CN105176713B - Fragrant and sweet type natural plant essential oils soap with bacteria resistance function and preparation method thereof - Google Patents
Fragrant and sweet type natural plant essential oils soap with bacteria resistance function and preparation method thereof Download PDFInfo
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- CN105176713B CN105176713B CN201510557876.0A CN201510557876A CN105176713B CN 105176713 B CN105176713 B CN 105176713B CN 201510557876 A CN201510557876 A CN 201510557876A CN 105176713 B CN105176713 B CN 105176713B
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Abstract
The invention discloses a kind of fragrant and sweet type natural plant essential oils soap with bacteria resistance function, it includes composite essential oil and soap base, and the composite essential oil is based on parts by volume, including following components：15 parts of bigarabe flower essential oil, 15 parts of Lavender, 25 parts of Melissa officinalis essential oil, 13 parts of yellow chamomile essential oil, 13 parts of frankincense essential oil, natural 79 94 parts of soap base.The essential oil soap of the present invention is in limpid fragrant and sweet smell, fragrance is fine and smooth, level enriches, lasting is lasting, product foaming abundancy, feel are fine and smooth, clean result is good and soap body resists that dry and cracked, stability is good, the effect of with restraining and sterilizing bacteria, it can effectively suppress the formation of skin surface bacterium, while auxiliary treatment disease of skin, improvement skin condition, also have pacify, calmness, sleeping, antidepression, anti-depression the effect of, improve the mood and the state of mind of user.
Description
Technical field
The present invention relates to daily chemical product field, particularly relates to a kind of essential oil soap.
Background technology
Perfumed soap is a kind of common daily necessities, in recent years, as the improvement of people's living standards, especially by bacterium sense
The outburst of extensive infectious disease, more exacerbates people to the demand with antibacterial type perfumed soap caused by dye.That is commonly used in perfumed soap kills
Microbial inoculum has sulphur, chloride bactericide such as triclosan etc., has research to compare the bacteria resistance function of current common commercially available perfumed soap,
It was found that indicate that the perfumed soap (sulphur, triclocarban, parachlorometaxylenol etc.) with degerming component is respectively provided with not in commercially available prod
With the fungistatic effect of degree, it is significantly higher than conventional toilet soaps (being free of degerming component).These chemical type bactericide also have its unfavorable
, to oral cavity, throat and stomach is irritant and corrosivity.In order to overcome these problems, people
Attempt to substitute the use of chemically synthesized product with natural plant extracts, be used as functional additive in perfumed soap and natural
Spices.
Plants essential oil (Essentialoil, EO) is from plant different tissues such as root, stem, leaf, flower, fruit, seed, limb
Or the general name with fragrance and (or fragrance) volatility oily liquid substance that secretion is raw material extraction.Generally, plant essence
Oil is for preparing essence and flavoring agent, but the research of recent decades is found, essential oil and one pack system have very strong suppression or killed
The characteristic of the dead microorganism such as bacterium and fungi.Under the situation that the disease as caused by bacterium, fungal infection is aggravated increasingly now, plant
Thing essential oil is very wide as a kind of efficient, security natural plants bactericide, application prospect.
The usage history of compound essential oil is long, it is generally believed that essential oil can bring allomeric function when being used in mixed way
Lifting.Find that in terms of bacterium infection is treated, the combination of essential oil combines institute's band more than 600 kinds by current literature search
The effect come is also classified into cooperateing with, is added, unrelated and four kinds of situations of antagonism.
A kind of essential oil soap of bactericidal function of CN201210516639.6 disclosure of the invention, it is by Sweet Almond Oil and small
Wheat germ oil, be put into a container and stir, then add tea tree ethereal oil, Pogostemon cablin essential, niaouli essential oil,
Cus-cus essential oil, myrrh essential oil and deodar essential oil, and stir；Again by cold process soap soap base, it is heated to cold after melting completely
But, when soap base temperature is cooled to 50 DEG C or so, deployed essential oil solution is added, and is stirred, finally pours into system
In the mould of soap, taken out after being cooled to room temperature.
