CN105055294A - Slurry soaking type facial mask manufacturing method - Google Patents
Slurry soaking type facial mask manufacturing method Download PDFInfo
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- CN105055294A CN105055294A CN201510514872.4A CN201510514872A CN105055294A CN 105055294 A CN105055294 A CN 105055294A CN 201510514872 A CN201510514872 A CN 201510514872A CN 105055294 A CN105055294 A CN 105055294A
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Abstract
The invention discloses a slurry soaking type facial mask manufacturing method. The method is characterized by comprising the steps that 1, materials are prepared, wherein the raw materials of water, glycerol, butanediol, crylic acid(ester)/ isodecanoic vinyl ester cross-linked polymer, xanthan gum, sclerotium gum, a skin conditioning agent, volcanic mud, butanediol, methylparaben, a pH conditioning agent and a corrosion remover are weighed according to the components; 2, the raw materials are preprocessed, wherein a phase A, a phase B and a phase C are prepared; 3, a reaction is performed in a reaction kettle, wherein after being heated, a phase A solution is added into the phase B, the temperature is decreased to be 70 DEG C and then the phase C solution and the pH conditioning agent are added in sequence; when the temperature is decreased to be smaller than 45 DEG C, an air bleeding valve is turned on, the corrosion remover is added into the reaction kettle, and stirring is performed to obtain a mixing solution; 4, discharging is performed; 5, the facial mask is obtained. According to the slurry soaking type facial mask manufacturing method, volcanic mud is used as main components of the facial mask, the ingredients of the volcanic mud are sufficiently released on the basis of the manufacturing method, the loss rate is low, and the production cost is greatly lowered.
Description
Technical field
The invention belongs to technical field of skin care, relate to a kind of mud dipping formula mask sheet compound method.
Background technology
Along with the kind of facial treatment mask product is on the market original more, the facial film that consumers prepares in natural material.Relative to traditional natural pureed facial film technique, general be all add on the basis of common cream pack there is efficacy effect plant extract, silica flour or titanium dioxide to reach the effect of moisturizing control wet goods, or the form with paste after with an organic solvent mixing with natural mud acts on skin, when adopting this kind of technique, the proportion of goods damageds are high, the effective ingredient of natural mud fails fully to discharge, and color easily remains on skin, larger to skin irritation.In addition, the cream pack made also not easily is preserved.
Summary of the invention
For overcoming the defect of prior art, the object of the present invention is to provide a kind of mud dipping formula mask sheet compound method, this compound method is simply efficient, the skin care ingredient of volcanic mud fully can be discharged; Further, make the form of mask sheet, convenient and swift during use, easily clear up.
The technical solution adopted in the present invention is as follows for achieving the above object:
A kind of mud dipping formula mask sheet compound method, is characterized in that comprising the following steps:
1) get the raw materials ready: take following raw material by weight percentage respectively:
The percentage by weight sum of above-mentioned raw materials is 100%;
2) pretreatment of raw material:
A) preparing A phase: water is added vacuum response still, is make water form whirlpool under the condition of 500rpm at rotating speed; Successively by acrylic acid (ester) class/isodecyl vinyl acetate cross linked polymer, xanthan gum and Scleroglucan are spilled in whirlpool; Finally glycerol, butanediol and skin conditioner are added in vacuum response still; After interpolation, arranging rotating speed is that 25rpm carries out homogenizing process, and heating makes solution warms to 75 ~ 85 DEG C, is then incubated 20min, obtains A phase;
B) prepare B phase: be ground to more than 3000 orders by after volcanic mud drying, then sieve, obtain B phase;
Volcanic mud in the present invention contains mineral, trace element and aminoacid, by volcanic mud is ground to more than 3000 orders, be conducive to the mineral in volcanic mud, trace element and aminoacid to be discharged to greatest extent, so in process the percentage by weight of volcanic mud in raw material components is defined as 10% ~ 15%, good effect can be reached by synergism with other compositions, lower the loss of volcanic mud, reduce production cost;
C) C phase is prepared: by butanediol and methyl hydroxybenzoate mixing, be heated to 60 ~ 70 DEG C, make it to dissolve completely and mix homogeneously, obtain C phase;
3) react in a kettle.:
I) A phase is heated to 85 DEG C in a kettle., B is added to reactor; Then setting reactor rotating speed is that 3600rpm carries out homogenizing process 10min, is incubated 20min after completing, and obtains the mixed liquor of A phase and B phase;
II) by step I) obtain A phase and be reduced to 70 DEG C with the temperature of the mixed liquor of B phase, then add C phase and pH adjusting agent successively in a kettle.; Open vacuum pump, set vacuum pressure as-0.07 ~-0.08Mpa, continue cooling simultaneously, obtain basal liquid;
III) when step II) in obtain basal liquid temperature when being reduced to below 45 DEG C, open the gas bleeder valve of reactor, add antiseptic in a kettle., stir 15min, make it fully mix, obtain mixed liquor;
4) discharging:
By step 3) in the mixed liquor that obtains take out from reactor, carry out successively drying, sampling, detection qualified after, cross more than sieving to 200 order, obtain mask matrix;
The present invention is by being prepared into solid-state mask matrix, and it is not easy to go bad, and resistance in storage, bulk transport is convenient, and use solid-state mask matrix can be processed as other forms of mask product further, processing conditions is flexible.
