CN105010925B - A kind of preparation method of antioxidant activity royal jelly freeze-dried powder - Google Patents
A kind of preparation method of antioxidant activity royal jelly freeze-dried powder Download PDFInfo
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- CN105010925B CN105010925B CN201510467541.XA CN201510467541A CN105010925B CN 105010925 B CN105010925 B CN 105010925B CN 201510467541 A CN201510467541 A CN 201510467541A CN 105010925 B CN105010925 B CN 105010925B
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- dried powder
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- 239000000843 powder Substances 0.000 title claims abstract description 78
- 230000003078 antioxidant effect Effects 0.000 title claims abstract description 58
- 229940109850 royal jelly Drugs 0.000 title claims abstract description 56
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 40
- 244000061456 Solanum tuberosum Species 0.000 claims abstract description 38
- 235000002595 Solanum tuberosum Nutrition 0.000 claims abstract description 38
- 235000020183 skimmed milk Nutrition 0.000 claims abstract description 20
- 229920002472 Starch Polymers 0.000 claims abstract description 19
- 235000019698 starch Nutrition 0.000 claims abstract description 19
- 230000000694 effects Effects 0.000 claims abstract description 11
- 238000009835 boiling Methods 0.000 claims abstract description 10
- 235000013336 milk Nutrition 0.000 claims abstract description 10
- 239000008267 milk Substances 0.000 claims abstract description 10
- 210000004080 milk Anatomy 0.000 claims abstract description 10
- 238000005238 degreasing Methods 0.000 claims abstract description 9
- 239000002775 capsule Substances 0.000 claims abstract description 7
- 238000001291 vacuum drying Methods 0.000 claims abstract description 7
- 238000007710 freezing Methods 0.000 claims description 15
- 230000008014 freezing Effects 0.000 claims description 15
- 230000009194 climbing Effects 0.000 claims description 12
- 238000004108 freeze drying Methods 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 7
- 238000004140 cleaning Methods 0.000 claims description 6
- 238000009928 pasteurization Methods 0.000 claims description 6
- 238000004321 preservation Methods 0.000 claims description 6
- 238000010411 cooking Methods 0.000 claims description 2
- 238000003860 storage Methods 0.000 claims description 2
- 238000009777 vacuum freeze-drying Methods 0.000 claims description 2
- 238000001704 evaporation Methods 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 235000006708 antioxidants Nutrition 0.000 description 30
- 238000001035 drying Methods 0.000 description 4
- 238000004925 denaturation Methods 0.000 description 3
- 230000036425 denaturation Effects 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000013049 sediment Substances 0.000 description 3
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 210000000697 sensory organ Anatomy 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 229920000881 Modified starch Polymers 0.000 description 1
- 239000004368 Modified starch Substances 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 241000209140 Triticum Species 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000002929 anti-fatigue Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 238000005213 imbibition Methods 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Medicinal Preparation (AREA)
- Jellies, Jams, And Syrups (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention discloses a kind of preparation methods of antioxidant activity royal jelly freeze-dried powder, belong to royal jelly activity freeze-dried powder preparing technical field, and technical points include the following steps：(1) after active fresh royal jelly cryogenic vacuum being lyophilized, it is for use to crush stored frozen；(2) fresh milk is sterilized, powder is lyophilized into cryogenic vacuum, then by centrifugal degreasing, then crush, it is spare；(3) it will smash to pieces, dry after Xia Bodi antioxidant potato boilings, then the molecular structure of centrifugal disruption Xia Bodi antioxidant potatos again, finally crush and filter and is spare；(4) by active royal jelly freeze-dried powder skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches, after mixing is mixed thoroughly in low-temperature vacuum drying environment, film-making or it is filled into capsule；The present invention is intended to provide a kind of stability is good, the preparation method of long shelf-life and the antioxidant activity royal jelly freeze-dried powder of craft science；Preparation for royal jelly activity freeze-dried powder.
