CN111345501A - Cigarette containing smoking capsule and capable of being heated without burning - Google Patents
Cigarette containing smoking capsule and capable of being heated without burning Download PDFInfo
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- CN111345501A CN111345501A CN201811569014.XA CN201811569014A CN111345501A CN 111345501 A CN111345501 A CN 111345501A CN 201811569014 A CN201811569014 A CN 201811569014A CN 111345501 A CN111345501 A CN 111345501A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
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Abstract
The invention relates to a heating non-burning cigarette containing a fuming capsule, which sequentially comprises a fuming section of the fuming capsule, a temperature regulating section and a filtering section according to the length ratio of 1-2: 1-3: 0.5 to 1.0. The cigarette prepared by the invention has the advantages of low cost, simple processing method, suitability for industrial production, great improvement on production efficiency and yield, large smoke quantity of the prepared cigarette, low smoke temperature entering the oral cavity and provision of a new path for the production of the cigarette which is not combusted by heating.
Description
[ technical field ] A method for producing a semiconductor device
The invention belongs to the technical field of novel tobacco. More particularly, the present invention relates to a heated non-burning tobacco rod containing a smoking capsule.
[ background of the invention ]
The cigarette which is heated and does not burn is a cigarette made of tobacco substances which are not combusted by electronic equipment, and no open fire or ash is used in the smoking process, so the cigarette is an environment-friendly cigarette. When the cigarette is smoked by adopting electronic heating equipment, a consumer can feel the fragrance of the tobacco, and the non-combustible cigarette is heated at a low temperature (300-500 ℃), so that the release of tar and harmful substances in mainstream smoke can be greatly reduced.
The existing heating non-combustible smoking section is composed of tobacco sheets, the production process is complex, and the quality defect of smoking is brought by the instability of tobacco raw materials. The smoking capsule can replace a sheet in heating non-combustible cigarettes, is used as a carrier for smoking, physiological strength and taste, and releases smoke and fragrance by heating, so that consumers can achieve physiological satisfaction. The smoke agents used in the market are polyalcohol and polyglycerol ester, the water solubility is good, the density of the smoke agents is higher than that of water, the problem cannot be solved by the existing oil capsule system, and the capsule prepared by an emulsifying method has serious liquid leakage phenomenon and is difficult to wrap the smoke agents. It has been found through investigation of the literature that exploratory tests can be performed using UV light curing, which refers to the photo-induced curing of a monomer, oligomer or polymer matrix, typically used in film forming processes. The technology has the characteristics of high efficiency, wide adaptability, economy, energy conservation and environmental protection. The light-cured resin has high water resistance and can be used as a rubber of a smoke agent.
Therefore, the present inventors have completed the present invention by extensive experiments and analyses aiming at various technical defects of the prior art.
[ summary of the invention ]
[ problem to be solved ]
The invention aims to provide a heating non-burning cigarette containing a smoking capsule.
[ solution ]
The invention is realized by the following technical scheme.
The invention relates to a heating non-burning cigarette containing a smoking capsule.
Should not burn a cigarette and be 1 ~ 2 according to length ratio by the capsule section of being fuming, section of adjusting temperature and filter segment in proper order: 1-3: 0.5 to 1.0; the length of the non-burning tobacco rod is not longer than 50 mm.
According to a preferred embodiment of the invention, the smoking capsule smoking segment is a filter rod or paper tube containing a smoking capsule.
According to another preferred embodiment of the invention, the smoking capsule is prepared by the following preparation method:
A. preparation of smoke agent core liquid
The glycerin smoke agent, the flavor substances and the alkaloid are mixed according to the weight ratio of 40-100: 0 to 20: 0.001-0.1, and uniformly mixing to obtain the smoke agent core liquid;
B. preparation of capsule wall material liquid
Uniformly mixing 60-70 parts by weight of epoxy resin oligomer, 10-20 parts by weight of reactive diluent, 1-10 parts by weight of photoinitiator and 1-10 parts by weight of ultraviolet absorbent to obtain capsule wall material liquid;
C. preparation of protective liquid
Water, glycerol and propylene glycol in a weight ratio of 60-80: 3-8: 20-35, and uniformly mixing to obtain the protective solution;
D. fuming capsule dropping system
And (4) dripping the capsule wall material liquid in the step (B) and the smoke agent core liquid in the step (A) into the protective liquid in the step (C) by using a capsule dripping device to obtain the smoke generating capsule.
According to another preferred embodiment of the invention, the flavour is a tobacco, mint, floral, fruity or bouquet flavour; the alkaloid is nicotine, caffeine, theophylline or arecoline.
According to another preferred embodiment of the present invention, the epoxy resin oligomer is a mixture of 3, 4-epoxycyclohexyl-3 ', 4' -epoxycyclohexyl formate and di- (3, 4-epoxycyclohexyl) adipate.
According to another preferred embodiment of the present invention, the reactive diluent is one or more reactive diluents selected from 1, 6-hexanediol diacrylate, triacrylate or pentaerythritol hexaacrylate; the photoinitiator is benzoin dimethyl ether, 1-hydroxycyclohexyl phenyl ketone or a mixture thereof.
According to another preferred embodiment of the present invention, the ultraviolet absorber is phenyl ortho-hydroxybenzoate, 2-hydroxy-4-methoxybenzophenone or a mixture thereof.