A kind of soap containing plants essential oil of CN200710177304.5 disclosure of the invention, it mainly by Geranium Essential,
Chamomile essential oil, honeysuckle essential oil, oil of Cymbopogon winterianus, thyme essence etc. are according to addition soap matrix system after certain ratio mixing
Into.Clearing heat and detoxicating, the sterilizing and itch-relieving of soap energy of the invention, Clean Living profit body.
CN201310577658.4 discloses a kind of beautifying and antibacterial toilet soap, and the raw material components of the perfumed soap include：Coconut oil 10-
13%th, palm oil 20-23%, olive oil 21-38.3%, sodium hydroxide 8.5-9%, water 20-23%, bighead atractylodes rhizome decocting liquid 1-3%,
Root of Dahurain angelica ultrasound alcohol extract 1-3%, lucid asparagus decocting liquid 1-3%, tea tree ethereal oil 0.2-2%.
CN201210459852.8 discloses a kind of antibacterial cold-resistant perfumed soap, and its major ingredient is fresh Conditions of Onion Juice, ginger juice,
Add folium artemisiae argyi, honeysuckle, folium isatidis, dandelion, the concentrate of the Chinese medicine such as Chinese gall, sodium hydroxide, SIMMONDSIA CHINENSIS SEED OIL and water according to
Certain ratio mixing, by stirring, solidifying, being stripped and form.
The content of the invention
In order to solve the above problems, the present invention provides a kind of with the natural plant essential oils soap of bacteria resistance function and its preparation side
Method.
A kind of natural plant essential oils soap with bacteria resistance function, it includes composite essential oil and soap base, and the composite essential oil is pressed
Parts by volume meter, including following components：Bigarabe flower essential oil 1-5 parts, Lavender 1-5 parts, Melissa officinalis essential oil 2-5 parts, yellow chamomile
Essential oil 1-3 parts, frankincense essential oil 1-3 parts, natural soap base 79-94 parts.
In one embodiment of the invention, the composite essential oil is based on parts by volume, including following components：Bigarabe flower essential oil
1-4 parts, Lavender 1-3 parts, Melissa officinalis essential oil 2-4 parts, yellow chamomile essential oil 1-3 parts, frankincense essential oil part 1-3 parts, natural soap
Base 83-94 parts.
In a preferred embodiment of the present invention, the composite essential oil is based on parts by volume, including following components：Bigarabe is spent
4 parts of essential oil, 2 parts of Lavender, 2 parts of Melissa officinalis essential oil, 2 parts of yellow chamomile essential oil, 2 parts of frankincense essential oil, natural 88 parts of soap base.
The present invention also provides the preparation method of the essential oil soap, and it comprises the following steps：
1) bigarabe flower essential oil, Lavender, Melissa officinalis essential oil, yellow chamomile essential oil, frankincense essential oil are mixed by proportioning equal
It is even, ultrasonic oscillation 5-15S, obtain composite essential oil；
2) soap base after soap base dissolving, is by volume mixed soap base and composite essential oil in 50-60 DEG C of heating water bath
Close, pour into mould, produce after cooling.
The Lavender used in the present invention extracts for Labiatae lavender ' capital smokes No. 1 ' flower spike, the kind lavender
For self-fertile kind, authorized by the forest variety certification committee of State Administration of Forestry breeding in 2014.Lavender is fragrant treatment
Most ancient in method, the widest essential oil of purposes, property is gentle, is adapted to any skin quality, and it is a small number of can directly with skin contact
One of essential oil.Poised state can be rebuild, the body ＆ mind of people is in the poised state of harmony, is put completely
Pine.There is certain inhibitory action to staphylococcus aureus and its antibody-resistant bacterium, pneumobacillus, Candida albicans.
