CN104970016B - Attractant of tomicus yunnanensis - Google Patents
Attractant of tomicus yunnanensis Download PDFInfo
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- CN104970016B CN104970016B CN201410133344.XA CN201410133344A CN104970016B CN 104970016 B CN104970016 B CN 104970016B CN 201410133344 A CN201410133344 A CN 201410133344A CN 104970016 B CN104970016 B CN 104970016B
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- attractant
- australene
- verbenol
- cis
- yunnan
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- 239000005667 attractant Substances 0.000 title claims abstract description 44
- 230000031902 chemoattractant activity Effects 0.000 title claims abstract description 44
- 241000346024 Tomicus yunnanensis Species 0.000 title abstract 5
- WONIGEXYPVIKFS-UHFFFAOYSA-N (+)-cis-Verbenol Natural products CC1=CC(O)C2C(C)(C)C1C2 WONIGEXYPVIKFS-UHFFFAOYSA-N 0.000 claims abstract description 46
- WONIGEXYPVIKFS-YIZRAAEISA-N (1s,2s,5s)-4,6,6-trimethylbicyclo[3.1.1]hept-3-en-2-ol Chemical compound CC1=C[C@H](O)[C@@H]2C(C)(C)[C@H]1C2 WONIGEXYPVIKFS-YIZRAAEISA-N 0.000 claims abstract description 35
- WONIGEXYPVIKFS-VGMNWLOBSA-N (1r,2s,5r)-4,6,6-trimethylbicyclo[3.1.1]hept-3-en-2-ol Chemical compound CC1=C[C@H](O)[C@H]2C(C)(C)[C@@H]1C2 WONIGEXYPVIKFS-VGMNWLOBSA-N 0.000 claims abstract description 12
- WTARULDDTDQWMU-UHFFFAOYSA-N Pseudopinene Natural products C1C2C(C)(C)C1CCC2=C WTARULDDTDQWMU-UHFFFAOYSA-N 0.000 claims abstract description 6
- RXBQNMWIQKOSCS-UHFFFAOYSA-N Myrthenol Natural products C1C2C(C)(C)C1CC=C2CO RXBQNMWIQKOSCS-UHFFFAOYSA-N 0.000 claims description 17
- RXBQNMWIQKOSCS-IUCAKERBSA-N [(1s,5r)-6,6-dimethyl-4-bicyclo[3.1.1]hept-3-enyl]methanol Chemical compound C1[C@@H]2C(C)(C)[C@H]1CC=C2CO RXBQNMWIQKOSCS-IUCAKERBSA-N 0.000 claims description 17
- 239000007787 solid Substances 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 9
- 150000001336 alkenes Chemical class 0.000 claims description 8
- 229930006720 (-)-alpha-pinene Natural products 0.000 claims description 4
- 150000002085 enols Chemical class 0.000 claims description 4
- GRWFGVWFFZKLTI-UHFFFAOYSA-N rac-alpha-Pinene Natural products CC1=CCC2C(C)(C)C1C2 GRWFGVWFFZKLTI-UHFFFAOYSA-N 0.000 claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- WONIGEXYPVIKFS-HRDYMLBCSA-N (1r,2r,5r)-4,6,6-trimethylbicyclo[3.1.1]hept-3-en-2-ol Chemical compound CC1=C[C@@H](O)[C@H]2C(C)(C)[C@@H]1C2 WONIGEXYPVIKFS-HRDYMLBCSA-N 0.000 claims description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims 1
- 239000010931 gold Substances 0.000 claims 1
- 229910052737 gold Inorganic materials 0.000 claims 1
- UAHWPYUMFXYFJY-UHFFFAOYSA-N beta-myrcene Chemical compound CC(C)=CCCC(=C)C=C UAHWPYUMFXYFJY-UHFFFAOYSA-N 0.000 abstract description 22
- XMGQYMWWDOXHJM-JTQLQIEISA-N (+)-α-limonene Chemical compound CC(=C)[C@@H]1CCC(C)=CC1 XMGQYMWWDOXHJM-JTQLQIEISA-N 0.000 abstract description 20
- XMGQYMWWDOXHJM-SNVBAGLBSA-N (-)-α-limonene Chemical compound CC(=C)[C@H]1CCC(C)=CC1 XMGQYMWWDOXHJM-SNVBAGLBSA-N 0.000 abstract description 20
- SLKPBCXNFNIJSV-HNNXBMFYSA-N Cuparene Chemical compound C1=CC(C)=CC=C1[C@@]1(C)C(C)(C)CCC1 SLKPBCXNFNIJSV-HNNXBMFYSA-N 0.000 abstract description 18
