CN105231480A - Application method of calcium carbonate in reconstituted tobacco coating liquid by being taken as perfuming carrier - Google Patents
Application method of calcium carbonate in reconstituted tobacco coating liquid by being taken as perfuming carrier Download PDFInfo
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- CN105231480A CN105231480A CN201510758854.0A CN201510758854A CN105231480A CN 105231480 A CN105231480 A CN 105231480A CN 201510758854 A CN201510758854 A CN 201510758854A CN 105231480 A CN105231480 A CN 105231480A
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- calcium carbonate
- reconstituted tobacco
- coating fluid
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Abstract
The invention discloses an application method of calcium carbonate in reconstituted tobacco coating liquid by being taken as a perfuming carrier. The method comprises the steps that acid-proof porous calcium carbonate serves as the perfuming carrier, and after essence and flavors are adsorbed by the acid-proof porous calcium carbonate, the calcium carbonate is applied in the reconstituted tobacco coating liquid. By means of the acid-proof porous calcium carbonate, hydrolysis of the acidic coating liquid can be avoided, the acid-proof porous calcium carbonate serves as a slow-released carrier, volatilization and escaping of the essence and flavors in the production process can be effectively slowed down, the calcium carbonate retention of reconstituted tobacco is increased, the porosity and the sensory quality of the reconstituted tobacco are improved, losses of the essence and flavors are reduced, and the production cost is reduced.
Description
Technical field
The present invention relates to a kind of method that calcium carbonate is applied as perfuming carrier in reconstituted tobacco coating fluid, belong to technical field of tobacco production.
Background technology
Reconstituted tobacco is as a tobacco articles, often need in process of production to add a certain amount of essence and flavoring agent to improve product aroma characteristic, cover assorted gas and give product individual style, but prepare in production process, be coated with, the storage transport of the operations such as drying and later product, fragrance matter is usually destroyed, and heat-sensitive substance or volatile substances there will be a large amount of losses.In recent years, adopt some sustained release agents and stabilizing agent to carry out the release of essence and flavoring agent in control procedure, the research extending the time of staying more and more causes the interest of people.
Summary of the invention
Object: in order to overcome the deficiencies in the prior art, the invention provides a kind of method that calcium carbonate is applied in reconstituted tobacco coating fluid as perfuming carrier.
Technical scheme: for solving the problems of the technologies described above, the technical solution used in the present invention is:
The method that calcium carbonate is applied in reconstituted tobacco coating fluid as perfuming carrier, comprises step as follows:
Step one: add water and calcium carbonate is thoroughly mixed to form calcium carbonate suspension in retort;
Step 2: essence and flavoring agent is slowly instilled in retort, control temperature, obtain mixed solution after high-speed stirred, cool to room temperature;
Step 3: after filtration, low-temperature vacuum drying obtains the calcium carbonate mixture adsorbing essence and flavoring agent;
Step 4: added to by calcium carbonate mixture in reconstituted tobacco coating fluid, is applied on reconstituted tobacco substrate and obtains reconstituted tobacco product.
Described calcium carbonate adopts acidproof porous calcium carbonate.
The ratio setting of described calcium carbonate and water is 1:9-5:5.
Described essence and flavoring agent is set to the above-mentioned one of ethyl myristate, Radix Glycyrrhizae essential oil, tree moss concrete, ethyl maltol, menthol, cinnamic acid, damascenone, heliotropin, honey element, tobacco leaf fragment supercritical extract.
Described essence and flavoring agent forms 1-2 part ethyl myristate, 5-10 part Radix Glycyrrhizae essential oil, 5-10 part tree moss concrete, 1-2 part ethyl maltol, 10-20 part menthol, 2-3 part cinnamic acid, 2-3 part damascenone, 1-2 part heliotropin, 5-10 part honey element, 38-50 part tobacco leaf fragment supercritical extract by the raw material of following mass fraction.
Essence and flavoring agent slowly instills in retort, and control temperature is at 30-80 DEG C, and mixing speed controls at 50r/min-300r/min, and mixing time is 1-3h; Mixed solution is obtained, cool to room temperature after high-speed stirred.
Beneficial effect: the method that a kind of calcium carbonate provided by the invention is applied in reconstituted tobacco coating fluid as perfuming carrier, calcium carbonate has comparatively large porosity and specific area as absorption carrier, effectively can adsorb essence and flavoring agent, can effectively slow down the volatilization of essence and flavoring agent in production process and escape, reduce the loss of essence and flavoring agent, reduce production cost, the feature of anti-acid can be avoided, in the coating fluid of acidity, hydrolysis occurs.In addition, use calcium carbonate as filler in the process that reconstituted tobacco itself is produced, this method also can increase reconstituted tobacco calcium carbonate retention rate, thus promotes gas porosity and the aesthetic quality of reconstituted tobacco.
Detailed description of the invention
In order to be illustrated more clearly in the present invention, below in conjunction with preferred embodiment, the present invention is described further.It will be appreciated by those skilled in the art that specifically described content is illustrative and nonrestrictive, should not limit the scope of the invention with this below.