The essential oil soap of the present invention is in limpid fragrant and sweet smell, and fragrance is fine and smooth, level enriches, and lasting is lasting, and product foam is rich
It is rich, feel is fine and smooth, clean result is good and soap body resists that dry and cracked, stability is good, there is the effect of restraining and sterilizing bacteria, can effectively suppress skin
The formation of skin surface bacteria, auxiliary treatment disease of skin, improve skin condition while, also have pacify, calmness, sleeping,
The effect of antidepression, anti-depression, improve the mood and the state of mind of user.
Embodiment
Following examples are used to illustrate the present invention, but are not limited to the scope of the present invention.
Embodiment 1
Take bigarabe flower essential oil 4ml, Lavender 2ml, Melissa officinalis essential oil 3ml, yellow chamomile essential oil 3ml, frankincense essential oil 1ml
It is well mixed in glass or rustless steel container, ultrasonic oscillation 10S, obtains mixed essential oil.
By soap base in 55 DEG C of heating water baths, 87ml soap bases, 13ml mixed essential oil are taken after soap base dissolving, in being mixed in container
Poured into after closing uniformly in mould, the essential oil soap made is put into 4 DEG C of refrigerator saved backup after cooling.
Antibacterial Activity：
1.1 disk diffusion method
Respectively by bacteria to be tested (Escherichia coli Escherichia coli ATCC 25922, staphylococcus aureus
Staphylococcus aureus subsp.Aureus ATCC25923, Pseudomonas aeruginosa (Pseudomonas aeruginosa)
ATCC27583 beef extract-peptone fluid nutrient medium cultures, each bacterium solution is diluted to 1 × 10 with than turbid instrument using preceding8CFU·
mL-1。
The beef extract-peptone agar medium of sterilizing is poured into diameter 9cm culture dish, after culture medium solidifying, with shifting
Liquid rifle is drawn each μ l of bacterium solution 100 and is spread evenly across on flat board, and the diameter 6mm filter papers after then taking hot air sterilization with tweezers are smooth
In flat board center.
Every kind of folk prescription essential oil, mixed essential oil cross 0.45 μm of miillpore filter in embodiment 1, and liquid-transfering gun draws 10 μ l drops
It is added on filter paper, each three repetition of processing.Distilled water is set to make blank control, to positive control selected by three kinds of bacteriums
(antibiotic) is respectively penicillin, streptomysin and cefotaxime (1mgmL-1).After essential oil is fully absorbed, 37 DEG C are inverted culture
24 hours, antibacterial circle diameter is determined, takes and measures average value three times.
The bacteriostasis (inhibition zone radius r=mm) of the compound essential oil of table 1
Note：Inhibition zone size unit is mm, accuracy 0.02mm
As can be seen from the above table, essential oil is when being used alone, to Escherichia coli, staphylococcus aureus and Pseudomonas aeruginosa all
There is certain inhibition, the inhibition of different essential oils has significant difference.For Escherichia coli (bacterium A), yellow chamomile essence
The inhibition of oil and frankincense essential oil is more notable, and the essential oil inhibition of lavender (commercial variety) extraction is poor, and has by oneself
The essential oil effect of kind (capital smokes No. 1) extraction is better than lavender commercial variety；For staphylococcus aureus (bacterium B), ' capital
Smoking No. 1 ' fungistatic effect of Lavender is notable, and the inhibition of other essential oils is poor；The resistance of Pseudomonas aeruginosa (bacterium C) compared with
By force, above-mentioned essential oil is not ideal to its inhibition, and comparatively speaking, the inhibition of yellow chamomile essential oil is slightly good.
There is preferable fungistatic effect to Escherichia coli, staphylococcus aureus after essential oil mixing in embodiment 1, it presses down
Bacterium loop diameter is noticeably greater than single essential oil and antibiotic control group；Single essential oil is better than to the inhibition of Pseudomonas aeruginosa, but it is weak
In the inhibition of antibiotic.