- CRPUJAZIXJMDBK-UHFFFAOYSA-N Toxaphene Natural products C1CC2C(=C)C(C)(C)C1C2 CRPUJAZIXJMDBK-UHFFFAOYSA-N 0.000 abstract description 17
- CRPUJAZIXJMDBK-DTWKUNHWSA-N (+)-camphene Chemical compound C1C[C@@H]2C(=C)C(C)(C)[C@H]1C2 CRPUJAZIXJMDBK-DTWKUNHWSA-N 0.000 abstract description 16
- YHQGMYUVUMAZJR-UHFFFAOYSA-N α-terpinene Chemical compound CC(C)C1=CC=C(C)CC1 YHQGMYUVUMAZJR-UHFFFAOYSA-N 0.000 abstract description 14
- VYBREYKSZAROCT-UHFFFAOYSA-N alpha-myrcene Natural products CC(=C)CCCC(=C)C=C VYBREYKSZAROCT-UHFFFAOYSA-N 0.000 abstract description 11
- 229940099369 (+)- limonene Drugs 0.000 abstract description 10
- 229960003595 (-)- limonene Drugs 0.000 abstract description 10
- CRPUJAZIXJMDBK-BDAKNGLRSA-N (-)-camphene Chemical compound C1C[C@H]2C(=C)C(C)(C)[C@@H]1C2 CRPUJAZIXJMDBK-BDAKNGLRSA-N 0.000 abstract description 9
- 229930006714 (-)-camphene Natural products 0.000 abstract description 9
- SLKPBCXNFNIJSV-UHFFFAOYSA-N cuparene Natural products C1=CC(C)=CC=C1C1(C)C(C)(C)CCC1 SLKPBCXNFNIJSV-UHFFFAOYSA-N 0.000 abstract description 9
- WVRVMHCZDFFAFB-UHFFFAOYSA-N epsilon-Cuprenene Natural products C1=CC(C)=CCC1C1(C)C(C)(C)CCC1 WVRVMHCZDFFAFB-UHFFFAOYSA-N 0.000 abstract description 9
- 239000000126 substance Substances 0.000 abstract description 9
- 230000002265 prevention Effects 0.000 abstract description 8
- 241000238631 Hexapoda Species 0.000 abstract description 7
- WSTYNZDAOAEEKG-UHFFFAOYSA-N Mayol Natural products CC1=C(O)C(=O)C=C2C(CCC3(C4CC(C(CC4(CCC33C)C)=O)C)C)(C)C3=CC=C21 WSTYNZDAOAEEKG-UHFFFAOYSA-N 0.000 abstract description 7
- 241000607479 Yersinia pestis Species 0.000 abstract description 6
- -1 (-)-Myrteneol Chemical compound 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 238000012544 monitoring process Methods 0.000 abstract description 3
- BQOFWKZOCNGFEC-BDAKNGLRSA-N (+)-Delta3-carene Chemical compound C1C(C)=CC[C@H]2C(C)(C)[C@@H]12 BQOFWKZOCNGFEC-BDAKNGLRSA-N 0.000 abstract description 2
- 229930006713 (+)-car-3-ene Natural products 0.000 abstract description 2
- GRWFGVWFFZKLTI-RKDXNWHRSA-N (+)-α-pinene Chemical compound CC1=CC[C@H]2C(C)(C)[C@@H]1C2 GRWFGVWFFZKLTI-RKDXNWHRSA-N 0.000 abstract description 2
- WTARULDDTDQWMU-IUCAKERBSA-N (-)-β-pinene Chemical compound C1[C@@H]2C(C)(C)[C@H]1CCC2=C WTARULDDTDQWMU-IUCAKERBSA-N 0.000 abstract description 2
- BQOFWKZOCNGFEC-UHFFFAOYSA-N Delta3-Carene Natural products C1C(C)=CCC2C(C)(C)C12 BQOFWKZOCNGFEC-UHFFFAOYSA-N 0.000 abstract description 2
- 206010059866 Drug resistance Diseases 0.000 abstract 1
- 244000144972 livestock Species 0.000 abstract 1
- 238000000034 method Methods 0.000 description 17
- 230000005532 trapping Effects 0.000 description 11
- 238000012360 testing method Methods 0.000 description 10
- 238000002474 experimental method Methods 0.000 description 7
- 150000000015 (+)-car-3-ene derivatives Chemical class 0.000 description 6
- 240000001987 Pyrus communis Species 0.000 description 6
- 235000014443 Pyrus communis Nutrition 0.000 description 6
- 239000003814 drug Substances 0.000 description 5
