CN105063422A - 一种抗菌能力强的医用石墨烯增强钛合金棒材 - Google Patents
一种抗菌能力强的医用石墨烯增强钛合金棒材 Download PDFInfo
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- CN105063422A CN105063422A CN201510476601.4A CN201510476601A CN105063422A CN 105063422 A CN105063422 A CN 105063422A CN 201510476601 A CN201510476601 A CN 201510476601A CN 105063422 A CN105063422 A CN 105063422A
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- titanium alloy
- alloy rod
- rod bar
- solution
- titanium
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- 229910001069 Ti alloy Inorganic materials 0.000 title claims abstract description 94
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 25
- 229910021389 graphene Inorganic materials 0.000 title claims abstract description 25
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 15
- 239000000843 powder Substances 0.000 claims abstract description 39
- 239000011248 coating agent Substances 0.000 claims abstract description 29
- 238000000576 coating method Methods 0.000 claims abstract description 29
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 22
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000010936 titanium Substances 0.000 claims abstract description 22
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 19
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000010955 niobium Substances 0.000 claims abstract description 10
- 229910052709 silver Inorganic materials 0.000 claims abstract description 10
- 239000004332 silver Substances 0.000 claims abstract description 10
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052684 Cerium Inorganic materials 0.000 claims abstract description 9
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims abstract description 9
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 claims abstract description 9
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims abstract description 9
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims abstract description 9
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 9
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 9
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052796 boron Inorganic materials 0.000 claims abstract description 9
- 229910052804 chromium Inorganic materials 0.000 claims abstract description 9
- 239000011651 chromium Substances 0.000 claims abstract description 9
- 229910052733 gallium Inorganic materials 0.000 claims abstract description 9
- 229910052735 hafnium Inorganic materials 0.000 claims abstract description 9
- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052742 iron Inorganic materials 0.000 claims abstract description 9
- 239000000395 magnesium oxide Substances 0.000 claims abstract description 9
- 229910052750 molybdenum Inorganic materials 0.000 claims abstract description 9
- 239000011733 molybdenum Substances 0.000 claims abstract description 9
- 229910052758 niobium Inorganic materials 0.000 claims abstract description 9
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000000126 substance Substances 0.000 claims abstract description 9
- 229910052715 tantalum Inorganic materials 0.000 claims abstract description 9
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 claims abstract description 9
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052720 vanadium Inorganic materials 0.000 claims abstract description 9
- 239000010456 wollastonite Substances 0.000 claims abstract description 9
- 229910052882 wollastonite Inorganic materials 0.000 claims abstract description 9
- 229910052726 zirconium Inorganic materials 0.000 claims abstract description 9
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 claims abstract 4
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims abstract 4
- 239000000243 solution Substances 0.000 claims description 58
- 238000005242 forging Methods 0.000 claims description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- 238000001816 cooling Methods 0.000 claims description 24
- 238000009413 insulation Methods 0.000 claims description 24
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 22
- 239000007789 gas Substances 0.000 claims description 20
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 claims description 20
- 230000007547 defect Effects 0.000 claims description 16
- 238000002360 preparation method Methods 0.000 claims description 14
- 238000005507 spraying Methods 0.000 claims description 14
- 229910002804 graphite Inorganic materials 0.000 claims description 13
