CN105131743A - Preparation method for architectural glass heat insulation coating - Google Patents
Preparation method for architectural glass heat insulation coating Download PDFInfo
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- CN105131743A CN105131743A CN201510640772.6A CN201510640772A CN105131743A CN 105131743 A CN105131743 A CN 105131743A CN 201510640772 A CN201510640772 A CN 201510640772A CN 105131743 A CN105131743 A CN 105131743A
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Abstract
The invention provides a preparation method for an architectural glass heat insulation coating. The preparation method includes the steps that ATO nanometer powder, lecithin, triethoxy-1H,1H,2H,2H-tridecafluoro-n-octylsilane and dioctyl sodium sulfosuccinate are added into deionized water and stirred, then silicon carbide whiskers are added, a sodium hydroxide solution with the mass concentration of 1% is dripped on the stirring condition, stirring continues to be carried out until no precipitation is generated, and precipitation is filtered, washed with deionized water and dried to obtain heat insulation powder; the heat insulation powder, SiO2 particles and a silane coupling agent KH-570 are mixed, and the mixture is ground on a ball grinder to obtain functional powder; the functional powder, polytetrafluoroethylene wax powder, perchlorovinyl resin, zinc phosphate, polyacrylamide, mannitol, chitosan, an uvioresistant agent and an antioxidant are mixed and stirred to obtain the architectural glass heat insulation coating. The coating has excellent weather resistance, chemical resistance, waterproof performance and hardness performance.
Description
Technical field
The invention belongs to technical field of coatings, be specifically related to a kind of preparation method of building glass thermal insulating coating.
Background technology
Affecting in the door and window of building energy consumption, body of wall, roof, the large fender member in ground four, the heat-insulating property of door and window is the poorest, is one of important factor affecting indoor thermal environment comfortableness and building energy consumption.The ratio that glass accounts for window areas is different according to the difference of frame material, but along with widely using of indoor large-area French window in glass curtain wall in public building and residential housing, the area that transparency area accounts for window becomes increasing, the thermal property of glass affects the thermal property of whole window to a great extent, and has very large impact to indoor human body comfort level.The thermal property such as shading performance, heat insulating of common single-glass is poor, can produce larger energy dissipation in the middle of use procedure.According to the dependence test of layer glass window thermal property, summer is when there being solar radiation, the energy that room conditioning refrigeration duty is lost because of single-glass can arrive 20-30%, and thermal load was approximately had 30-50% and scattered and disappeared by single-glass window when there being indoor heating winter.
Mainly there is the outstanding problem of following four aspects in current building glass thermal insulating coating: (1) slurry dispersing mode is comparatively single, and dispersion stabilization is poor; (2) visible light-transmissive and infrared barrier photo-thermal index are attended to one thing and lose sight of another, and light thermal property, physicals and Safety and Environmental Protection are difficult to take into account simultaneously, lack the integrated data under photo-thermal balance index (visible light transmissivity and shading coefficient ratio); (3) research of anti-aging and uvioresistant performance is less and the anti-aging time is short; (4) the concrete effect of heat insulation of building glass thermal insulating coating and the research of quantizating index aspect less, lack the clear and comprehensive Experiment of Thermophysics of thermal parameter setting, be short of the concrete thermal parameter of film heat-protecting glass and parameter area.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art and the preparation method that provides a kind of building glass thermal insulating coating, gained coating coating of the present invention has excellent weather-proof, chemicals-resistant, water-fast, hardness performance.
