CN105211994A - Carbonated water and manufacture method thereof - Google Patents
Carbonated water and manufacture method thereof Download PDFInfo
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- CN105211994A CN105211994A CN201410270244.1A CN201410270244A CN105211994A CN 105211994 A CN105211994 A CN 105211994A CN 201410270244 A CN201410270244 A CN 201410270244A CN 105211994 A CN105211994 A CN 105211994A
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- water
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Abstract
The present invention relates to a kind of container dress carbonated water and preparation method thereof, and then providing a kind of base-material as pick-me-up optimum carbonated water, described container dress carbonated water meets the content of (A) calcium: the content of 25 ~ 48.5ppm or (B) magnesium: any one in 7.8 ~ 15ppm.The invention still further relates to a kind of alcoholic drink mixing above-mentioned carbonated water and Spirit and obtain.Inventive container dress carbonated water carbonic acid excitement is excellent, does not have strong bitter taste, astringent taste.
Description
Technical field
The present invention relates to container dress carbonated water and preparation method thereof, and then provide a kind of base-material as pick-me-up optimum carbonated water.Inventive container dress carbonated water does not have strong carbonic acid excitement and bitter taste, astringent taste.
Background technology
Carbonated water (also known as soda water, sodawater) because its excitement for tongue and the bitterness sense of its uniqueness, and brings the people that drink with pleasant mouthfeel, by widely as beverage, cocktail base-material and using.In recent years, along with the variation of taste and preference, and people are for the pursuit of the pleasant mouthfeel of carbonated water, and the manufacturer of carbonated water passes through carbonic acid excitement and bitter taste, astringent taste that various diverse ways regulates carbonated water.Such as, the excitement (frank sense) being carried out regulation of carbon dioxide gas by sweet ingredient is proposed in patent document 1.Propose in patent document 2 to improve calcium content in soda water by adding calcium chloride, but its role is to improve the calcium content in soda water, and do not mention by adding calcium salt or its mixture thus carbonic acid excitement and the bitter taste of soda water can being regulated.
All do not mention in prior art and by regulating the content of contained calcium salt itself, magnesium salts in former water (natural water such as underground water, mineral water), the mouthfeel (excitement and bitter taste, astringent taste) of carbonated water can be regulated.
The present invention causes the salt of the basic reason of carbonated water bitter taste, astringent taste by regulating, regulate the mouthfeel (excitement and bitter taste, astringent taste) of carbonated water, reduce the use of other additives in carbonated water, reduces the absorption of people for additive.
Existing patent document:
Patent document 1: Chinese patent announces CN102227173A
Patent document 2: Chinese patent announces CN101744336A
Summary of the invention
Carbon dioxide in carbonated water has a kind of excitement (carbonic acid excitement) of uniqueness to oral cavity, throat, thus forms frankness sense when drinking and after drinking.Carbonated water, except drinking separately, after can also mixing, forms the wine of CO 2 aerated body with alcoholic drink.
But in simple carbonated water for the excitement of oral cavity, throat than stronger, bitter taste wherein, astringent taste are stronger, can not bring sufficient pleasant sense.
In order to solve the problem, present inventor is through attentively studying discovery, by controlling the content of calcium (Ca) in carbonated water, magnesium (Mg), the RO film process water of the former water of mixing hardness more than 100 and described former water improves carbonic acid excitement and bitter taste, the astringent taste of carbonated water.Thus complete the present invention.
Namely the invention provides following content:
(1) a container dress carbonated water, is characterized in that, meet any one in following (A) or (B):
(A) content of calcium: 25 ~ 48.5ppm
(B) content of magnesium: 7.8 ~ 15ppm.
(2) as described in container dress carbonated water, it is characterized in that, meet described (A) and described (B).
(3) the container dress carbonated water as described in (1) or (2), it is obtained by mixing following (C) and (D),
(C) the former water of hardness more than 100
(D) the RO film process water of described former water
(4) the container dress carbonated water as described in any one of (1) ~ (3), hardness is 70.5 ~ 138.
(5) the container dress carbonated water as described in any one of (1) ~ (4), wherein, the concentration of carbonic acid gas is 0.55 ~ 0.75 % by weight.
(6) a kind of manufacture method of container dress carbonated water, it is characterized in that, the RO film process water of the former water of mixing hardness more than 100 and described former water obtains mixing water, carbonic acid gas is made to be dissolved in described mixing water, wherein, described container dress carbonated water meets any one in following (A) or (B):
(A) content of calcium: 25 ~ 48.5ppm
(B) content of magnesium: 7.8 ~ 15ppm.