According to another preferred embodiment of the present invention, the temperature adjusting section is a cylinder which is formed by extrusion molding food grade silica gel, has a solid middle part and is gear-shaped on the periphery.
According to another preferred embodiment of the invention, the filter segment is a cellulose acetate filter rod, a polylactic acid filter rod or a mixture thereof.
According to another preferred embodiment of the invention, the circumference of the smoking section, the temperature adjusting section and the filtering section is 16-25 cm.
The present invention will be described in detail below.
The invention relates to a heating non-burning cigarette containing a smoking capsule.
Should not burn a cigarette and be 1 ~ 2 according to length ratio by the capsule section of being fuming, section of adjusting temperature and filter segment in proper order: 1-3: 0.5 to 1; the length of the non-burning tobacco rod is not longer than 50 mm.
According to the invention, the smoking capsule smoking segment is a filter rod or a paper hollow tube containing a smoking capsule.
In the invention, the fuming capsule is prepared by adopting the following preparation method:
A. preparation of smoke agent core liquid
The glycerin smoke agent, the flavor substances and the alkaloid are mixed according to the weight ratio of 40-100: 0 to 20: 0.001-0.1, and uniformly mixing to obtain the smoke agent core liquid;
in the present invention, the main role of the glycerol smoking agent in the smoking agent bore fluid is as a solvent carrier and smoke donor. The glycerol used in the present invention is a product currently on the market.
In the present invention, the primary role of the flavor in the liquid of the smoker core is to provide the consumer with an aroma.
The flavor substances used in the invention are tobacco flavor, mint flavor, floral flavor, fruity flavor or vinous flavor substances.
The tobacco flavor used in the present invention is a yunyan tobacco extract, yunyan absolute, burley absolute or aromatic tobacco extract, which are currently commercially available products, such as yunyan tobacco extract sold under the trade name yunyan tobacco extract by guanzhou article research and food technology ltd, and aromatic tobacco extract sold under the trade name aromatic tobacco extract by guanzhou article research and food technology ltd.
The mint flavor used in the present invention is menthol, WS-3 (menthane carboxamide), peppermint oil or peppermint oil, which are all currently marketed products, such as menthol sold under the trade name menthol by Shanghai Jiuxing Kogyo, Inc., WS-3 sold under the trade name menthane carboxamide by Zhengzhongmingyu chemical products, Inc.
The flower fragrance flavor substance used by the invention is gardenia, rose, sweet osmanthus or lily, which are prepared by Yunnan Balaophora mushroom biotechnology limited company and are products sold in the market at present.
The fruity flavor substances used by the invention are lemon, passion fruit, pawpaw or mango, which are prepared by Yunnan Balginia Biotechnology limited company and are products sold in the market at present.
The wine flavor substance used by the invention is Maotai-flavor, Luzhou-flavor, foreign wine flavor or Qu wine, which are prepared by Yunnan Balaozi Biotechnology limited company and are products sold in the market at present.
In the present invention, the primary role of alkaloids in the liquid core of the smoking agent is to provide the consumer with a physiological satisfaction.
The alkaloid used in the invention is nicotine, caffeine, theophylline or arecoline. The tobacco leaves, coffee beans, tea leaves and areca nuts are extracted and refined by the constant handle science and technology limited company of Yunnan, and are products sold in the market at present.
In the present invention, when the amounts of the flavor and the alkaloid are within the above ranges, if the amount of the glycerin smoke generator is less than 40, the amount of smoke is small; if the using amount of the glycerin smoke agent is more than 100, the smoke amount is too large, the smoke is sweet, and the capture of flavor substances is covered; therefore, the amount of the glycerin smoke agent is preferably 40 to 100, more preferably 50 to 85, and still more preferably 58 to 75.
When the consumption of the glycerin smoke agent and the alkaloid is in the range, if the consumption of the flavor substance is higher than 20, the smoke is full of fragrance, and the oral cavity residue is heavy, so that the consumption experience is influenced; therefore, the amount of the flavor is preferably 0 to 20, more preferably 5 to 15, and most preferably 8 to 12.
When the amount of the glycerin smoking agent and the flavoring substance is within the above range, if the amount of the alkaloid is less than 0.001, the strength of the smoking product is weakened and the physiological strength of the consumer is difficult to satisfy; if the dosage of the alkaloid is higher than 0.1, the strength is too high during suction, and discomfort is easily caused; therefore, the amount of the alkaloid is preferably 0.001 to 0.1, more preferably 0.005 to 0.05, and most preferably 0.008 to 0.08.
Preferably, the weight ratio of the glycerin smoke agent to the flavor substance to the alkaloid is 50-85: 5-15: 0.005-0.05.
More preferably, the weight ratio of the glycerin smoke agent, the flavor substances and the alkaloid is 58-75: 8-12: 0.008 to 0.08.
B. Preparation of capsule wall material liquid
Uniformly mixing 60-70 parts by weight of epoxy resin oligomer, 10-20 parts by weight of reactive diluent, 1-10 parts by weight of photoinitiator and 1-10 parts by weight of ultraviolet absorbent to obtain capsule wall material liquid;
in the invention, the main function of the epoxy resin oligomer in the capsule wall material liquid is to form a core material for wrapping the smoke agent, the flavor substance and the alkaloid, and the epoxy resin oligomer is a basic material for forming the capsule shell of the smoke capsule.