- 239000002023 wood Substances 0.000 description 5
- 241000545593 Scolytinae Species 0.000 description 4
- 150000003505 terpenes Chemical class 0.000 description 4
- 235000007586 terpenes Nutrition 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 244000144977 poultry Species 0.000 description 3
- 229950010257 terpin Drugs 0.000 description 3
- VVFXXDIPJNSMPW-UHFFFAOYSA-N 1,1,4a-trimethyl-7-propan-2-yl-2,3,4,4b,5,6,8a,10a-octahydrophenanthrene Chemical compound C1=CC2C(C)(C)CCCC2(C)C2C1C=C(C(C)C)CC2 VVFXXDIPJNSMPW-UHFFFAOYSA-N 0.000 description 2
- IAQORZCEBSUZRH-UHFFFAOYSA-N 3,3-dimethyl-2-methylidenebicyclo[2.2.1]heptane Chemical compound C1CC2C(=C)C(C)(C)C1C2.C1CC2C(=C)C(C)(C)C1C2 IAQORZCEBSUZRH-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000036039 immunity Effects 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- WUOACPNHFRMFPN-VIFPVBQESA-N (R)-(+)-alpha-terpineol Chemical compound CC1=CC[C@H](C(C)(C)O)CC1 WUOACPNHFRMFPN-VIFPVBQESA-N 0.000 description 1
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 102100033538 Clusterin-associated protein 1 Human genes 0.000 description 1
- 101000945057 Danio rerio Clusterin-associated protein 1 homolog Proteins 0.000 description 1
- 101000945060 Homo sapiens Clusterin-associated protein 1 Proteins 0.000 description 1
- 235000005205 Pinus Nutrition 0.000 description 1
- 241000218602 Pinus <genus> Species 0.000 description 1
- 241000220324 Pyrus Species 0.000 description 1
- 241000546225 Tomicus Species 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000010137 moulding (plastic) Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 235000021017 pears Nutrition 0.000 description 1
- 239000003016 pheromone Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000001932 seasonal effect Effects 0.000 description 1
- 239000003620 semiochemical Substances 0.000 description 1
- GOLXNESZZPUPJE-UHFFFAOYSA-N spiromesifen Chemical compound CC1=CC(C)=CC(C)=C1C(C(O1)=O)=C(OC(=O)CC(C)(C)C)C11CCCC1 GOLXNESZZPUPJE-UHFFFAOYSA-N 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses an attractant of tomicus yunnanensis. The attractant comprises one or more of the following components: S-(-)-alpha-pinene, 1R-(+)-alpha-pinene, myrcene, (+)-camphene, (-)-camphene, alpha-terpinene, (+)-3-carene, (1s)-(-)-beta-pinene, (-)-limonene, (+)-limonene, (-)-Myrteneol, (s)-cis-verbenol, (-)-trans-verbenol and Cuparene. According to the attractant disclosed by the invention, the attractant containing a host and polypide volatile matter is utilized for attract tomicus yunnanensis massively, so that the tomicus yunnanensis is gathered in a certain device and then is killed; the attractant has the advantages of low cost, high efficiency, complete environmental friendliness, safety to people and livestock, incapability of generating drug resistance to insects and the like, so that the traditional passive chemical prevention and treatment can be replaced by active biological prevention and treatment; meanwhile, the aims of monitoring and forecasting the forestry insect pests can be achieved according to the amount of tomicus yunnanensis in the attractant.
