CN105105328A - Brittle solid spice bead for cigarette filter stick and preparation method thereof - Google Patents
Brittle solid spice bead for cigarette filter stick and preparation method thereof Download PDFInfo
- Publication number
- CN105105328A CN105105328A CN201510472854.4A CN201510472854A CN105105328A CN 105105328 A CN105105328 A CN 105105328A CN 201510472854 A CN201510472854 A CN 201510472854A CN 105105328 A CN105105328 A CN 105105328A
- Authority
- CN
- China
- Prior art keywords
- cigarette filter
- pearl
- solid spice
- loud
- filter rod
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000007787 solid Substances 0.000 title claims abstract description 27
- 235000013599 spices Nutrition 0.000 title claims abstract description 27
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000011324 bead Substances 0.000 title abstract description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 14
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000004014 plasticizer Substances 0.000 claims abstract description 10
- 229920000642 polymer Polymers 0.000 claims abstract description 10
- 239000002861 polymer material Substances 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 235000011187 glycerol Nutrition 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 11
- 239000011248 coating agent Substances 0.000 claims description 10
- 238000000576 coating method Methods 0.000 claims description 10
- 239000000243 solution Substances 0.000 claims description 10
- 238000009833 condensation Methods 0.000 claims description 6
- 230000005494 condensation Effects 0.000 claims description 6
- 238000007493 shaping process Methods 0.000 claims description 6
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 5
- 239000006187 pill Substances 0.000 claims description 5
- 235000010413 sodium alginate Nutrition 0.000 claims description 5
- 239000000661 sodium alginate Substances 0.000 claims description 5
- 229940005550 sodium alginate Drugs 0.000 claims description 5
- 108010010803 Gelatin Proteins 0.000 claims description 4
- 239000008273 gelatin Substances 0.000 claims description 4
- 229920000159 gelatin Polymers 0.000 claims description 4
- 235000019322 gelatine Nutrition 0.000 claims description 4
- 235000011852 gelatine desserts Nutrition 0.000 claims description 4
- 239000011259 mixed solution Substances 0.000 claims description 4
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 239000004925 Acrylic resin Substances 0.000 claims description 3
- 229920002565 Polyethylene Glycol 400 Polymers 0.000 claims description 3
- 235000010489 acacia gum Nutrition 0.000 claims description 3
- 239000001785 acacia senegal l. willd gum Substances 0.000 claims description 3
- 239000001913 cellulose Substances 0.000 claims description 3
- 229920002678 cellulose Polymers 0.000 claims description 3
- JLFNLZLINWHATN-UHFFFAOYSA-N pentaethylene glycol Chemical compound OCCOCCOCCOCCOCCO JLFNLZLINWHATN-UHFFFAOYSA-N 0.000 claims description 3
- 239000004615 ingredient Substances 0.000 abstract 2
- 229920002959 polymer blend Polymers 0.000 abstract 1
- 239000011257 shell material Substances 0.000 description 20
- 239000007788 liquid Substances 0.000 description 7
- 239000002304 perfume Substances 0.000 description 6
- 239000001856 Ethyl cellulose Substances 0.000 description 5
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 5
- 235000019325 ethyl cellulose Nutrition 0.000 description 5
- 229920001249 ethyl cellulose Polymers 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 239000003292 glue Substances 0.000 description 3
- 230000001476 alcoholic effect Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 235000006679 Mentha X verticillata Nutrition 0.000 description 1
- 235000002899 Mentha suaveolens Nutrition 0.000 description 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 238000013475 authorization Methods 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000009569 green tea Nutrition 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
Abstract
The invention provides a brittle solid spice bead for a cigarette filter stick. The brittle solid spice bead comprises a spherical soft kernel and a brittle shell, wherein the brittle shell covers the surface of the spherical soft kernel in a lagging cover manner, and raw materials of the spherical soft kernel is prepared from the following ingredients in percentage by mass: 65 to 90 percent of PEG (polyethylene glycol) polymer or a PEG polymer mixture with a molecular weight of 2000 to 6000, 5 to 25 percent of glycerinum and 0.5 to 15 percent of essence, and raw materials of the brittle shell is prepared from the following ingredients in percentage in mass: 3 to 50 percent of natural high polymer material, 1 to 10 percent of plasticizer, and 60 to 90 percent of water. The invention also provides a preparation method of the brittle solid spice bead for the cigarette filter stick. The brittle solid spice bead is not subjected to the limitation of the essence type and characteristics and high in applicability.