Description
Technical field
The present invention relates to a kind of preparation methods of royal jelly freeze-dried powder, more specifically more particularly to a kind of anti-oxidant work
The preparation method of property royal jelly freeze-dried powder.
Background technology
In traditional handicraft, use wheat, rice modified starch as active royal jelly freeze-dried powder auxiliary material.This technique system
Standby active royal jelly freeze-dried powder, haves the shortcomings that oxidizable, influences the qualification rate of active nutritional composition and sense organ, can not be long-term
Time keeps its nutrient substance.Moreover, this freeze-dried powder, condition of storing in a warehouse and edible conditions are harsh, under normal temperature condition,
It can cause within 180 days or so to become dark colour (yellowish-brown) by light colour, water imbibition is strong.
Invention content
It is an object of the invention in view of the above shortcomings of the prior art, provide a kind of good stability, long shelf-life and work
The preparation method of the antioxidant activity royal jelly freeze-dried powder of skill science, taste good.
The technical proposal of the invention is realized in this way：A kind of preparation method of antioxidant activity royal jelly freeze-dried powder, packet
Include following step：
(1) after active fresh royal jelly being lyophilized by cryogenic vacuum, 100~150 mesh is crushed to and obtain active royal jelly freeze-drying
Powder, stored frozen are for use；
(2) fresh milk is sterilized by freeze preservation with pasteurization, is lyophilized in -30 DEG C~-40 DEG C cryogenic vacuums
Cheng Fen, then by high speed freezing centrifuge degreasing, 100~150 mesh are then comminuted into, it is spare to obtain skim milk freeze-dried powder；
(3) it removes the peel after cleaning up Xia Bodi antioxidant potatos, is smashed to pieces after boiling, pass through 80 DEG C of water-baths liter film
Evaporator is dried, and then destroys the molecular structure of Xia Bodi antioxidant potatos by high speed freezing centrifuge again, finally
It crushes and filters, Xia Bodi antioxidant potato converted starches are made, it is spare；
(4) by active royal jelly freeze-dried powder skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches, -30
DEG C~-35 DEG C of low-temperature vacuum drying environment in be mixed evenly after, film-making or be filled into capsule；The activity royal jelly freeze-drying
The weight ratio of powder, skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches is 75~85：3~6：8~12.
In a kind of preparation method of above-mentioned antioxidant activity royal jelly freeze-dried powder, step (1) the cryogenic vacuum freeze-drying
For -30 DEG C~-40 DEG C low temperature of use；The temperature of the stored frozen is -18 DEG C.
In a kind of preparation method of above-mentioned antioxidant activity royal jelly freeze-dried powder, in step (3), the boiling is high pressure
Boiling, cooking pressure are 0.85~0.95Mpa.
In a kind of preparation method of above-mentioned antioxidant activity royal jelly freeze-dried powder, in step (3), the anti-oxidant horses of Xia Bodi
The time that bell potato passes through climbing film evaporator tubulation is 0.6~1 second.
In a kind of preparation method of above-mentioned antioxidant activity royal jelly freeze-dried powder, in step (3), high speed freezing centrifuge
Rotating speed be 26000~26500rpm.
In a kind of preparation method of above-mentioned antioxidant activity royal jelly freeze-dried powder, in step (3), the filtering mesh number is
80~100 mesh.
In a kind of preparation method of above-mentioned antioxidant activity royal jelly freeze-dried powder, in step (4), the activity royal jelly
The weight ratio of freeze-dried powder, skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches is 85：5：10.
