CN105062258A - Fireproof coating - Google Patents

Fireproof coating Download PDF

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Publication number
CN105062258A
CN105062258A CN201510498774.6A CN201510498774A CN105062258A CN 105062258 A CN105062258 A CN 105062258A CN 201510498774 A CN201510498774 A CN 201510498774A CN 105062258 A CN105062258 A CN 105062258A
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parts
retardant coating
titanium dioxide
mass percent
percent concentration
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CN201510498774.6A
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沈宇杰
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Abstract

The invention belongs to the technical field of coatings and particularly relates to a fireproof coating. The fireproof coating is characterized by comprising raw materials in parts by weight as follows: 15 parts of a carboxyethyl cellulose aqueous solution, 18 parts of a polyvinyl acetate emulsion, 25 parts of tri(2-chloroethyl)phosphate, 1.5 parts of an OP-10 emulsifier, 20 parts of talcum powder, 16 parts of titanium dioxide, 1.5 parts of potassium tripolyphosphate, 1.5 parts of mica powder with the finesses smaller than 200 meshes, 3 parts of boric acid, 3.5 parts of a fireproofing agent, 10 parts of distilled water, 3 parts of magnesium hydroxide, 3 parts of silicone oil and 3 parts of dioctyl phthalate. The fireproof coating has the main benefits as follows: the fireproof performance is good, the preparation is convenient, the preparation method is simple, the equipment investment is small, coating is facilitated, and the fireproof coating can be sprayed on machines.

Description

A kind of frie retardant coating
The present invention is that name is called: a kind of frie retardant coating, application number are: 201310218608.7, the applying date is: the divisional application of the patent of invention on June 4th, 2013.
Technical field
The invention belongs to technical field of coatings, especially relate to a kind of frie retardant coating.
Background technology
Coating is as the product of beautifying the environment, be widely used on various buildings, be mainly used in hiding building surface, beautiful enjoyment is obtained to make people, but regrettably coating fire resistance of the prior art is poor, therefore, if the situation having metope other buildings, furniture etc. burned repeatly occurs, cause great injury to the life of people and property.
Summary of the invention
In order to solve the problem, the object of the invention is to disclose a kind of frie retardant coating, it can effectively stop the combustion of flame and spread, and the present invention is achieved through the following technical solutions.
A kind of frie retardant coating, it is characterized in that it includes the raw material of following weight part: mass percent concentration is the carboxyethyl cellulose aqueous solution of 30%: 10 ~ 15 parts, mass percent concentration is the polyvinyl acetate emulsion of 60%: 15 ~ 18 parts, trichloroethyl phosphate: 18 ~ 25 parts, OP-10 type emulsifying agent: 0.5 ~ 1.5 part, talcum powder: 13 ~ 20 parts, titanium dioxide: 13 ~ 16 parts, Potassium tripolyphosphate: 0.5 ~ 1.5 part, fineness is less than 200 object mica powders: 0.5 ~ 1.5 part, boric acid: 1 ~ 3 part, fireproofing agent: 2.5 ~ 3.5 parts, distilled water: 6 ~ 10 parts, magnesium hydroxide: 1 ~ 3 part, silicone oil: 1 ~ 3 part, dioctyl phthalate (DOP): 1 ~ 3 part, described frie retardant coating adopts following methods to obtain: first, take above-mentioned each raw material by weight respectively, secondly, be the carboxyethyl cellulose aqueous solution of 30% by the above-mentioned mass percent concentration claimed, trichloroethyl phosphate, OP-10 type emulsifying agent, talcum powder, titanium dioxide, Potassium tripolyphosphate, fineness be less than 200 object mica powders, boric acid, fireproofing agent, distilled water, magnesium hydroxide fully mix and grind, make it by 200 object filter screens, obtain mixed solution, then, in mixed solution, silicone oil and dioctyl phthalate (DOP) is added while stirring until mix and obtain frie retardant coating.
