wherein, described compositions comprises following component by weight: 30 parts, class mycetocyte element sample aminoacid, UV absorbent 2.5 parts, red pigment from camellia japonica 65 parts.
5. a preparation method for biological anti-ultraviolet rouge cosmetic composition, described method comprises:
Step one, choose Thallus Porphyrae as class mycetocyte element sample amino acid whose extraction source, the silt in cleaning Thallus Porphyrae, in vacuum freeze drier, carry out drying, baking temperature is-10 ~-30 DEG C, and drying time is 15 ~ 20h; Secondly, get dried Thallus Porphyrae 10g, be dissolved in the methanol of 500mL, 2 ~ 2.5h is heated with 50 ~ 60 DEG C, cooling, high speed centrifugation, centrifugal rotating speed is 3000 ~ 3500 revs/min, time is 5 ~ 6min, filter, add wherein in the dichloromethane of 800mL, high speed centrifugation, centrifugal rotating speed is 3000 ~ 3500 revs/min, time is 5 ~ 6min, obtains transparent supernatant, when noble gas, evaporative removal solvent, the deionized water dissolving adding 50mL is prepared into high performance liquid chromatography sample; Finally, carry out high performance liquid chromatography separation and draw pure class mycetocyte element sample aminoacid, wherein, high performance liquid chromatography separation condition is: column temperature: 30 DEG C, mobile phase 0.2% glacial acetic acid aqueous solution, and flow velocity is 0.5mL/min, mensuration wavelength is 330nm, and sample size is 20 μ L, sample introduction 30min analysis time;
Step 2, choose Flos Camelliae Japonicae and as the extraction source of red pigment from camellia japonica, red pigment from camellia japonica is extracted, specifically comprise: the citric acid-sodium citrate buffer of preparation pH=4.50, after the fragmentation of fresh Flos Camelliae Japonicae petal, under 40 ~ 65 DEG C of temperature conditions, the citric acid-sodium citrate buffer of 15 ~ 30 milliliters of preparation pH=4.75 is used, soak extraction 9 ~ 12h by every gram of fresh Flos Camelliae Japonicae petal; Soak is filtered rear absorption with macroporous adsorbent resin; With the ethanol water eluting macroporous adsorbent resin that mass ratio is 75%, elution flow rate is 12 ~ 15BV/h, collects eluent; Red pigment from camellia japonica is obtained after eluent being adopted vacuum rotary evaporator spin concentration, vacuum lyophilization;
The preparation of step 3, biological anti-ultraviolet rouge cosmetic composition: one or more of selection plant Anthraquinones, Flavonoids and plant polyphenol apoplexy due to endogenous wind are as UV absorbent, in UV absorbent described in 0.5 ~ 5 weight portion, add class mycetocyte element sample aminoacid 20 ~ 35 parts of weight portions that described step one obtains and the red pigment from camellia japonica 60-70 weight portion that described step 2 obtains, carry out ultramicronising by dry pulverization process technology or waterproof pulverization technology and obtain biological sun care preparations.
6. the preparation method of biological anti-ultraviolet rouge cosmetic composition as claimed in claim 5, wherein, in described step one, the baking temperature of vacuum lyophilization is-20 DEG C, and drying time is 18h.
7. the preparation method of biological anti-ultraviolet rouge cosmetic composition as claimed in claim 5, wherein, in step 2, the baking temperature of vacuum lyophilization is-20 ~-30 DEG C, and drying time is 15 ~ 18h.
8. the preparation method of biological anti-ultraviolet rouge cosmetic composition as claimed in claim 5, wherein, what the ultramicronising in described step 3 adopted is dynamic high-pressure microjet ultramicronising technology, concrete steps: shearing, broken and homogenizing, wherein operating pressure is 150 ~ 180MPa, and operating temperature is 20 ~ 25 DEG C.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110530755A (en) * | 2019-09-09 | 2019-12-03 | 江苏省原子医学研究所 | The test method and purposes of photaesthesia drug vacuum freeze drying time |
-
2015
- 2015-10-31 CN CN201510731946.XA patent/CN105232396A/en active Pending
Non-Patent Citations (1)
| Title |
|---|
| 陶岑: ""类菌胞素氨基酸（MAAs）Porphyra-334的提取及其新功能研究", 《中国学位论文全文数据库》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110530755A (en) * | 2019-09-09 | 2019-12-03 | 江苏省原子医学研究所 | The test method and purposes of photaesthesia drug vacuum freeze drying time |
| CN110530755B (en) * | 2019-09-09 | 2021-06-08 | 江苏省原子医学研究所 | Method for testing vacuum freeze drying time of photosensitive medicine and application |
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