A preparation method for building glass thermal insulating coating, comprises the following steps:
Step 1, with parts by weight, ATO nano powder 20 ~ 30 parts, 2 ~ 7 parts, Yelkin TTS, ten trifluoro octyltri-ethoxysilane 1 ~ 8 part, dioctyl succinate disulfonate acid 2 ~ 9 parts are added in deionized water 40 ~ 60 parts, stir, then add silicon carbide whisker 2 ~ 6 parts, drip the sodium hydroxide solution 10 ~ 20 parts that mass concentration is 1% while stirring, continue to be stirred to and generate without precipitation, filtering-depositing, through deionization cleaning post-drying, obtains heat insulation powder;
Step 2, with parts by weight, by heat insulation for step 1 gained powder 20 ~ 40 parts, SiO
2particle 5 ~ 12 parts and Silane coupling reagent KH-570 3 ~ 9 parts mixing, mixture grinds on ball mill, obtains function powder;
Step 3, with parts by weight, function powder 10 ~ 30 parts is mixed with 5 ~ 9 parts, tetrafluoroethylene wax powder, supervinyi chloride resin 2 ~ 7 parts, zinc phosphate 1 ~ 4 part, polyacrylamide 1 ~ 3 part, 2 ~ 6 parts, N.F,USP MANNITOL, chitosan 3 ~ 7 parts, anti ultraviolet agent 1 ~ 6 part, 2 ~ 5 parts, oxidation inhibitor, stir.
Further, in step 1, bake out temperature is 110 ~ 140 DEG C, and the time is 20 ~ 40min.
Further, silicon carbide whisker diameter is 0.6 ~ 0.8 μm, length is 30 ~ 40 μm.
Further, the particle diameter of function powder is 40 ~ 60 μm.
Further, anti ultraviolet agent is UV-326, UV-327 or UV-531.
Further, oxidation inhibitor is Hinered phenols antioxidant, such as: antioxidant 264, antioxidant 1076.
Further, in step 3, whipping temp is 30 ~ 50 DEG C, and the time is 20 ~ 40min, and speed is 300 ~ 600rpm.
Further, also need in step 3 to add dimethylol propionic acid 3 ~ 7 parts.
Coating of the present invention has excellent weather-proof, chemicals-resistant, water-fast, hardness performance.
Embodiment
Embodiment 1
A preparation method for building glass thermal insulating coating, comprises the following steps:
Step 1, with parts by weight, ATO nano powder 20 parts, 2 parts, Yelkin TTS, ten trifluoro octyltri-ethoxysilane 1 part, dioctyl succinate disulfonate acid 2 parts are added in deionized water 40 parts, stir, then add silicon carbide whisker 2 parts, drip the sodium hydroxide solution 10 parts that mass concentration is 1% while stirring, continue to be stirred to and generate without precipitation, filtering-depositing, through deionization cleaning post-drying, obtains heat insulation powder;
Step 2, with parts by weight, by heat insulation for step 1 gained powder 20 parts, SiO
2particle 5 parts and Silane coupling reagent KH-570 3 parts mixing, mixture grinds on ball mill, obtains function powder;
Step 3, with parts by weight, mixes function powder 10 parts with 5 parts, tetrafluoroethylene wax powder, supervinyi chloride resin 2 parts, zinc phosphate 1 part, polyacrylamide 1 part, 2 parts, N.F,USP MANNITOL, chitosan 3 parts, anti ultraviolet agent 1 part, 2 parts, oxidation inhibitor, stirs.
Wherein, in step 1, bake out temperature is 110 DEG C, and the time is 40min; Silicon carbide whisker diameter is 0.6 μm, length is 30 μm; The particle diameter of function powder is 40 μm; Anti ultraviolet agent is UV-326; Oxidation inhibitor is antioxidant 264; In step 3, whipping temp is 30 DEG C, and the time is 40min, and speed is 300rpm.
Embodiment 2
A preparation method for building glass thermal insulating coating, comprises the following steps:
Step 1, with parts by weight, ATO nano powder 22 parts, 6 parts, Yelkin TTS, ten trifluoro octyltri-ethoxysilane 4 parts, dioctyl succinate disulfonate acid 7 parts are added in deionized water 45 parts, stir, then add silicon carbide whisker 5 parts, drip the sodium hydroxide solution 14 parts that mass concentration is 1% while stirring, continue to be stirred to and generate without precipitation, filtering-depositing, through deionization cleaning post-drying, obtains heat insulation powder;
Step 2, with parts by weight, by heat insulation for step 1 gained powder 25 parts, SiO
2particle 5 parts and Silane coupling reagent KH-570 8 parts mixing, mixture grinds on ball mill, obtains function powder;
Step 3, with parts by weight, mixes function powder 15 parts with 7 parts, tetrafluoroethylene wax powder, supervinyi chloride resin 4 parts, zinc phosphate 3 parts, polyacrylamide 2 parts, 5 parts, N.F,USP MANNITOL, chitosan 5 parts, anti ultraviolet agent 3 parts, 4 parts, oxidation inhibitor, stirs.