Description
Technical field
The present invention relates to terpenes and monoterpenol as Yunnan tangent epiderivative attractant application and to cut the tip little in a kind of Yunnan
Moth-eaten attractant.
Background technology
Yunnan tangent epiderivative (Tomicus yunn α nensis Kirkendall and Faccoli) is a kind of important
Trunk borer, occurs mainly in the areas such as the Yunnan and Sichuan of China, the multiple kinds of harm Pinus.But up to the present, with regard to
Tangent epiderivative Research Literature at home and abroad in Yunnan is few, and is concentrated mainly on biology, Tropical area etc..Adjusted according to applicant
Look into, it is as follows in Yunnan prevention and control bark beetle major measure at present：1. quarantine is strengthened.Forbid wooden allocation and transportation of harming, prevent aggrieved nursery stock
Other places are diffused into by epidemic-stricken area.2. wood of harming is cleared up.To prevent insect pest from spreading, all aggrieved wood of woodland are felled, and in skill
Under the supervision of art personnel, carry out medicament fumigating or burn process.3. trap-tree trapping.In the sample ground of bark beetle Burst Regions, random selection
Aggrieved trap-tree is simultaneously cuted down, and is placed in woodland, and investigation is new to invade hole count, and finally trap-tree is processed.4. chemical control.The method is
Punching moth medicine is carried out to the aggrieved wood of woodland.
But, cleaning wood of harming can leak and cut down and cause large batch of pinaster to be forced to cut down and remove.The effect of trap-tree trapping is poor.Beat
Hole moth medicine pollutes the environment, and destroys the balance of forest ecosystem, affects its bio-diversity.The Forest Tourism Resources in Yunnan are non-
Often enrich, local government and forest department attach great importance to the prevention and control of trunk borer, but up to the present, never compare in production
Relatively rationally, the method effectively monitored and prevent and treat.
With the fast development of chemical ecology, carry out prevention and control bark beetle using the infochemical of insecticide and obtained abroad
To good certification.The method has efficient, environmental friendliness, positioning strong.In order to preferably prevent and treat the worm, emphasis of the present invention is directed to
Its semiochemicals is studied, and be have developed and lured agent prescription.
The content of the invention
It is an object of the invention to provide by terpenes and terpenol as Yunnan tangent epiderivative attractant application.
It is a further object to provide it is a kind of have it is efficient, environmentally friendly, to person poultry safety, produce insect
The drug-fast attractant of life.
For achieving the above object, the present invention takes technical scheme below：
S- (-)-australene (S- (-)-α-pinene), 1R- (+)-australene (1R- (+)-α-pinene), myrcene
(myrcene), (+)-camphene ((+)-camphene), (-)-camphene ((-)-camphene), α-terpinene (α-
Terpinene), (+) -3- carenes ((+) -3-carene), (1S)-(-)-nopinene ((1s)-(-)-β-pinene), (-)-lemon
Lemon alkene ((-)-limonene), (+)-limonene ((+)-limonene), (-)-myrtenol ((-)-Myrtenol), (S)-
Cis-verbenol (s)-cis-verbenol, (-)-trans-verbenol ((-)-trans-verbenol) and flower side
Application of one or more in cupressene (Cuparene) as Yunnan tangent epiderivative attractant.