Embodiment 1
Step one: the water and the 1 ton of anti-acid calcium carbonate that drop into 9 tons in retort, fully stirs and forms calcium carbonate suspension;
Step 2: again the Radix Glycyrrhizae essential oil of 100kg is slowly added in retort, under temperature 50 C, mixing speed is that 300r/min stirs 3h, cool to room temperature;
Step 3: after strainer filtering, vacuum drying obtains the calcium carbonate mixture adsorbing essence and flavoring agent;
Step 4: added to by mixture in reconstituted tobacco coating fluid, is applied on reconstituted tobacco substrate and obtains reconstituted tobacco product.
Embodiment 2
Step one: the water and the 1 ton of anti-acid calcium carbonate that drop into 9 tons in retort, fully stirs and forms calcium carbonate suspension;
Step 2: again the ethyl maltol of 30kg is slowly added in retort, at temperature 30 DEG C, mixing speed is that 100r/min stirs 1.5h, cool to room temperature;
Step 3: after strainer filtering, room temperature in vacuo drying obtains the calcium carbonate mixture adsorbing essence and flavoring agent;
Step 4: added to by mixture in reconstituted tobacco coating fluid, is applied on reconstituted tobacco substrate and obtains reconstituted tobacco product.
Embodiment 3
Step one: drop into as ratio is water and the anti-acid calcium carbonate of 5:5 in retort, fully stir formation calcium carbonate suspension;
Step 2: again the tree moss concrete of 150kg is slowly added in retort, at temperature 80 DEG C, mixing speed is that 150r/min stirs 2h, obtains mixture;
Step 3: after strainer filtering, room temperature in vacuo drying obtains the calcium carbonate mixture adsorbing essence and flavoring agent;
Step 4: added to by mixture in reconstituted tobacco coating fluid, is applied on reconstituted tobacco substrate and obtains reconstituted tobacco product.
Through detecting, compare with directly being added in coating fluid by essence and flavoring agent, the essence and flavoring agent yield through calcium carbonate absorption improves 55.89 parts.Reconstituted tobacco calcium carbonate content raises, and ash content obviously increases, and product bulk improves, and organoleptic quality promotes to some extent, reduces the loss of essence and flavoring agent, reduces production cost.
The above is only the preferred embodiment of the present invention; be noted that for those skilled in the art; under the premise without departing from the principles of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (6)
1. the method applied in reconstituted tobacco coating fluid as perfuming carrier of calcium carbonate, is characterized in that: comprise step as follows:
Step one: add water and calcium carbonate is thoroughly mixed to form calcium carbonate suspension in retort;
Step 2: essence and flavoring agent is slowly instilled in retort, control temperature, obtain mixed solution after high-speed stirred, cool to room temperature;
Step 3: after filtration, low-temperature vacuum drying obtains the calcium carbonate mixture adsorbing essence and flavoring agent;
Step 4: added to by calcium carbonate mixture in reconstituted tobacco coating fluid, is applied on reconstituted tobacco substrate and obtains reconstituted tobacco product.
2. the method applied in reconstituted tobacco coating fluid as perfuming carrier of a kind of calcium carbonate according to claim 1, is characterized in that: described calcium carbonate adopts acidproof porous calcium carbonate.
3. the method applied in reconstituted tobacco coating fluid as perfuming carrier of a kind of calcium carbonate according to claim 1, is characterized in that: the ratio setting of described calcium carbonate and water is 1:9-5:5.
4. the method applied in reconstituted tobacco coating fluid as perfuming carrier of a kind of calcium carbonate according to claim 1, is characterized in that: described essence and flavoring agent is set to the above-mentioned one of ethyl myristate, Radix Glycyrrhizae essential oil, tree moss concrete, ethyl maltol, menthol, cinnamic acid, damascenone, heliotropin, honey element, tobacco leaf fragment supercritical extract.
5. the method applied in reconstituted tobacco coating fluid as perfuming carrier of a kind of calcium carbonate according to claim 1, is characterized in that: described essence and flavoring agent forms 1-2 part ethyl myristate, 5-10 part Radix Glycyrrhizae essential oil, 5-10 part tree moss concrete, 1-2 part ethyl maltol, 10-20 part menthol, 2-3 part cinnamic acid, 2-3 part damascenone, 1-2 part heliotropin, 5-10 part honey element, 38-50 part tobacco leaf fragment supercritical extract by the raw material of following mass fraction.
