CN105614775A - Preparing method for freeze-dried waxberry buccal tablets - Google Patents
Preparing method for freeze-dried waxberry buccal tablets Download PDFInfo
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- CN105614775A CN105614775A CN201610113058.6A CN201610113058A CN105614775A CN 105614775 A CN105614775 A CN 105614775A CN 201610113058 A CN201610113058 A CN 201610113058A CN 105614775 A CN105614775 A CN 105614775A
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- waxberry
- myricae rubrae
- fructus myricae
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- 235000012851 Myrica pensylvanica Nutrition 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title claims abstract description 37
- 239000006189 buccal tablet Substances 0.000 title abstract description 10
- 230000018044 dehydration Effects 0.000 claims abstract description 21
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- 238000007710 freezing Methods 0.000 claims abstract description 13
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000009455 aseptic packaging Methods 0.000 claims abstract description 9
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 8
- 238000004108 freeze drying Methods 0.000 claims abstract description 8
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- 238000004519 manufacturing process Methods 0.000 claims description 24
- 238000010298 pulverizing process Methods 0.000 claims description 17
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- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical class O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 5
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- 239000004615 ingredient Substances 0.000 abstract description 2
- 208000005156 Dehydration Diseases 0.000 abstract 1
- 238000000498 ball milling Methods 0.000 abstract 1
- 238000000227 grinding Methods 0.000 abstract 1
- 238000004321 preservation Methods 0.000 abstract 1
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- 229940046011 buccal tablet Drugs 0.000 description 6
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- 230000008022 sublimation Effects 0.000 description 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
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- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
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- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 description 1
- 206010002660 Anoxia Diseases 0.000 description 1
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- 230000000996 additive effect Effects 0.000 description 1
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 1
- 230000007953 anoxia Effects 0.000 description 1
- 229930014669 anthocyanidin Natural products 0.000 description 1
- 150000001452 anthocyanidin derivatives Chemical class 0.000 description 1
- 235000008758 anthocyanidins Nutrition 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
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- 239000004310 lactic acid Substances 0.000 description 1
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- 230000000050 nutritive effect Effects 0.000 description 1
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- 239000002994 raw material Substances 0.000 description 1
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- Preparation Of Fruits And Vegetables (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a preparing method for freeze-dried waxberry buccal tablets. The preparing method comprises the steps that firstly, waxberry is steeped in saline with the concentration ranging from 3% to 5% for 10-15 min, then saline matter is washed away with clear water, and the waxberry is subjected to grading picking, drainage of moisture in the waxberry, cartoning freezing and the like for processing; freeze-dried waxberry is obtained through low-temperature freeze-drying dehydration treatment; the freeze-dried waxberry is subjected to ball milling grinding in a sealed room with the humidity ranging from 10% to 30% and the temperature ranging from 15 DEG C to 25 DEG C, the ground freeze-dried waxberry is screened with a 60-100-mesh screen, packaged for use, and then tableted in a sealed room with the humidity ranging from 10% to 30% and the temperature ranging from 15 DEG C to 25 DEG C, the tableted freeze-dried waxberry is subjected to physical coloring and aseptic packaging, and then the freeze-dried waxberry buccal tablets are obtained. The freeze-dried waxberry buccal tablets prepared through the preparing method are convenient to take, good in nutritional ingredient preservation degree, high in taking safety and convenient to transport and store.
Description
Technical field
The invention belongs to food processing technology field, particularly relate to the manufacture method of a kind of lyophilizing waxberry lozenge.
Background technology
Waxberry fruit is containing glucose, fructose, citric acid, malic acid, oxalic acid, lactic acid and waxiness etc.; Single glycoside containing anthocyanidin and a small amount of double; two glycoside again. Waxberry fruit is bright in colour, juice is many, sweet and sour palatability, being of high nutritive value, but exist and produce the shortcoming that the cycle in season is short, shelf-life durations is short, room temperature preserves and is usually no more than 2 days, transport extremely inconvenient, having had a strong impact on the popularization of Fructus Myricae rubrae product, and major part Fructus Myricae rubrae is made the form of preserved fruit, its local flavor, nutrition run off serious.
Freeze-dried fruit sheet is quick freezing, vacuum ice-like dehydration, save the outward appearance of original color, nutritional labeling and original material, and there is good rehydration, and without any additive, be desirable natural wholesome food, with preserved fruit the difference is that, freeze-dried fruit sheet can farthest preserve the nutritional labeling in fruit, and application prospect is good.
