CN105168030A - Preparation process and preparation method of variable-color lipstick - Google Patents
Preparation process and preparation method of variable-color lipstick Download PDFInfo
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- CN105168030A CN105168030A CN201510531229.2A CN201510531229A CN105168030A CN 105168030 A CN105168030 A CN 105168030A CN 201510531229 A CN201510531229 A CN 201510531229A CN 105168030 A CN105168030 A CN 105168030A
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Abstract
The invention belongs to the technological field of natural plant compounded cosmetic, concretely relates to compounding of variable-color lipstick, and also relates to a preparation process and a preparation method of variable-color lipstick. The variable-color lipstick is composed of the following raw materials in parts by weight: 30-100 parts of anthocyanidin, 100-250 parts of grease, 20-100 parts of volatile aliphatic acid, 50-300 parts of a surfactant, 50-150 parts of an auxiliary surfactant, and 100-500 parts of deionized water. The main composition of the variable-color lipstick is the natural product anthocyanidin extracted from plants and possesses efficacies of resisting oxidation, delaying ageing and other biological efficacies, and the variable-color lipstick does not contain chemical pigments, is a safe free-stimulation natural plant cosmetic, and is directly edible, possesses extremely high practicability and wide market application prospect.
Description
Technical field
The invention belongs to the technology category of the composite cosmetics of natural plants, be specifically related to the composite of a kind of color-changing lipstick, also relate to preparation process and the preparation method of above-mentioned color-changing lipstick.
Background technology
Anthocyanidin is the natural pigment that nature one class is extensively present in plant, belongs to flavonoids.Main color-generation material in plant petals.Anthocyanidin is present in the epidermis cell of the flower of plant and the tissue of fruit and stem and leaf, can change color along with the soda acid of Cell sap.Cell sap is that acidity is then partially red, and Cell sap is that alkalescence is then partially blue.Edible acid-base indicator is called by people.All anthocyanidin is contained in the many fruits and vegetables of occurring in nature, such as, blue berry, Fructus Vitis viniferae, Rhizoma Dioscoreae esculentae, black currant etc.
Anthocyanidin is described as " oral cosmetics for skin ", has a lot of biological functions.Anthocyanidin molecular structure has multiple hydroxyl, is hydroxyl donor, and be also a kind of free radical scavenger, prevent the generation of body endoperoxides product, therefore, anthocyanidin has effect of antioxidation, slow down aging simultaneously.Anthocyanidin also has the effects such as prophylaxis of cancer, improving water flood, blood pressure lowering blood sugar lowering.
The present invention is that color-changing lipstick prepared by main color-generation material has feature that is nontoxic, that can eat with anthocyanidin, toxic and side effects is not had to human body, to be that multiple natural, green, safe constituent is composite form in simultaneously the present invention, the development trend of cosmetics will be become, there is wide market prospect and economic worth.
Summary of the invention
The invention provides the composite and preparation method thereof of a kind of natural, nontoxic and direct-edible color-changing lipstick;
The technical solution used in the present invention is:
A kind of color-changing lipstick compounded formula, is made up of following parts by weight raw material:
Anthocyanidin 30-100 part oils and fats 100-250 part
Volatile fatty acid 20-100 part surfactant 40-300 part
Cosurfactant 20-150 part deionized water 100-500 part
When described anthocyanidin, it is the natural extract extracted from blue berry, blackberry, Semen Vitis viniferae.Its extraction process flow process is carried out as follows: 0.5% HCl extract (twice) (the solid-liquid ratio 20:1) → filtration → macroporous resin AB-8 getting 28.5g above-mentioned raw materials → cleaning → pulverizing → 570mL adsorbs (aperture 13-14nm) → 60% ethanol elution (6-8mL) → vacuum concentration → lyophilization → anthocyanidin finished product.
When at least one that described oils and fats is stearic acid, lecithin, glycerol, Cera Flava, mineral oil.
When at least one that described volatile fatty acid is acetic acid, propanoic acid, butanoic acid.
When at least one that described surfactant is soybean phospholipid, Tween-60, tween 80 or Arlacel-60.
When at least one that described cosurfactant is ethanol, propanol, PEG400 or isopropyl alcohol.
By formula proportion, anthocyanidin is dissolved in oils and fats, supersonic frequency 10-15kHz, room temperature-40 DEG C is ultrasonic until anthocyanidin dissolves completely, adds surfactant, stir 40-60min, add cosurfactant again, continue to stir 40-60min, finally by deionized water and volatile fatty acid mixing, slowly pour in oil phase, ultrasonic 40-60min, form transparent kermesinus emulsion, sealing is kept in Dark Place.
