CN105062192A - Fast red for water-based ink and preparation method thereof - Google Patents
Fast red for water-based ink and preparation method thereof Download PDFInfo
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- CN105062192A CN105062192A CN201510551921.1A CN201510551921A CN105062192A CN 105062192 A CN105062192 A CN 105062192A CN 201510551921 A CN201510551921 A CN 201510551921A CN 105062192 A CN105062192 A CN 105062192A
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Abstract
The invention discloses fast red for water-based ink and a preparation method thereof. The fast red for water-based ink is prepared from, by weight parts, 5-8 parts of fast red, 20-25 parts of deionized water, 11-18 parts of polyvinyl alcohol, 5-11 parts of bisphenol-A diglycidyl ether, 4-8 parts of di-amine-propyl polydimethylsiloxane, 4-7 parts of amide modified hydrogenated castor oil, 4-7 parts of calcium carbonate, 3-5 parts of magnesium oxide, 2-3 parts of barium titanate, 1-3 parts of octamethyl cyclotetrasiloxane, 1-2 parts of ammonium persulfate and 1-2 parts of poly(3,4-ethylenedioxythiophene). The invention further provides a method for preparing the fast red for the water-based ink.
Description
Technical field
The invention belongs to water color ink field, particularly one sun-proof used for water color ink is red and preparation method thereof.
Background technology
Ink is the important materials for printing, and is by printing by pattern, literal table now on the substrate.Ink comprises main component and ancillary component, primarily of compositions such as low-melting ink vehicle, pigment, filler, auxiliary agent and solvents.Ink is widely used in the various printings such as books and periodicals, packing and decorating, building decoration and electronic circuit sheet material.
The maximum difference of water color ink and solvent type ink, is that the solvent that it uses is water instead of organic solvent, obviously reduces VOC quantity discharged, energy air conservation, does not affect HUMAN HEALTH, nonflammable, bright in luster, do not corrode plate, simple to operate, low price, after print, attached outstanding power is good, and water resisting property is strong, rapidly dry, therefore water color ink is specially adapted to the package printed matters such as food, beverage, medicine, is universally acknowledged environment-friendly type printing material.
Summary of the invention
For above-mentioned demand, invention especially provides a kind of sun-proof used for water color ink red and preparation method thereof.
Object of the present invention can be achieved through the following technical solutions:
A kind of sun-proof used for water color ink is red, is made up of the component comprising following weight part:
The red 5-8 part of sun-proof,
Deionized water 20-25 part,
Polyvinyl alcohol 11-18 part,
Dihydroxyphenyl propane bisglycidyl ether 5-11 part,
Diamine propyl group polydimethylsiloxane 4-8 part,
Amide modifications hydrogenated castor oil 4-7 part,
Calcium carbonate 4-7 part,
Magnesium oxide 3-5 part,
Barium titanate 2-3 part,
Octamethylcyclotetrasiloxane 1-3 part,
Ammonium persulphate 1-2 part,
Polyglycolic acid fibre 1-2 part.
Described component also comprises Polycarbosilane 0-1 weight part.
Described component also comprises N-BUTYL ACETATE 0-1 weight part.
The molecular-weight average of described polyvinyl alcohol is 5000-8000.
The preparation method that sun-proof used for water color ink is red, the method comprises the following steps:
(1) the red 5-8 weight part of sun-proof, polyvinyl alcohol 11-18 weight part, dihydroxyphenyl propane bisglycidyl ether 5-11 weight part, diamine propyl group polydimethylsiloxane 4-8 weight part, barium titanate 2-3 weight part, octamethylcyclotetrasiloxane 1-3 weight part, ammonium persulphate 1-2 weight part, Polyglycolic acid fibre 1-2 weight part, Polycarbosilane 0-1 weight part and N-BUTYL ACETATE 0-1 weight part is taken, by clarifixator at 55-65 DEG C, mixing 0.5-1 hour
(2) ionized water 20-25 weight part, amide modifications hydrogenated castor oil 4-7 weight part, calcium carbonate 4-7 weight part and magnesium oxide 3-5 weight part is added, add in stirrer, stir 2-4 hour, in vacuum defoamation machine, deaeration 1 hour, obtains sun-proof used for water color ink red.