Frie retardant coating described in first embodiment of the present invention, it is characterized in that it includes the raw material of following weight part: mass percent concentration is the carboxyethyl cellulose aqueous solution of 30%: 10 parts, mass percent concentration is the polyvinyl acetate emulsion of 60%: 15 parts, trichloroethyl phosphate: 18 parts, OP-10 type emulsifying agent: 0.5 part, talcum powder: 13 parts, titanium dioxide: 13 parts, Potassium tripolyphosphate: 0.5 part, fineness is less than 200 object mica powders: 0.5 part, boric acid: 1 part, fireproofing agent: 2.5 parts, distilled water: 6 parts, magnesium hydroxide: 1 part, silicone oil: 1 part, dioctyl phthalate (DOP): 1 part, described frie retardant coating adopts following methods to obtain: first, take above-mentioned each raw material by weight respectively, secondly, be the carboxyethyl cellulose aqueous solution of 30% by the above-mentioned mass percent concentration claimed, trichloroethyl phosphate, OP-10 type emulsifying agent, talcum powder, titanium dioxide, Potassium tripolyphosphate, fineness be less than 200 object mica powders, boric acid, fireproofing agent, distilled water, magnesium hydroxide fully mix and grind, make it by 200 object filter screens, obtain mixed solution, then, in mixed solution, silicone oil and dioctyl phthalate (DOP) is added while stirring until mix and obtain frie retardant coating.
Frie retardant coating described in second embodiment of the present invention, it is characterized in that it includes the raw material of following weight part: mass percent concentration is the carboxyethyl cellulose aqueous solution of 30%: 12 parts, mass percent concentration is the polyvinyl acetate emulsion of 60%: 16 parts, trichloroethyl phosphate: 20 parts, OP-10 type emulsifying agent: 1 part, talcum powder: 16 parts, titanium dioxide: 14 parts, Potassium tripolyphosphate: 1 part, fineness is less than 200 object mica powders: 1 part, boric acid: 2 parts, fireproofing agent: 3 parts, distilled water: 8 parts, magnesium hydroxide: 2 parts, silicone oil: 2 parts, dioctyl phthalate (DOP): 2 parts, described frie retardant coating adopts following methods to obtain: first, take above-mentioned each raw material by weight respectively, secondly, be the carboxyethyl cellulose aqueous solution of 30% by the above-mentioned mass percent concentration claimed, trichloroethyl phosphate, OP-10 type emulsifying agent, talcum powder, titanium dioxide, Potassium tripolyphosphate, fineness be less than 200 object mica powders, boric acid, fireproofing agent, distilled water, magnesium hydroxide fully mix and grind, make it by 200 object filter screens, obtain mixed solution, then, in mixed solution, silicone oil and dioctyl phthalate (DOP) is added while stirring until mix and obtain frie retardant coating.
Frie retardant coating described in 3rd embodiment of the present invention, it is characterized in that it includes the raw material of following weight part: mass percent concentration is the carboxyethyl cellulose aqueous solution of 30%: 15 parts, mass percent concentration is the polyvinyl acetate emulsion of 60%: 18 parts, trichloroethyl phosphate: 25 parts, OP-10 type emulsifying agent: 1.5 parts, talcum powder: 20 parts, titanium dioxide: 16 parts, Potassium tripolyphosphate: 1.5 parts, fineness is less than 200 object mica powders: 1.5 parts, boric acid: 3 parts, fireproofing agent: 3.5 parts, distilled water: 10 parts, magnesium hydroxide: 3 parts, silicone oil: 3 parts, dioctyl phthalate (DOP): 3 parts, described frie retardant coating adopts following methods to obtain: first, take above-mentioned each raw material by weight respectively, secondly, be the carboxyethyl cellulose aqueous solution of 30% by the above-mentioned mass percent concentration claimed, trichloroethyl phosphate, OP-10 type emulsifying agent, talcum powder, titanium dioxide, Potassium tripolyphosphate, fineness be less than 200 object mica powders, boric acid, fireproofing agent, distilled water, magnesium hydroxide fully mix and grind, make it by 200 object filter screens, obtain mixed solution, then, in mixed solution, silicone oil and dioctyl phthalate (DOP) is added while stirring until mix and obtain frie retardant coating.