The color-changing lipstick prepared by preparation method of above-mentioned a kind of color-changing lipstick and relevant product thereof are all in invention which is intended to be protected, and protection scope of the present invention is not limited to this.
The present invention is that color-changing lipstick prepared by main color-generation material has feature that is nontoxic, that can eat with anthocyanidin, toxic and side effects is not had to human body, to be that multiple natural, green, safe constituent is composite form in simultaneously the present invention, the development trend of cosmetics will be become, there is wide market prospect and economic worth.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described, so that those skilled in the art more understands the present invention, but does not therefore limit the present invention.
Embodiment 1
Anthocyanidin 30 parts of glycerol 100 parts
Acetic acid 30 parts of tween 80s 150 parts
PEG400 75 parts of deionized waters 350 parts
Anthocyanidin 30 parts is dissolved in glycerol 100 parts, supersonic frequency 15kHz, room temperature is ultrasonic until anthocyanidin dissolves completely, adds 150 parts of tween 80s, stir 40min, add 75 parts of PEG400s again, continue to stir 40min, finally by deionized water 350 parts and acetic acid 30 parts mixing, slowly pour in oil phase, ultrasonic 40min, form transparent kermesinus emulsion, sealing is kept in Dark Place.
The beneficial effect of technique to color-changing lipstick according to embodiment 1 is tested, and result shows, initial lip pomade is kermesinus, and As time goes on, the minimizing of volatile fatty acid, color-changing lipstick gradual change, finally becomes lavender.
Embodiment 2
Anthocyanidin 90 parts of propolis 200 parts
Propanoic acid 100 parts of soybean phospholipids 250 parts
PEG400 125 parts of deionized waters 250 parts
Anthocyanidin 90 parts is dissolved in Cera Flava 20ml, supersonic frequency 15kHz, room temperature is ultrasonic until anthocyanidin dissolves completely, adds 250 parts of soybean phospholipids, stir 40min, add 125 parts of PEG400s again, continue to stir 40min, finally by deionized water 250 parts and acetic acid 100 parts mixing, slowly pour in oil phase, ultrasonic 40min, form transparent kermesinus emulsion, sealing is kept in Dark Place.
According to the technique of embodiment 2, color-changing lipstick and regular lipstick are carried out to the comparative experiments of technical specification, result is as shown in table 1.
Table 1 color-changing lipstick with contrast lip pomade technical specification and compare
Embodiment 3
Anthocyanidin 70 parts of palmitic acid 170 parts
Acetic acid 80 parts of Tween-60s 180 parts
PEG400 90 parts of deionized waters 400 parts
Anthocyanidin 70 parts is dissolved in palmitic acid 170 parts, supersonic frequency 15kHz, room temperature is ultrasonic until anthocyanidin dissolves completely, adds 180 parts of Tween-60s, stir 40min, add 90 parts of PEG400s again, continue to stir 40min, finally by deionized water 40 parts and acetic acid 80 parts mixing, slowly pour in oil phase, ultrasonic 40min, form transparent kermesinus emulsion, sealing is kept in Dark Place.
Technique according to embodiment 3 carries out sensory evaluation contrast experiment to the beneficial effect of color-changing lipstick and regular lipstick, and result is as shown in table 2.
Table 2 color-changing lipstick with contrast lip pomade organoleptic indicator and compare (5 points /)
Claims (8)
1. a color-changing lipstick, its formula is made up of the following raw material counted by weight:
Anthocyanidin 30-100 part oils and fats 100-250 part
Volatile fatty acid 20-100 part surfactant 40-300 part
Cosurfactant 20-150 part deionized water 100-500 part.
2. a kind of color-changing lipstick as claimed in claim 1, is characterized in that, described anthocyanidin is the natural extract extracted from blue berry, blackberry, Semen Vitis viniferae; Its extraction process flow process is carried out as follows: 0.5% HCl extract (twice) (the solid-liquid ratio 20:1) → filtration → macroporous resin AB-8 getting 28.5g above-mentioned raw materials → cleaning → pulverizing → 570mL adsorbs (aperture 13-14nm) → 60% ethanol elution (6-8mL) → vacuum concentration → lyophilization → anthocyanidin finished product.