The epoxy resin oligomer used in the present invention is a mixture of 3, 4-epoxycyclohexyl-3 ', 4' -epoxycyclohexyl formate and bis- (3, 4-epoxycyclohexyl) adipate in any weight ratio. They are all products which are currently marketed, for example 3, 4-epoxycyclohexyl-3 ', 4' -epoxycyclohexyl formate sold under the name cycloaliphatic epoxy resin by Satsukuwa Tech technologies, Inc., and di- (3, 4-epoxycyclohexyl) adipate sold under the name cycloaliphatic epoxy resin by Shanghai Neisseria Kogyo, Inc.
In the invention, the main function of the reactive diluent in the capsule wall material liquid is to improve the crosslinking degree of the epoxy resin oligomer, thereby improving the compactness of the rubber.
The reactive diluent used in the present invention is one or more selected from 1, 6-hexanediol diacrylate, triacrylate, or pentaerythritol hexaacrylate; they are all products currently on the market.
In the present invention, the main function of the photoinitiator in the capsule wall material liquid is to initiate the mutual crosslinking of the epoxy resin oligomers under the irradiation of light and to enable the crosslinked epoxy resin oligomers to be cured.
The photoinitiator used in the invention is benzoin dimethyl ether, 1-hydroxycyclohexyl phenyl ketone or a mixture thereof; they are all products currently marketed, for example benzoin dimethyl ether sold under the name benzoin diethyl ether by Wuhana white pharmaceutical chemicals Co., Ltd, 1-hydroxycyclohexyl phenyl ketone sold under the name photoinitiator UV184 by Sigma Aldrich trade Co., Ltd.
In the present invention, the main role of the ultraviolet absorber in the capsule wall material liquid is to increase the curing rate of the smoke generating capsule shell.
The ultraviolet absorbent used in the invention is phenyl o-hydroxybenzoate, 2-hydroxy-4-methoxybenzophenone or a mixture thereof; they are all products which are currently marketed, for example phenyl o-hydroxybenzoate which is sold under the name 2-hydroxybenzoic acid by Guanghai Biotech limited, Hubei, and 2-hydroxy-4-methoxybenzophenone which is sold under the name benzophenone-3 by Shanghai Kanglang Biotech limited.
In the present invention, when the amounts of the reactive diluent, the photoinitiator and the ultraviolet absorber are within the above ranges, if the amount of the epoxy resin oligomer is less than 60 parts by weight, the capsule skin becomes thin and it is difficult to wrap the core liquid; if the dosage of the epoxy resin oligomer is higher than 70 parts by weight, the thickness of the capsule rubber is increased, and the hand feeling of kneading and bursting is influenced; therefore, the use amount of the epoxy resin oligomer is reasonable from 60 to 70 parts by weight; preferably 63 to 68 parts by weight.
When the dosage of the epoxy resin oligomer, the photoinitiator and the ultraviolet absorbent is in the range, if the dosage of the active diluent is less than 10 parts by weight, the concentration of the glue solution is high, and the dynamic strength of the glue solution is influenced; if the amount of the active diluent is more than 20 parts by weight, the concentration of the glue solution becomes thin, and the capsule molding is not easy to happen; therefore, the amount of the reactive diluent is preferably 10 to 20 parts by weight; preferably 12 to 16 parts by weight.
When the amounts of the epoxy resin oligomer, the reactive diluent and the ultraviolet absorber are within the above ranges, if the amount of the photoinitiator is less than 1 part by weight, the curing efficiency of the capsule is low and secondary curing is required; if the using amount of the photoinitiator is more than 10 parts by weight, more initiator residues exist in the rubber, and the odor absorption is influenced; therefore, the photoinitiator is suitably used in an amount of 1 to 10 parts by weight; preferably 2 to 7 parts by weight.
When the amount of the epoxy resin oligomer, the reactive diluent and the photoinitiator is within the range, if the amount of the ultraviolet absorber is less than 1 part by weight, curing efficiency and the degree of crosslinking between resins may be reduced; if the amount of the ultraviolet absorber is more than 10 parts by weight, excessive curing occurs, and the capsule becomes hard and hard to be crushed; therefore, the amount of the ultraviolet absorber is 1 to 10 parts by weight; preferably 3 to 8 parts by weight.
Preferably, the weight ratio of the epoxy resin oligomer, the reactive diluent, the photoinitiator and the ultraviolet absorber is 63-68: 12-16: 2-7: 3 to 8.
C. Preparation of protective liquid
Water, glycerol and propylene glycol in a weight ratio of 60-80: 3-8: 20-35, and uniformly mixing to obtain the protective solution;
in the present invention, the main function of the protective liquid in the preparation of the smoking capsule is to shape the smoking capsule.
