CN105008339B - 具有后调节步骤的环氧化工艺 - Google Patents
具有后调节步骤的环氧化工艺 Download PDFInfo
- Publication number
- CN105008339B CN105008339B CN201480012837.6A CN201480012837A CN105008339B CN 105008339 B CN105008339 B CN 105008339B CN 201480012837 A CN201480012837 A CN 201480012837A CN 105008339 B CN105008339 B CN 105008339B
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- CN
- China
- Prior art keywords
- catalyst
- chloride
- concentration
- moderator
- temperature
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
- C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
- C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
- C07D301/10—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
- C07C29/10—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes
- C07C29/103—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers
- C07C29/106—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers of oxiranes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Epoxy Compounds (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201361751465P | 2013-01-11 | 2013-01-11 | |
US61/751,465 | 2013-01-11 | ||
PCT/US2014/010768 WO2014110194A1 (fr) | 2013-01-11 | 2014-01-09 | Procédé d'époxydation ayant une étape de post-conditionnement |
Publications (2)
Publication Number | Publication Date |
---|---|
CN105008339A CN105008339A (zh) | 2015-10-28 |
CN105008339B true CN105008339B (zh) | 2017-09-12 |
Family
ID=51165623
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201480012837.6A Active CN105008339B (zh) | 2013-01-11 | 2014-01-09 | 具有后调节步骤的环氧化工艺 |
Country Status (5)
Country | Link |
---|---|
US (1) | US9067902B2 (fr) |
EP (1) | EP2943477B1 (fr) |
KR (1) | KR102155073B1 (fr) |
CN (1) | CN105008339B (fr) |
WO (1) | WO2014110194A1 (fr) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP3484860B1 (fr) * | 2016-07-18 | 2021-01-13 | Scientific Design Company, Inc. | Procédé d'époxydation |
US11059017B2 (en) | 2017-09-15 | 2021-07-13 | MultiPhase Solutions, Inc. | Halogen selective detection gas chromatography for the on-line analysis and control of selective oxidation chemical production processes |
CN114057670B (zh) * | 2020-07-29 | 2024-06-07 | 中国石油化工股份有限公司 | 一种用于启动乙烯环氧化工艺的方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1041591A (zh) * | 1988-07-25 | 1990-04-25 | 国际壳牌研究有限公司 | 环氧乙烷的生产方法 |
US5155242A (en) * | 1991-12-05 | 1992-10-13 | Shell Oil Company | Process for starting-up an ethylene oxide reactor |
CN101679333A (zh) * | 2007-05-09 | 2010-03-24 | 国际壳牌研究有限公司 | 生产环氧烷、1,2-二醇、1,2-二醇醚、1,2-碳酸酯或烷醇胺的方法 |
CN102666514A (zh) * | 2009-12-17 | 2012-09-12 | 科学设计公司 | 用于环氧化启动的方法 |
Family Cites Families (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1170663A (en) | 1967-03-22 | 1969-11-12 | Shell Int Research | Process for preparing Silver Catalysts |
US3702259A (en) | 1970-12-02 | 1972-11-07 | Shell Oil Co | Chemical production of metallic silver deposits |
US4766105A (en) | 1986-10-31 | 1988-08-23 | Shell Oil Company | Ethylene oxide catalyst and process for preparing the catalyst |
US4761394A (en) | 1986-10-31 | 1988-08-02 | Shell Oil Company | Ethylene oxide catalyst and process for preparing the catalyst |
US5057481A (en) | 1987-02-20 | 1991-10-15 | Union Carbide Chemicals And Plastics Technology Corporation | Catalyst composition for oxidation of ethylene to ethylene oxide |
US4908343A (en) | 1987-02-20 | 1990-03-13 | Union Carbide Chemicals And Plastics Company Inc. | Catalyst composition for oxidation of ethylene to ethylene oxide |