- 239000010439 graphite Substances 0.000 claims description 13
- -1 graphite alkene Chemical class 0.000 claims description 13
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 12
- 239000003513 alkali Substances 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- 230000008569 process Effects 0.000 claims description 12
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 claims description 12
- 239000007921 spray Substances 0.000 claims description 12
- 241000252506 Characiformes Species 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 10
- 235000021110 pickles Nutrition 0.000 claims description 10
- 229940001516 sodium nitrate Drugs 0.000 claims description 10
- 235000010344 sodium nitrate Nutrition 0.000 claims description 10
- 239000004317 sodium nitrate Substances 0.000 claims description 10
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 8
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 8
- 239000004411 aluminium Substances 0.000 claims description 8
- 239000000084 colloidal system Substances 0.000 claims description 8
- 239000008367 deionised water Substances 0.000 claims description 8
- 238000007598 dipping method Methods 0.000 claims description 8
- 230000004927 fusion Effects 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 8
- 238000005554 pickling Methods 0.000 claims description 8
- FZHAPNGMFPVSLP-UHFFFAOYSA-N silanamine Chemical compound [SiH3]N FZHAPNGMFPVSLP-UHFFFAOYSA-N 0.000 claims description 8
- 238000007669 thermal treatment Methods 0.000 claims description 8
- NSOXQYCFHDMMGV-UHFFFAOYSA-N Tetrakis(2-hydroxypropyl)ethylenediamine Chemical compound CC(O)CN(CC(C)O)CCN(CC(C)O)CC(C)O NSOXQYCFHDMMGV-UHFFFAOYSA-N 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 6
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 6
- UREZNYTWGJKWBI-UHFFFAOYSA-M benzethonium chloride Chemical compound [Cl-].C1=CC(C(C)(C)CC(C)(C)C)=CC=C1OCCOCC[N+](C)(C)CC1=CC=CC=C1 UREZNYTWGJKWBI-UHFFFAOYSA-M 0.000 claims description 6
- RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Substances C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 claims description 6
- 230000003647 oxidation Effects 0.000 claims description 6
- 238000007254 oxidation reaction Methods 0.000 claims description 6
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 239000011775 sodium fluoride Substances 0.000 claims description 6
- 235000013024 sodium fluoride Nutrition 0.000 claims description 6
- 229910052582 BN Inorganic materials 0.000 claims description 4
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 4
- 239000004593 Epoxy Substances 0.000 claims description 4
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 4
- 239000006004 Quartz sand Substances 0.000 claims description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 4
- 238000010306 acid treatment Methods 0.000 claims description 4
- 230000032683 aging Effects 0.000 claims description 4
- 238000005275 alloying Methods 0.000 claims description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 4
- 239000012159 carrier gas Substances 0.000 claims description 4
- 238000004140 cleaning Methods 0.000 claims description 4
- 239000000470 constituent Substances 0.000 claims description 4
- 229910021641 deionized water Inorganic materials 0.000 claims description 4
- 239000012153 distilled water Substances 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 238000011010 flushing procedure Methods 0.000 claims description 4
- 230000033444 hydroxylation Effects 0.000 claims description 4
- 238000005805 hydroxylation reaction Methods 0.000 claims description 4
- 238000002347 injection Methods 0.000 claims description 4
- 239000007924 injection Substances 0.000 claims description 4
- 238000005461 lubrication Methods 0.000 claims description 4
- 238000002844 melting Methods 0.000 claims description 4
- 230000008018 melting Effects 0.000 claims description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 238000000465 moulding Methods 0.000 claims description 4
- 230000007935 neutral effect Effects 0.000 claims description 4
- 239000001301 oxygen Substances 0.000 claims description 4
- 229910052760 oxygen Inorganic materials 0.000 claims description 4
- 238000002161 passivation Methods 0.000 claims description 4
- 238000007750 plasma spraying Methods 0.000 claims description 4