Volatile matter by the use of host and polypide of the invention can attract substantial amounts of Yunnan tangent epiderivative as attractant so as to
Be gathered in certain device and killed again, with low cost, efficiently, it is completely environmentally friendly, to person poultry safety, do not make evil
The advantages of worm develops immunity to drugs so that in the past passive chemical prevention is changed into the Biological control of active, while can also be according to trapping
In device Yunnan tangent epiderivative quantity number, reach monitoring and forecast forestry insect pest purpose.
A kind of Yunnan tangent epiderivative attractant, the attractant by S- (-)-australene, 1R- (+)-australene, myrcene,
(+)-camphene, (-)-camphene, α-terpinene, (1S)-(-)-nopinene, (-)-limonene, (+)-limonene, (-)-Fructus Rhodomyrti alkene
Alcohol and cuparene are constituted, S- (-)-australene, 1R- (+)-australene, myrcene, (+)-camphene, (-)-camphene, α-terpene
The volume ratio of product alkene, (1S)-(-)-nopinene, (-)-limonene, (+)-limonene, (-)-myrtenol and cuparene
For：5-10：1-3：1-3：1-3：0.2-0.5：0.05-0.1：1-5：0.01-0.1：0.01-0.1：0.01-0.1：0.05-0.3.
Preferably, S- (-)-australene, 1R- (+)-australene, myrcene, (+)-camphene, (-)-camphene, α-terpin
The volume ratio of alkene, (1S)-(-)-nopinene, (-)-limonene, (+)-limonene, (-)-myrtenol and cuparene is：
8：1：1.5：1.6：0.36：0.07：3.75：0.03：0.07：0.07：0.13.
A kind of Yunnan tangent epiderivative attractant, the attractant by S- (-)-australene, 1R- (+)-australene, myrcene,
(+)-camphene, (-)-camphene, α-terpinene, (+) -3- carenes, (-)-limonene, (+)-limonene, (-)-myrtenol,
(S)-cis-verbenol, (-)-trans-verbenol and cuparene composition, S- (-)-australene, 1R-
(+)-australene, myrcene, (+)-camphene, (-)-camphene, α-terpinene, (+) -3- carenes, (-)-limonene, (+)-Fructus Citri Limoniae
The volume ratio of alkene, (-)-myrtenol, (S)-cis-verbenol, (-)-trans-verbenol and cuparene
For：30-50：10-20：5-10：5-10：2-6：0.1-0.5： 0.01-0.1：0.05-0.3：0.05-0.3：0.01-0.05：
0.005-0.15：0.01-0.05：0.1-1；Wherein, S- (-)-australene, 1R- (+)-australene, myrcene, (+)-camphane
Alkene, (-)-camphene, α-terpinene, (+) -3- carenes, (-)-limonene, (+)-limonene, (-)-myrtenol, (-)-anti-
Formula-verbenol and cuparene are in units of ml, and (S)-cis-verbenol is solid, with cm3For unit.
Preferably, S- (-)-australene, 1R- (+)-australene, myrcene, (+)-camphene, (-)-camphene, α-terpin
Alkene, (+) -3- carenes, (-)-limonene, (+)-limonene, (-)-myrtenol, (S)-cis-verbenol, (-)-anti-
The volume ratio of formula-verbenol and cuparene is：39：14：9：7：3：0.35：0.05：0.18：0.16：0.03：0.01：
0.03：0.5；Wherein, S- (-)-australene, 1R- (+)-australene, myrcene, (+)-camphene, (-)-camphene, α-terpin
Alkene, (+) -3- carenes, (-)-limonene, (+)-limonene, (-)-myrtenol, (-)-trans-verbenol and flower side
Cupressene is in units of ml, and (S)-cis-verbenol is solid, with cm3For unit.
A kind of Yunnan tangent epiderivative attractant, the attractant is by S- (-)-australene and (s)-cis-verbenol group
Into S- (-)-australene, cis-verbenol volume ratio are 25-100：0.075-0.5；Wherein, S- (-)-α-
Pinene is in units of ml, and (S)-cis-verbenol is solid, with cm3For unit.