Chinese patent CN201310525130.2 discloses the processing technique of a kind of lyophilizing waxberry flesh, be by cleaned for fresh Fructus Myricae rubrae, sterilization, quick-freezing, vacuum lyophilization, discharging, sarcocarp is peeled off, packaging prepares, the Fructus Myricae rubrae produced is prone to utilize manually and sarcocarp is peeled off by other physical methods from pit, thus obtaining the raw material of Fructus Myricae rubrae fruit grain beverage. But, the product that this processing technique produces can not instant use, it is necessary to could eat through rehydration, inconvenient.
It is crisp that Chinese patent CN201410610919.2 discloses a kind of lyophilizing Fructus Myricae rubrae; described Fructus Myricae rubrae is crisp is quickly effectively kill the microorganism of Fructus Myricae rubrae inside and outside by superhigh temperature atmospheric steam instantaneous sterilizing method after red bayberry fresh fruit cleaning; reach sterilization functions; impregnate sugar liquid again and form layer protecting film, effectively solve the problem that external microbe is frangible to the secondary pollution of Fructus Myricae rubrae and finished product. Fructus Myricae rubrae after immersion cools down rapidly freezes, carry out vacuum lyophilization again, adopt low operating pressure (50 80Pa), relatively low sublimation temperature (50 DEG C 60 DEG C) carries out sublimation drying, it is dried in the frozen state, ice crystal rapid sublimation, shortens the sublimation drying time, adopts suitable desorption temperature (40 DEG C 50 DEG C) to make Fructus Myricae rubrae crisp. But destroying the nutritional labeling of Fructus Myricae rubrae in the manufacturing process that this Fructus Myricae rubrae is crisp, edibility is low.
Therefore be badly in need of a kind of instant, nutritional labeling preserves the Fructus Myricae rubrae instant food manufacture method that degree is good, to meet the market quality requirements for Fructus Myricae rubrae product.
Summary of the invention
For the defect existed in prior art, it is an object of the invention to provide the manufacture method of a kind of lyophilizing waxberry lozenge.
For reaching object above, the present invention adopts the technical scheme that:
A kind of manufacture method of lyophilizing waxberry lozenge, manufacture method includes:
Step S01, Fructus Myricae rubrae primary election: be immersed in by Fructus Myricae rubrae in the saline of 3%��5% and soak 10-15 minute, then wash away salt with clear water, select through graduation, drain the moisture in Fructus Myricae rubrae, and it is to be processed that vanning is freezing etc.; Saline soak is fresh-keeping degerming, simple.
Step S02, by step S01 process after Fructus Myricae rubrae through low-temperature freeze drying processed, obtain lyophilizing Fructus Myricae rubrae; Adopting vacuum lyophilization is after freezing containing Fructus Adinae, will keep freezing state, heat under vacuum conditions, make ice be sublimed into steam and discharge, thus deviating from moisture in Fructus Myricae rubrae to obtain the process of freeze-dried products. Owing to this process carries out under low-temp low-pressure, and moisture directly distils without liquid, and freeze-dried products can keep its natural colored and abnormal smells from the patient is basically unchanged, face shaping is basically unchanged, various nutritional labeling is basically unchanged, intrinsic material does not lose substantially.
Step S03, waxberry lozenge molding flow process: by lyophilizing Fructus Myricae rubrae humidity 10%��30%, temperature 15 DEG C��25 DEG C sealing room in ball mill pulverizing, sieve in 60��100 orders and package spare, tabletting in humidity 10%��30%, 15 DEG C��25 DEG C sealing rooms of temperature, obtains lyophilizing waxberry lozenge through physics then aseptic packaging of painting.
Further, in step S01, freezing temperature is 0 DEG C��4 DEG C.
Further, in step S02, the step of low-temperature freeze drying processed is:
Step a, lyophilizing Fructus Myricae rubrae are through slicing treatment;
Step b, pre-freeze to-40 DEG C that Fructus Myricae rubrae is cut into slices, dehydration in freeze-drier, complete dehydration to during lower than 5% moisture;
The pack of step c, dehydration final vacuum is standby, obtains lyophilizing Fructus Myricae rubrae.
Further, in step a, the thickness of section is 3mm��5mm.