Frie retardant coating described above, is characterized in that the model of described fireproofing agent is FRX-100 or FRX-210 of Arichem company of U.S. production or domestic FR-28.
Frie retardant coating described above, is characterized in that the model of described titanium dioxide is TR52 or R820.
In the present invention, owing to having magnesium hydroxide, fireproofing agent in frie retardant coating, therefore, flameproof effect is excellent, reaches the grade of not firing, through the flame combustion test of oxycetylene flame, do not fire in 10 minutes, and generally, the temperature of combustion of flame is far below the temperature of oxycetylene flame, therefore, this product has excellent fire resistance.In addition, slightly present alkalescence in this product, and without any bubble in product, be convenient to very much coating, this product can also be applicable to machine spraying, and this production method is simple, and equipment is thrown and entered less; Various raw materials in this product commercially all can by name and/or model purchase.
Therefore, the present invention has following main beneficial effect: fire resistance is good, easy to make, making method is simple, equipment investment is few, be convenient to coating, is also suitable for machine spraying.
Embodiment
Public from understanding the present invention better in order to make, now best embodiment is described in detail.
embodiment 1
A kind of frie retardant coating, is characterized in that it includes the raw material of following weight part: mass percent concentration is the carboxyethyl cellulose aqueous solution of 30%: 10 parts, mass percent concentration is the polyvinyl acetate emulsion of 60%: 15 parts, trichloroethyl phosphate: 18 parts, OP-10 type emulsifying agent: 0.5 part, talcum powder: 13 parts, titanium dioxide: 13 parts, Potassium tripolyphosphate: 0.5 part, fineness is less than 200 object mica powders: 0.5 part, boric acid: 1 part, fireproofing agent: 2.5 parts, distilled water: 6 parts, magnesium hydroxide: 1 part, silicone oil: 1 part, dioctyl phthalate (DOP): 1 part; Described frie retardant coating adopts following methods to obtain: first, take above-mentioned each raw material by weight respectively; Secondly, be the carboxyethyl cellulose aqueous solution of 30% by the above-mentioned mass percent concentration claimed, trichloroethyl phosphate, OP-10 type emulsifying agent, talcum powder, titanium dioxide, Potassium tripolyphosphate, fineness be less than 200 object mica powders, boric acid, fireproofing agent, distilled water, magnesium hydroxide fully mix and grind, make it by 200 object filter screens, obtain mixed solution; Then, in mixed solution, silicone oil and dioctyl phthalate (DOP) is added while stirring until mix and obtain frie retardant coating.
embodiment 2
A kind of frie retardant coating, is characterized in that it includes the raw material of following weight part: mass percent concentration is the carboxyethyl cellulose aqueous solution of 30%: 12 parts, mass percent concentration is the polyvinyl acetate emulsion of 60%: 16 parts, trichloroethyl phosphate: 20 parts, OP-10 type emulsifying agent: 1 part, talcum powder: 16 parts, titanium dioxide: 14 parts, Potassium tripolyphosphate: 1 part, fineness is less than 200 object mica powders: 1 part, boric acid: 2 parts, fireproofing agent: 3 parts, distilled water: 8 parts, magnesium hydroxide: 2 parts, silicone oil: 2 parts, dioctyl phthalate (DOP): 2 parts; Described frie retardant coating adopts following methods to obtain: first, take above-mentioned each raw material by weight respectively; Secondly, be the carboxyethyl cellulose aqueous solution of 30% by the above-mentioned mass percent concentration claimed, trichloroethyl phosphate, OP-10 type emulsifying agent, talcum powder, titanium dioxide, Potassium tripolyphosphate, fineness be less than 200 object mica powders, boric acid, fireproofing agent, distilled water, magnesium hydroxide fully mix and grind, make it by 200 object filter screens, obtain mixed solution; Then, in mixed solution, silicone oil and dioctyl phthalate (DOP) is added while stirring until mix and obtain frie retardant coating.