1.2 human hands are tested
Subject cleans each of right-hand man with clear water, the essential oil soap of embodiment 1 and certain commercially available brand bacteriostatic soap respectively
Finger, flowing water cleaning after use by autoclave sterilization non-woven fabrics wipe, after drying again respectively with it is anhydrous spin cloth 1h, 2h,
To the random swabing sampling of finger of right-hand man in 3h, 4h period, anhydrous spinning cloth is put into containing containing MH meat soup cultures afterwards
In the conical flask of base number of bacteria is recorded in constant incubator with than turbid instrument after culture 18h.Compared by the concentration of bacterium and matched somebody with somebody
The fungistatic effect of the essential oil soap of system.Study subject bacterial concentration (× 108CFUmL-1) changes in table 24h
As can be seen from the above table, either with the essential oil soap in embodiment 1 or certain commercially available brand bacteriostatic soap, with when
Between extend, the number of bacteria of subject on hand all can showed increased, but its increased degree is different：To three subjects
Speech, the essential oil soap fungistatic effect of preceding 2 hour embodiments 1 is notable, and number of bacteria on hand is substantially less than certain commercially available brand perfumed soap
Experimental group；In 3-4 hours, 1,2 bacterial number on hand of subject still is below certain commercially available brand perfumed soap experimental group, and subject 3
Number of bacteria on hand exceeded certain commercially available brand perfumed soap experimental group at 3 hours.
Embodiment 2
Take bigarabe flower essential oil 4ml, Lavender 2ml, Melissa officinalis essential oil 2ml, yellow chamomile essential oil 2ml, frankincense essential oil 2ml
It is well mixed in glass or rustless steel container, ultrasonic oscillation 10S, obtains mixed essential oil.
By soap base in 60 DEG C of heating water baths, 88 parts of soap bases, 12ml mixed essential oil are taken after soap base dissolving, in being mixed in container
Poured into after closing uniformly in mould, the essential oil soap made is put into 4 DEG C of refrigerator saved backup after cooling.
Antibacterial Activity：
1.1 disk diffusion method
Respectively by bacteria to be tested (Escherichia coli Escherichia coli ATCC 25922, staphylococcus aureus
Staphylococcus aureus subsp.Aureus ATCC25923, Pseudomonas aeruginosa (Pseudomonas aeruginosa)
ATCC27583 beef extract-peptone fluid nutrient medium cultures, each bacterium solution is diluted to 1x10 with than turbid instrument using preceding8CFU·
mL-1。
The beef extract-peptone agar medium of sterilizing is poured into diameter 9cm culture dish, after culture medium solidifying, with shifting
Liquid rifle is drawn each μ l of bacterium solution 100 and is spread evenly across on flat board, and the diameter 6mm filter papers after then taking hot air sterilization with tweezers are smooth
In flat board center.
Every kind of folk prescription essential oil, mixed essential oil cross 0.45 μm of miillpore filter in embodiment 2, and liquid-transfering gun draws 10 μ l drops
It is added on filter paper, each three repetition of processing.Distilled water is set to make blank control, to positive control selected by three kinds of bacteriums
(antibiotic) is respectively penicillin, streptomysin and cefotaxime (1mgmL-1).After essential oil is fully absorbed, 37 DEG C are inverted culture
24 hours, antibacterial circle diameter is determined, takes and measures average value three times.
The bacteriostasis (inhibition zone radius r=mm) of the compound essential oil of table 3
Note：Inhibition zone size unit is mm, accuracy 0.02mm
Escherichia coli, staphylococcus aureus and Pseudomonas aeruginosa are respectively provided with preferably after essential oil mixing in embodiment 2
Fungistatic effect, its antibacterial circle diameter are noticeably greater than single essential oil and antibiotic control group, illustrate have between each essential oil component
Synergy.