Wherein, in step 1, bake out temperature is 130 DEG C, and the time is 30min; Silicon carbide whisker diameter is 0.7 μm, length is 35 μm; The particle diameter of function powder is 50 μm; Anti ultraviolet agent is UV-531; Oxidation inhibitor is antioxidant 1076; In step 3, whipping temp is 40 DEG C, and the time is 30min, and speed is 500rpm.
Embodiment 3
A preparation method for building glass thermal insulating coating, comprises the following steps:
Step 1, with parts by weight, ATO nano powder 27 parts, 6 parts, Yelkin TTS, ten trifluoro octyltri-ethoxysilane 7 parts, dioctyl succinate disulfonate acid 5 parts are added in deionized water 50 parts, stir, then add silicon carbide whisker 4 parts, drip the sodium hydroxide solution 18 parts that mass concentration is 1% while stirring, continue to be stirred to and generate without precipitation, filtering-depositing, through deionization cleaning post-drying, obtains heat insulation powder;
Step 2, with parts by weight, by heat insulation for step 1 gained powder 35 parts, SiO
2particle 5 parts and Silane coupling reagent KH-570 6 parts mixing, mixture grinds on ball mill, obtains function powder;
Step 3, with parts by weight, mixes function powder 25 parts with 8 parts, tetrafluoroethylene wax powder, supervinyi chloride resin 5 parts, zinc phosphate 3 parts, polyacrylamide 2 parts, 5 parts, N.F,USP MANNITOL, chitosan 6 parts, anti ultraviolet agent 3 parts, 4 parts, oxidation inhibitor, stirs.
Wherein, in step 1, bake out temperature is 130 DEG C, and the time is 20min; Silicon carbide whisker diameter is 0.7 μm, length is 40 μm; The particle diameter of function powder is 50 μm; Anti ultraviolet agent is UV-327; Oxidation inhibitor is antioxidant 264; In step 3, whipping temp is 40 DEG C, and the time is 30min, and speed is 500rpm.
Embodiment 4
A preparation method for building glass thermal insulating coating, comprises the following steps:
Step 1, with parts by weight, ATO nano powder 30 parts, 7 parts, Yelkin TTS, ten trifluoro octyltri-ethoxysilane 8 parts, dioctyl succinate disulfonate acid 9 parts are added in deionized water 60 parts, stir, then add silicon carbide whisker 6 parts, drip the sodium hydroxide solution 20 parts that mass concentration is 1% while stirring, continue to be stirred to and generate without precipitation, filtering-depositing, through deionization cleaning post-drying, obtains heat insulation powder;
Step 2, with parts by weight, by heat insulation for step 1 gained powder 40 parts, SiO
2particle 5 parts and Silane coupling reagent KH-570 9 parts mixing, mixture grinds on ball mill, obtains function powder;
Step 3, with parts by weight, mixes function powder 30 parts with 9 parts, tetrafluoroethylene wax powder, supervinyi chloride resin 7 parts, zinc phosphate 4 parts, polyacrylamide 3 parts, 6 parts, N.F,USP MANNITOL, chitosan 7 parts, anti ultraviolet agent 6 parts, 5 parts, oxidation inhibitor, stirs.
Wherein, in step 1, bake out temperature is 110 DEG C, and the time is 40min; Silicon carbide whisker diameter is 0.6 μm, length is 30 μm; The particle diameter of function powder is 40 μm; Anti ultraviolet agent is UV-326; Oxidation inhibitor is antioxidant 264; In step 3, whipping temp is 30 DEG C, and the time is 40min, and speed is 300rpm.
Embodiment 5
The difference of the present embodiment and embodiment 3 is: also need in step 3 to add dimethylol propionic acid 3 ~ 7 parts.