- 238000005488 sandblasting Methods 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 239000006104 solid solution Substances 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 229910021642 ultra pure water Inorganic materials 0.000 claims description 4
- 239000012498 ultrapure water Substances 0.000 claims description 4
- 238000010792 warming Methods 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- 230000000415 inactivating effect Effects 0.000 claims description 2
- 229910000108 silver(I,III) oxide Inorganic materials 0.000 claims description 2
- 230000009466 transformation Effects 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 8
- 229910045601 alloy Inorganic materials 0.000 abstract description 7
- 239000000956 alloy Substances 0.000 abstract description 7
- 210000000988 bone and bone Anatomy 0.000 abstract description 4
- NDVLTYZPCACLMA-UHFFFAOYSA-N silver oxide Chemical compound [O-2].[Ag+].[Ag+] NDVLTYZPCACLMA-UHFFFAOYSA-N 0.000 abstract 2
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 abstract 1
- 229910001923 silver oxide Inorganic materials 0.000 abstract 1
- 210000001519 tissue Anatomy 0.000 abstract 1
- 210000004746 tooth root Anatomy 0.000 abstract 1
- 239000010408 film Substances 0.000 description 8
- 229910000883 Ti6Al4V Inorganic materials 0.000 description 5
- ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 description 5
- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 5
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 3
- 238000005260 corrosion Methods 0.000 description 3
- 239000007943 implant Substances 0.000 description 3
- 239000010409 thin film Substances 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000001338 self-assembly Methods 0.000 description 2
- 206010061218 Inflammation Diseases 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 230000017423 tissue regeneration Effects 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
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- Materials For Medical Uses (AREA)
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107352705A (zh) * | 2017-09-03 | 2017-11-17 | 李瑞卿 | 一种节省空间的净水单元组件及净水管路 |
CN111035805A (zh) * | 2019-12-13 | 2020-04-21 | 深圳先进技术研究院 | 一种具有石墨烯-二氧化钛复合抗菌涂层的工件及其制备方法 |
CN112335678A (zh) * | 2020-12-11 | 2021-02-09 | 深圳中汇新材料科技有限公司 | 一种石墨烯复合银离子的可持久杀毒抗菌液 |
CN112933292A (zh) * | 2021-01-25 | 2021-06-11 | 天琪(广东)科技发展有限公司 | 一种改性的牙科种植体及其制备方法 |
CN115403945A (zh) * | 2022-09-07 | 2022-11-29 | 兰州空间技术物理研究所 | 一种镁合金表面复合防腐涂层及其制备方法 |
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CN1686643A (zh) * | 2005-05-19 | 2005-10-26 | 河北工业大学 | 表面有TiO2涂层的钛合金生物医学复合材料及其制备方法 |
CN101608295A (zh) * | 2009-07-17 | 2009-12-23 | 东北大学 | 一种钛合金表面渗硼用粉末渗剂及其使用方法 |
CN101709474A (zh) * | 2009-11-26 | 2010-05-19 | 攀钢集团江油长城特殊钢有限公司 | 一种钛合金的碱酸洗方法 |
CN101724764A (zh) * | 2009-12-10 | 2010-06-09 | 中南大学 | 一种生物医用β-钛合金的制备工艺 |
CN101892403A (zh) * | 2010-06-30 | 2010-11-24 | 大连理工大学 | 一种低Nb含量的生物医用β-钛合金 |
CN102758169A (zh) * | 2012-07-31 | 2012-10-31 | 西北工业大学 | TiAl合金表面包埋共渗Al-Si-Y的工艺方法 |
CN103320734A (zh) * | 2013-06-26 | 2013-09-25 | 西安赛特金属材料开发有限公司 | 医用细晶钛/钛合金棒材的生产方法 |
CN104018145A (zh) * | 2014-06-11 | 2014-09-03 | 上海交通大学 | 一种钛合金表面石墨烯薄膜的制备方法 |
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CN1686643A (zh) * | 2005-05-19 | 2005-10-26 | 河北工业大学 | 表面有TiO2涂层的钛合金生物医学复合材料及其制备方法 |
CN101608295A (zh) * | 2009-07-17 | 2009-12-23 | 东北大学 | 一种钛合金表面渗硼用粉末渗剂及其使用方法 |
CN101709474A (zh) * | 2009-11-26 | 2010-05-19 | 攀钢集团江油长城特殊钢有限公司 | 一种钛合金的碱酸洗方法 |
CN101724764A (zh) * | 2009-12-10 | 2010-06-09 | 中南大学 | 一种生物医用β-钛合金的制备工艺 |
CN101892403A (zh) * | 2010-06-30 | 2010-11-24 | 大连理工大学 | 一种低Nb含量的生物医用β-钛合金 |
CN102758169A (zh) * | 2012-07-31 | 2012-10-31 | 西北工业大学 | TiAl合金表面包埋共渗Al-Si-Y的工艺方法 |
CN103320734A (zh) * | 2013-06-26 | 2013-09-25 | 西安赛特金属材料开发有限公司 | 医用细晶钛/钛合金棒材的生产方法 |
CN104018145A (zh) * | 2014-06-11 | 2014-09-03 | 上海交通大学 | 一种钛合金表面石墨烯薄膜的制备方法 |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107352705A (zh) * | 2017-09-03 | 2017-11-17 | 李瑞卿 | 一种节省空间的净水单元组件及净水管路 |
CN111035805A (zh) * | 2019-12-13 | 2020-04-21 | 深圳先进技术研究院 | 一种具有石墨烯-二氧化钛复合抗菌涂层的工件及其制备方法 |
CN111035805B (zh) * | 2019-12-13 | 2022-02-11 | 深圳先进技术研究院 | 一种具有石墨烯-二氧化钛复合抗菌涂层的工件及其制备方法 |
CN112335678A (zh) * | 2020-12-11 | 2021-02-09 | 深圳中汇新材料科技有限公司 | 一种石墨烯复合银离子的可持久杀毒抗菌液 |
CN112933292A (zh) * | 2021-01-25 | 2021-06-11 | 天琪(广东)科技发展有限公司 | 一种改性的牙科种植体及其制备方法 |
CN115403945A (zh) * | 2022-09-07 | 2022-11-29 | 兰州空间技术物理研究所 | 一种镁合金表面复合防腐涂层及其制备方法 |
CN115403945B (zh) * | 2022-09-07 | 2023-08-22 | 兰州空间技术物理研究所 | 一种镁合金表面复合防腐涂层及其制备方法 |
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