1.2 human hands are tested
Subject cleans each of right-hand man with clear water, the essential oil soap of embodiment 2 and certain commercially available brand bacteriostatic soap respectively
Finger, flowing water cleaning after use by autoclave sterilization non-woven fabrics wipe, after drying again respectively with it is anhydrous spin cloth 1h, 2h,
To the random swabing sampling of finger of right-hand man in 3h, 4h period, anhydrous spinning cloth is put into containing containing MH meat soup cultures afterwards
In the conical flask of base number of bacteria is recorded in constant incubator with than turbid instrument after culture 18h.Compared by the concentration of bacterium and matched somebody with somebody
The fungistatic effect of the essential oil soap of system.
Study subject bacterial concentration (× 10 in table 44h8CFU·mL-1) change
As can be seen from the above table, either with the essential oil soap in embodiment 2 or certain commercially available brand bacteriostatic soap, with when
Between extend, the number of bacteria of subject on hand all can showed increased, but its increased degree is different：Stage on-test, three
Name subject is slightly above certain commercially available brand perfumed soap experimental group using the number of bacteria of essential oil soap on hand, but as time went on
(in 2-4 hours), three subjects are substantially less than certain commercially available brand perfumed soap experimental group using the number of bacteria of essential oil soap on hand, held
Continuous bacteriostasis is notable.
Embodiment 3
Take bigarabe flower essential oil 1ml, Lavender 3ml, Melissa officinalis essential oil 3ml, yellow chamomile essential oil 3ml, 1 part of frankincense essential oil
It is well mixed in glass or rustless steel container, ultrasonic oscillation 10S, obtains mixed essential oil.
By soap base in 60 DEG C of heating water baths, 89ml soap bases, 11ml mixed essential oils are taken after soap base dissolving, in being mixed in container
Poured into after uniformly in mould, the essential oil soap made is put into 4 DEG C of refrigerator saved backup after cooling.
Antibacterial Activity：
1.1 disk diffusion method
Respectively by bacteria to be tested (Escherichia coli Escherichia coli ATCC 25922, staphylococcus aureus
Staphylococcus aureus subsp.Aureus ATCC25923, Pseudomonas aeruginosa (Pseudomonas aeruginosa)
ATCC27583 beef extract-peptone fluid nutrient medium cultures, each bacterium solution is diluted to 1x10 with than turbid instrument using preceding8CFU·
mL-1。
The beef extract-peptone agar medium of sterilizing is poured into diameter 9cm culture dish, after culture medium solidifying, with shifting
Liquid rifle is drawn each μ l of bacterium solution 100 and is spread evenly across on flat board, and the diameter 6mm filter papers after then taking hot air sterilization with tweezers are smooth
In flat board center.
Every kind of folk prescription essential oil, mixed essential oil cross 0.45 μm of miillpore filter in embodiment 1, and liquid-transfering gun draws 10 μ l drops
It is added on filter paper, each three repetition of processing.Distilled water is set to make blank control, to positive control selected by three kinds of bacteriums
(antibiotic) is respectively penicillin, streptomysin and cefotaxime (1mgmL-1).After essential oil is fully absorbed, 37 DEG C are inverted culture
24 hours, antibacterial circle diameter is determined, takes and measures average value three times.
The bacteriostasis (inhibition zone radius r=mm) of the compound essential oil of table 5
Note：Inhibition zone size unit is mm, accuracy 0.02mm
The essential oil of embodiment 3 has preferable fungistatic effect to Escherichia coli, staphylococcus aureus, its inhibition zone
Diameter is noticeably greater than single essential oil and antibiotic control group；Single essential oil is better than to the inhibition of Pseudomonas aeruginosa, but is slightly weaker than
The inhibition of antibiotic.