5) mask sheet is prepared:
By step 4) in the mask matrix that obtains with water dissolution, forming surface membrane matrix solution, wherein the weight of water is 3 ~ 6 times of mask matrix weight; Be soaked in completely in mask matrix solution as carrier using non-woven fabrics facial film, obtain mask sheet.
Using mask sheet as carrier in the present invention, simple and convenient during use, be easy to cleaning.
As the preferred scheme of one of the present invention, in step 1) in, described skin conditioner comprises betanin, trehalose and allantoin; Wherein, the total weight percent that betanin accounts for all raw materials is 1.7 ~ 2.2%, and the total weight percent that trehalose accounts for all raw materials is 0.42 ~ 0.6%, and the total weight percent that allantoin accounts for all raw materials is 0.1 ~ 0.2%.
The allantoin that the present invention adopts has Promote cell's growth, accelerating wound, the physiological functions such as horny layer softening albumen, and skin can be made to keep moisture content, moist and soft.
As the preferred scheme of one of the present invention, in step 1) in, described antiseptic comprises imidazolidinyl urea and phenoxyethanol; Wherein, the total weight percent that imidazolidinyl urea accounts for all raw materials is 0.2 ~ 0.5%, and the total weight percent that phenoxyethanol accounts for all raw materials is 0.1 ~ 0.5%.
As the preferred scheme of one of the present invention, in step 1) in, take following raw material by weight percentage respectively:
As the preferred scheme of one of the present invention, in step 1) in described skin conditioner, the total weight percent that betanin accounts for all raw materials is 2%, and the total weight percent that trehalose accounts for all raw materials is 0.5%, and the total weight percent that allantoin accounts for all raw materials is 0.2%.
As the preferred scheme of one of the present invention, in step 1) in described antiseptic, the total weight percent that imidazolidinyl urea accounts for all raw materials is 0.25%, and the total weight percent that phenoxyethanol accounts for all raw materials is 0.2%.
As the preferred scheme of one of the present invention, in step 1) in, described pH adjusting agent is triethanolamine.
Water described in the present invention is deionized water or distilled water.
Beneficial effect of the present invention is:
1, the present invention uses volcanic mud as the main component of mask sheet, and its compound method makes the composition of volcanic mud fully discharge, and the proportion of goods damageds are low, greatly lower production cost;
2, intermediate product of the present invention is solid-state mask matrix, and it is not easy to go bad, and resistance in storage, bulk transport is convenient, and use solid-state mask matrix can be processed as other forms of mask product further, processing conditions is flexible;
3, the present invention is with the form of mask sheet, convenient and swift during use, easily clears up.
Detailed description of the invention
Below in conjunction with concrete embodiment, the present invention is described in further detail:
Embodiment 1:
A kind of mud dipping formula mask sheet compound method, is characterized in that comprising the following steps:
1) get the raw materials ready: take following raw material by weight percentage respectively by table 1:
Table 1
2) pretreatment of raw material:
A) preparing A phase: water is added vacuum response still, is make water form whirlpool under the condition of 500rpm at rotating speed; Successively by acrylic acid (ester) class/isodecyl vinyl acetate cross linked polymer, xanthan gum and Scleroglucan are spilled in whirlpool; Finally glycerol, butanediol and skin conditioner are added in vacuum response still; After interpolation, arranging rotating speed is that 25rpm carries out homogenizing process, and heating makes solution warms to 75 DEG C, is then incubated 20min, obtains A phase;
B) prepare B phase: be ground to more than 3000 orders by after volcanic mud drying, then sieve, obtain B phase;
C) C phase is prepared: by butanediol and methyl hydroxybenzoate mixing, be heated to 60 DEG C, make it to dissolve completely and mix homogeneously, obtain C phase;
3) react in a kettle.:
I) A phase is heated to 85 DEG C in a kettle., B is added to reactor; Then setting reactor rotating speed is that 3600rpm carries out homogenizing process 10min, is incubated 20min after completing, and obtains the mixed liquor of A phase and B phase;
II) by step I) obtain A phase and be reduced to 70 DEG C with the temperature of the mixed liquor of B phase, then add C phase solution and pH adjusting agent successively in a kettle.; Open vacuum pump, setting vacuum pressure is-0.08Mpa, continues cooling simultaneously, obtains basal liquid;
III) work as step II) in obtain basal liquid temperature be reduced to less than 45 DEG C, open the gas bleeder valve of reactor, add antiseptic in a kettle., stir 15min, make it fully mix, obtain mixed liquor;
4) discharging:
By step 3) in the mixed liquor that obtains take out from reactor, carry out successively drying, sampling, detection qualified after, cross more than sieving to 200 order, obtain mask matrix;
5) mask sheet is prepared:
By step 4) in the mask matrix that obtains with water dissolution, forming surface membrane matrix solution, wherein the weight of water is 4 times of mask matrix weight; Be soaked in completely in mask matrix solution as carrier using non-woven fabrics facial film, obtain mask sheet.