After the present invention uses above-mentioned technique, it is lyophilized by Xia Bodi antioxidant potato converted starch combining skimmed milks
Powder.Both the stabilization that royal jelly nutritive active ingredient can have been protected prevents fresh royal jelly freeze-dried powder nutrition to be lost in.In 20 DEG C of temperature
Lower storage 180 days, sense organ is constant, the original light color state of color keep.Pure fragrant mouthfeel with milk again, reduces royal jelly
Uncomfortable mouthfeel caused by sour, puckery, peppery stimulation, non-oxidation water suction phenomenon, easy to maintain, instant edible, while carrying of conveniently going out,
Travelling is all suitable at home.Royal jelly activity freeze-dried powder prepared by this technique significantly reduces stored under refrigeration condition during logistics transportation,
Reduce transportation cost.
Meanwhile there are following beneficial functionals：
(1) immunity is improved, promotes sleep, slow down aging；
(2) auxiliary adjustment blood glucose, blood fat, blood pressure；
(3) antifatigue, radioresistance is anti-oxidant.
Specific implementation mode
With reference to specific embodiment, the present invention is described in further detail, but does not constitute to any of the present invention
Limitation.
A kind of preparation method of antioxidant activity royal jelly freeze-dried powder of the present invention, includes the following steps：
(1) after active fresh royal jelly being lyophilized by -30 DEG C~-40 DEG C cryogenic vacuums, being crushed to 100~150 mesh must be living
Property royal jelly freeze-dried powder, stored frozen is for use under -18 DEG C of environment；
(2) fresh milk is sterilized by freeze preservation with pasteurization, is lyophilized in -30 DEG C~-40 DEG C cryogenic vacuums
Cheng Fen, then by high speed freezing centrifuge degreasing, 100~150 mesh are then comminuted into, it is spare to obtain skim milk freeze-dried powder；
(3) it removes the peel after cleaning up Xia Bodi antioxidant potatos, is smash after boiling under the pressure of 0.85~0.95Mpa
It is broken, it is dried with climbing film evaporator by 80 DEG C of water-baths, in drying process, Xia Bodi antioxidant potatos are steamed by liter film
The time for sending out device tubulation is 0.6~1 second；Then the molecule of Xia Bodi antioxidant potatos is destroyed by high speed freezing centrifuge again
The rotating speed of structure, high speed freezing centrifuge is preferably 26000~26500rpm, finally crushes and filters, and filtering mesh number is
Converted starch is made in 80~100 mesh, spare；
(4) by active royal jelly freeze-dried powder skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches, -30
DEG C~-35 DEG C of low-temperature vacuum drying environment in be mixed evenly after, film-making or be filled into capsule；The activity royal jelly freeze-drying
The weight ratio of powder, skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches is 75~85：3~6：8~12, preferably
Weight ratio is 85：5：10.
Embodiment 1
(1) after active fresh royal jelly being lyophilized by -30 DEG C of cryogenic vacuums, 100 mesh is crushed to and obtain active royal jelly freeze-drying
Powder, stored frozen is for use under -18 DEG C of environment；
(2) fresh milk is sterilized by freeze preservation with pasteurization combination climbing film evaporator, it is true in -30 DEG C of low temperature
It is lyophilized into powder in the air, then by high speed freezing centrifuge degreasing, is then comminuted into 100 mesh, it is spare to obtain skim milk freeze-dried powder；
(3) it removes the peel after cleaning up Xia Bodi antioxidant potatos, is smashed to pieces after boiling under the pressure of 0.85Mpa, led to
It crosses 80 DEG C of water-baths to be dried with climbing film evaporator, in drying process, Xia Bodi antioxidant potatos pass through climbing film evaporator
The time of tubulation is 0.6 second；Then the molecular structure of Xia Bodi antioxidant potatos is destroyed by high speed freezing centrifuge again, it is high
The rotating speed of fast refrigerated centrifuge is preferably 26000rpm, finally crushes and filters, and filtering mesh number is 80 mesh, and denaturation is made and forms sediment
Powder, it is spare；
(4) by active royal jelly freeze-dried powder skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches, -30
After being mixed evenly in DEG C low-temperature vacuum drying environment, film-making or it is filled into capsule；The activity royal jelly freeze-dried powder, degreasing
The weight ratio of milk freeze-dried powder and Xia Bodi antioxidant potato converted starches is 75：3：8.