6. the method applied in reconstituted tobacco coating fluid as perfuming carrier of a kind of calcium carbonate according to claim 1, it is characterized in that: in described step 2, temperature controls at 30-80 DEG C, mixing speed controls at 50r/min-300r/min, and mixing time is 1-3h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510758854.0A CN105231480B (en) | 2015-11-10 | 2015-11-10 | A kind of method that calcium carbonate is applied as perfuming carrier in reconstituted tobacco coating fluid |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510758854.0A CN105231480B (en) | 2015-11-10 | 2015-11-10 | A kind of method that calcium carbonate is applied as perfuming carrier in reconstituted tobacco coating fluid |
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| CN105231480A true CN105231480A (en) | 2016-01-13 |
| CN105231480B CN105231480B (en) | 2017-07-04 |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105707969A (en) * | 2016-03-25 | 2016-06-29 | 广东省金叶科技开发有限公司 | Tobacco sheet coating liquid and preparation method thereof |
| CN106235374A (en) * | 2016-08-30 | 2016-12-21 | 河南卷烟工业烟草薄片有限公司 | A kind of papermaking-method reconstituted tobaccos applying filler method |
| CN109576058A (en) * | 2018-12-20 | 2019-04-05 | 湖北中烟工业有限责任公司 | A kind of cumin flavor essence and its preparation method and application for cigarette dripping pill |
| CN109966505A (en) * | 2019-03-29 | 2019-07-05 | 厦门大学 | A kind of natural sustained and controlled release carrier material of nano-pore channel type and preparation method |
| CN111248486A (en) * | 2020-03-18 | 2020-06-09 | 浙江中烟工业有限责任公司 | Method for improving reconstituted tobacco quality by adopting filler as Maillard reactant carrier |
| CN113180274A (en) * | 2021-04-26 | 2021-07-30 | 河南中烟工业有限责任公司 | Reconstituted tobacco |
| CN113455699A (en) * | 2021-07-12 | 2021-10-01 | 河南中烟工业有限责任公司 | Heating cigarette with uniform fragrance release amount by mouth |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101007984A (en) * | 2007-01-26 | 2007-08-01 | 北京化工大学 | Nano loaded control release type perfume and its preparation method |
| US20090235941A1 (en) * | 2006-12-13 | 2009-09-24 | Masahiro Chida | Flavor bead and cigarette filter |
| CN101828769A (en) * | 2010-04-16 | 2010-09-15 | 云南正邦生物技术有限公司 | Preparation method of cigarette flavor compensating particles |
| CN102823945A (en) * | 2012-09-17 | 2012-12-19 | 川渝中烟工业有限责任公司 | Essence particle additive as well as preparation method and application thereof |
| CN104336776A (en) * | 2013-08-05 | 2015-02-11 | 贵州中烟工业有限责任公司 | Slow release aromatic base material, particles as well as preparation method and application thereof |
-
2015
- 2015-11-10 CN CN201510758854.0A patent/CN105231480B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20090235941A1 (en) * | 2006-12-13 | 2009-09-24 | Masahiro Chida | Flavor bead and cigarette filter |
| CN101007984A (en) * | 2007-01-26 | 2007-08-01 | 北京化工大学 | Nano loaded control release type perfume and its preparation method |
| CN101828769A (en) * | 2010-04-16 | 2010-09-15 | 云南正邦生物技术有限公司 | Preparation method of cigarette flavor compensating particles |
| CN102823945A (en) * | 2012-09-17 | 2012-12-19 | 川渝中烟工业有限责任公司 | Essence particle additive as well as preparation method and application thereof |
| CN104336776A (en) * | 2013-08-05 | 2015-02-11 | 贵州中烟工业有限责任公司 | Slow release aromatic base material, particles as well as preparation method and application thereof |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105707969A (en) * | 2016-03-25 | 2016-06-29 | 广东省金叶科技开发有限公司 | Tobacco sheet coating liquid and preparation method thereof |
| CN105707969B (en) * | 2016-03-25 | 2017-03-15 | 广东省金叶科技开发有限公司 | A kind of reconstituted tobacoo coating fluid and preparation method thereof |
| CN106235374A (en) * | 2016-08-30 | 2016-12-21 | 河南卷烟工业烟草薄片有限公司 | A kind of papermaking-method reconstituted tobaccos applying filler method |
| CN106235374B (en) * | 2016-08-30 | 2018-05-22 | 河南卷烟工业烟草薄片有限公司 | A kind of papermaking-method reconstituted tobaccos applying filler method |
| CN109576058A (en) * | 2018-12-20 | 2019-04-05 | 湖北中烟工业有限责任公司 | A kind of cumin flavor essence and its preparation method and application for cigarette dripping pill |
| CN109966505A (en) * | 2019-03-29 | 2019-07-05 | 厦门大学 | A kind of natural sustained and controlled release carrier material of nano-pore channel type and preparation method |
| CN111248486A (en) * | 2020-03-18 | 2020-06-09 | 浙江中烟工业有限责任公司 | Method for improving reconstituted tobacco quality by adopting filler as Maillard reactant carrier |
| CN113180274A (en) * | 2021-04-26 | 2021-07-30 | 河南中烟工业有限责任公司 | Reconstituted tobacco |
| CN113455699A (en) * | 2021-07-12 | 2021-10-01 | 河南中烟工业有限责任公司 | Heating cigarette with uniform fragrance release amount by mouth |
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| CN105231480B (en) | 2017-07-04 |
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