Embodiment 2:
A kind of mud dipping formula mask sheet compound method, is characterized in that comprising the following steps:
1) get the raw materials ready:
Following raw material is by weight percentage taken respectively by table 2:
Table 2
Other preparation processes are identical with embodiment 1.
Embodiment 3:
A kind of mud dipping formula mask sheet compound method, is characterized in that comprising the following steps:
1) get the raw materials ready:
Following raw material is by weight percentage taken respectively by table 3:
Table 3
2) pretreatment of raw material:
A) preparing A phase: water is added vacuum response still, is make water form whirlpool under the condition of 500rpm at rotating speed; Successively by acrylic acid (ester) class/isodecyl vinyl acetate cross linked polymer, xanthan gum and Scleroglucan are spilled in whirlpool; Finally glycerol, butanediol and skin conditioner are added in vacuum response still; After interpolation, arranging rotating speed is that 25rpm carries out homogenizing process, and heating makes solution warms to 85 DEG C, is then incubated 20min, obtains A phase;
B) prepare B phase: be ground to more than 3000 orders by after volcanic mud drying, then sieve, obtain B phase;
C) C phase is prepared: by butanediol and methyl hydroxybenzoate mixing, be heated to 70 DEG C, make it to dissolve completely and mix homogeneously, obtain C phase;
3) react in a kettle.:
I) A phase is heated to 85 DEG C in a kettle., B is added to reactor; Then setting reactor rotating speed is that 3600rpm carries out homogenizing process 10min, is incubated 20min after completing, and obtains the mixed liquor of A phase and B phase;
II) by step I) obtain A phase and be reduced to 70 DEG C with the temperature of the mixed liquor of B phase, then add C phase solution and pH adjusting agent successively in a kettle.; Open vacuum pump, setting vacuum pressure is-0.08Mpa, continues cooling simultaneously, obtains basal liquid;
III) work as step II) in obtain basal liquid temperature be reduced to less than 45 DEG C, open the gas bleeder valve of reactor, add antiseptic in a kettle., stir 15min, make it fully mix, obtain mixed liquor;
4) discharging:
By step 3) in the mixed liquor that obtains take out from reactor, carry out successively drying, sampling, detection qualified after, cross more than sieving to 200 order, obtain mask matrix;
5) mask sheet is prepared:
With step 4) in the mask matrix that obtains with water dissolution, forming surface membrane matrix solution, wherein the weight of water is 6 times of mask matrix weight; Be soaked in completely in mask matrix solution as carrier using non-woven fabrics facial film, obtain mask sheet.
For a person skilled in the art, according to technical scheme described above and design, other various corresponding change and distortion can be made, and all these change and distortion all should belong within the protection domain of the claims in the present invention.