Embodiment 2
(1) after active fresh royal jelly being lyophilized by -35 DEG C of cryogenic vacuums, 120 mesh is crushed to and obtain active royal jelly freeze-drying
Powder, stored frozen is for use under -18 DEG C of environment；
(2) fresh milk is sterilized by freeze preservation with pasteurization combination climbing film evaporator, it is true in -35 DEG C of low temperature
It is lyophilized into powder in the air, then by high speed freezing centrifuge degreasing, is then comminuted into 120 mesh, it is spare to obtain skim milk freeze-dried powder；
(3) it is removed the peel after cleaning up Xia Bodi antioxidant potatos, smashs to pieces, pass through after boiling under the pressure of 0.9Mpa
80 DEG C of water-baths are dried with climbing film evaporator, and in drying process, Xia Bodi antioxidant potatos are arranged by climbing film evaporator
The time of pipe is 0.8 second；Then the molecular structure of Xia Bodi antioxidant potatos, high speed are destroyed by high speed freezing centrifuge again
The rotating speed of refrigerated centrifuge is preferably 26200rpm, finally crushes and filters, and filtering mesh number is 80 mesh, and denaturation is made and forms sediment
Powder, it is spare；
(4) by active royal jelly freeze-dried powder skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches, -32
After being mixed evenly in DEG C low-temperature vacuum drying environment, film-making or it is filled into capsule；The activity royal jelly freeze-dried powder, degreasing
The weight ratio of milk freeze-dried powder and Xia Bodi antioxidant potato converted starches is 85：5：10.
Embodiment 3
(1) after active fresh royal jelly being lyophilized by -40 DEG C of cryogenic vacuums, 150 mesh is crushed to and obtain active royal jelly freeze-drying
Powder, stored frozen is for use under -18 DEG C of environment；
(2) fresh milk is sterilized by freeze preservation with pasteurization combination climbing film evaporator, it is true in -40 DEG C of low temperature
It is lyophilized into powder in the air, then by high speed freezing centrifuge degreasing, is then comminuted into 150 mesh, it is spare to obtain skim milk freeze-dried powder；
(3) it removes the peel after cleaning up Xia Bodi antioxidant potatos, is smashed to pieces after boiling under the pressure of 0.95Mpa, led to
It crosses 80 DEG C of water-baths to be dried with climbing film evaporator, in drying process, Xia Bodi antioxidant potatos pass through climbing film evaporator
The time of tubulation is 1 second；Then the molecular structure of Xia Bodi antioxidant potatos, high speed are destroyed by high speed freezing centrifuge again
The rotating speed of refrigerated centrifuge is preferably 26500rpm, finally crushes and filters, and filtering mesh number is 100 mesh, and denaturation is made and forms sediment
Powder, it is spare；
(4) by active royal jelly freeze-dried powder skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches, -30
DEG C~-35 DEG C of low-temperature vacuum drying environment in be mixed evenly after, film-making or be filled into capsule；The activity royal jelly freeze-drying
The weight ratio of powder, skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches is 85：6：12.