When the dosage of the glycerol and the propylene glycol is in the range, if the dosage of the water is lower than 60, the density of the protective solution is higher, the capsule is slowly descended, and the production efficiency is reduced; if the using amount of the water is higher than 80, the falling speed of the capsule is high, and the breakage rate is increased; therefore, the amount of water is suitably from 60 to 80, preferably from 66 to 72;
when the amount of water and propylene glycol is within the above range, if the amount of glycerin is less than 3, the density and viscosity of the protective solution are reduced, and the capsule is not easily molded; if the dosage of the glycerol is higher than 8, the density of the protective liquid is increased, and the capsule can float on the upper layer of the protective liquid and is difficult to fall; therefore, the amount of glycerin is suitably 3 to 8, preferably 4 to 6;
when the amount of water and glycerin is within the above range, if the amount of propylene glycol is less than 20, the density of the protective solution decreases, the capsule descends too quickly, and the capsule is not easily molded; if the dosage of the propylene glycol is higher than 35, the viscosity of the protective solution is increased, and the particle size of the capsule is not easy to control; therefore, the amount of propylene glycol is suitably from 20 to 35, preferably from 26 to 30;
preferably, the weight ratio of water, glycerol and propylene glycol is 66-72: 4-6: 26 to 30.
D. Fuming capsule dropping system
And (4) dripping the capsule wall material liquid in the step (B) and the smoke agent core liquid in the step (A) into the protective liquid in the step (C) by using a capsule dripping device to obtain the smoke generating capsule.
The capsule dripping device used by the invention is a dripping pill machine sold by Yunnan Balginetia indica biotechnology limited company under the trade name of cigarette bead blasting dripping device.
The filter stick or the paper hollow tube used by the invention is a filter stick or a paper hollow tube which is commonly used in the technical field and sold in the current market.
According to the invention, the temperature adjusting section has a function of cooling on one hand and is used for connecting the smoking section and the filtering section on the other hand. The temperature adjusting section is a cylinder which is formed by extrusion molding of food-grade silica gel, is solid in the middle and is gear-shaped on the periphery.
The food grade silicone gum and extruder used in the present invention are commonly used in the art and are also commercially available.
According to the invention, the filter segment is a cellulose acetate filter rod, a polylactic acid filter rod or a mixture thereof. Acetate fiber filter sticks and polylactic acid filter sticks are both filter sticks commonly used in the art.
The heating non-combustion cigarette containing the smoking capsule comprises a smoking section, a temperature adjusting section and a filtering section of the smoking capsule in sequence according to the length ratio of 1-2: 1-3: 0.5 to 1.0; lengths of the smoking capsule smoking segment, temperature regulating segment and filter segment outside of the ranges described are undesirable because the condensation effect and smoke path of the smoking capsule smoke can be lengthened, affecting the smoking experience.
The circumference of the smoking section, the temperature adjusting section and the filtering section is 16-25 cm.
The preparation method of the cigarette without burning by heating comprises the following steps: firstly preparing a smoking capsule according to the method described above, and then adding the prepared smoking capsule into a smoking section hollow tube by using a capsule filter rod machine commonly used in the technical field to obtain a smoking section containing the smoking capsule; a cylinder which is formed by extrusion molding of food-grade silica gel, is solid in the middle and gear-shaped at the periphery is used as a temperature adjusting section; the acetate fiber filter stick and the polylactic acid filter stick which are commonly used in the technical field are used as filter sections;
according to the invention, the heating non-combustion cigarette containing the smoking capsule comprises the following components in percentage by weight: a temperature adjusting section: the length ratio of the filtering sections is 1-2: 1-3: 0.5-1.0, the circumference of the cigarette is 16-25 cm, the length of the cigarette is not more than 50mm, and the smoking section, the temperature regulating section and the filtering section are compounded by using a ternary compound filter rod machine to obtain the cigarette which is not combusted by heating.
The specific structure of the cigarette without burning by heating in the invention is shown in figure 1, wherein 1 represents a smoking section; 2 represents a smoking capsule; 3 represents a temperature adjusting section; 4 represents a filtration section; 5 represents a paper empty tube; and 6 represents a tow filter rod.
According to the GB5606.4-2005 cigarette sensory technical requirement smoking standard, a smoking panel consisting of 7 smoking experts is organized to smoke the heated non-burning cigarette prepared by the invention, and smoking results show that the smoking capsule-containing heated non-burning cigarette prepared by the invention can well provide the smoke amount, the fragrance satisfaction and the physiological strength when being smoked by adopting a central heating mode or a peripheral heating mode, has better taste than the commercially sold non-burning cigarette using a tobacco sheet, is comfortable in taste and attractive in fragrance, and meets the psychological and physiological requirements of consumers.
[ advantageous effects ]
The invention has the beneficial effects that:
the cigarette structure is suitable for central and peripheral heating modes for smoking, and the smoking section does not need plant slices to provide smoke volume and physiological satisfaction. The smoking capsule can replace a sheet in heating non-combustible cigarettes, is used as a carrier for smoking, physiological strength and taste, and releases smoke and fragrance by heating, so that consumers can achieve physiological satisfaction. The cigarette prepared by the invention has the advantages of low cost, simple processing method, suitability for industrial production, great improvement on production efficiency and yield, large smoke quantity of the prepared cigarette, low smoke temperature entering the oral cavity and provision of a new path for the production of the cigarette which is not combusted by heating.
[ description of the drawings ]
FIG. 1 is a schematic representation of a heated non-combustible cigarette containing a smoke generating capsule according to the present invention;
the left figure is a heating non-burning cigarette using paper hollow tube;
the right figure is a heated non-burning cigarette using a tow filter rod;
in the figure:
1-a smoke generation section; 2-fuming capsules; 3-temperature adjusting section; 4-a filtration section; 5-paper empty tube; 6-tow filter stick.