A preparation method for building glass thermal insulating coating, comprises the following steps:
Step 1, with parts by weight, ATO nano powder 27 parts, 6 parts, Yelkin TTS, ten trifluoro octyltri-ethoxysilane 7 parts, dioctyl succinate disulfonate acid 5 parts are added in deionized water 50 parts, stir, then add silicon carbide whisker 4 parts, drip the sodium hydroxide solution 18 parts that mass concentration is 1% while stirring, continue to be stirred to and generate without precipitation, filtering-depositing, through deionization cleaning post-drying, obtains heat insulation powder;
Step 2, with parts by weight, by heat insulation for step 1 gained powder 35 parts, SiO
2particle 5 parts and Silane coupling reagent KH-570 6 parts mixing, mixture grinds on ball mill, obtains function powder;
Step 3, with parts by weight, function powder 25 parts is mixed with 8 parts, tetrafluoroethylene wax powder, supervinyi chloride resin 5 parts, zinc phosphate 3 parts, polyacrylamide 2 parts, 5 parts, N.F,USP MANNITOL, chitosan 6 parts, anti ultraviolet agent 3 parts, 4 parts, oxidation inhibitor, dimethylol propionic acid 6 parts, stirs.
Wherein, in step 1, bake out temperature is 130 DEG C, and the time is 20min; Silicon carbide whisker diameter is 0.7 μm, length is 40 μm; The particle diameter of function powder is 50 μm; Anti ultraviolet agent is UV-327; Oxidation inhibitor is antioxidant 264; In step 3, whipping temp is 40 DEG C, and the time is 30min, and speed is 500rpm.
At ambient temperature, be coated in embodiment 1 to 5 gained paint brush without on the pretreated glass baseplate of surface second, then coating is carried out performance test, result is as follows:
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Examination criteria | |
| Sticking power/level | 1 | 1 | 1 | 1 | 0 | GB/T9286-1998 |
| Hardness | 2H | 2H | 2H | 2H | 3H | GB/T6739-2006 |
| Scratch resistance | 1300g | 1300g | 1300g | 1300g | 1700g | GB/T9279-2007 |
| Water tolerance | 96h | 96h | 96h | 96h | 120h | GB/T1733-1993 |
| Temperature-change resistance | Without exception | GB/T25-1999 |
| Ultraviolet aging resistance | Non-foaming, do not peel off, flawless | GB/T1766-2008 |
As seen from the above table, coating of the present invention has excellent weather-proof, chemicals-resistant, water-fast, hardness performance.
Claims (9)
1. a preparation method for building glass thermal insulating coating, is characterized in that: comprise the following steps:
Step 1, with parts by weight, ATO nano powder 20 ~ 30 parts, 2 ~ 7 parts, Yelkin TTS, ten trifluoro octyltri-ethoxysilane 1 ~ 8 part, dioctyl succinate disulfonate acid 2 ~ 9 parts are added in deionized water 40 ~ 60 parts, stir, then add silicon carbide whisker 2 ~ 6 parts, drip the sodium hydroxide solution 10 ~ 20 parts that mass concentration is 1% while stirring, continue to be stirred to and generate without precipitation, filtering-depositing, through deionization cleaning post-drying, obtains heat insulation powder;
Step 2, with parts by weight, by heat insulation for step 1 gained powder 20 ~ 40 parts, SiO
2particle 5 ~ 12 parts and Silane coupling reagent KH-570 3 ~ 9 parts mixing, mixture grinds on ball mill, obtains function powder;
Step 3, with parts by weight, function powder 10 ~ 30 parts is mixed with 5 ~ 9 parts, tetrafluoroethylene wax powder, supervinyi chloride resin 2 ~ 7 parts, zinc phosphate 1 ~ 4 part, polyacrylamide 1 ~ 3 part, 2 ~ 6 parts, N.F,USP MANNITOL, chitosan 3 ~ 7 parts, anti ultraviolet agent 1 ~ 6 part, 2 ~ 5 parts, oxidation inhibitor, stir.
2. the preparation method of building glass thermal insulating coating according to claim 1, is characterized in that: in step 1, bake out temperature is 110 ~ 140 DEG C, and the time is 20 ~ 40min.
3. the preparation method of building glass thermal insulating coating according to claim 1, is characterized in that: silicon carbide whisker diameter is 0.6 ~ 0.8 μm, length is 30 ~ 40 μm.