Claims (5)
1. a kind of preparation method of antioxidant activity royal jelly freeze-dried powder, which is characterized in that include the following steps：
(1) after active fresh royal jelly being lyophilized by cryogenic vacuum, 100~150 mesh is crushed to and obtain active royal jelly freeze-dried powder, it is cold
It is for use to freeze storage；
(2) fresh milk is sterilized by freeze preservation with pasteurization, is lyophilized into -30 DEG C~-40 DEG C cryogenic vacuums
Powder, then by high speed freezing centrifuge degreasing, 100~150 mesh are then comminuted into, it is spare to obtain skim milk freeze-dried powder；
(3) it removes the peel after cleaning up Xia Bodi antioxidant potatos, is smashed to pieces after boiling, pass through 80 DEG C of water-bath climbing-film evaporations
Device is dried, and then destroys the molecular structure of Xia Bodi antioxidant potatos by high speed freezing centrifuge again, finally carries out
It crushes and filtering, obtained Xia Bodi antioxidant potato converted starches is spare；The boiling is autoclaving, and cooking pressure is
0.85~0.95Mpa；The time that Xia Bodi antioxidant potatos pass through climbing film evaporator tubulation is 0.6~1 second；
(4) by active royal jelly freeze-dried powder, skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches, at -30 DEG C
After being mixed evenly in~-35 DEG C of low-temperature vacuum drying environment, film-making or it is filled into capsule；The activity royal jelly freeze-drying
The weight ratio of powder, skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches is 75~85：3~6：8~12.
2. a kind of preparation method of antioxidant activity royal jelly freeze-dried powder according to claim 1, which is characterized in that step
(1) the cryogenic vacuum freeze-drying is -30 DEG C~-40 DEG C low temperature of use；The temperature of the stored frozen is -18 DEG C.
3. a kind of preparation method of antioxidant activity royal jelly freeze-dried powder according to claim 1, which is characterized in that step
(3) in, the rotating speed of high speed freezing centrifuge is 26000~26500rpm.
4. a kind of preparation method of antioxidant activity royal jelly freeze-dried powder according to claim 1, which is characterized in that step
(3) in, the filtering mesh number is 80~100 mesh.
5. a kind of preparation method of antioxidant activity royal jelly freeze-dried powder according to claim 1, which is characterized in that step
(4) in, it is described activity royal jelly freeze-dried powder, skim milk freeze-dried powder and Xia Bodi antioxidant potato converted starches weight ratio
It is 85：5：10.
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| CN201510467541.XA CN105010925B (en) | 2015-07-31 | 2015-07-31 | A kind of preparation method of antioxidant activity royal jelly freeze-dried powder |
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| CN201510467541.XA CN105010925B (en) | 2015-07-31 | 2015-07-31 | A kind of preparation method of antioxidant activity royal jelly freeze-dried powder |
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| CN105010925B true CN105010925B (en) | 2018-08-07 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1440758A (en) * | 2002-02-25 | 2003-09-10 | 宋玉华 | Bioactive powder of wild bee purple gold and its preparation method |
| CN1919335A (en) * | 2006-06-22 | 2007-02-28 | 上海健治一号高科技有限公司 | Albumen powder capsule |
| CN101248848A (en) * | 2007-02-02 | 2008-08-27 | M.食品株式会社 | Pelletization method for raw royal jelly |
| CN102125098A (en) * | 2010-12-31 | 2011-07-20 | 内蒙古伊利实业集团股份有限公司 | Liquid dairy product containing royal jelly and preparation method thereof |
| CN102150796A (en) * | 2011-02-22 | 2011-08-17 | 广州市华侨糖厂 | Method for producing potato flake with high dietary fiber content |
-
2015
- 2015-07-31 CN CN201510467541.XA patent/CN105010925B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1440758A (en) * | 2002-02-25 | 2003-09-10 | 宋玉华 | Bioactive powder of wild bee purple gold and its preparation method |
| CN1919335A (en) * | 2006-06-22 | 2007-02-28 | 上海健治一号高科技有限公司 | Albumen powder capsule |
| CN101248848A (en) * | 2007-02-02 | 2008-08-27 | M.食品株式会社 | Pelletization method for raw royal jelly |
| CN102125098A (en) * | 2010-12-31 | 2011-07-20 | 内蒙古伊利实业集团股份有限公司 | Liquid dairy product containing royal jelly and preparation method thereof |
| CN102150796A (en) * | 2011-02-22 | 2011-08-17 | 广州市华侨糖厂 | Method for producing potato flake with high dietary fiber content |
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