Description
Technical field
The present invention relates to technical field of cigarettes, specifically a kind of loud and clear solid spice pearl for cigarette filter rod and preparation method thereof.
Background technology
At present, most of cigarette manufacturer is by reaching the object of cigarette flavouring to the mode of adding liquid perfumed beads in cigarette filter rod.Chinese patent (Authorization Notice No.: CN102108136B, authorized announcement date: on October 24th, 2012) adopt sodium alginate soln as the glue of perfumed beads shell, by dropping preparation method liquid essence is wrapped in glue and forms capsule, when firmly extruding this perfumed beads, can not only scentetd composition, be also attended by loud and clear sound.But during owing to preparing liquid perfume pearl, high to the surface tension requirements of liquid perfume, must match with the surface tension of glue, otherwise dripping can not become ball, there is significant limitation, therefore need to seek a kind of new perfumed beads preparation method, expand the scope being suitable for essence.
Summary of the invention
For the above-mentioned deficiency of prior art, the invention provides a kind of loud and clear solid spice pearl for cigarette filter rod and preparation method thereof, the restriction of essence classification and character can not be subject to, there is very strong applicability.
The technical solution used in the present invention is as follows:
A kind of loud and clear solid spice pearl for cigarette filter rod, comprise spherical soft core and brittle shell, brittle shell is wrapped in spherical soft core surface by the mode of dressing, the raw material of described spherical soft core is composed as follows according to mass percent: molecular weight is PEG (polyethylene glycol) polymer or its mixture 65%-90% of 2000-6000, glycerine 5%-25%, essence 0.5%-15%, the raw material of described brittle shell is composed as follows according to mass percent: natural macromolecular material 3%-50%, plasticizer 1%-10%, water 60%-90%.
Preferably, described natural macromolecular material is gelatin, Arabic gum or sodium alginate.
Preferably, described plasticizer is glycerine, propane diols or PEG400.
Preferably, described spherical soft nuclear diameter is 0.1-10mm, and the thickness of described brittle shell is 0.01-5mm.
Preferably, mode by dressing between spherical soft core and brittle shell first wraps up one deck waterproof high polymer material, one deck waterproof high polymer material is also wrapped up on brittle shell surface, make solid spice pearl state more stable, described waterproof high polymer material is cellulose derivative (as ethyl cellulose), PVP or polyacrylic resin.
Preferably, described spherical soft nuclear diameter is 1.5mm-4mm.
Preferably, the thickness of described brittle shell is 0.05mm-2mm.
Preferably, for reaching better loud and clear effect, the crushing strength of described spherical soft core is 30pa-700pa.
Preferably, for reaching better loud and clear effect, the crushing strength of described brittle shell is 500pa-1500pa.
For a preparation method for the loud and clear solid spice pearl of cigarette filter rod, comprise the steps:
(1) the first heat fused in the water-bath of 70 DEG C by a certain amount of PEG polymer (molecular weight 2000-6000) or its mixture, and then add essence and glycerine by a certain percentage wherein, wherein each material is composed as follows according to mass percent: PEG polymer (molecular weight 2000-6000) or its mixture 65%-90%, glycerine 5%-25%, essence 0.5%-15%, mix rear standing 2h
(2) utilized by above-mentioned mixed solution automation pill dripping machine to instill condensation cured in atoleine shaping to obtain described spherical soft core, described atoleine temperature is between-4 DEG C-0 DEG C, so that the rapid condensation of drop of instillation is shaping;
(3) natural macromolecular material, plasticizer and water are mixed by following mass percent: natural macromolecular material 3%-50%, plasticizer 1%-10%, water 60%-90%, after stirring, leave standstill 2h, for subsequent use;
(4) using the solution of preparation in step (3) as brittle shell coating solution, adopt coating pan that spherical soft core is carried out dressing, finally obtain product.