embodiment 3
A kind of frie retardant coating, is characterized in that it includes the raw material of following weight part: mass percent concentration is the carboxyethyl cellulose aqueous solution of 30%: 15 parts, mass percent concentration is the polyvinyl acetate emulsion of 60%: 18 parts, trichloroethyl phosphate: 25 parts, OP-10 type emulsifying agent: 1.5 parts, talcum powder: 20 parts, titanium dioxide: 16 parts, Potassium tripolyphosphate: 1.5 parts, fineness is less than 200 object mica powders: 1.5 parts, boric acid: 3 parts, fireproofing agent: 3.5 parts, distilled water: 10 parts, magnesium hydroxide: 3 parts, silicone oil: 3 parts, dioctyl phthalate (DOP): 3 parts; Described frie retardant coating adopts following methods to obtain: first, take above-mentioned each raw material by weight respectively; Secondly, be the carboxyethyl cellulose aqueous solution of 30% by the above-mentioned mass percent concentration claimed, trichloroethyl phosphate, OP-10 type emulsifying agent, talcum powder, titanium dioxide, Potassium tripolyphosphate, fineness be less than 200 object mica powders, boric acid, fireproofing agent, distilled water, magnesium hydroxide fully mix and grind, make it by 200 object filter screens, obtain mixed solution; Then, in mixed solution, silicone oil and dioctyl phthalate (DOP) is added while stirring until mix and obtain frie retardant coating.
Through the repetition test of the applicant, find the coating adopting following formula and method to prepare, all having excellently has fire resistance.
A kind of frie retardant coating, it is characterized in that it includes the raw material of following weight part: mass percent concentration is the carboxyethyl cellulose aqueous solution of 30%: 10 ~ 15 parts, mass percent concentration is the polyvinyl acetate emulsion of 60%: 15 ~ 18 parts, trichloroethyl phosphate: 18 ~ 25 parts, OP-10 type emulsifying agent: 0.5 ~ 1.5 part, talcum powder: 13 ~ 20 parts, titanium dioxide: 13 ~ 16 parts, Potassium tripolyphosphate: 0.5 ~ 1.5 part, fineness is less than 200 object mica powders: 0.5 ~ 1.5 part, boric acid: 1 ~ 3 part, fireproofing agent: 2.5 ~ 3.5 parts, distilled water: 6 ~ 10 parts, magnesium hydroxide: 1 ~ 3 part, silicone oil: 1 ~ 3 part, dioctyl phthalate (DOP): 1 ~ 3 part, described frie retardant coating adopts following methods to obtain: first, take above-mentioned each raw material by weight respectively, secondly, be the carboxyethyl cellulose aqueous solution of 30% by the above-mentioned mass percent concentration claimed, trichloroethyl phosphate, OP-10 type emulsifying agent, talcum powder, titanium dioxide, Potassium tripolyphosphate, fineness be less than 200 object mica powders, boric acid, fireproofing agent, distilled water, magnesium hydroxide fully mix and grind, make it by 200 object filter screens, obtain mixed solution, then, in mixed solution, silicone oil and dioctyl phthalate (DOP) is added while stirring until mix and obtain frie retardant coating.
Frie retardant coating described in above-mentioned arbitrary embodiment, is characterized in that the model of described fireproofing agent is FRX-100 or FRX-210 of Arichem company of U.S. production or domestic FR-28; Commercially can buy by model and title.