1.2 human hands are tested
Subject cleans each of right-hand man with clear water, the essential oil soap of embodiment 3 and certain commercially available brand bacteriostatic soap respectively
Finger, flowing water cleaning after use by autoclave sterilization non-woven fabrics wipe, after drying again respectively with it is anhydrous spin cloth 1h, 2h,
To the random swabing sampling of finger of right-hand man in 3h, 4h period, anhydrous spinning cloth is put into containing containing MH meat soup cultures afterwards
In the conical flask of base number of bacteria is recorded in constant incubator with than turbid instrument after culture 18h.Compared by the concentration of bacterium and matched somebody with somebody
The fungistatic effect of the essential oil soap of system.
Study subject bacterial concentration (× 10 in table 64h8CFU·mL-1) change
As can be seen from the above table, either with the essential oil soap in embodiment 3 or certain commercially available brand bacteriostatic soap, with when
Between extend, the number of bacteria of subject on hand all can showed increased, but its increased degree is different：Stage on-test (1-2
In hour), subject 1 using essential oil soap number of bacteria on hand close to certain commercially available brand perfumed soap experimental group, but with when
Between extend (in 2-4 hours), subject 1 is substantially less than commercially available certain brand perfumed soap using the number of bacteria of essential oil soap on hand and tested
Group, it is notable to continue bacteriostasis；Subject 2 was substantially less than certain commercially available product in 3 hours using the number of bacteria of essential oil soap on hand
Board perfumed soap experimental group, fungistatic effect is good, 3.5 hours or so, is slightly above certain commercially available product using the number of bacteria of essential oil soap on hand
Board perfumed soap experimental group；Subject 3 is consistently lower than certain commercially available brand perfumed soap experimental group using the number of bacteria of essential oil soap on hand, continues
Bacteriostasis is notable.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, without departing from the technical principles of the invention, some improvements and modifications can also be made, these improvements and modifications
Also it should be regarded as protection scope of the present invention.
Claims (5)
1. a kind of fragrant and sweet type natural plant essential oils soap with bacteria resistance function, it is made up of following components：Bigarabe flower essential oil 1-5
Part, Lavender 1-5 parts, Melissa officinalis essential oil 2-5 parts, yellow chamomile essential oil 1-3 parts, frankincense essential oil 1-3 parts, natural soap base 79-
94 parts, wherein, the essential oil is based on parts by volume.
2. essential oil soap as claimed in claim 1, it is characterised in that be made up of following components：Bigarabe flower essential oil 1-4 parts, smoke clothing
Careless essential oil 1-3 parts, Melissa officinalis essential oil 2-4 parts, yellow chamomile essential oil 1-3 parts, frankincense essential oil part 1-3 parts, natural soap base 83-94 parts,
Wherein, the essential oil is based on parts by volume.
3. essential oil soap as claimed in claim 2, it is characterised in that be made up of following components：4 parts of bigarabe flower essential oil, lavender
2 parts of essential oil, 2 parts of Melissa officinalis essential oil, 2 parts of yellow chamomile essential oil, 2 parts of frankincense essential oil, natural 88 parts of soap base, wherein, the essential oil
Based on parts by volume.
4. the essential oil soap as described in claim any one of 1-3, it is characterised in that described Lavender is that Labiatae smokes clothing
Careless ' capital smokes No. 1 ' flower spike extraction.
5. the preparation method of the essential oil soap described in claim any one of 1-4, it comprises the following steps：
1）Bigarabe flower essential oil, Lavender, Melissa officinalis essential oil, yellow chamomile essential oil, frankincense essential oil are well mixed by proportioning, surpassed
Sound wave shock 5-15S, obtains composite essential oil；
2）By soap base in 50-60 DEG C of heating water bath, after soap base dissolving, soap base and composite essential oil are mixed by volume,
Pour into mould, produce after cooling.
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| CN201510557876.0A CN105176713B (en) | 2015-09-02 | 2015-09-02 | Fragrant and sweet type natural plant essential oils soap with bacteria resistance function and preparation method thereof |
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