Claims (7)
1. a mud dipping formula mask sheet compound method, is characterized in that comprising the following steps:
1) get the raw materials ready: take following raw material by weight percentage respectively:
2) pretreatment of raw material:
A) preparing A phase: water is added vacuum response still, is make water form whirlpool under the condition of 500rpm at rotating speed; Successively by acrylic acid (ester) class/isodecyl vinyl acetate cross linked polymer, xanthan gum and Scleroglucan are spilled in whirlpool; Finally glycerol, butanediol and skin conditioner are added in vacuum response still; After interpolation, arranging rotating speed is that 25rpm carries out homogenizing process, and heating makes solution warms to 75 ~ 85 DEG C, is then incubated 20min, obtains A phase;
B) prepare B phase: be ground to more than 3000 orders by after volcanic mud drying, then sieve, obtain B phase;
C) C phase is prepared: by butanediol and methyl hydroxybenzoate mixing, be heated to 60 ~ 70 DEG C, make it to dissolve completely and mix homogeneously, obtain C phase;
3) react in a kettle.:
I) A phase is heated to 85 DEG C in a kettle., B is added to reactor; Then setting reactor rotating speed is that 3600rpm carries out homogenizing process 10min, is incubated 20min after completing, and obtains the mixed liquor of A phase and B phase;
II) by step I) obtain A phase and be reduced to 70 DEG C with the temperature of the mixed liquor of B phase, then add C phase and pH adjusting agent successively in a kettle.; Open vacuum pump, set vacuum pressure as-0.07 ~-0.08Mpa, continue cooling simultaneously, obtain basal liquid;
III) when step II) in obtain basal liquid temperature when being reduced to below 45 DEG C, open the gas bleeder valve of reactor, add antiseptic in a kettle., stir 15min, make it fully mix, obtain mixed liquor;
4) discharging:
By step 3) in the mixed liquor that obtains take out from reactor, carry out successively drying, sampling, detection qualified after, cross more than sieving to 200 order, obtain mask matrix;
5) mask sheet is prepared:
By step 4) in the mask matrix that obtains with water dissolution, forming surface membrane matrix solution, wherein the weight of water is 3 ~ 6 times of mask matrix weight; Be soaked in completely in mask matrix solution as carrier using non-woven fabrics facial film, obtain mask sheet.
2. mud dipping formula mask sheet compound method according to claim 1, is characterized in that: in step 1) in, described skin conditioner comprises betanin, trehalose and allantoin; Wherein, the total weight percent that betanin accounts for all raw materials is 1.7 ~ 2.2%, and the total weight percent that trehalose accounts for all raw materials is 0.42 ~ 0.6%, and the total weight percent that allantoin accounts for all raw materials is 0.1 ~ 0.2%.
3. mud dipping formula mask sheet compound method according to claim 1, is characterized in that: in step 1) in, described antiseptic comprises imidazolidinyl urea and phenoxyethanol; Wherein, the total weight percent that imidazolidinyl urea accounts for all raw materials is 0.2 ~ 0.5%, and the total weight percent that phenoxyethanol accounts for all raw materials is 0.1 ~ 0.5%.
4. mud dipping formula mask sheet compound method according to claim 1, is characterized in that: in step 1) in, take following raw material by weight percentage respectively:
5. mud dipping formula mask sheet compound method according to claim 4, it is characterized in that: in step 1) in described skin conditioner, the total weight percent that betanin accounts for all raw materials is 2%, the total weight percent that trehalose accounts for all raw materials is 0.5%, and the total weight percent that allantoin accounts for all raw materials is 0.2%.
6. mud dipping formula mask sheet compound method according to claim 4, it is characterized in that: in step 1) in described antiseptic, the total weight percent that imidazolidinyl urea accounts for all raw materials is 0.25%, and the total weight percent that phenoxyethanol accounts for all raw materials is 0.2%.
7., according to the arbitrary described mud dipping formula mask sheet compound method of claim 1 and 4, it is characterized in that: in step 1) in, described pH adjusting agent is triethanolamine.
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| CN201510514872.4A CN105055294A (en) | 2015-08-20 | 2015-08-20 | Slurry soaking type facial mask manufacturing method |
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| CN201510514872.4A CN105055294A (en) | 2015-08-20 | 2015-08-20 | Slurry soaking type facial mask manufacturing method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107789303A (en) * | 2016-08-30 | 2018-03-13 | 陈磊 | A kind of aerolite facial mask and its manufacture craft |
| CN111329770A (en) * | 2018-12-18 | 2020-06-26 | 抚顺金达莱生物科技有限公司 | Deep-sea volcano sulfur paste mask cream and preparation method thereof |
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| KR20130028192A (en) * | 2011-09-09 | 2013-03-19 | 주식회사 금황제지 | Yellow soil, mineral compound mixed korean paper loess therapy massage face mask sheet pack |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR20130028192A (en) * | 2011-09-09 | 2013-03-19 | 주식회사 금황제지 | Yellow soil, mineral compound mixed korean paper loess therapy massage face mask sheet pack |
| CN104352371A (en) * | 2014-10-11 | 2015-02-18 | 宁佳伟 | Skin-whitening, anti-ageing and anti-freckle facial mask liquid and preparation method thereof, as well as facial mask |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107789303A (en) * | 2016-08-30 | 2018-03-13 | 陈磊 | A kind of aerolite facial mask and its manufacture craft |
| CN111329770A (en) * | 2018-12-18 | 2020-06-26 | 抚顺金达莱生物科技有限公司 | Deep-sea volcano sulfur paste mask cream and preparation method thereof |
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Application publication date: 20151118 |
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