US4874879A (en) | 1988-07-25 | 1989-10-17 | Shell Oil Company | Process for starting-up an ethylene oxide reactor |
DE68925767T2 (de) | 1988-08-30 | 1996-08-14 | Union Carbide Corp | Katalysatoren für die Herstellung von Ethylenoxid und Verfahren zur deren Herstellung |
US5187140A (en) | 1989-10-18 | 1993-02-16 | Union Carbide Chemicals & Plastics Technology Corporation | Alkylene oxide catalysts containing high silver content |
US5102848A (en) | 1990-09-28 | 1992-04-07 | Union Carbide Chemicals & Plastics Technology Corporation | Catalyst composition for oxidation of ethylene to ethylene oxide |
US5407888A (en) | 1992-05-12 | 1995-04-18 | Basf Aktiengesellschaft | Silver catalyst |
CA2494767C (fr) * | 2002-06-28 | 2012-07-17 | John Robert Lockemeyer | Methode de demarrage d'un procede d'epoxydation et procede d'epoxydation d'une olefine |
US7684865B2 (en) | 2003-03-14 | 2010-03-23 | Endovx, Inc. | Methods and apparatus for treatment of obesity |
US20110015549A1 (en) | 2005-01-13 | 2011-01-20 | Shimon Eckhouse | Method and apparatus for treating a diseased nail |
US8791280B2 (en) | 2005-08-10 | 2014-07-29 | Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg | Process for preparation of catalyst carrier and its use in catalyst preparation |
BRPI0614756A2 (pt) * | 2005-08-11 | 2011-04-12 | Shell Int Research | método para preparar um catalisador moldado, o catalisador, e uso do catalisador |
KR101485955B1 (ko) * | 2007-05-11 | 2015-01-22 | 베리 제이. 빌릭 | 산화올레핀 제조 공장에서의 고선택성 촉매의 개시 방법 |
US20090028339A1 (en) | 2007-07-24 | 2009-01-29 | Brian Gerard Goodman | Auto-Configuration of a Drive List for Encryption |
CN102056909B (zh) * | 2008-05-07 | 2014-03-05 | 国际壳牌研究有限公司 | 环氧化工艺的开车方法及环氧乙烷、1,2-二醇、1,2-二醇醚、1,2-碳酸酯或链烷醇胺的制备方法 |
CN102421766B (zh) * | 2009-04-21 | 2015-03-25 | 陶氏技术投资有限公司 | 提高铼助催化的环氧化催化剂的效率的方法以及使用它们的环氧化方法 |
US8624045B2 (en) * | 2009-12-17 | 2014-01-07 | Scientific Design Company, Inc. | Process for olefin oxide production |
RU2538969C2 (ru) * | 2009-12-23 | 2015-01-10 | Сайентифик Дизайн Компани, Инк. | Способ инициирования высокоселективного катализатора получения этиленоксида |
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2014
- 2014-01-09 WO PCT/US2014/010768 patent/WO2014110194A1/fr active Application Filing
- 2014-01-09 CN CN201480012837.6A patent/CN105008339B/zh active Active
- 2014-01-09 KR KR1020157021679A patent/KR102155073B1/ko active IP Right Grant
- 2014-01-09 EP EP14738161.0A patent/EP2943477B1/fr active Active
- 2014-01-10 US US14/152,519 patent/US9067902B2/en active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1041591A (zh) * | 1988-07-25 | 1990-04-25 | 国际壳牌研究有限公司 | 环氧乙烷的生产方法 |
US5155242A (en) * | 1991-12-05 | 1992-10-13 | Shell Oil Company | Process for starting-up an ethylene oxide reactor |
CN101679333A (zh) * | 2007-05-09 | 2010-03-24 | 国际壳牌研究有限公司 | 生产环氧烷、1,2-二醇、1,2-二醇醚、1,2-碳酸酯或烷醇胺的方法 |
CN102666514A (zh) * | 2009-12-17 | 2012-09-12 | 科学设计公司 | 用于环氧化启动的方法 |
Also Published As
Publication number | Publication date |
---|---|
WO2014110194A1 (fr) | 2014-07-17 |
EP2943477A1 (fr) | 2015-11-18 |
EP2943477A4 (fr) | 2016-06-29 |
KR20150105451A (ko) | 2015-09-16 |
EP2943477B1 (fr) | 2018-03-07 |
KR102155073B1 (ko) | 2020-09-11 |
CN105008339A (zh) | 2015-10-28 |
US20140200357A1 (en) | 2014-07-17 |
US9067902B2 (en) | 2015-06-30 |
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GR01 | Patent grant |