Preferably, described spherical soft nuclear diameter is 1.5mm-4mm.
Preferably, the thickness of described brittle shell is 0.05mm-2mm.
Preferably, for reaching better loud and clear effect, the crushing strength of described spherical soft core is 30pa-700pa.
Preferably, for reaching better loud and clear effect, the crushing strength of described brittle shell is 500pa-1500pa.
Preferably, before parcel brittle shell coating solution, first wrap up one deck waterproof high polymer material, final solid spice pearl case surface also wraps up one deck waterproof high polymer material, completely cut off with water and air, make its state more stable, described waterproof high polymer material is cellulose derivative (as ethyl cellulose), PVP or polyacrylic resin class.
By regulating the speed, temperature etc. of pill dripping machine and the parameter such as spray velocity, rotating speed, kettle temperature of coating pan, reach optimum efficiency, this is the routine techniques that those skilled in the art can grasp.
Advantage of the present invention is: (1) existing liquid perfume pearl owing to being subject to capillary restriction in dripping forming process, be only applicable to the use of several limited oil soluble perfume, and the PEG polymeric material that spherical soft core adopts, no matter be water-based essence or oiliness essence, all can be dispersed in wherein, breach the restriction of liquid perfume pearl to essence, range of application is more extensive; (2) adopt traditional art for coating at soft core surface parcel brittle shell material, regulate spherical soft core and the formula of brittle shell and the coating thickness of brittle shell by experiment, obtain applicable intensity, can make its send when crumbing " bang " sound, there is the sound be similar to when liquid perfume pearl is crumbed.
Detailed description of the invention
Below in conjunction with the embodiment in the present invention, be described further, should be appreciated that the specific embodiment described by this part only can be used for explaining the present invention, be not intended to limit the present invention.
Embodiment 1
(1) according to mass percent by PEG polymer (molecular weight 2000) heat fused in the water-bath of 70 DEG C of 75%, and then add 10% Mint Essence and 15% glycerine wherein, mix rear standing 2h.
(2) utilized by above-mentioned mixed solution automation pill dripping machine to instill condensation cured in atoleine shaping to obtain described spherical soft core, the diameter of described soft core is 2mm, and crushing strength is 500pa.
(3) according to mass percent, 5% sodium alginate, 5% propane diols and 90% water are mixed, after stirring, leave standstill 2h, for subsequent use.
(4) coating pan is first adopted ethyl cellulose alcoholic solution to be wrapped in soft core surface, with isolated moisture, and then solution in step (3) is wrapped in spherical soft core surface and forms brittle shell, prepare solid spice pearl, described solid spice pearl brittle shell thickness is 1mm, and crushing strength is 1000Pa.
Embodiment 2
(1) by the PEG polymer (molecular weight 2000) of 55% and PEG polymer (molecular weight 6000) heat fused in the water-bath of 70 DEG C of 30%, and then add 5% Green tea essence and 10% glycerine wherein, mix rear standing 2h.
(2) utilized by above-mentioned mixed solution automation pill dripping machine to instill condensation cured in atoleine shaping to obtain described spherical soft core, the diameter of described soft core is 2.5mm, and crushing strength is 650pa.
(3) 3% gelatin, 9% glycerine and 88% water are mixed by a certain percentage, after stirring, leave standstill 2h, for subsequent use.
(4) coating pan is first adopted ethyl cellulose alcoholic solution to be wrapped in soft core surface, with isolated moisture, and then solution in step (3) is wrapped in spherical soft core surface and forms brittle shell, prepare solid spice pearl, finally wrap up one deck ethyl cellulose at solid spice pearl outer surface again, prepare final products, described solid spice pearl brittle shell thickness is 1.5mm, and crushing strength is 1200Pa.
The above; be only the specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, anyly belongs to those skilled in the art in the technical scope that the present invention discloses; the change that can expect easily or replacement, all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claim.
Claims (10)
1. the loud and clear solid spice pearl for cigarette filter rod, it is characterized in that: comprise spherical soft core and brittle shell, brittle shell is wrapped in spherical soft core surface by the mode of dressing, the raw material of described spherical soft core is composed as follows according to mass percent: molecular weight is polyethylene glycol polymer or its mixture 65%-90% of 2000-6000, glycerine 5%-25%, essence 0.5%-15%, the raw material of described brittle shell is composed as follows according to mass percent: natural macromolecular material 3%-50%, plasticizer 1%-10%, water 60%-90%.