Preferably, S- (-)-australene, the volume ratio of (s)-cis-verbenol are 50：0.125；Wherein, institute
S- (-)-australene is stated in units of ml, and (S)-cis-verbenol is solid, with cm3For unit.
A kind of constituent of Yunnan tangent epiderivative attractant, by S- (-)-australene, (s)-cis-verbenol,
(-)-trans-verbenol composition, S- (-)-australene, (s)-cis-verbenol, (-)-trans-Herba Verbenae
The volume ratio of enol is 25-100：0.075-0.5：0.075-0.5；Wherein, S- (-)-australene, (-)-trans-horsewhip
Oxalene alcohol is in units of ml, and (S)-cis-verbenol is solid, with cm3For unit.
Preferably, S- (-)-australene, (s)-cis-verbenol and (-)-trans-verbenol, its ratio
Example is respectively 50ml：0.125cm3：0.125ml.
A kind of Yunnan tangent epiderivative attractant, the attractant is by S- (-)-australene, (-)-myrtenol, (S)-suitable
Formula-verbenene composition, S- (-)-australene, (-)-myrtenol, the volume ratio of (S)-cis-verbenene are
25-100：0.1-1：0.075-0.5；Wherein, S- (-)-australene, (-)-myrtenol be in units of ml, and
(S)-cis-verbenol is solid, with cm3For unit.
Preferably, S- (-)-australene, (-)-myrtenol, the volume ratio of (S)-cis-verbenene are 50：
0.5：0.125；Wherein, S- (-)-australene, (-)-myrtenol are in units of ml, and (S)-cis-Herba Verbenae
Enol is solid, with cm3For unit.
A kind of Yunnan tangent epiderivative attractant, the attractant by S- (-)-australene, 1R- (+)-australene, (s)-cis-
Verbenol is constituted, and S- (-)-australene, 1R- (+)-australene, the volume ratio of (s)-cis-verbenol are
25-100：25-100：0.075-0.5；Wherein, S- (-)-australene, 1R- (+)-australene be in units of ml, and
(S)-cis-verbenol is solid, with cm3For unit.
Preferably, S- (-)-australene, 1R- (+)-australene, the volume ratio of (s)-cis-verbenol are
50：50：0.125；Wherein, S- (-)-australene, 1R- (+)-australene are in units of ml, and (S）- cis-Herba Verbenae
Enol is solid, with cm3For unit.
It is an advantage of the invention that：
1st, with the infochemical of host and polypide Yunnan tangent epiderivative is lured than traditional chemical pest control low cost
Much, terpenes preparation (the online quotation of domestic Production in Chemical Plant：7800 yuan/ton) more external low price, and 10mi terpenes (folding
Close 0.08 yuan or so) can continuously use 2 first quarter moons.The method economical and effective, can save substantial amounts of manpower and materials.
2nd, the use of attractant be not subject to seasonal restrictions and can life-time service, in Yunnan tangent epiderivative sprout wings harm it is whole when
Between section can trapping pests, and chemical prevention and the killed wood of cleaning need to implement in a certain special time period, too early or too late all
Impact effect.Therefore, the present invention is trying to explore and put into practice to frontier science and technology, with important scientific value and social valency
Value.
3rd, the present invention attracts in a large number Yunnan tangent epiderivative using containing host and polypide semiochemicalses so as to be gathered in
Is killed again in certain device, with efficient, complete environmental friendliness, to person poultry safety, do not make insect develop immunity to drugs
Advantage so that in the past passive chemical prevention is changed into the Biological control of active.
4 according in trapper Yunnan tangent epiderivative quantity number, reach monitoring and forecast forestry insect pest purpose.
Description of the drawings
Fig. 1 averagely traps spirogram table for the different formulations of embodiment 1 to the female male worm of Yunnan tangent epiderivative, and (in January, 2011 exists
The big pear tree village in Qujing carries out testing experiment).
Fig. 2 averagely traps spirogram table (in January, 2012 Qujing to Yunnan tangent epiderivative female adult for the different disposal of embodiment 2
Big pear tree village proceeds testing experiment).