(7) manufacture method of the container dress carbonated water as described in (6), described container dress carbonated water meets described (A) and described (B).
(8) manufacture method of the container dress carbonated water as described in (6) or (7), carbonic acid hardness of water is 70.5 ~ 138.
(9) manufacture method of the container dress carbonated water as described in any one of (6) ~ (8), wherein, the concentration of carbonic acid gas is 0.55 ~ 0.75 % by weight.
(10) a kind of mixing alcoholic drink that carbonated water and Spirit obtain as described in any one of (1)-(5).
The former water of hardness in the present invention more than 100 can be the natural water of hardness more than 100, such as underground water, mineral water etc.The mouthfeel of calm carbonated water easy to control and the aspect reduced costs are considered, the former water of former hardness of water preferably greater than 100, below 150, further preferably 100 ~ 140, more preferably 110 ~ 140, particularly preferably 115 ~ 140.
RO film process water in the present invention and reverse osmosis membrane processing water in brief, are the process water that the mineral matter of the removing mineral matter manufactured is few, and the water that the former water that itself and mineral matter enrich can be mixed.RO film process water, as long as content of mineral substances is low, and stable within the specific limits.From the viewpoint of stability, easily to control carbonated water mouthfeel and reduce costs, RO film process hardness of water is 0 ~ 10, preferably 1 ~ 8, further preferably 2 ~ 6, more preferably 3 ~ 5.5.
The mixed proportion of the former water of the hardness in the present invention more than 100 and RO film process water is not particularly limited, as long as the mixing water obtained can be made to meet, and the content of (A) calcium: 25 ~ 48.5ppm; (B) content of magnesium: any one in 7.8 ~ 15ppm.From reducing the use amount of additive, the angle that reduces costs is considered, the ratio (the former water of hardness more than 100: RO film process water) of the former water of hardness more than 100 and RO film process water is generally 1:99 ~ 80:20, preferred 40:60 ~ 80:20, more preferably 50:50 ~ 70:30.
From the viewpoint of carbonic acid excitement and bitter taste, the astringent taste of improving carbonated water, carbonic acid hardness of water of the present invention is 70.5 ~ 138, preferably 75 ~ 130, more preferably 80 ~ 120.
From the angle of the carbonic acid excitement of carbonated water, the concentration of the carbonic acid gas of carbonated water of the present invention is 0.55 ~ 0.75 % by weight, preferably 0.6 ~ 0.7 % by weight.
Spirit in the present invention refers to the wine manufactured by the method for distillation, such as whiskey (English name: Whisky, Whiskey), brandy (English name: Brandy), vodka (English name: Vodka), Rum (English name: Rum), mescal (English name: Tequila), China white wine etc.
Detailed description of the invention
[RO film process water]
RO film process water (reverse osmosis membrane processing water) as long as handling procedure can remove the method for mineral matter, have no particular limits, reverse osmosis membrane processing can be carried out by known method, such as, the method recorded in Japanese Patent Laid-Open 11-128919 reverse osmosis membrane treatment method:
Be 16kg/cm at operating pressure in RO membrane treatment appts (Nitto Denko Corp's system 4 inches of RO films " NTR-759HR ")
2, the rate of recovery 70% treatment conditions under pass into former water.Former water and acid-base modifier after mixer stirs, by the process of RO film, the process water of the RO film obtained, then through the filtration of ion exchange resin, thus obtain processing water.
In addition, the resin that anion exchange resin (Kurita Water Industries Ltd's system " EXAG ") and cationic ion-exchange resin (Kurita Water Industries Ltd's system " EXCG ") mix with the ratio of 2:1 is used, at SV=50hr in mixed bed type ion interchange unit
-1condition under water flowing.
The pH of RO feedwater is generally the neutrallty condition of 7.0, and with frequency once in 168 hours, in 3 hours, the pH of RO feedwater is the alkalescence of 10.0, during pH is adjusted to alkalescence, also fetches water.
[calcium]
Calcium source used in the present invention, has no particular limits, and can be come from the calcium in former water, also can be the calcium added.The calcium added, can enumerate such as calcium hydroxide, calcium carbonate, calcium bicarbonate, calcium chloride, calcium benzosulphimide, calcium lactate, one-lime phosphate, Dicalcium Phosphate, tricalcium phosphate, calcium sulfate, calcium citrate, calcium malate, calcium gluconae, calcium maleate, calcium tartrate, calcium succinate, fumaric acid calcium, calcium benzoate, calcium sorbate, calcium citrate malate etc.