Described in step (2), stir speed (S.S.) is 800-950 rev/min.
Compared with prior art, its beneficial effect is in the present invention:
(1) sun-proof used for water color ink that obtains of the present invention is red, by adding, sun-proof is red, deionized water, polyvinyl alcohol, dihydroxyphenyl propane bisglycidyl ether, diamine propyl group polydimethylsiloxane, amide modifications hydrogenated castor oil, calcium carbonate, magnesium oxide, barium titanate, octamethylcyclotetrasiloxane, ammonium persulphate and Polyglycolic acid fibre, obtained sun-proof used for water color ink is red has good tack and homogeneity, has good result of use.
(2) sun-proof used for water color ink that obtains of the present invention is red has satisfactory stability, and color is lasting.
(3) sun-proof used for water color ink of the present invention is red, and its preparation method is simple, is easy to suitability for industrialized production.
Embodiment
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
(1) take the red 5kg of sun-proof, molecular-weight average be 5000 polyvinyl alcohol 11kg, dihydroxyphenyl propane bisglycidyl ether 5kg, diamine propyl group polydimethylsiloxane 4kg, barium titanate 2kg, octamethylcyclotetrasiloxane 1kg, ammonium persulphate 1kg, Polyglycolic acid fibre 1kg, Polycarbosilane 1kg and N-BUTYL ACETATE 1kg, by clarifixator at 55 DEG C, mix 0.5 hour
(2) add ionized water 20kg, amide modifications hydrogenated castor oil 4kg, calcium carbonate 4kg and magnesium oxide 3kg, add in stirrer, stir 2 hours with 800 revs/min, in vacuum defoamation machine, deaeration 1 hour, obtains sun-proof used for water color ink red.
The performance test results obtaining sun-proof used for water color ink red is as shown in table 1.
Embodiment 2
(1) take the red 5kg of sun-proof, molecular-weight average be 5000 polyvinyl alcohol 11kg, dihydroxyphenyl propane bisglycidyl ether 5kg, diamine propyl group polydimethylsiloxane 4kg, barium titanate 2kg, octamethylcyclotetrasiloxane 1kg, ammonium persulphate 1kg and Polyglycolic acid fibre 1kg, by clarifixator at 55 DEG C, mix 0.5 hour
(2) add ionized water 20kg, amide modifications hydrogenated castor oil 4kg, calcium carbonate 4kg and magnesium oxide 3kg, add in stirrer, stir 2 hours with 800 revs/min, in vacuum defoamation machine, deaeration 1 hour, obtains sun-proof used for water color ink red.
The performance test results obtaining sun-proof used for water color ink red is as shown in table 1.
Embodiment 3
(1) take the red 8kg of sun-proof, molecular-weight average be 8000 polyvinyl alcohol 18kg, dihydroxyphenyl propane bisglycidyl ether 11kg, diamine propyl group polydimethylsiloxane 8kg, barium titanate 3kg, octamethylcyclotetrasiloxane 3kg, ammonium persulphate 2kg, Polyglycolic acid fibre 2kg, Polycarbosilane 1kg and N-BUTYL ACETATE 1kg, by clarifixator at 65 DEG C, mix 1 hour
(2) add ionized water 25kg, amide modifications hydrogenated castor oil 7kg, calcium carbonate 7kg and magnesium oxide 5kg, add in stirrer, stir 4 hours with 950 revs/min, in vacuum defoamation machine, deaeration 1 hour, obtains sun-proof used for water color ink red.
The performance test results obtaining sun-proof used for water color ink red is as shown in table 1.