Fig. 3 averagely traps spirogram table (in January, 2012 Qujing to Yunnan tangent epiderivative male worm for the different disposal of embodiment 2
Big pear tree village proceeds testing experiment).
Fig. 4 averagely traps spirogram table (the big pears in January, 2012 Qujing to Yunnan tangent epiderivative for the different disposal of embodiment 2
Tree village proceeds testing experiment).
Specific embodiment
The Yunnan tangent epiderivative attractant of the present invention is pear tree village public welfare forest big in Qujing City of Yunnan Province Qilin District Yue Zhou towns
The testing experiment result of continuous 2 years.The purity of compound used therefor and manufacturer are shown in Table 1
The sample purity of the main volatile standard substance of table 1 and manufacturer
Note：* (s)-page-verbenol is solid, and unit is cm3, the unit of remaining compound is ml.Similarly hereinafter.
Embodiment 1
Test 1 is carried out in January, 2011 in the big pear tree village in Qujing, according to host's volatile matter and bark beetle pheromone analysis
As a result, 3 kinds are configured with and lure agent prescription (its numbering is respectively A, B, C), and set the blank of an extension trapper and (compiled
Number D).The concrete proportioning of formula is shown in Table 2.
The mixed liquor of 40mL is loaded into the slow release bottle (the plastic molding and processing plant's production of three one-tenth of Shanxi province Taiyuan city Xiaodian District) of 100mL, should
Slow release bottle release rate of s- (-)-australene s- (-)-α-pinene at 20 DEG C is about 50mg/d.The high 81em width 37cm of trapper
(middle prompt four directions, Beijing), bottom has a plastic collection bottle, and slow release bottle is fixed on trapper bottom.Trapper hangs over woodland cloud
Between southern pinaster, bottom is liftoff 1.5m is spaced 40m.Often process and be repeated 5 times, once trapping amount was investigated every 5 days, and will trapping
Device is exchanged at random.
The different disposal of the table field test of in December, 22011
D is the control without formula,
Note：* (s)-cis-verbenol is solid, and unit is cm3, the unit of remaining compound is ml.Similarly hereinafter.
As shown in figure 1, trapping Yunnan tangent epiderivative 68 (F=10.74 of female adult altogether using said method；Df=3,8；P=
0.004), 44 (F=9.27 of male worm；Df=3,8；P=0.006).From the point of view of female adult, process C trappings amounts noticeably greater than process A and
B, all process are significantly higher than blank D.From the point of view of male worm, process C trappings amount and noticeably greater than process B, process B significantly big
In blank.Each female and male ratio and no significant difference (Mann-Whitney U detections, P in processing>0.251).Entirely
The female and male ratio of experimental period ordinary bending is respectively 1.67 (A, n=24), 1.57 (B, n=27), 1.70 (C, n=41), 1.82
(D, n=45), and 1.50 (F, n=8).
Embodiment 2
Proceed testing experiment in the big pear tree village in Qujing in January, 2012.9 process are provided with altogether, are attractant and are matched somebody with somebody
Side, numbering is respectively C, E, F, G, K, L, M.Wherein formula C is the optimum formula filtered out from embodiment 1, in this experiment
By as control treatment；Other formula are the new formula formed on the basis of C formula, and its composition and ratio are shown in Table 3.Each process
It is repeated 5 times, woodland implementation is with embodiment 1.
The different disposal of the table field test of in January, 32012
As shown in Figure 2, Figure 3 and Figure 4, the test lures altogether tangent epiderivative female male worm in Yunnan to be respectively 335 and 246.Place
The reason female male worm of Yunnan tangent epiderivative lured of C, E, F and G be significantly more than H, I, J, K and L five process (female adult F=7.890, df=8,
36, P=0.0001, see Fig. 2；Male worm F=24.788, df=8,36, P=0.0001 is shown in Fig. 3).C, E, G show to the trapping amount of female adult
It is higher than F to write, and E, F, G are significantly higher than C to the trapping amount of male worm.Female male worm is merged, Fig. 4 is obtained, it is little that C, E, F and G cut the tip to Yunnan
The comprehensive attracting action of moth-eaten female male worm is processed apparently higher than H, I, J, K and L five, and E, G are significantly higher than C.Each processes neutral
Than and no significant difference (Mann-Whitney U detect, P >=0.114).Entirely the Yunnan tangent epiderivative of experimental period collection is female
Male ratio respectively 0.7 (C, n=118), 0.6 (E, n=153), 0.5 (F, n=131), 0.7 (G, n=142), 1 (H, n=48), 1.2
(I, n=49), 1 (J, n=63), 0.8 (K, n=47), 0.8 (L, n=50).