[ detailed description ] embodiments
The invention will be better understood from the following examples.
Example 1: preparation of the invention heating non-burning cigarette
The implementation of this example is as follows:
first, a smoking capsule is prepared, which comprises the following steps:
A. preparation of smoke agent core liquid
The glycerin smoke agent, the tobacco flavor substance yunyan extract and the nicotine are mixed according to the weight ratio of 70: 15: 0.01, and uniformly mixing to obtain the smoke agent core liquid;
B. preparation of capsule wall material liquid
Uniformly mixing 64 parts by weight of a mixture epoxy resin oligomer consisting of 3, 4-epoxycyclohexyl-3 ', 4' -epoxycyclohexyl formate and di- (3, 4-epoxycyclohexyl) adipate according to the weight ratio of 1:1, 16 parts by weight of 1, 6-hexanediol diacrylate active diluent, 4 parts by weight of benzoin dimethyl ether photoinitiator and 8 parts by weight of phenyl o-hydroxybenzoate ultraviolet absorbent to obtain a capsule wall material liquid;
C. preparation of protective liquid
Water, glycerol and propylene glycol in a weight ratio of 76: 5: 32, uniformly mixing to obtain the protective solution;
D. fuming capsule dropping system
And D, dripping the capsule wall material liquid obtained in the step B and the smoke agent core obtained in the step A into the protective liquid obtained in the step C by using capsule dripping equipment sold by Yunnan Balginia Biotechnology Co.
And adding the prepared smoking capsules into the hollow smoking section tube by using a capsule filter rod machine to obtain the smoking section containing the smoking capsules.
Extruding food-grade silica gel to form a cylinder with a solid middle part and gear-shaped periphery to obtain a temperature regulating section; a cellulose acetate filter rod was used as the filter segment.
Secondly, preparing the heating non-burning cigarette containing the fuming capsule;
according to the smoking section: a temperature adjusting section: filter segment length ratio 2.0: 1.0: 0.8, 18cm of circumference and 48.0mm of cigarette length, and compounding the smoking section, the temperature regulating section and the filtering section which are described above by using a ternary compound filter rod machine to obtain the cigarette which is not burnt by heating.
Sensory evaluation was performed on the heated non-burning cigarettes prepared in this example according to the evaluation method described in the specification, and the evaluation results are shown in table 1.
Example 2: preparation of the invention heating non-burning cigarette
The implementation of this example is as follows:
first, a smoking capsule is prepared, the steps of which are as follows:
A. preparation of smoke agent core liquid
The weight ratio of the glycerin smoke agent to the mint flavor substance to the caffeine is 85: 20: 0.05, uniformly mixing to obtain the smoke agent core liquid;
B. preparation of capsule wall material liquid
Uniformly mixing 67 parts by weight of a mixture epoxy resin oligomer consisting of 3, 4-epoxycyclohexyl-3 ', 4' -epoxycyclohexyl formate and bis- (3, 4-epoxycyclohexyl) adipate according to a weight ratio of 1:0.5, 20 parts by weight of triacrylate reactive diluent, 5 parts by weight of 1-hydroxycyclohexyl phenyl ketone photoinitiator and 6 parts by weight of 2-hydroxy-4-methoxybenzophenone ultraviolet absorbent to obtain a capsule wall material liquid;
C. preparation of protective liquid
Water, glycerol and propylene glycol in a weight ratio of 60: 6: 20, uniformly mixing to obtain the protective solution;
D. fuming capsule dropping system
And D, dripping the capsule wall material liquid obtained in the step B and the smoke agent core obtained in the step A into the protective liquid obtained in the step C by using capsule dripping equipment sold by Yunnan Balginia Biotechnology Co.
And adding the prepared smoking capsule into the hollow tube of the smoking section by using a capsule filter rod machine to obtain the smoking section containing the smoking capsule.
Extruding food-grade silica gel to form a cylinder with a solid middle part and gear-shaped periphery to obtain a temperature regulating section;
a polylactic acid filter rod is used as the filter segment.
Secondly, preparing the heating non-burning cigarette containing the fuming capsule;
according to the smoking section: a temperature adjusting section: the length ratio of the filter segments is 1.8: 3.0: 0.9, the circumference of the cigarette is 20cm, the length of the cigarette is 49.0mm, and the smoking section, the temperature regulating section and the filtering section are compounded by using a ternary compound filter rod machine to obtain the cigarette which is not burnt by heating.
Sensory evaluation was performed on the heated non-burning cigarettes prepared in this example according to the evaluation method described in the specification, and the evaluation results are shown in table 1.