Further, in step b, in freeze-drier, dehydration is: when 5Pa��10Pa, adopts the section of 1000W microwave treatment Fructus Myricae rubrae. Dehydration carries out under condition of high vacuum degree; oxygen is few; readily oxidizable substance is protected; and the sterilizing or suppress the vigor of some antibacterial because of anoxia; the material being dried will not oxidation deterioration; the heat-sensitive ingredients easily played in material will not degeneration or lose vigor; the material being dried when freezing can form " skeleton "; hold its shape after drying; do not have shrinkage phenomenon, and internal in loose porous sponge structure, the moisture of about 90%��95% can be got rid of time dry; can preserve for a long time at normal temperatures 2��5 years after drying, and be readily transported because of lightweight.
Further, in step c, vacuum bagging is that pack seals when 10Pa��20Pa.
Further, in step S03, the time of ball mill pulverizing is 15 minutes��30 minutes. Ball mill pulverizing is easy to tabletting.
Further, in step S03, tabletting is: in the saturated white sugar solution of interpolation lyophilizing Fructus Myricae rubrae gross weight 10% Fructus Myricae rubrae after pulverizing, under the pressure condition of 60kN, being pressed into diameter is 10mm, and thickness is the waxberry lozenge just sheet of 3mm. Just sheet mouthfeel is good for the waxberry lozenge obtained, it is easy to absorb, it is possible to instant edible.
Further, in step S03, physics colouring is: the purple potato pigment spray solution with 15% is in waxberry lozenge just sheet. Natural purple potato pigment can not only be painted to buccal tablet, more can improve the peculiar flavour of buccal tablet, safe and harmless.
Further, in step S03, needing before aseptic packaging waxberry lozenge just sheet drying and processing to water content is 5%��8%, and the mouthfeel of buccal tablet is more crisp, can preserve 2��5 years without any preservative when simultaneously.
Compared with prior art, it is an advantage of the current invention that:
1. lyophilizing waxberry lozenge is on lyophilizing Fructus Myricae rubrae finished product basis, reprocess, it maintains the original composition of Fructus Myricae rubrae, carry out under low-temp low-pressure, and moisture directly distils without liquid, freeze-dried products can keep its natural colored and abnormal smells from the patient is basically unchanged, face shaping is basically unchanged, various nutritional labeling is basically unchanged, intrinsic material does not lose substantially.
2. under very strict environment, pulverizing with special process, then use special installation compression molding, finally carry out aseptic packaging, foodsafety is high.
3. this product is with health role, because being natural food, as the Ms at conceived initial stage, the reaction for the pregnancy period has good assosting effect.
4. this waxberry lozenge dehydration is thorough, can get rid of the moisture of about 90%��95%, can preserve for a long time at normal temperatures 2��5 years after drying, and be readily transported because of lightweight time dry.
Detailed description of the invention
Embodiment 1
A kind of manufacture method of lyophilizing waxberry lozenge, manufacture method includes:
(1) Fructus Myricae rubrae primary election: be immersed in by Fructus Myricae rubrae in the saline of 3% and soak 10 minutes, then wash away salt with clear water, selects through graduation, drains the moisture in Fructus Myricae rubrae, case to be processed in 0 DEG C of freezing etc.;
(2) by Fructus Myricae rubrae through slicing treatment, the thickness of section is 3mm, then Fructus Myricae rubrae is cut into slices pre-freeze to-40 DEG C, when 5Pa, adopt the section dehydration of 1000W microwave treatment Fructus Myricae rubrae, completing dehydration to during lower than 5% moisture, after dehydration, when 10Pa, pack seals standby, obtains lyophilizing Fructus Myricae rubrae.
(3) by lyophilizing Fructus Myricae rubrae in humidity 10%, ball mill pulverizing in the sealing room of temperature 15 DEG C, the time of ball mill pulverizing is 15 minutes, sieve in 60 orders and package spare, in humidity 10%, in 15 DEG C of sealing rooms of temperature under the pressure condition of 60kN, being pressed into diameter is 10mm, thickness is the waxberry lozenge just sheet of 3mm, in the saturated white sugar solution of interpolation lyophilizing Fructus Myricae rubrae gross weight 10% Fructus Myricae rubrae after pulverizing, purple potato pigment spray solution with 15% is painted to physics in waxberry lozenge just sheet, then it is 5% to waxberry lozenge just sheet drying and processing to water content, Fructus Myricae rubrae lyophilizing buccal tablet is obtained then through aseptic packaging.