Frie retardant coating described in above-mentioned arbitrary embodiment, frie retardant coating described above, is characterized in that the model of described titanium dioxide is TR52 or R820; Commercially can buy by model and title.
In the present invention, owing to having magnesium hydroxide, fireproofing agent in frie retardant coating, therefore, flameproof effect is excellent, reaches the grade of not firing, through the flame combustion test of oxycetylene flame, do not fire in 10 minutes, and generally, the temperature of combustion of flame is far below the temperature of oxycetylene flame, therefore, this product has excellent fire resistance.In addition, slightly present alkalescence in this product, and without any bubble in product, be convenient to very much coating, this product can also be applicable to machine spraying, and this production method is simple, and equipment is thrown and entered less; Various raw materials in this product commercially all can by name and/or model purchase.
Therefore, the present invention has following main beneficial effect: fire resistance is good, easy to make, making method is simple, equipment investment is few, be convenient to coating, is also suitable for machine spraying.
The present invention is not limited to above-mentioned preferred forms, and should be appreciated that design of the present invention can be implemented to use by other various forms, they drop in protection scope of the present invention equally.

Claims (4)

1. a frie retardant coating, it is characterized in that it includes the raw material of following weight part: mass percent concentration is the carboxyethyl cellulose aqueous solution of 30%: 15 parts, mass percent concentration is the polyvinyl acetate emulsion of 60%: 18 parts, trichloroethyl phosphate: 25 parts, OP-10 type emulsifying agent: 1.5 parts, talcum powder: 20 parts, titanium dioxide: 16 parts, Potassium tripolyphosphate: 1.5 parts, fineness is less than 200 object mica powders: 1.5 parts, boric acid: 3 parts, fireproofing agent: 3.5 parts, distilled water: 10 parts, magnesium hydroxide: 3 parts, silicone oil: 3 parts, dioctyl phthalate (DOP): 3 parts, described frie retardant coating adopts following methods to obtain: first, take above-mentioned each raw material by weight respectively, secondly, be the carboxyethyl cellulose aqueous solution of 30% by the above-mentioned mass percent concentration claimed, trichloroethyl phosphate, OP-10 type emulsifying agent, talcum powder, titanium dioxide, Potassium tripolyphosphate, fineness be less than 200 object mica powders, boric acid, fireproofing agent, distilled water, magnesium hydroxide fully mix and grind, make it by 200 object filter screens, obtain mixed solution, then, in mixed solution, silicone oil and dioctyl phthalate (DOP) is added while stirring until mix and obtain frie retardant coating, the model of described titanium dioxide is TR52 or R820, the model of described fireproofing agent is FRX-100 or FRX-210 or FR-28.
2. a frie retardant coating, it is characterized in that it includes the raw material of following weight part: mass percent concentration is the carboxyethyl cellulose aqueous solution of 30%: 10 ~ 15 parts, mass percent concentration is the polyvinyl acetate emulsion of 60%: 15 ~ 18 parts, trichloroethyl phosphate: 18 ~ 25 parts, OP-10 type emulsifying agent: 0.5 ~ 1.5 part, talcum powder: 13 ~ 20 parts, titanium dioxide: 13 ~ 16 parts, Potassium tripolyphosphate: 0.5 ~ 1.5 part, fineness is less than 200 object mica powders: 0.5 ~ 1.5 part, boric acid: 1 ~ 3 part, fireproofing agent: 2.5 ~ 3.5 parts, distilled water: 6 ~ 10 parts, magnesium hydroxide: 1 ~ 3 part, silicone oil: 1 ~ 3 part, dioctyl phthalate (DOP): 1 ~ 3 part, described frie retardant coating adopts following methods to obtain: first, take above-mentioned each raw material by weight respectively, secondly, be the carboxyethyl cellulose aqueous solution of 30% by the above-mentioned mass percent concentration claimed, trichloroethyl phosphate, OP-10 type emulsifying agent, talcum powder, titanium dioxide, Potassium tripolyphosphate, fineness be less than 200 object mica powders, boric acid, fireproofing agent, distilled water, magnesium hydroxide fully mix and grind, make it by 200 object filter screens, obtain mixed solution, then, in mixed solution, silicone oil and dioctyl phthalate (DOP) is added while stirring until mix and obtain frie retardant coating, the model of described titanium dioxide is TR52 or R820, the model of described fireproofing agent is FR-28.