4. the preparation method of building glass thermal insulating coating according to claim 1, is characterized in that: the particle diameter of function powder is 40 ~ 60 μm.
5. the preparation method of building glass thermal insulating coating according to claim 1, is characterized in that: anti ultraviolet agent is UV-326, UV-327 or UV-531.
6. the preparation method of building glass thermal insulating coating according to claim 1, is characterized in that: oxidation inhibitor is Hinered phenols antioxidant.
7. the preparation method of building glass thermal insulating coating according to claim 6, is characterized in that: described Hinered phenols antioxidant is antioxidant 264 or antioxidant 1076.
8. the preparation method of building glass thermal insulating coating according to claim 1, is characterized in that: in step 3, whipping temp is 30 ~ 50 DEG C, and the time is 20 ~ 40min, and speed is 300 ~ 600rpm.
9. the preparation method of building glass thermal insulating coating according to claim 1, is characterized in that: also need in step 3 to add dimethylol propionic acid 3 ~ 7 parts.
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| CN201510640772.6A CN105131743A (en) | 2015-09-30 | 2015-09-30 | Preparation method for architectural glass heat insulation coating |
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| CN201510640772.6A CN105131743A (en) | 2015-09-30 | 2015-09-30 | Preparation method for architectural glass heat insulation coating |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105440751A (en) * | 2015-12-28 | 2016-03-30 | 太仓耀华玻璃有限公司 | Thermal insulation coating for curtain-wall glass and production method of thermal insulation coating |
| CN105461237A (en) * | 2015-12-28 | 2016-04-06 | 太仓耀华玻璃有限公司 | LOW-E low-radiation vacuum heat preservation glass and production method thereof |
| CN105462373A (en) * | 2015-12-30 | 2016-04-06 | 曲少春 | Ultraviolet-resistant paint and preparation method thereof |
| CN105563958A (en) * | 2015-12-28 | 2016-05-11 | 太仓耀华玻璃有限公司 | High-heat-insulation noise-reducing anti-radiation vacuum glass and manufacture method thereof |
| CN105565684A (en) * | 2015-12-28 | 2016-05-11 | 太仓耀华玻璃有限公司 | Vacuum glass provided with heat insulation and preservation coating layer and manufacture method thereof |
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| CN103436127A (en) * | 2013-09-06 | 2013-12-11 | 深圳市文浩建材科技有限公司 | Transparent, hydrophobic and heat-insulating coating material for glass and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105440751A (en) * | 2015-12-28 | 2016-03-30 | 太仓耀华玻璃有限公司 | Thermal insulation coating for curtain-wall glass and production method of thermal insulation coating |
| CN105461237A (en) * | 2015-12-28 | 2016-04-06 | 太仓耀华玻璃有限公司 | LOW-E low-radiation vacuum heat preservation glass and production method thereof |
| CN105563958A (en) * | 2015-12-28 | 2016-05-11 | 太仓耀华玻璃有限公司 | High-heat-insulation noise-reducing anti-radiation vacuum glass and manufacture method thereof |
| CN105565684A (en) * | 2015-12-28 | 2016-05-11 | 太仓耀华玻璃有限公司 | Vacuum glass provided with heat insulation and preservation coating layer and manufacture method thereof |
| CN105565684B (en) * | 2015-12-28 | 2018-05-29 | 太仓耀华玻璃有限公司 | A kind of vacuum glass and its manufacturing method with thermal insulation coat |
| CN105461237B (en) * | 2015-12-28 | 2018-05-29 | 太仓耀华玻璃有限公司 | A kind of LOW-E Low emissivities vacuum insulating glass and its production method |
| CN105462373A (en) * | 2015-12-30 | 2016-04-06 | 曲少春 | Ultraviolet-resistant paint and preparation method thereof |
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Inventor after: Sun Zhenbin Inventor after: Su Fu Inventor after: Tong Pengfei Inventor after: Zhao Qing Inventor after: Sun Jun Inventor after: Zou Wei Inventor before: Tong Pengfei Inventor before: Zhao Qing Inventor before: Sun Jun Inventor before: Zou Wei |
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Application publication date: 20151209 |