Embodiment 2
A kind of manufacture method of lyophilizing waxberry lozenge, manufacture method includes:
(1) Fructus Myricae rubrae primary election: be immersed in by Fructus Myricae rubrae in the saline of 5% and soak 15 minutes, then wash away salt with clear water, selects through graduation, drains the moisture in Fructus Myricae rubrae, case to be processed in 4 DEG C of freezings etc.;
(2) by Fructus Myricae rubrae through slicing treatment, the thickness of section is 5mm, then Fructus Myricae rubrae is cut into slices pre-freeze to-40 DEG C, when 10Pa, adopt the section dehydration of 1000W microwave treatment Fructus Myricae rubrae, completing dehydration to during lower than 5% moisture, after dehydration, when 20Pa, pack seals standby, obtains lyophilizing Fructus Myricae rubrae.
(3) by lyophilizing Fructus Myricae rubrae in humidity 30%, ball mill pulverizing in the sealing room of temperature 25 DEG C, the time of ball mill pulverizing is 30 minutes, sieve in 100 orders and package spare, in humidity 30%, in 25 DEG C of sealing rooms of temperature under the pressure condition of 60kN, being pressed into diameter is 10mm, thickness is the waxberry lozenge just sheet of 3mm, in the saturated white sugar solution of interpolation lyophilizing Fructus Myricae rubrae gross weight 10% Fructus Myricae rubrae after pulverizing, purple potato pigment spray solution with 15% is painted to physics in waxberry lozenge just sheet, then it is 8% to waxberry lozenge just sheet drying and processing to water content, Fructus Myricae rubrae lyophilizing buccal tablet is obtained then through aseptic packaging.
Embodiment 3
A kind of manufacture method of lyophilizing waxberry lozenge, manufacture method includes:
(1) Fructus Myricae rubrae primary election: be immersed in by Fructus Myricae rubrae in the saline of 4% and soak 12.5 minutes, then wash away salt with clear water, selects through graduation, drains the moisture in Fructus Myricae rubrae, case to be processed in 2 DEG C of freezings etc.;
(2) by Fructus Myricae rubrae through slicing treatment, the thickness of section is 4mm, then Fructus Myricae rubrae is cut into slices pre-freeze to-40 DEG C, when 7.5Pa, adopt the section dehydration of 1000W microwave treatment Fructus Myricae rubrae, completing dehydration to during lower than 5% moisture, after dehydration, when 15Pa, pack seals standby, obtains lyophilizing Fructus Myricae rubrae.
(3) by lyophilizing Fructus Myricae rubrae in humidity 20%, ball mill pulverizing in the sealing room of temperature 20 DEG C, the time of ball mill pulverizing is 22.5 minutes, sieve in 80 orders and package spare, in humidity 20%, in 22.5 DEG C of sealing rooms of temperature under the pressure condition of 60kN, being pressed into diameter is 10mm, thickness is the waxberry lozenge just sheet of 3mm, in the saturated white sugar solution of interpolation lyophilizing Fructus Myricae rubrae gross weight 10% Fructus Myricae rubrae after pulverizing, purple potato pigment spray solution with 15% is painted to physics in waxberry lozenge just sheet, then it is 5%��8% to waxberry lozenge just sheet drying and processing to water content, Fructus Myricae rubrae lyophilizing buccal tablet is obtained then through aseptic packaging.
Experimental example
The microbiological indicator of the lyophilizing waxberry lozenge obtained by the embodiment of the present invention 1��3: total plate count��10000cfu/g, coliform��0.3MPN/g, mycete, yeast��50cfu/g, without Salmonella, staphylococcus aureus, shigella without detection.
In lyophilizing waxberry lozenge obtained by the embodiment of the present invention 1��3, guarantor's flow of Fructus Myricae rubrae nutritional labeling is all >=90%.
The present invention is not limited to above-mentioned embodiment, for those skilled in the art, under the premise without departing from the principles of the invention, it is also possible to make some improvements and modifications, and these improvements and modifications are also considered as within protection scope of the present invention. The content not being described in detail in this specification belongs to the known prior art of professional and technical personnel in the field.