Wherein angle that is excellent from mouthfeel and that be easy to obtain considers preferred calcium carbonate, calcium bicarbonate, calcium chloride, calcium benzosulphimide, calcium lactate, one-lime phosphate, Dicalcium Phosphate, tricalcium phosphate, calcium sulfate, calcium citrate, calcium malate, calcium gluconae, calcium maleate, calcium tartrate, calcium succinate, fumaric acid calcium.More preferably calcium carbonate, calcium bicarbonate, calcium chloride, calcium benzosulphimide, calcium lactate, one-lime phosphate, Dicalcium Phosphate, tricalcium phosphate, calcium sulfate.
These calcium salts, can one be used alone also can be used together two or more.
[magnesium]
Magnesium source used in the present invention, just has no particular limits, and can be come from the magnesium in former water, also can be the magnesium added.The magnesium added, be such as selected from the group be made up of magnesium hydroxide, magnesium carbonate, magnesium bicarbonate, magnesium chloride, magnesium lactate, magnesium phosphate, magnesium sulfate, magnesium citrate, magnesium malate, magnesium gluconate more than one.Wherein angle that is excellent from mouthfeel and that be easy to obtain considers preferred magnesium hydroxide, magnesium carbonate, magnesium bicarbonate, magnesium chloride, magnesium phosphate, magnesium sulfate.
These magnesium salts, can one be used alone also can be used together two or more.
[other compositions]
Except above-mentioned calcium component, magnesium component, carbonated water of the present invention, in order to improve the meltage of carbon dioxide, productivity ratio and efficiency, reduce the use cost of carbon dioxide, taste the carbonic acid excitement of appropriateness, acid can also be added so that the pH of carbonated water is adjusted to 2.0 ~ 4.5, preferably be adjusted to 2.5 ~ 4.5, be more preferably adjusted to 2.7 ~ 4.0.By the pH of carbonated water is adjusted to above-mentioned scope, the meltage of carbon dioxide, productivity ratio and efficiency can be improved, reduce the use cost of carbon dioxide.As the acid added, as long as from food acids, any acid can be used, specifically can enumerate phosphoric acid, citric acid, lactic acid, malic acid, maleic acid, adipic acid, butanedioic acid, fumaric acid, tartaric acid, gluconic acid, ascorbic acid and two or more the mixture in them.
Container dress carbonated water, can not high-temperature heating sterilization because to be filled into after in container, so mostly use anticorrisive agent.In carbonated water of the present invention, normally used food (or beverage) also can be used to use anticorrisive agent.As anticorrisive agent, benzoate, sorbate, ascorbic acid, SHMP, EDTA, BHA, BHT, TBHQ, dehydroacetic acid, dimethyl dicarboxylate, ethoxyquin, n Heptyl p hydroxybenzoate can be enumerated, and more than a kind that selects from the mixture of these materials.These anticorrisive agents (benzoate wherein) have the distinctive bitter taste of anticorrisive agent, become the main cause increasing bitter taste in carbonated water.Carbonated water of the present invention does not preferably mix or retains minimum anticorrisive agent.When using benzoate as anticorrisive agent, owing to can reduce the mouthfeel of carbonated water from benzoic bitter taste, excitement, so its addition is preferably below 150ppm, more preferably below 100ppm, further preferably below 50ppm, particularly preferably 0ppm.
And then as required, also can the raw material of mixing usually in mixed carbonic acid water as required in carbonated water of the present invention, the such as functional materials such as caffeine, amino acid, the colouring agents such as caramel or pigment, defoamer, tackifier, emulsifying agent etc.
[container]
Carbonated water of the present invention can directly be drunk, and drinks after also can mixing with alcohol type.Carbonated water of the present invention is filled in preservable container, such as: bottle, tank, packaging bag etc.Particularly, it is the container molding (PET bottle, PET bag etc.) of main component that the container of filling carbonated water of the present invention can be enumerated with PETG, the metal bottle such as aluminium, stainless steel, tank.
[manufacture method]
Carbonated water of the present invention can use the manufacture method of carbonated water in the past to manufacture, and has no particular limits.Such as, plunging or premixed method can be utilized to manufacture.From the easiness of carbonated water manufacture, preferably use plunging.When utilizing plunging to manufacture, can be listed below as concrete grammar: by the former water of the hardness of proper ratio more than 100 and the mixing of RO film process water, add appropriate magnesium salts and/or calcium salt as required, the content making carbonated water meet calcium is 25 ~ 48.5ppm, the content of magnesium is 7.8 ~ 15ppm, at least one in two conditions.Then carry out degassed, sterilization processing as required, cool, be pressed into carbon dioxide wherein by usual method and formed, be filled in container.