Example 3: preparation of the invention heating non-burning cigarette
The implementation of this example is as follows:
first, a smoking capsule is prepared, the steps of which are as follows:
A. preparation of smoke agent core liquid
The glycerin smoke agent, the flower fragrance flavor substance gardenia and the theophylline are mixed according to the weight ratio of 40: 18: 0.001 and evenly mixing to obtain the smoke agent core liquid;
B. preparation of capsule wall material liquid
Uniformly mixing 70 parts by weight of a mixture epoxy resin oligomer consisting of 3, 4-epoxycyclohexyl-3 ', 4' -epoxycyclohexyl formate and di- (3, 4-epoxycyclohexyl) adipate in a weight ratio of 1:1.6, 15 parts by weight of pentaerythritol hexaacrylate reactive diluent, 1 part by weight of a mixture of benzoin dimethyl ether and 1-hydroxycyclohexyl phenyl ketone (weight ratio of 1:1) photoinitiator, 1 part by weight of a mixture of phenyl o-hydroxybenzoate and 2-hydroxy-4-methoxy benzophenone (weight ratio of 1:1) ultraviolet absorbent to obtain a capsule wall material liquid;
C. preparation of protective liquid
Water, glycerol and propylene glycol in a weight ratio of 64: 3: 35, uniformly mixing to obtain the protective solution;
D. fuming capsule dropping system
And D, dripping the capsule wall material liquid obtained in the step B and the smoke agent core obtained in the step A into the protective liquid obtained in the step C by using capsule dripping equipment sold by Yunnan Balginia Biotechnology Co.
And adding the prepared smoking capsule into the hollow tube of the smoking section by using a capsule filter rod machine to obtain the smoking section containing the smoking capsule.
Extruding food-grade silica gel to form a cylinder with a solid middle part and gear-shaped periphery to obtain a temperature regulating section;
a cellulose acetate filter rod was used as the filter segment.
Secondly, preparing the heating non-burning cigarette containing the fuming capsule;
according to the smoking section: a temperature adjusting section: the length ratio of the filter segments is 1.2: 2.5: 0.5, the circumference of the cigarette is 16cm, the length of the cigarette is 48.5mm, and the ternary composite filter rod machine is used for compounding the smoking section, the temperature regulating section and the filtering section which are described above to obtain the cigarette which is not burnt by heating.
Sensory evaluation was performed on the heated non-burning cigarettes prepared in this example according to the evaluation method described in the specification, and the evaluation results are shown in table 1.
Example 4: preparation of the invention heating non-burning cigarette
The implementation of this example is as follows:
first, a smoking capsule is prepared, the steps of which are as follows:
A. preparation of smoke agent core liquid
The weight ratio of the glycerin fuming agent to the fruity flavor substance, namely the lemon to the arecoline, is 55: 0: 0.005 evenly mixing to obtain the smoke agent core liquid;
B. preparation of capsule wall material liquid
Uniformly mixing 60 parts by weight of a mixture epoxy resin oligomer consisting of 3, 4-epoxycyclohexyl-3 ', 4' -epoxycyclohexyl formate and di- (3, 4-epoxycyclohexyl) adipate in a weight ratio of 1:2.0, 10 parts by weight of a mixture of 1, 6-hexanediol diacrylate and triacrylate in a weight ratio of 2:1 to obtain a reactive diluent, 10 parts by weight of a mixture of benzoin dimethyl ether and 1-hydroxycyclohexyl phenyl ketone in a weight ratio of 2:1 to obtain a photoinitiator, and 10 parts by weight of a mixture of phenyl o-hydroxybenzoate and 2-hydroxy-4-methoxy benzophenone in a weight ratio of 2:3 to obtain an ultraviolet absorber to obtain a capsule wall material liquid;
C. preparation of protective liquid
Water, glycerol and propylene glycol in a weight ratio of 68: 4: 28, uniformly mixing to obtain the protective solution;
D. fuming capsule dropping system
And D, dripping the capsule wall material liquid obtained in the step B and the smoke agent core obtained in the step A into the protective liquid obtained in the step C by using capsule dripping equipment sold by Yunnan Balginia Biotechnology Co.
And adding the prepared smoking capsule into the hollow tube of the smoking section by using a capsule filter rod machine to obtain the smoking section containing the smoking capsule.
Extruding food-grade silica gel to form a cylinder with a solid middle part and gear-shaped periphery to obtain a temperature regulating section;
a polylactic acid filter rod is used as the filter segment.
Secondly, preparing the heating non-burning cigarette containing the fuming capsule;
according to the smoking section: a temperature adjusting section: filter segment length ratio 1.0: 1.4: 0.6, the circumference of the cigarette is 25cm, the length of the cigarette is 50.0mm, and the smoking section, the temperature regulating section and the filtering section are compounded by using a ternary compound filter rod machine to obtain the cigarette which is not burnt by heating.
Sensory evaluation was performed on the heated non-burning cigarettes prepared in this example according to the evaluation method described in the specification, and the evaluation results are shown in table 1.
Example 5: preparation of the invention heating non-burning cigarette
The implementation of this example is as follows:
first, a smoking capsule is prepared, the steps of which are as follows:
A. preparation of smoke agent core liquid
The ratio of the alkaloids in the mixture of the glycerin smoke agent, the wine flavor substance, the soy sauce flavor type and the nicotine and caffeine (weight ratio is 1:1) is 100: 5: 0.08, mixing uniformly to obtain the smoke agent core liquid;
B. preparation of capsule wall material liquid
Uniformly mixing 62 parts by weight of a mixture epoxy resin oligomer consisting of 3, 4-epoxycyclohexyl-3 ', 4' -epoxycyclohexyl formate and di- (3, 4-epoxycyclohexyl) adipate in a weight ratio of 1:0.8, 12 parts by weight of a triacrylate-pentaerythritol hexaacrylate mixture (in a weight ratio of 1:2) reactive diluent, 8 parts by weight of a benzoin dimethyl ether-1-hydroxycyclohexyl phenyl ketone mixture (in a weight ratio of 1:3) photoinitiator, 4 parts by weight of phenyl o-hydroxybenzoate-2-hydroxy-4-methoxy benzophenone mixture (in a weight ratio of 3:1) ultraviolet absorbent to obtain a capsule wall material liquid;
C. preparation of protective liquid
Water, glycerol and propylene glycol in a weight ratio of 72: 8: 24, uniformly mixing to obtain the protective solution;
D. fuming capsule dropping system
And D, dripping the capsule wall material liquid obtained in the step B and the smoke agent core obtained in the step A into the protective liquid obtained in the step C by using capsule dripping equipment sold by Yunnan Balginia Biotechnology Co.