Claims (8)
1. a kind of attractant is used to lure the application of Yunnan tangent epiderivative, it is characterised in that the attractant is by S- (-)-australene
Alkene and (s)-cis-verbenol composition, S- (-)-australene, the volume ratio of (s)-cis-verbenol are 25-
100：0.075-0.5；Wherein, S- (-)-australene is in units of ml, and (S)-cis-verbenol is solid, with
cm3For unit.
2. according to claim 1 attractant is used to lure the application of Yunnan tangent epiderivative, it is characterised in that the attractant
Middle S- (-)-australene, the volume ratio of (s)-cis-verbenol are 50：0.125.
3. a kind of attractant is used to lure the application of Yunnan tangent epiderivative, it is characterised in that the attractant by S- (-)-α-
Pinene, (s)-cis-verbenol, (-)-trans-verbenol composition, S- (-)-australene, (s)-cis-horse
Whip oxalene alcohol, the volume ratio of (-)-trans-verbenol is 25-100：0.075-0.5：0.075-0.5；Wherein, the S-
(-)-australene, (-)-trans-verbenol are in units of ml, and (S)-cis-verbenol is solid, with cm3
For unit.
4. according to claim 3 attractant is used to lure the application of Yunnan tangent epiderivative, it is characterised in that the attractant
The volume ratio of middle S- (-)-australene, (s)-cis-verbenol and (-)-trans-verbenol is 50ml：
0.125cm3：0.125ml.
5. a kind of attractant is used to lure the application of Yunnan tangent epiderivative, it is characterised in that the attractant is by S- (-)-australene
Alkene, (-)-myrtenol, (S)-cis-verbenene composition, S- (-)-australene, (-)-myrtenol, (S)-
The volume ratio of cis-verbenene is 25-100：0.1-1：0.075-0.5；Wherein, S- (-)-australene, (-)-Fructus Persicae gold
Ma's enol is in units of ml, and (S)-cis-verbenol is solid, with cm3For unit.
6. according to claim 5 attractant is used to lure the application of Yunnan tangent epiderivative, it is characterised in that the attractant
Middle S- (-)-australene, (-)-myrtenol, the volume ratio of (S)-cis-verbenene are 50：0.5：0.125.
7. a kind of attractant is used to lure the application of Yunnan tangent epiderivative, it is characterised in that the attractant is by S- (-)-australene
Alkene, 1R- (+)-australene, (s)-cis-verbenol composition, S- (-)-australene, 1R- (+)-australene, (s)-
The volume ratio of cis-verbenol is 25-100：25-100：0.075-0.5；Wherein, S- (-)-australene, 1R-
(+)-australene is in units of ml, and (S)-cis-verbenol is solid, with cm3For unit.
8. according to claim 7 attractant is used to lure the application of Yunnan tangent epiderivative, it is characterised in that the attractant
Middle S- (-)-australene, 1R- (+)-australene, the volume ratio of (s)-cis-verbenol are 50：50：0.125.
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| CN106614575B (en) * | 2015-10-30 | 2018-12-04 | 中国检验检疫科学研究院 | A kind of material bark beetle category attractant |
| CN106070288A (en) * | 2016-06-03 | 2016-11-09 | 华南农业大学 | A kind of pine tumor is as attractant |
| CN112075426B (en) * | 2020-10-09 | 2021-11-30 | 云南省林业和草原科学院 | Odor composition for attracting Yunnan tomaytom bark beetles |
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