Embodiment 4
(1) take the red 8kg of sun-proof, molecular-weight average be 8000 polyvinyl alcohol 18kg, dihydroxyphenyl propane bisglycidyl ether 11kg, diamine propyl group polydimethylsiloxane 4kg, barium titanate 3kg, octamethylcyclotetrasiloxane 3kg, ammonium persulphate 2kg, Polyglycolic acid fibre 2kg, Polycarbosilane 1kg and N-BUTYL ACETATE 1kg, by clarifixator at 65 DEG C, mix 1 hour
(2) add ionized water 25kg, amide modifications hydrogenated castor oil 7kg, calcium carbonate 7kg and magnesium oxide 5kg, add in stirrer, stir 4 hours with 950 revs/min, in vacuum defoamation machine, deaeration 1 hour, obtains sun-proof used for water color ink red.
The performance test results obtaining sun-proof used for water color ink red is as shown in table 1.
Embodiment 5
(1) take the red 6kg of sun-proof, molecular-weight average be 7000 polyvinyl alcohol 14kg, dihydroxyphenyl propane bisglycidyl ether 8kg, diamine propyl group polydimethylsiloxane 6kg, barium titanate 2kg, octamethylcyclotetrasiloxane 2kg, ammonium persulphate 1kg, Polyglycolic acid fibre 1kg, Polycarbosilane 1kg and N-BUTYL ACETATE 1kg, by clarifixator at 60 DEG C, mix 1 hour
(2) add ionized water 22kg, amide modifications hydrogenated castor oil 5kg, calcium carbonate 5kg and magnesium oxide 4kg, add in stirrer, stir 3 hours with 850 revs/min, in vacuum defoamation machine, deaeration 1 hour, obtains sun-proof used for water color ink red.
The performance test results obtaining sun-proof used for water color ink red is as shown in table 1.
Comparative example 1
(1) take the red 8kg of sun-proof, molecular-weight average be 8000 polyvinyl alcohol 18kg, dihydroxyphenyl propane bisglycidyl ether 11kg, barium titanate 3kg, octamethylcyclotetrasiloxane 3kg, ammonium persulphate 2kg, Polyglycolic acid fibre 2kg, Polycarbosilane 1kg and N-BUTYL ACETATE 1kg, by clarifixator at 65 DEG C, mix 1 hour
(2) add ionized water 25kg, amide modifications hydrogenated castor oil 7kg, calcium carbonate 7kg and magnesium oxide 5kg, add in stirrer, stir 4 hours with 950 revs/min, in vacuum defoamation machine, deaeration 1 hour, obtains sun-proof used for water color ink red.
The performance test results obtaining sun-proof used for water color ink red is as shown in table 1.
Comparative example 2
(1) take the red 8kg of sun-proof, molecular-weight average be 8000 polyvinyl alcohol 18kg, dihydroxyphenyl propane bisglycidyl ether 11kg, diamine propyl group polydimethylsiloxane 8kg, barium titanate 3kg, octamethylcyclotetrasiloxane 3kg, ammonium persulphate 2kg, Polyglycolic acid fibre 2kg, Polycarbosilane 1kg and N-BUTYL ACETATE 1kg, by clarifixator at 65 DEG C, mix 1 hour
(2) add ionized water 25kg, calcium carbonate 7kg and magnesium oxide 5kg, add in stirrer, stir 4 hours with 950 revs/min, in vacuum defoamation machine, deaeration 1 hour, obtains sun-proof used for water color ink red.
The performance test results obtaining sun-proof used for water color ink red is as shown in table 1.
Comparative example 3
(1) take the red 8kg of sun-proof, molecular-weight average be 8000 polyvinyl alcohol 18kg, dihydroxyphenyl propane bisglycidyl ether 11kg, diamine propyl group polydimethylsiloxane 8kg, barium titanate 3kg, octamethylcyclotetrasiloxane 3kg, ammonium persulphate 2kg, Polycarbosilane 1kg and N-BUTYL ACETATE 1kg, by clarifixator at 65 DEG C, mix 1 hour
(2) add ionized water 25kg, amide modifications hydrogenated castor oil 7kg, calcium carbonate 7kg and magnesium oxide 5kg, add in stirrer, stir 4 hours with 950 revs/min, in vacuum defoamation machine, deaeration 1 hour, obtains sun-proof used for water color ink red.