Claims (10)
1. the manufacture method of a lyophilizing waxberry lozenge, it is characterised in that described manufacture method includes:
Step S01, Fructus Myricae rubrae primary election: be immersed in by Fructus Myricae rubrae in the saline of 3%��5% and soak 10-15 minute, then wash away salt with clear water, select through graduation, drain the moisture in Fructus Myricae rubrae, and it is to be processed that vanning is freezing etc.;
Step S02, by step S01 process after Fructus Myricae rubrae through low-temperature freeze drying processed, obtain lyophilizing Fructus Myricae rubrae;
Step S03, waxberry lozenge molding flow process: by lyophilizing Fructus Myricae rubrae humidity 10%��30%, temperature 15 DEG C��25 DEG C sealing room in ball mill pulverizing, sieve in 60��100 orders and package spare, tabletting in humidity 10%��30%, 15 DEG C��25 DEG C sealing rooms of temperature, obtains lyophilizing waxberry lozenge through physics then aseptic packaging of painting.
2. manufacture method according to claim 1, it is characterised in that in step S01, the temperature of described freezing is 0 DEG C��4 DEG C.
3. manufacture method according to claim 1, it is characterised in that in described step S02, the step of described low-temperature freeze drying processed is:
Step a, lyophilizing Fructus Myricae rubrae are through slicing treatment;
Step b, pre-freeze to-40 DEG C that Fructus Myricae rubrae is cut into slices, dehydration in freeze-drier, complete dehydration to during lower than 5% moisture;
The pack of step c, dehydration final vacuum is standby, obtains lyophilizing Fructus Myricae rubrae.
4. manufacture method according to claim 3, it is characterised in that in step a, the thickness of described section is 3mm��5mm.
5. manufacture method according to claim 3, it is characterised in that in step b, described in freeze-drier dehydration be: when 5Pa��10Pa, adopt 1000W microwave treatment Fructus Myricae rubrae section.
6. manufacture method according to claim 3, it is characterised in that in step c, described vacuum bagging is that pack seals when 10Pa��20Pa.
7. manufacture method according to claim 1, it is characterised in that in step S03, the time of described ball mill pulverizing is 15 minutes��30 minutes.
8. manufacture method according to claim 1, it is characterised in that in step S03, described tabletting is: in the saturated white sugar solution of interpolation lyophilizing Fructus Myricae rubrae gross weight 10% Fructus Myricae rubrae after pulverizing, under the pressure condition of 60kN, being pressed into diameter is 10mm, and thickness is the waxberry lozenge just sheet of 3mm.
9. manufacture method according to claim 1, it is characterised in that in step S03, the colouring of described physics is: the purple potato pigment spray solution with 15% is in waxberry lozenge just sheet.
10. manufacture method according to claim 1, it is characterised in that in step S03, needing before described aseptic packaging waxberry lozenge just sheet drying and processing to water content is 5%��8%.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107853547A (en) * | 2017-10-26 | 2018-03-30 | 温州市瑶溪杨梅专业合作社 | A kind of preparation method of lyophilized bowl mandarin orange lozenge |
| CN111194869A (en) * | 2018-11-19 | 2020-05-26 | 内蒙古伊利实业集团股份有限公司 | Food with rose color |
| CN111802605A (en) * | 2020-07-10 | 2020-10-23 | 漳州福友食品有限公司 | Processing method of freeze-dried waxberries |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104247947A (en) * | 2013-06-27 | 2014-12-31 | 南京乐呵呵庄园农业科技有限公司 | Lozenge capable of dispelling effects of alcohol and production method thereof |
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| CN105192606A (en) * | 2015-10-21 | 2015-12-30 | 宁夏林业研究所股份有限公司 | Preparation method of leaf Lycium chinense Miller buccal tablet |
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| CN105146395A (en) * | 2015-10-21 | 2015-12-16 | 宁夏林业研究所股份有限公司 | Preparation technology of whole wolfberry powder lozenge |
| CN105192606A (en) * | 2015-10-21 | 2015-12-30 | 宁夏林业研究所股份有限公司 | Preparation method of leaf Lycium chinense Miller buccal tablet |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107853547A (en) * | 2017-10-26 | 2018-03-30 | 温州市瑶溪杨梅专业合作社 | A kind of preparation method of lyophilized bowl mandarin orange lozenge |
| CN111194869A (en) * | 2018-11-19 | 2020-05-26 | 内蒙古伊利实业集团股份有限公司 | Food with rose color |
| CN111194869B (en) * | 2018-11-19 | 2023-03-21 | 内蒙古伊利实业集团股份有限公司 | Food with rose color |
| CN111802605A (en) * | 2020-07-10 | 2020-10-23 | 漳州福友食品有限公司 | Processing method of freeze-dried waxberries |
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