3. a frie retardant coating, it is characterized in that it includes the raw material of following weight part: mass percent concentration is the carboxyethyl cellulose aqueous solution of 30%: 10 parts, mass percent concentration is the polyvinyl acetate emulsion of 60%: 15 parts, trichloroethyl phosphate: 18 parts, OP-10 type emulsifying agent: 0.5 part, talcum powder: 13 parts, titanium dioxide: 13 parts, Potassium tripolyphosphate: 0.5 part, fineness is less than 200 object mica powders: 0.5 part, boric acid: 1 part, fireproofing agent: 2.5 parts, distilled water: 6 parts, magnesium hydroxide: 1 part, silicone oil: 1 part, dioctyl phthalate (DOP): 1 part, described frie retardant coating adopts following methods to obtain: first, take above-mentioned each raw material by weight respectively, secondly, be the carboxyethyl cellulose aqueous solution of 30% by the above-mentioned mass percent concentration claimed, trichloroethyl phosphate, OP-10 type emulsifying agent, talcum powder, titanium dioxide, Potassium tripolyphosphate, fineness be less than 200 object mica powders, boric acid, fireproofing agent, distilled water, magnesium hydroxide fully mix and grind, make it by 200 object filter screens, obtain mixed solution, then, in mixed solution, silicone oil and dioctyl phthalate (DOP) is added while stirring until mix and obtain frie retardant coating, the model of described titanium dioxide is TR52 or R820, the model of described fireproofing agent is FR-28.
4. frie retardant coating according to claim 1, it is characterized in that it includes the raw material of following weight part: mass percent concentration is the carboxyethyl cellulose aqueous solution of 30%: 12 parts, mass percent concentration is the polyvinyl acetate emulsion of 60%: 16 parts, trichloroethyl phosphate: 20 parts, OP-10 type emulsifying agent: 1 part, talcum powder: 16 parts, titanium dioxide: 14 parts, Potassium tripolyphosphate: 1 part, fineness is less than 200 object mica powders: 1 part, boric acid: 2 parts, fireproofing agent: 3 parts, distilled water: 8 parts, magnesium hydroxide: 2 parts, silicone oil: 2 parts, dioctyl phthalate (DOP): 2 parts, described frie retardant coating adopts following methods to obtain: first, take above-mentioned each raw material by weight respectively, secondly, be the carboxyethyl cellulose aqueous solution of 30% by the above-mentioned mass percent concentration claimed, trichloroethyl phosphate, OP-10 type emulsifying agent, talcum powder, titanium dioxide, Potassium tripolyphosphate, fineness be less than 200 object mica powders, boric acid, fireproofing agent, distilled water, magnesium hydroxide fully mix and grind, make it by 200 object filter screens, obtain mixed solution, then, in mixed solution, silicone oil and dioctyl phthalate (DOP) is added while stirring until mix and obtain frie retardant coating, the model of described titanium dioxide is TR52 or R820, the model of described fireproofing agent is FR-28.
CN201510498774.6A 2013-06-04 2013-06-04 Fireproof coating Pending CN105062258A (en)

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CN104860604A (en) * 2015-04-23 2015-08-26 铜陵祥云消防科技有限责任公司 Anti-corrosion anti-permeability fire-retardant coating
CN107011761A (en) * 2017-05-05 2017-08-04 常州大学 A kind of oil resistant anti-mildew fireproof coating and preparation method thereof
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