2., as claimed in claim 1 for the loud and clear solid spice pearl of cigarette filter rod, it is characterized in that: described natural macromolecular material is gelatin, Arabic gum or sodium alginate.
3., as claimed in claim 1 for the loud and clear solid spice pearl of cigarette filter rod, it is characterized in that: described plasticizer is glycerine, propane diols or PEG400.
4. as claimed in claim 1 for the loud and clear solid spice pearl of cigarette filter rod, it is characterized in that: described spherical soft nuclear diameter is 0.1-10mm, the thickness of described brittle shell is 0.01-5mm.
5., as claimed in claim 1 for the loud and clear solid spice pearl of cigarette filter rod, it is characterized in that: wrap up one deck waterproof high polymer material by the mode of dressing between spherical soft core and brittle shell, one deck waterproof high polymer material is also wrapped up on brittle shell surface.
6., as claimed in claim 5 for the loud and clear solid spice pearl of cigarette filter rod, it is characterized in that: described waterproof high polymer material is cellulose derivative, PVP or polyacrylic resin.
7., for a preparation method for the loud and clear solid spice pearl of cigarette filter rod, it is characterized in that comprising the steps:
(1) by a certain amount of molecular weight be first polyethylene glycol polymer or its mixture heat fused in the water-bath of 70 DEG C of 2000-6000, and then add essence and glycerine by a certain percentage wherein, wherein each material is composed as follows according to mass percent: molecular weight is polyethylene glycol polymer or its mixture 65%-90% of 2000-6000, glycerine 5%-25%, essence 0.5%-15%, mix rear standing 2h
(2) utilized by above-mentioned mixed solution automation pill dripping machine to instill condensation cured in atoleine shaping to obtain described spherical soft core, described atoleine temperature is between-4 DEG C-0 DEG C, so that the rapid condensation of drop of instillation is shaping;
(3) natural macromolecular material, plasticizer and water are mixed by following mass percent: natural macromolecular material 3%-50%, plasticizer 1%-10%, water 60%-90%, after stirring, leave standstill 2h, for subsequent use;
(4) using the solution of preparation in step (3) as brittle shell coating solution, adopt coating pan that spherical soft core is carried out dressing, finally obtain product.
8., as claimed in claim 7 for the preparation method of the loud and clear solid spice pearl of cigarette filter rod, it is characterized in that: described natural macromolecular material is gelatin, Arabic gum or sodium alginate.
9., as claimed in claim 7 for the preparation method of the loud and clear solid spice pearl of cigarette filter rod, it is characterized in that: described plasticizer is glycerine, propane diols or PEG400.
10., as claimed in claim 7 for the preparation method of the loud and clear solid spice pearl of cigarette filter rod, it is characterized in that: described spherical soft nuclear diameter is 0.1-10mm, the thickness of described brittle shell is 0.01-5mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510472854.4A CN105105328B (en) | 2015-08-05 | 2015-08-05 | A kind of loud and clear solid spice pearl and preparation method thereof for cigarette filter rod |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510472854.4A CN105105328B (en) | 2015-08-05 | 2015-08-05 | A kind of loud and clear solid spice pearl and preparation method thereof for cigarette filter rod |
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| CN105105328A true CN105105328A (en) | 2015-12-02 |
| CN105105328B CN105105328B (en) | 2018-07-17 |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105495686A (en) * | 2016-01-27 | 2016-04-20 | 云南芯韵科技开发有限公司 | Moisture-proof and embrittling treatment method of cigarette capsules and product obtained by treatment method |