And adding the prepared smoking capsule into the hollow tube of the smoking section by using a capsule filter rod machine to obtain the smoking section containing the smoking capsule.
Extruding food-grade silica gel to form a cylinder with a solid middle part and gear-shaped periphery to obtain a temperature regulating section;
a cellulose acetate filter rod was used as the filter segment.
Secondly, preparing the heating non-burning cigarette containing the fuming capsule;
according to the smoking section: a temperature adjusting section: the length ratio of the filter segments is 1.4: 2.0: 1.0, the circumference of the cigarette is 22cm, the length of the cigarette is 49.5mm, and the smoking section, the temperature regulating section and the filtering section are compounded by using a ternary compound filter rod machine to obtain the cigarette which is not burnt by heating.
Sensory evaluation was performed on the heated non-burning cigarettes prepared in this example according to the evaluation method described in the specification, and the evaluation results are shown in table 1.
Example 6: preparation of the invention heating non-burning cigarette
The implementation of this example is as follows:
first, a smoking capsule is prepared, the steps of which are as follows:
A. preparation of smoke agent core liquid
The smoking agent is prepared from glycerin, mint-flavor and fruit-flavor passion fruit mixture (weight ratio is 2:3), and theophylline and arecoline mixture (weight ratio is 1:3), wherein the ratio of alkaloids is 60: 10: 0.1, uniformly mixing to obtain the smoke agent core liquid;
B. preparation of capsule wall material liquid
Uniformly mixing 65 parts by weight of a mixture epoxy resin oligomer consisting of 3, 4-epoxycyclohexyl-3 ', 4' -epoxycyclohexyl formate and di- (3, 4-epoxycyclohexyl) adipate in a weight ratio of 1:1.2, 14 parts by weight of a mixture of 1, 6-hexanediol diacrylate and pentaerythritol hexaacrylate in a weight ratio of 3:2, 6 parts by weight of a photoinitiator and a mixture of benzoin dimethyl ether and 1-hydroxycyclohexyl phenyl ketone in a weight ratio of 3:1, and 5 parts by weight of an ultraviolet absorber and a mixture of phenyl o-hydroxybenzoate and 2-hydroxy-4-methoxy benzophenone in a weight ratio of 5:1 to obtain a capsule wall material liquid;
C. preparation of protective liquid
Water, glycerol and propylene glycol according to a weight ratio of 80: 7: 22, uniformly mixing to obtain the protective solution;
D. fuming capsule dropping system
And D, dripping the capsule wall material liquid obtained in the step B and the smoke agent core obtained in the step A into the protective liquid obtained in the step C by using capsule dripping equipment sold by Yunnan Balginia Biotechnology Co.
And adding the prepared smoking capsule into the hollow tube of the smoking section by using a capsule filter rod machine to obtain the smoking section containing the smoking capsule.
Extruding food-grade silica gel to form a cylinder with a solid middle part and gear-shaped periphery to obtain a temperature regulating section;
a polylactic acid filter rod is used as the filter segment.
Secondly, preparing the heating non-burning cigarette containing the fuming capsule;
according to the smoking section: a temperature adjusting section: the length ratio of the filter segments is 1.5: 1.6: 0.7, the circumference of the cigarette is 20cm, the length of the cigarette is 49.2mm, and the smoking section, the temperature regulating section and the filtering section are compounded by using a ternary compound filter rod machine to obtain the cigarette which is not burnt by heating.
Sensory evaluation was performed on the heated non-burning cigarettes prepared in this example according to the evaluation method described in the specification, and the evaluation results are shown in table 1.
Sensory evaluation was also conducted using a currently marketed cigarette without combustion by heating using a tobacco sheet as a control sample, and the evaluation results are also shown in table 1.
Table 1: the sensory evaluation result of the cigarette containing the smoking capsule and heated and not burnt
The results of the panel test in Table 1 show that: the capsule containing smoke can well provide the smoke amount, the fragrance satisfaction and the physiological strength when the capsule containing smoke is heated and the cigarette is not combusted by using a central heating mode or a peripheral heating mode, has slightly better mouthfeel compared with the cigarette which is not combusted by heating and is sold and used by using tobacco sheets in the market, has comfortable mouthfeel and beautiful fragrance, and meets the psychological and physiological requirements of consumers.
Claims (10)
1. The utility model provides a heating that contains capsule of fuming is not fired and is propped up cigarette, its characterized in that it is 1 ~ 2 according to length ratio by capsule of fuming section, section of adjusting temperature and filter segment in proper order: 1-3: 0.5 to 1.0; the length of the non-burning tobacco rod is not longer than 50 mm.