[drinking method]
Carbonated water of the present invention can be drunk separately, and the beverage that also can be mixed to get containing wine as the base-material of pick-me-up and Spirit is drunk.The ratio mixed with Spirit as base-material can according to the kind of wine, drinking person need suitably select, there is no particular limitation.
[embodiment]
The present invention will be described below to enumerate embodiment, but the present invention is not limited to these embodiments.
Embodiment 1 ~ 3, comparative example 1 ~ 2
According to the ratio mixing RO film process water described in table 1 and Yuan Shui, according to common plunging press-in carbon dioxide, preparation carbonated water.Mouthfeel for the carbonated water obtained is tested by sense the method carrying out evaluating and is carried out following evaluation, and it the results are shown in Table 1.
Hardness in the water of the present embodiment Central Plains obtains total hardness by the assay method of 4.9 total hardnesss in standard GB/T/T8538-2008 natural mineral water detection method.
In the present embodiment, in carbonated water, the content of calcium is measured by the 4.13.1 disodium ethylene diamine tetraacetate titration of 4.13 calcium in standard GB/T/T8538-2008 natural mineral water detection method.
In the present embodiment, in carbonated water, the content of magnesium is measured by the 4.14.1 disodium ethylene diamine tetraacetate titration of 4.14 magnesium in standard GB/T/T8538-2008 natural mineral water detection method.
[sensory evaluation]
5 sensory evaluation persons by excellent training are divided into full marks with 5, and the presence or absence for " carbonic acid excitement " and " bitter taste, astringent taste " is evaluated.
[metewand]
[carbonic acid excitement]
Feel very strong carbonic acid excitement: 5 points;
Carbonic acid excitement can be felt: 4 points;
Feel carbonic acid excitement a little: 3 points;
Only feel some carbonic acid excitements: 2 points;
Imperceptible carbonic acid excitement: 1 point.
[bitter taste, astringent taste]
Imperceptible bitter taste, astringent taste: 5 points;
A little bitter taste, astringent taste can be felt: 4 points;
Only feel some bitter tastes, astringent taste: 3 points;
Feel a little to obtain bitter taste, astringent taste: 2 points;
Feel very strong bitter taste, astringent taste: 1 point.
Calculating the mean value evaluated and divide, evaluating based on following benchmark according to commenting average.
In addition, preferably at more than metewand B, more preferably metewand A's.
[scoring benchmark]
D: mean value more than 1.0 ~ less than 2.0
C: mean value more than 2.0 ~ less than 3.0
B: mean value more than 3.0 ~ less than 4.0
A: mean value less than more than 4.0 ~ 5.0.
In addition, prepare the sample of former water 100 % by weight, RO film process water 100 % by weight as comparative example, its mouthfeel is similarly evaluated according to sensory test.Its result is shown in table 1.
Table 1
※ 1:n.d. refers to that this index is under detectability, can not testedly make.
Embodiment 4
The carbonated water of mixing 45ml embodiment 2, the whiskey 135ml of the alcohol number of degrees 40 degree, obtain the wine of CO 2 aerated body.
Claims (10)
1. a container dress carbonated water, is characterized in that, meet any one in following (A) or (B):
(A) content of calcium: 25 ~ 48.5ppm
(B) content of magnesium: 7.8 ~ 15ppm.
2. container dress carbonated water as claimed in claim 1, is characterized in that, meet described (A) and described (B).
3. container dress carbonated water as claimed in claim 1 or 2, it is obtained by mixing following (C) and (D),
(C) the former water of hardness more than 100
(D) the RO film process water of described former water
4. the container dress carbonated water as described in any one of claims 1 to 3, hardness is 70.5 ~ 138.
5. the container dress carbonated water as described in any one of Claims 1 to 4, it is characterized in that, the concentration of carbonic acid gas is 0.55 ~ 0.75 % by weight.
6. the manufacture method of a container dress carbonated water, it is characterized in that, the RO film process water of the former water of mixing hardness more than 100 and described former water obtains mixing water, carbonic acid gas is made to be dissolved in described mixing water, wherein, described container dress carbonated water meets any one in following (A) or (B):
(A) content of calcium: 25 ~ 48.5ppm
(B) content of magnesium: 7.8 ~ 15ppm.
7. the manufacture method of container dress carbonated water as claimed in claim 6, described container dress carbonated water meets described (A) and described (B).
8. as claimed in claims 6 or 7 container dress carbonated water manufacture method, described carbonic acid hardness of water is 70.5 ~ 138.