| CN106220905A (en) * | 2016-08-30 | 2016-12-14 | 湖北中烟工业有限责任公司 | A kind of drop pill lapping improving cigarette drop pill stability and preparation method thereof |
| CN106235403A (en) * | 2016-08-31 | 2016-12-21 | 云南巴菰生物科技有限公司 | A kind of slow-release fragrance filter stick and preparation method thereof |
| CN107594618A (en) * | 2017-11-08 | 2018-01-19 | 湖北中烟工业有限责任公司 | Sustained release pellet based on natural perfume material Ultramicro-powder and preparation method thereof |
| CN108835712A (en) * | 2018-03-21 | 2018-11-20 | 云南中烟工业有限责任公司 | The complex additive and its preparation method and application of crotonaldehyde release amount in a kind of reduction flue gas |
| CN109846083A (en) * | 2019-02-22 | 2019-06-07 | 广西中烟工业有限责任公司 | A kind of cigarette of appearance setting waterproof wax coat is with quick-fried pearl and preparation method thereof |
| CN110419775A (en) * | 2019-07-10 | 2019-11-08 | 云南巴菰生物科技有限公司 | A kind of quick-fried pearl of anti-seep water and preparation method thereof |
| CN110680010A (en) * | 2019-10-31 | 2020-01-14 | 湖北中烟工业有限责任公司 | Magnolia bark gel bead for cigarettes and preparation method thereof |
| CN110754688A (en) * | 2019-11-11 | 2020-02-07 | 云南恩典科技产业发展有限公司 | Fragrant bead capable of pinching and breaking hollow large-particle filter stick and preparation method thereof |
| WO2021143150A1 (en) * | 2020-01-13 | 2021-07-22 | 云南南中科技有限公司 | Explosion bead for flavored cigarettes and preparation method therefor |
| CN114938861A (en) * | 2022-06-30 | 2022-08-26 | 安徽中烟工业有限责任公司 | Traditional cigarette flavoring particle coating material and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105495686A (en) * | 2016-01-27 | 2016-04-20 | 云南芯韵科技开发有限公司 | Moisture-proof and embrittling treatment method of cigarette capsules and product obtained by treatment method |
| CN106220905A (en) * | 2016-08-30 | 2016-12-14 | 湖北中烟工业有限责任公司 | A kind of drop pill lapping improving cigarette drop pill stability and preparation method thereof |
| CN106220905B (en) * | 2016-08-30 | 2018-05-25 | 湖北中烟工业有限责任公司 | A kind of raising cigarette dripping pill lapping of dripping pill stability and preparation method thereof |
| CN106235403A (en) * | 2016-08-31 | 2016-12-21 | 云南巴菰生物科技有限公司 | A kind of slow-release fragrance filter stick and preparation method thereof |
| CN107594618A (en) * | 2017-11-08 | 2018-01-19 | 湖北中烟工业有限责任公司 | Sustained release pellet based on natural perfume material Ultramicro-powder and preparation method thereof |
| CN108835712A (en) * | 2018-03-21 | 2018-11-20 | 云南中烟工业有限责任公司 | The complex additive and its preparation method and application of crotonaldehyde release amount in a kind of reduction flue gas |
| CN109846083A (en) * | 2019-02-22 | 2019-06-07 | 广西中烟工业有限责任公司 | A kind of cigarette of appearance setting waterproof wax coat is with quick-fried pearl and preparation method thereof |
| CN110419775A (en) * | 2019-07-10 | 2019-11-08 | 云南巴菰生物科技有限公司 | A kind of quick-fried pearl of anti-seep water and preparation method thereof |
| CN110680010A (en) * | 2019-10-31 | 2020-01-14 | 湖北中烟工业有限责任公司 | Magnolia bark gel bead for cigarettes and preparation method thereof |
| CN110754688A (en) * | 2019-11-11 | 2020-02-07 | 云南恩典科技产业发展有限公司 | Fragrant bead capable of pinching and breaking hollow large-particle filter stick and preparation method thereof |
| CN110754688B (en) * | 2019-11-11 | 2021-06-25 | 云南恩典科技产业发展有限公司 | Fragrant bead capable of pinching and breaking hollow large-particle filter stick and preparation method thereof |
| WO2021143150A1 (en) * | 2020-01-13 | 2021-07-22 | 云南南中科技有限公司 | Explosion bead for flavored cigarettes and preparation method therefor |
| CN114938861A (en) * | 2022-06-30 | 2022-08-26 | 安徽中烟工业有限责任公司 | Traditional cigarette flavoring particle coating material and application thereof |
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