2. The heated non-combustible cigarette according to claim 1, wherein the smoking segment of the smoking capsule is a filter rod or a paper hollow tube containing the smoking capsule.
3. The heated non-combustible tobacco rod of claim 1 or 2, wherein the smoking capsule is prepared by the following method of preparation:
A. preparation of smoke agent core liquid
The glycerin smoke agent, the flavor substances and the alkaloid are mixed according to the weight ratio of 40-100: 0 to 20: 0.001-0.1, and uniformly mixing to obtain the smoke agent core liquid;
B. preparation of capsule wall material liquid
Uniformly mixing 60-70 parts by weight of epoxy resin oligomer, 10-20 parts by weight of reactive diluent, 1-10 parts by weight of photoinitiator and 1-10 parts by weight of ultraviolet absorbent to obtain capsule wall material liquid;
C. preparation of protective liquid
Water, glycerol and propylene glycol in a weight ratio of 60-80: 3-8: 20-35, and uniformly mixing to obtain the protective solution;
D. fuming capsule dropping system
And (4) dripping the capsule wall material liquid in the step (B) and the smoke agent core liquid in the step (A) into the protective liquid in the step (C) by using a capsule dripping device to obtain the smoke generating capsule.
4. The heated non-combustible tobacco rod of claim 1 or 2 wherein the flavoring is a tobacco, mint, floral, fruity or vinous flavoring; the alkaloid is nicotine, caffeine, nicotine, theophylline or arecoline.
5. The non-combustible heated tobacco rod of claim 3 wherein the epoxy oligomer is a mixture of 3, 4-epoxycyclohexyl-3 ', 4' -epoxycyclohexyl formate and bis- (3, 4-epoxycyclohexyl) adipate.
6. The non-combustible heated tobacco rod of claim 3 wherein the reactive diluent is one or more reactive diluents selected from the group consisting of 1, 6-hexanediol diacrylate, triacrylate, and pentaerythritol hexaacrylate; the photoinitiator is benzoin dimethyl ether, 1-hydroxycyclohexyl phenyl ketone or a mixture thereof.
7. The non-combustible heated tobacco rod of claim 1 wherein the ultraviolet light absorber is phenyl paraben, 2-hydroxy-4-methoxybenzophenone or a mixture thereof.
8. The cigarette as claimed in claim 1, wherein the temperature control section is a cylinder formed by extrusion molding food grade silica gel, and having a solid middle part and gear-shaped periphery.
9. The heated nonflammable tobacco rod of claim 1, wherein said filter segment is a cellulose acetate filter rod, a polylactic acid filter rod or a mixture thereof.
10. The heated non-combustible tobacco rod of claim 1, wherein the circumference of the smoking section, the temperature regulating section and the filter section is 16-25 cm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201811569014.XA CN111345501A (en) | 2018-12-21 | 2018-12-21 | Cigarette containing smoking capsule and capable of being heated without burning |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811569014.XA CN111345501A (en) | 2018-12-21 | 2018-12-21 | Cigarette containing smoking capsule and capable of being heated without burning |
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| CN111345501A true CN111345501A (en) | 2020-06-30 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201811569014.XA Pending CN111345501A (en) | 2018-12-21 | 2018-12-21 | Cigarette containing smoking capsule and capable of being heated without burning |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112205666A (en) * | 2020-11-19 | 2021-01-12 | 云南纯旭生物科技有限公司 | A cigarette containing Arecae semen component and capable of being heated without burning |
| CN113349436A (en) * | 2021-06-17 | 2021-09-07 | 武汉市昱宸峰科技有限公司 | Heating non-combustion cigarette with fuming blasting beads |
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| CN112205666A (en) * | 2020-11-19 | 2021-01-12 | 云南纯旭生物科技有限公司 | A cigarette containing Arecae semen component and capable of being heated without burning |
| CN113349436A (en) * | 2021-06-17 | 2021-09-07 | 武汉市昱宸峰科技有限公司 | Heating non-combustion cigarette with fuming blasting beads |
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Address after: 650220 floor 5, building 2, Yunnan returnees Pioneer Park, No. 80, chunman Avenue, Luoyang sub district office, Kunming area, China (Yunnan) pilot Free Trade Zone, Kunming, Yunnan Applicant after: Yunnan Bazi Biotechnology Co.,Ltd. Address before: Room 501-513 502-526, 5th floor, building 2, Yunnan returnees Pioneer Park, 80 chunman Avenue, information industry base, Kunming Economic and Technological Development Zone, Kunming, Yunnan 650220 Applicant before: YUNNAN BAGU BIOTECHNOLOGY Co.,Ltd. |
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Effective date of registration: 20220106 Address after: 650220 floor 5, building 2, Yunnan returnees Pioneer Park, No. 80, chunman Avenue, Luoyang sub district office, Kunming area, China (Yunnan) pilot Free Trade Zone, Kunming, Yunnan Applicant after: Yunnan Bazi Biotechnology Co.,Ltd. Applicant after: Yunnan Chunxu Biotechnology Co.,Ltd. Address before: 650220 floor 5, building 2, Yunnan returnees Pioneer Park, No. 80, chunman Avenue, Luoyang sub district office, Kunming area, China (Yunnan) pilot Free Trade Zone, Kunming, Yunnan Applicant before: Yunnan Bazi Biotechnology Co.,Ltd. |
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Application publication date: 20200630 |