9. the manufacture method of the container dress carbonated water as described in any one of claim 6 ~ 8, wherein, the concentration of carbonic acid gas is 0.55 ~ 0.75 % by weight.
10. one kind mixes the pick-me-up that carbonated water and Spirit obtain as described in any one of claim 1-5.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410270244.1A CN105211994A (en) | 2014-06-17 | 2014-06-17 | Carbonated water and manufacture method thereof |
| JP2015115825A JP6566732B2 (en) | 2014-06-17 | 2015-06-08 | Carbonated water and method for producing the same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410270244.1A CN105211994A (en) | 2014-06-17 | 2014-06-17 | Carbonated water and manufacture method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105211994A true CN105211994A (en) | 2016-01-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410270244.1A Pending CN105211994A (en) | 2014-06-17 | 2014-06-17 | Carbonated water and manufacture method thereof |
Country Status (2)
| Country | Link |
|---|---|
| JP (1) | JP6566732B2 (en) |
| CN (1) | CN105211994A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112262940A (en) * | 2020-10-15 | 2021-01-26 | 上海巴克斯酒业有限公司 | Method for improving water gas retention of bubbles |
| CN112794542A (en) * | 2019-11-14 | 2021-05-14 | 名牌食品股份有限公司 | Preparation method of micromolecule bubble water and micromolecule bubble water |
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| US20020034576A1 (en) * | 1999-05-27 | 2002-03-21 | Burgess James Micheal | Carbonated beverage for strengthening acid resistancy of teeth (with the taste of cream soda) |
| CN101426383A (en) * | 2006-02-28 | 2009-05-06 | 戴维·R·比曼 | Water formulation |
| CN101744336A (en) * | 2010-01-19 | 2010-06-23 | 乌鲁木齐古得亚科技开发有限公司 | mineralized soda water |
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| JP2002205070A (en) * | 2001-01-09 | 2002-07-23 | Hitachi Ltd | Method of making mineral water from marine deep water and system of making for the same |
| JP2004065196A (en) * | 2002-08-09 | 2004-03-04 | Suntory Ltd | Mineral composition produced by using seawater |
| JP2005087894A (en) * | 2003-09-18 | 2005-04-07 | Goshu Yakuhin Kk | Hardness-regulated natural water |
| JP2009274980A (en) * | 2008-05-14 | 2009-11-26 | Suntory Holdings Ltd | Drinking water having relaxing effect |
| KR100918273B1 (en) * | 2009-02-18 | 2009-09-18 | 한애삼 | Decreasing composition of waterhardness |
| JP2010252702A (en) * | 2009-04-24 | 2010-11-11 | Ito En Ltd | High mineral-containing carbonated drink and method for producing the same |
| JP2013000011A (en) * | 2011-06-13 | 2013-01-07 | Kirin Beverage Corp | PACKAGED CARBONATED BEVERAGE ADJUSTED TO HAVE NEUTRAL pH RANGE |
| JP5860232B2 (en) * | 2011-06-27 | 2016-02-16 | サントリー食品インターナショナル株式会社 | How to improve the back of carbonated drinks |
| JP6047386B2 (en) * | 2012-11-29 | 2016-12-21 | キリンビバレッジ株式会社 | Sugar-free carbonated beverage and method for producing the same |
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2014
- 2014-06-17 CN CN201410270244.1A patent/CN105211994A/en active Pending
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- 2015-06-08 JP JP2015115825A patent/JP6566732B2/en not_active Expired - Fee Related
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| US20020034576A1 (en) * | 1999-05-27 | 2002-03-21 | Burgess James Micheal | Carbonated beverage for strengthening acid resistancy of teeth (with the taste of cream soda) |
| CN101426383A (en) * | 2006-02-28 | 2009-05-06 | 戴维·R·比曼 | Water formulation |
| CN101744336A (en) * | 2010-01-19 | 2010-06-23 | 乌鲁木齐古得亚科技开发有限公司 | mineralized soda water |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112794542A (en) * | 2019-11-14 | 2021-05-14 | 名牌食品股份有限公司 | Preparation method of micromolecule bubble water and micromolecule bubble water |
| CN112262940A (en) * | 2020-10-15 | 2021-01-26 | 上海巴克斯酒业有限公司 | Method for improving water gas retention of bubbles |
| CN112262940B (en) * | 2020-10-15 | 2023-09-01 | 上海巴克斯酒业有限公司 | Method for improving air-holding property of bubble water |
Also Published As
| Publication number | Publication date |
|---|---|
| JP6566732B2 (en) | 2019-08-28 |
| JP2016002083A (en) | 2016-01-12 |
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Application publication date: 20160106 |