The performance test results obtaining sun-proof used for water color ink red is as shown in table 1.
Table 1
The invention is not restricted to embodiment here, those skilled in the art, according to announcement of the present invention, do not depart from improvement that scope makes and amendment all should within protection scope of the present invention.
Claims (6)
1. a sun-proof used for water color ink is red, it is characterized in that, is made up of the component comprising following weight part:
The red 5-8 part of sun-proof,
Deionized water 20-25 part,
Polyvinyl alcohol 11-18 part,
Dihydroxyphenyl propane bisglycidyl ether 5-11 part,
Diamine propyl group polydimethylsiloxane 4-8 part,
Amide modifications hydrogenated castor oil 4-7 part,
Calcium carbonate 4-7 part,
Magnesium oxide 3-5 part,
Barium titanate 2-3 part,
Octamethylcyclotetrasiloxane 1-3 part,
Ammonium persulphate 1-2 part,
Polyglycolic acid fibre 1-2 part.
2. sun-proof used for water color ink is red according to claim 1, it is characterized in that, described component also comprises Polycarbosilane 0-1 weight part.
3. sun-proof used for water color ink is red according to claim 1, it is characterized in that, described component also comprises N-BUTYL ACETATE 0-1 weight part.
4. sun-proof used for water color ink is red according to claim 1, it is characterized in that, the molecular-weight average of described polyvinyl alcohol is 5000-8000.
5. the preparation method that sun-proof used for water color ink is red, is characterized in that, the method comprises the following steps:
(1) the red 5-8 weight part of sun-proof, polyvinyl alcohol 11-18 weight part, dihydroxyphenyl propane bisglycidyl ether 5-11 weight part, diamine propyl group polydimethylsiloxane 4-8 weight part, barium titanate 2-3 weight part, octamethylcyclotetrasiloxane 1-3 weight part, ammonium persulphate 1-2 weight part, Polyglycolic acid fibre 1-2 weight part, Polycarbosilane 0-1 weight part and N-BUTYL ACETATE 0-1 weight part is taken, by clarifixator at 55-65 DEG C, mixing 0.5-1 hour
(2) ionized water 20-25 weight part, amide modifications hydrogenated castor oil 4-7 weight part, calcium carbonate 4-7 weight part and magnesium oxide 3-5 weight part is added, add in stirrer, stir 2-4 hour, in vacuum defoamation machine, deaeration 1 hour, obtains sun-proof used for water color ink red.
6. the preparation method that sun-proof used for water color ink according to claim 5 is red, is characterized in that, described in step (2), stir speed (S.S.) is 800-950 rev/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510551921.1A CN105062192A (en) | 2015-09-01 | 2015-09-01 | Fast red for water-based ink and preparation method thereof |
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| CN201510551921.1A CN105062192A (en) | 2015-09-01 | 2015-09-01 | Fast red for water-based ink and preparation method thereof |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1451698A (en) * | 2002-04-17 | 2003-10-29 | 幸伟 | Water quick-drying ink for ink-jet printer |
| CN102358810A (en) * | 2011-09-14 | 2012-02-22 | 哈尔滨大东方卷烟材料科技开发有限责任公司 | Environment-friendly type water-based intaglio ink used for package printing and preparation method thereof |
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- 2015-09-01 CN CN201510551921.1A patent/CN105062192A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1451698A (en) * | 2002-04-17 | 2003-10-29 | 幸伟 | Water quick-drying ink for ink-jet printer |
| CN102358810A (en) * | 2011-09-14 | 2012-02-22 | 哈尔滨大东方卷烟材料科技开发有限责任公司 | Environment-friendly type water-based intaglio ink used for package printing and preparation method thereof |
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Application publication date: 20151118 |
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