3. a kind of color-changing lipstick as claimed in claim 1, is characterized in that, described oils and fats is at least one of stearic acid, lecithin, glycerol, Cera Flava, mineral oil.
4. a kind of color-changing lipstick as claimed in claim 1, is characterized in that, described volatile fatty acid is at least one of acetic acid, propanoic acid, butanoic acid.
5. a kind of color-changing lipstick as claimed in claim 1, is characterized in that, described surfactant is at least one of soybean phospholipid, Tween-60, tween 80 or Arlacel-60.
6. a kind of color-changing lipstick as claimed in claim 1, is characterized in that, described cosurfactant is at least one of ethanol, propanol, PEG400 or isopropyl alcohol.
7. a kind of color-changing lipstick as described in claim 5 or 6, is characterized in that, described surfactant and the ratio of cosurfactant are 2:1.
8. the preparation method of color-changing lipstick as claimed in claim 1, is characterized in that: concrete steps are:
By above-mentioned formula proportion, anthocyanidin is dissolved in oils and fats, supersonic frequency 10-15kHz, room temperature-40 DEG C of sonic oscillation process, until anthocyanidin dissolves completely, add surfactant, stir 40-60min, add cosurfactant again, continue to stir 40-60min, finally by deionized water and volatile fatty acid mixing, slowly pour in oil phase, ultrasonic 40-60min, form transparent kermesinus emulsion, sealing is kept in Dark Place.
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| CN201510531229.2A CN105168030B (en) | 2015-08-26 | 2015-08-26 | The preparation process and preparation method of color-changing lipstick |
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| CN105168030B CN105168030B (en) | 2018-06-01 |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106074317A (en) * | 2016-08-30 | 2016-11-09 | 杭州高峰蓝莓种植有限公司 | Blue berry lipstick and preparation method thereof |
| CN106265274A (en) * | 2016-08-30 | 2017-01-04 | 杭州高峰蓝莓种植有限公司 | Blue berry lip pomade and preparation method thereof |
| CN106806161A (en) * | 2017-03-29 | 2017-06-09 | 珠海京工检测技术有限公司 | One kind extracts kapok anthocyanidin and prepares color-changing lipstick and preparation method thereof |
| CN108478506A (en) * | 2018-05-17 | 2018-09-04 | 范子华 | Color-changing lipstick and preparation method thereof |
| CN110585071A (en) * | 2019-09-16 | 2019-12-20 | 上海花迷化妆品有限公司 | Aqueous color-changing lipstick and preparation method thereof |
| CN113398000A (en) * | 2021-06-21 | 2021-09-17 | 广州易和生物科技有限公司 | Dual-agent color-changing whitening essence and preparation method thereof |
| CN113749379A (en) * | 2021-07-28 | 2021-12-07 | 宁波爱诗化妆品有限公司 | Double-color sandwich eyebrow pencil lead and preparation method thereof |
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| CN1813667A (en) * | 2005-11-23 | 2006-08-09 | 云南农业大学 | Natural red cyanidin cosmetics |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106074317A (en) * | 2016-08-30 | 2016-11-09 | 杭州高峰蓝莓种植有限公司 | Blue berry lipstick and preparation method thereof |
| CN106265274A (en) * | 2016-08-30 | 2017-01-04 | 杭州高峰蓝莓种植有限公司 | Blue berry lip pomade and preparation method thereof |
| CN106806161A (en) * | 2017-03-29 | 2017-06-09 | 珠海京工检测技术有限公司 | One kind extracts kapok anthocyanidin and prepares color-changing lipstick and preparation method thereof |
| CN108478506A (en) * | 2018-05-17 | 2018-09-04 | 范子华 | Color-changing lipstick and preparation method thereof |
| CN110585071A (en) * | 2019-09-16 | 2019-12-20 | 上海花迷化妆品有限公司 | Aqueous color-changing lipstick and preparation method thereof |
| CN113398000A (en) * | 2021-06-21 | 2021-09-17 | 广州易和生物科技有限公司 | Dual-agent color-changing whitening essence and preparation method thereof |
| CN113749379A (en) * | 2021-07-28 | 2021-12-07 | 宁波爱诗化妆品有限公司 | Double-color sandwich eyebrow pencil lead and preparation method thereof |
| CN113749379B (en) * | 2021-07-28 | 2024-03-22 | 宁波爱诗化妆品有限公司 | Double-color sandwich eyebrow pencil lead and preparation method thereof |
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| CN105168030B (en) | 2018-06-01 |
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